CN106135615A - A kind of production method of radix puerariae sugar - Google Patents
A kind of production method of radix puerariae sugar Download PDFInfo
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- CN106135615A CN106135615A CN201610477280.4A CN201610477280A CN106135615A CN 106135615 A CN106135615 A CN 106135615A CN 201610477280 A CN201610477280 A CN 201610477280A CN 106135615 A CN106135615 A CN 106135615A
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- sugar
- radix puerariae
- juice
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- 238000004519 manufacturing process Methods 0.000 title claims abstract description 18
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims abstract description 36
- 239000000284 extract Substances 0.000 claims abstract description 19
- 239000000843 powder Substances 0.000 claims abstract description 19
- 239000012528 membrane Substances 0.000 claims abstract description 17
- 239000000919 ceramic Substances 0.000 claims abstract description 15
- 235000021028 berry Nutrition 0.000 claims abstract description 13
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims abstract description 10
- 229930006000 Sucrose Natural products 0.000 claims abstract description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 9
- 238000002156 mixing Methods 0.000 claims abstract description 8
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 claims abstract description 6
- 238000002137 ultrasound extraction Methods 0.000 claims abstract description 6
- 238000010926 purge Methods 0.000 claims abstract description 5
- 238000000926 separation method Methods 0.000 claims abstract description 5
- 239000003456 ion exchange resin Substances 0.000 claims abstract description 4
- 229920003303 ion-exchange polymer Polymers 0.000 claims abstract description 4
- 238000009835 boiling Methods 0.000 claims abstract description 3
- 238000001694 spray drying Methods 0.000 claims abstract description 3
- 238000010612 desalination reaction Methods 0.000 claims abstract 2
- 230000009467 reduction Effects 0.000 claims abstract 2
- 238000009834 vaporization Methods 0.000 claims abstract 2
- 230000008016 vaporization Effects 0.000 claims abstract 2
- 238000001914 filtration Methods 0.000 claims description 18
- 235000007201 Saccharum officinarum Nutrition 0.000 claims description 11
- 240000000111 Saccharum officinarum Species 0.000 claims description 11
- 238000001471 micro-filtration Methods 0.000 claims description 9
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims description 8
- 239000000203 mixture Substances 0.000 claims description 8
- 238000000108 ultra-filtration Methods 0.000 claims description 8
- 238000000605 extraction Methods 0.000 claims description 6
- 239000000706 filtrate Substances 0.000 claims description 6
- 238000001035 drying Methods 0.000 claims description 5
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 claims description 4
- 229930003268 Vitamin C Natural products 0.000 claims description 4
- 238000002425 crystallisation Methods 0.000 claims description 4
- 230000008025 crystallization Effects 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 4
- 239000007788 liquid Substances 0.000 claims description 4
- 239000002002 slurry Substances 0.000 claims description 4
- 239000007787 solid Substances 0.000 claims description 4
- 235000019154 vitamin C Nutrition 0.000 claims description 4
- 239000011718 vitamin C Substances 0.000 claims description 4
- 239000007921 spray Substances 0.000 claims description 3
- 235000008733 Citrus aurantifolia Nutrition 0.000 claims description 2
- 235000011941 Tilia x europaea Nutrition 0.000 claims description 2
- 238000004061 bleaching Methods 0.000 claims description 2
- 239000006071 cream Substances 0.000 claims description 2
- 239000004571 lime Substances 0.000 claims description 2
- 238000003801 milling Methods 0.000 claims description 2
- 239000002994 raw material Substances 0.000 claims description 2
- 238000012216 screening Methods 0.000 claims description 2
- 238000005507 spraying Methods 0.000 claims description 2
- 230000008719 thickening Effects 0.000 claims description 2
- 229910052573 porcelain Inorganic materials 0.000 claims 2
- 235000016709 nutrition Nutrition 0.000 abstract description 6
- 238000002372 labelling Methods 0.000 abstract description 5
- 238000004090 dissolution Methods 0.000 abstract description 3
- 239000013078 crystal Substances 0.000 abstract description 2
- 230000000050 nutritive effect Effects 0.000 abstract description 2
- 238000001223 reverse osmosis Methods 0.000 abstract description 2
- 238000006386 neutralization reaction Methods 0.000 abstract 1
- 229960004793 sucrose Drugs 0.000 abstract 1
- 239000000047 product Substances 0.000 description 13
- 239000000243 solution Substances 0.000 description 13
- 238000000034 method Methods 0.000 description 10
- 241000219780 Pueraria Species 0.000 description 7
- 230000000694 effects Effects 0.000 description 7
- 241000196324 Embryophyta Species 0.000 description 4
- 239000004615 ingredient Substances 0.000 description 4
- 239000008280 blood Substances 0.000 description 3
- 210000004369 blood Anatomy 0.000 description 3
- 238000004042 decolorization Methods 0.000 description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 235000010575 Pueraria lobata Nutrition 0.000 description 2
- 244000046146 Pueraria lobata Species 0.000 description 2
- RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 239000003729 cation exchange resin Substances 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 230000008020 evaporation Effects 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 229910052500 inorganic mineral Inorganic materials 0.000 description 2
- 238000005342 ion exchange Methods 0.000 description 2
- GOMNOOKGLZYEJT-UHFFFAOYSA-N isoflavone Chemical compound C=1OC2=CC=CC=C2C(=O)C=1C1=CC=CC=C1 GOMNOOKGLZYEJT-UHFFFAOYSA-N 0.000 description 2
- CJWQYWQDLBZGPD-UHFFFAOYSA-N isoflavone Natural products C1=C(OC)C(OC)=CC(OC)=C1C1=COC2=C(C=CC(C)(C)O3)C3=C(OC)C=C2C1=O CJWQYWQDLBZGPD-UHFFFAOYSA-N 0.000 description 2
- 235000008696 isoflavones Nutrition 0.000 description 2
- 239000011707 mineral Substances 0.000 description 2
- 235000010755 mineral Nutrition 0.000 description 2
- 238000011017 operating method Methods 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 239000012466 permeate Substances 0.000 description 2
- 239000011347 resin Substances 0.000 description 2
- 229920005989 resin Polymers 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- 239000005720 sucrose Substances 0.000 description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 241000238366 Cephalopoda Species 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 229940123457 Free radical scavenger Drugs 0.000 description 1
- 206010028980 Neoplasm Diseases 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- RXUWDKBZZLIASQ-UHFFFAOYSA-N Puerarin Natural products OCC1OC(Oc2c(O)cc(O)c3C(=O)C(=COc23)c4ccc(O)cc4)C(O)C(O)C1O RXUWDKBZZLIASQ-UHFFFAOYSA-N 0.000 description 1
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 235000001014 amino acid Nutrition 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 230000003064 anti-oxidating effect Effects 0.000 description 1
- 230000001754 anti-pyretic effect Effects 0.000 description 1
- 239000002221 antipyretic Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 201000011510 cancer Diseases 0.000 description 1
- 239000013064 chemical raw material Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 230000013872 defecation Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000002526 effect on cardiovascular system Effects 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 229930003944 flavone Natural products 0.000 description 1
- 150000002213 flavones Chemical class 0.000 description 1
- 235000011949 flavones Nutrition 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 229930013032 isoflavonoid Natural products 0.000 description 1
- 150000003817 isoflavonoid derivatives Chemical class 0.000 description 1
- 235000012891 isoflavonoids Nutrition 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 235000018102 proteins Nutrition 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- HKEAFJYKMMKDOR-VPRICQMDSA-N puerarin Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1C1=C(O)C=CC(C2=O)=C1OC=C2C1=CC=C(O)C=C1 HKEAFJYKMMKDOR-VPRICQMDSA-N 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000002516 radical scavenger Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 229910052711 selenium Inorganic materials 0.000 description 1
- 239000011669 selenium Substances 0.000 description 1
- 239000002893 slag Substances 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
- 235000013619 trace mineral Nutrition 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G3/00—Sweetmeats; Confectionery; Marzipan; Coated or filled products
- A23G3/34—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
- A23G3/36—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
- A23G3/48—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds containing plants or parts thereof, e.g. fruits, seeds, extracts
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G3/00—Sweetmeats; Confectionery; Marzipan; Coated or filled products
- A23G3/34—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
- A23G3/36—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
- A23G3/364—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds containing microorganisms or enzymes; containing paramedical or dietetical agents, e.g. vitamins
- A23G3/368—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds containing microorganisms or enzymes; containing paramedical or dietetical agents, e.g. vitamins containing vitamins, antibiotics
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G3/00—Sweetmeats; Confectionery; Marzipan; Coated or filled products
- A23G3/34—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
- A23G3/50—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by shape, structure or physical form, e.g. products with supported structure
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B20/00—Purification of sugar juices
- C13B20/02—Purification of sugar juices using alkaline earth metal compounds
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B20/00—Purification of sugar juices
- C13B20/14—Purification of sugar juices using ion-exchange materials
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B20/00—Purification of sugar juices
- C13B20/16—Purification of sugar juices by physical means, e.g. osmosis or filtration
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B20/00—Purification of sugar juices
- C13B20/16—Purification of sugar juices by physical means, e.g. osmosis or filtration
- C13B20/165—Purification of sugar juices by physical means, e.g. osmosis or filtration using membranes, e.g. osmosis, ultrafiltration
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B50/00—Sugar products, e.g. powdered, lump or liquid sugar; Working-up of sugar
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B50/00—Sugar products, e.g. powdered, lump or liquid sugar; Working-up of sugar
- C13B50/002—Addition of chemicals or other foodstuffs
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G2200/00—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF containing organic compounds, e.g. synthetic flavouring agents
- A23G2200/04—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF containing organic compounds, e.g. synthetic flavouring agents containing vitamins, antibiotics, other medicaments
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G2200/00—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF containing organic compounds, e.g. synthetic flavouring agents
- A23G2200/14—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF containing organic compounds, e.g. synthetic flavouring agents containing fruits, nuts, e.g. almonds, seeds, plants, plant extracts, essential oils
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The invention discloses the production method of a kind of radix puerariae sugar: comprise the following steps: Caulis Sacchari sinensis, after squeeze juice extracting, neutralization, obtains clear juice with ceramic membrane filter；Clear juice, after ion exchange resin desalination, decolouring, through reductions vaporization, cane sugar boiling and crystal, purging, is dried and sieves and obtain the refined white sugar of different-grain diameter；Radix Puerariae cleans, use ultrasound assisted extraction after chopping and defibrination, is performing centrifugal separation on, reverse osmosis concentration and spray drying make Radix Puerariae extract dry powder；By caster sugar, berry sugar and Radix Puerariae extract etc. according to certain proportioning mixing, compressing through Cube sugar machine, be dried to obtain radix puerariae sugar.Product obtained by present invention dissolution velocity in water is fast, has strong Radix Puerariae taste, and contains the most of nutritional labeling in Radix Puerariae, has higher nutritive value, can quickly regain one's strength of body, and being suitable for travels to brew at home drinks.
Description
Technical field
The invention belongs to sucrose processing technique field, particularly relate to the production method of a kind of radix puerariae sugar.
Background technology
Radix Puerariae is the food and medicament dual-purpose natural plant resource that China is traditional, Radix Puerariae rich in isoflavonoid, Pueraria lobota therein
Root element is the distinctive composition of Radix Puerariae, has and promotes cardiovascular and cerebrovascular vessel blood flowing, antioxidation, blood sugar lowering, blood fat reducing, cancer-resisting
Effect, additionally Radix Puerariae also has and relieves the effect of alcohol, antipyretic, enhancing human body immunity power, improves memory and face-nourishing health-care effect, rich in Radix Puerariae
The mineral of the needed by human such as iron content, calcium, phosphorus, zinc, copper, selenium and trace element, therefore Radix Puerariae not only has and also has with Nutrition
There is health-care effect.
Yunnan is medi-edible plant resource kingdom, and unique geography and weather conditions are especially suitable for the growth of Radix Puerariae, in recent years
The exploitation of Radix Puerariae continue to increase, and artificial growth scale constantly expands, Yunnan Radix Puerariae aboundresources, low price.
Radix Puerariae mainly makes injection or oral formulations, defecation process by purification effective ingredient therein at field of medicaments
Complexity, production cost is higher.The most mainly make powder of Radix Puerariae directly eat in edible field or add in other food, powder process
Process have passed through immersion, grinds, filters, rinses, precipitates, the manufacturing process such as is dried, and the product color obtained is pure white, granule is thin
Micro-, but the nutritional labeling major part of Radix Puerariae runs off, and active constituent content is little, greatly reduces the utilization effect of kudzu vine root
Rate.
Caulis Sacchari sinensis is our province lower latitude plateau Ways of Special Agricultural Products, is carried out with abundant medi-edible plant resource by the sugar industry in Yunnan
Organically combining, exploitation has the functional product of high added value, is possible not only to widen sugar industry chain, can be also that Yunnan Guanyuan is special
A prolongable space is opened up in the exploitation of color medi-edible plant resource.
Summary of the invention
Present invention aims to above-mentioned the deficiencies in the prior art, it is provided that the producer of a kind of radix puerariae sugar
Method, by the effective ingredient that will extract in Radix Puerariae, is combined production and obtains a kind of added value higher pueraria root functional sugar product with sucrose
Product.
To achieve these goals, the technical scheme that the present invention provides is as follows:
A kind of production method of radix puerariae sugar, step is as follows:
(1) through 100 mesh filter screen coarse filtration after cane milling extraction of the juice, coarse filtration juice is obtained；By coarse filtration juice with lime cream regulation pH value extremely
7.0, afterwards sugarcane juice it is heated to boiling and keeps 5min, obtaining heating sugarcane juice.
(2) heating sugarcane juice is through microfiltration, ultrafiltration two-stage ceramic membrane filter, obtains colour and is less than less than 5000 IU, turbidity
The clear juice of 150 MAU.
(3) clear juice takes off through macroporous ion exchange resin, salt decolours, and obtains the colour decolouring clear juice less than 1000 IU, ion
Exchange decolorization operations condition is: bleaching temperature 40～70 DEG C, crosses post flow 8～10 BV/h.
(4) decolouring clear juice through be evaporated under reduced pressure, crystallization, purging and be dried make top grade white sugar, through vibrating screen classifier sieve,
Collect and obtain caster sugar and the berry sugar of 0.45～0.8 mm that granularity is 0.14～0.45 mm.
(5) fresh Radix Puerariae clean, broken after, the water adding Radix Puerariae weight 8～10 times carries out defibrination, and gained slurry is through ultrasonic
Extraction 60～90min, carries out solid-liquid separation with centrifuge, and filtering residue repeats to extract once, merging filtrate.
(6) filtrate is concentrated into solid content through rolled film and reaches 30-40%, obtains by crossing 80 mesh sieves after being spray-dried
Radix Puerariae extract dry powder.
(7) caster sugar step (4) made and berry sugar and Radix Puerariae extract dry powder are by weight by caster sugar 25 ~ 35
Part, berry sugar 25 ~ 35 parts and the mixing of 30 ~ 40 parts of Radix Puerariae extract dry powder, through spraying humidification and mix, be pressed into a size of 1.5
The Cube sugar of cm × 1.5 cm × 1.0cm, obtains radix puerariae sugar through microwave drying.
Further, in step (2), microfiltration, ultrafiltration two-stage ceramic membrane filter device use series system to run, and every grade by 3
The ceramic film component composition that group is in parallel；
The microfiltration ceramic membrane aperture selected in step (2) is 500 ~ 800nm, controls filtration temperature at 70 ~ 80 DEG C, filter pressure
0.1 ~ 0.4 MPa, transmembrane pressure 0.1 ~ 0.2 MPa；Ultrafiltration ceramic membrane aperture is 50 ~ 100nm, controls filtration temperature 70 ~ 80
DEG C, filter pressure 0.1 ~ 0.4 MPa, transmembrane pressure 0.05 ~ 0.2 MPa.
In step (5), fiberizer used is disc type paste mill, can be by fully dispersed for Radix Puerariae fiber brooming, beneficially in Radix Puerariae
The leaching of effective ingredient, fiberizer aperture of filter screen is 0.1～0.3mm；Supersound extraction frequency is 40KHz, ultrasonic time 1.5 seconds,
Being spaced 0.8～1.5 second, supersound extraction temperature is 70～80 DEG C.The mesh size of filtering centrifuge is 400 mesh, rotating speed 1200～
1600r/min。
Extracting solution is concentrated, with spray drying by the rolled film using molecular cut off to be 200 ~ 250Da in step (6)
Concentrated solution is dried by device, it is possible to decrease the feed temperature of concentration process, minimizing energy consumption, is spray-dried the wink that can realize extracting solution
Between be dried, it is to avoid the loss of effective active composition under long-time high temperature.Rolled film operating condition is: thickening temperature 30～50 DEG C,
Filter pressure 1.0～4.0MPa；It is spray-dried inlet temperature 140 DEG C, outlet temperature 70～80 DEG C, compressed air pressure 0.3
MPa。
Step (7) is selected the refined white sugar of different-grain diameter, the bond effect of crystal in Cube sugar pressing process can be improved,
Intergranular texture loosens, and in water, dissolution velocity is very fast.
As preferably, Radix Puerariae Cube sugar described in step (7) is formed by the raw material mixing compacting of following weight portion: caster sugar 25
~ 35 parts, berry sugar 25 ~ 35 parts, 30 ~ 40 parts of Radix Puerariae extract powder, vitamin C 1 ~ 3 part.
Compared with prior art, the beneficial effect that the present invention possesses:
The production process of white sugar of the present invention uses pure physics mode to carry out clarifying treatment, removes sugarcane by micro-filtration membrane and ultrafilter membrane
Impurity in juice and macromole coloring matter, utilize ion exchange resin to decolour sugarcane juice, is added without clear in production process
Clear agent and flocculant, replace stove drying decolouring with ion exchange decolouring, it is to avoid chemical raw material and sulfur dioxide in final products
Residual.
The present invention uses by carrying out the effective ingredient of Radix Puerariae extracting, and the product solving directly interpolation powder of Radix Puerariae brews
Rear particle is many, solutions turbid and affect the outward appearance of product and the situation of mouthfeel.
The present invention uses water-swollen squid kudzu vine root, uses ultrasound assisted extraction can shorten extraction time, improves Pueraria lobota
The extraction efficiency of active component in root, extracts process simple, easily operates, in extracting solution in addition to Radix Puerariae total flavones, puerarin, and Pueraria lobota
The compositions such as protein in root, aminoacid, minerals and vitamins are also extracted utilization, farthest remain in Radix Puerariae
Nutritional labeling.Product obtained by present invention dissolution velocity in water is fast, has strong Radix Puerariae taste, and contains in Radix Puerariae
Major part nutritional labeling, has higher nutritive value, can quickly regain one's strength of body, and being suitable for travels to brew at home drinks.
Radix Puerariae isoflavone has stronger oxidation resistance, is good free radical scavenger, and the radix puerariae sugar of the present invention is joined
Side with the addition of vitamin C component, the nutritional labeling of radix puerariae sugar can be increased, the oxidation resistance of Radix Puerariae isoflavone is played simultaneously
The effect strengthened, the most also enriches the taste of radix puerariae sugar, sour-sweet moderate, good in taste.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is described in further detail, but protection scope of the present invention not office
It is limited to this.Composition number of the present invention is according to weight meter.
Embodiment 1:
A kind of production method of radix puerariae sugar, operating procedure is as follows:
(1) Caulis Sacchari sinensis is after squeeze juice extracting, excessively 100 mesh sieve coarse filtrations, and regulation sugarcane juice pH value is 7.0, after heated and boiled keeps 5min,
Deliver to be incubated juice storage box and carry out microfiltration, filtration temperature 78 DEG C by the ceramic membrane filter equipment that ceramic membrane aperture is 500nm, enter film
Pressure 0.21 MPa, transmembrane pressure 0.11 MPa；Permeate via hole diameter again is the ceramic membrane filter equipment ultrafiltration of 50nm, ultrafiltration temperature
Spend 73 DEG C, enter film pressure 0.27 MPa, transmembrane pressure 0.12 MPa, obtain colour be 4139IU, turbidity be the clear of 116MAU
Juice, clear juice is after D001FD storng-acid cation exchange resin and the resin dedicated decolouring of ZGD730 Sugarcane juice decolorization, and decolour mixed liquor
Sample colour is 473IU, meets top grade white sugar product quality requirement, warp through evaporation, crystallization, purging, dried products obtained therefrom
It is 0.14～0.45mm and the caster sugar of 0.45～0.8mm and berry sugar that screening obtains particle diameter.
(2) being cleaned by Radix Puerariae, shred, the water adding 8 times of volumes of Radix Puerariae weight carries out defibrination, and defibrination disposed slurry is at 80 DEG C
Extract 60 min through the ultrasonic assistant of 40 KHz supersonic frequencies, after filter through the centrifuge that aperture of filter screen is 400 mesh, filtering residue
Repeating to extract once, filtrate merging obtains Radix Puerariae extracting solution.
(3) carry out separating concentration by rolled film equipment by Radix Puerariae extracting solution, operate temperature 35 DEG C, filter pressure 2.2
MPa, obtains the Radix Puerariae that solid content is 38.3% and extracts concentrated solution；The spray-dried powder process of concentrated solution, crosses 80 mesh sieves and obtains Pueraria lobota
Root water extract dry powder.
(3) by berry sugar 35 parts and Pueraria lobota that caster sugar 25 parts that granularity is 0.14～0.45 mm, granularity are 0.45～0.8
40 parts of root extract dry powder is sufficiently mixed, through steam spray humidification, mixing, compressing on Cube sugar machine, obtains through microwave drying
It is 1.5 cm × 1.5 cm × 1.0cm radix puerariae sugar to overall dimensions.
Embodiment 2:
A kind of production method of radix puerariae sugar, operating procedure is as follows:
(1) Caulis Sacchari sinensis is after squeeze juice extracting, excessively 100 mesh sieve coarse filtrations, and regulation sugarcane juice pH value is 7.0, after heated and boiled keeps 5min,
It is pumped into insulation juice storage box and carries out microfiltration, filtration temperature 75 DEG C by the ceramic membrane filter equipment that ceramic membrane aperture is 800nm, enter
Film pressure 0.28 MPa, transmembrane pressure 0.13 MPa；Permeate via hole diameter again is that the ceramic membrane filter equipment of 100 nm filters, mistake
Filter temperature 73 DEG C, enter film pressure 0.28 MPa, transmembrane pressure 0.12 MPa, obtain colour be 4729 IU, turbidity be 98 MAU
Clear juice, clear juice is after D001FD storng-acid cation exchange resin and the resin dedicated decolouring of ZGD730 Sugarcane juice decolorization, and decolouring is mixed
Closing liquid sample colour is 385IU, meets top grade white sugar product quality want through evaporation, crystallization, purging, dried products obtained therefrom
Ask, screened obtain 0.14～0.45mm and the caster sugar of 0.45～0.8mm and berry sugar.
(2) being cleaned by Radix Puerariae, shred, the water adding 10 times of volumes of Radix Puerariae weight carries out defibrination, and defibrination disposed slurry is at 80 DEG C
The lower ultrasonic assistant through 40KHz supersonic frequency extracts 50 min, after filter through centrifuge that aperture of filter screen is 400 mesh, filter
Slag repeats to extract once, and filtrate merging obtains Radix Puerariae extracting solution.
(3) carry out separating concentration by reverse osmosis membrane separation equipment by Radix Puerariae extracting solution, operate temperature 37 DEG C, filter pressure
2.6 MPa, obtain the Radix Puerariae that solid content is 36.5% and extract concentrated solution；The spray-dried powder process of concentrated solution, crosses 80 mesh sieves and obtains
To Radix Puerariae water extract dry powder.
(4) by berry sugar 30 parts and Pueraria lobota that caster sugar 30 parts that granularity is 0.14～0.45 mm, granularity are 0.45～0.8
38 parts of root extract dry powder, 2 parts of vitamin C powder are put in mixing machine, through steam spray humidification, mixing, press on Cube sugar machine
Making type, obtaining overall dimensions through microwave drying is 1.5 cm × 1.5 cm × 1.0cm Radix Puerariae Cube sugar.
Claims (6)
1. the production method of a radix puerariae sugar, it is characterised in that comprise the following steps:
(1) coarse filtration juice is obtained through 100 mesh filter screen coarse filtration after cane milling extraction of the juice, by coarse filtration juice with lime cream regulation pH value to 7.0
It is heated to boiling afterwards and keeps 5min, obtaining heating sugarcane juice；
(2) heating sugarcane juice filters through microfiltration and ultrafiltration two-stage ceramic membrane filter device, obtains colour less than 5000 IU, turbidity
Clear juice less than 150 MAU；
(3) clear juice is through macroporous ion exchange resin desalination, decolouring, obtains the colour decolouring clear juice less than 1000 IU, operating condition
For: bleaching temperature 40 ~ 70 DEG C, cross post flow 8 ~ 10 BV/h；
(4) decolouring clear juice through reduction vaporization, crystallization, purging and is dried to obtain the colour top grade white sugar less than 60 IU, through vibration
Screening machine sieves, and collects and obtains the caster sugar that granularity is 0.14 ~ 0.45 mm and the berry sugar that granularity is 0.45 ~ 0.8 mm, treats
With；
(5), after fresh Radix Puerariae is clean, broken, the water adding Radix Puerariae weight 8 ~ 10 times carries out defibrination, and gained slurry is through ultrasonic extraction
50 ~ 60min, carries out solid-liquid separation with centrifuge, and filtering residue repeats to extract once, merging filtrate；
(6) filtrate is concentrated into solid content through rolled film and reaches 30-40%, obtains Radix Puerariae by spray dried 80 mesh sieves and carries
Take thing dry powder；
(7) caster sugar step (4) made and berry sugar and Radix Puerariae extract dry powder by weight by caster sugar 25 ~ 35 parts,
Berry sugar 25 ~ 35 parts and the mixing of 30 ~ 40 parts of Radix Puerariae extract dry powder, through spraying humidification and mix, be pressed into a size of 1.5 cm
The Cube sugar of × 1.5 cm × 1.0cm, obtains radix puerariae sugar through microwave drying.
2. the production method of the radix puerariae sugar as described in claim 1, it is characterised in that: microfiltration, ultrafiltration two-stage pottery in step (2)
Porcelain film filter uses series system to run, and every grade is made up of 3 groups of ceramic film components in parallel.
3. the production method of the radix puerariae sugar as described in claim 1 or 2, it is characterised in that: the microfiltration pottery selected in step (2)
Porcelain membrane aperture is 500 ~ 800nm, controls filtration temperature at 70 ~ 80 DEG C, filter pressure 0.1 ~ 0.4 MPa, transmembrane pressure 0.1 ~ 0.2
MPa；Ultrafiltration ceramic membrane aperture is 50 ~ 100nm, controls filtration temperature at 70 ~ 80 DEG C, filter pressure 0.1 ~ 0.4 MPa, transmembrane pressure
Differ from 0.05 ~ 0.2 MPa.
4. the production method of the radix puerariae sugar as described in claim 1, it is characterised in that: step (5) carries out defibrination employing dish
Formula fiberizer, the aperture of filter screen of this fiberizer is 0.1 ~ 0.3mm；The frequency of ultrasonic extraction is 40KHz, ultrasonic time 1.5 seconds,
Every 0.8 ~ 1.5 second, controlling temperature during ultrasonic extraction was 70 ~ 80 DEG C；The mesh size of solid-liquid separation centrifuge is 400 mesh, turns
Speed is 1200 ~ 1600r/min.
5. the production method of the radix puerariae sugar as described in claim 1, it is characterised in that: in step (6), rolled film retains molecule
Amount is 200 ~ 250Da, and thickening temperature is 30 ~ 50 DEG C, filter pressure 1.0 ~ 4.0MPa；Inlet temperature 140 is controlled during spray drying
DEG C, leaving air temp 70 ~ 80 DEG C, compressed air pressure 0.3 MPa.
6. the production method of the radix puerariae sugar as described in claim 1, it is characterised in that: Radix Puerariae Cube sugar described in step (7) by
The raw material mixing compacting of following weight portion forms: caster sugar 25 ~ 35 parts, berry sugar 25 ~ 35 parts, Radix Puerariae extract powder 30 ~ 40
Part, vitamin C 1 ~ 3 part.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109007213A (en) * | 2018-07-10 | 2018-12-18 | 青岛高新区尚达医药研究所 | A kind of relieving alcoholism and protecting liver sugar cube and preparation method thereof |
| CN109007688A (en) * | 2018-06-15 | 2018-12-18 | 恩施硒谷科技股份有限公司 | A kind of preparation method of selenium-rich pueraria lobata activity powder |
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| CN102100291A (en) * | 2009-12-17 | 2011-06-22 | 苏州知微堂生物科技有限公司 | Preparation technology of functional confectionary with radix puerariae sugar |
| CN103937913A (en) * | 2014-04-20 | 2014-07-23 | 厦门世达膜科技有限公司 | White granulated sugar production technology |
| CN103976124A (en) * | 2014-05-29 | 2014-08-13 | 洛阳本草生物制药股份有限公司 | Process for preparing kudzu root candies |
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| CN102100291A (en) * | 2009-12-17 | 2011-06-22 | 苏州知微堂生物科技有限公司 | Preparation technology of functional confectionary with radix puerariae sugar |
| CN102031315A (en) * | 2010-11-30 | 2011-04-27 | 华南理工大学 | Method for regenerating sugar making decolorized and decalcified resin and method for recycling regeneration waste liquid |
| CN103937913A (en) * | 2014-04-20 | 2014-07-23 | 厦门世达膜科技有限公司 | White granulated sugar production technology |
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| CN109007688A (en) * | 2018-06-15 | 2018-12-18 | 恩施硒谷科技股份有限公司 | A kind of preparation method of selenium-rich pueraria lobata activity powder |
| CN109007213A (en) * | 2018-07-10 | 2018-12-18 | 青岛高新区尚达医药研究所 | A kind of relieving alcoholism and protecting liver sugar cube and preparation method thereof |
| CN115363130A (en) * | 2018-07-10 | 2022-11-22 | 青岛高新区尚达医药研究所 | Alcohol-dispelling and liver-protecting cube sugar and application thereof |
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