CN106135213A - A kind of Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor and preparation and application thereof - Google Patents

A kind of Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor and preparation and application thereof Download PDF

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Publication number
CN106135213A
CN106135213A CN201610512818.0A CN201610512818A CN106135213A CN 106135213 A CN106135213 A CN 106135213A CN 201610512818 A CN201610512818 A CN 201610512818A CN 106135213 A CN106135213 A CN 106135213A
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lodging
hot
tritici aestivi
semen tritici
liquor
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李明
费云鹏
王新玉
王书平
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Beijing Tianchenyun Farm Technology Co Ltd
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Beijing Tianchenyun Farm Technology Co Ltd
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Priority to CN201610512818.0A priority Critical patent/CN106135213A/en
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/34Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
    • A01N43/40Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom six-membered rings
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01GHORTICULTURE; CULTIVATION OF VEGETABLES, FLOWERS, RICE, FRUIT, VINES, HOPS OR SEAWEED; FORESTRY; WATERING
    • A01G7/00Botany in general
    • A01G7/06Treatment of growing trees or plants, e.g. for preventing decay of wood, for tingeing flowers or wood, for prolonging the life of plants
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/02Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
    • A01N25/04Dispersions, emulsions, suspoemulsions, suspension concentrates or gels
    • A01N25/06Aerosols
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N33/00Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
    • A01N33/02Amines; Quaternary ammonium compounds
    • A01N33/12Quaternary ammonium compounds
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/10Aromatic or araliphatic carboxylic acids, or thio analogues thereof; Derivatives thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/90Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system

Abstract

The invention belongs to agricultural technology field, relate to a kind of Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor, Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor, each component mixes according to following parts by weight proportioning: active component 2 30%, solvent 5 15%, surfactant 2 6%, water 43 87.9%.Have the beneficial effects that with strong points, nontoxic pollution-free, low cost, easy to operate, effect stability is notable, can prevent and resist the harm of hot dry wind and lodging, make Semen Tritici aestivi normally be in the milk and obtain preferable yield and quality, and there is the functional characteristic of " having calamity mitigation, increase production without calamity ".

Description

A kind of Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor and preparation and application thereof
Technical field
The invention belongs to agricultural technology field, relate to a kind of Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor and preparation thereof and use Method.
Background technology
Hot dry wind also known as " dry wind ", " hot run test ", custom is referred to as " fire south wind " or " windburn ", after being Growth of Wheat A kind of high temperature, low humidity the comprehensive agricultural meteorological disaster with certain wind-force that phase occurs, is northern China Winter Wheat Area Semen Tritici aestivi One of meteorological disaster main in production.Hot dry wind is also the environmental stress factor of Semen Tritici aestivi, and Semen Tritici aestivi is during hot dry wind, rising Intensity increases, and moisture supply-demand imbalance, normal physiological activity is suppressed or destroys, and promotes Wheat in Grain Filling Stage to shorten, mass of 1000 kernel Decline, can make time serious Semen Tritici aestivi blue or green dry force ripe.General time hot dry wind can make wheat yield 10%~20%, the serious time underproduction More than 30%.
After Semen Tritici aestivi is endangered by hot dry wind, showing as grain husk shell greyish white unglazed in formalness, awns point is withered to bleach, and the awn of wheat is opened The angle opened is ascending, and boot leaf moves back Lu, wilting, and cane green grass or young crops is withered, and severe one Jiao's head explodes awns, and stem and leaf is gloomy unglazed.Hot dry wind disaster Mainly having a three types: 1, the low wet type of high temperature: be characterized in high temperature, arid, have certain wind-force, wind exacerbates dry, hot shadow Ringing, this weather makes that the dry point of Semen Tritici aestivi, plant be withered and yellow, wheat grain is done not plump and affected yield.It is the main class of wheat district, north hot dry wind Type.2, dead ripeness type after rain: being characterized in after rain high temperature and the finest, Exposure to Sunlight is strong, and hot blast blows hard, and causes the blue or green withered and dead ripeness of Semen Tritici aestivi. 3, drought wind type: feature is that humidity is low, wind speed big, but daily maximum temperature is not necessarily higher than 30 degree.
Wheat lodging disaster refers to, gives birth to middle and late stage at Semen Tritici aestivi, because climate factor or cultivation step are improper, causes little Wheat large area is toppled over, and has a strong impact on Semen Tritici aestivi ripe, reduces mass of 1000 kernel, causes a kind of phenomenon of the underproduction.Lodging is that Semen Tritici aestivi is close Plant high-yield culturing and the serious significant obstacle factor reducing marketing quality.Data shows according to the study: Semen Tritici aestivi is in lodging meeting in boot stage The underproduction 31%, the pustulation period lodging meeting underproduction 25%, kernel maturity stage lodging the underproduction 12%, even straw bending also can cause and subtract Produce.
Wheat lodging is mainly affected by the factor of kind lodging resistance, cultivation step and natural disaster.Can be divided into root lodging with Stem lodges.Root lodging is bad mainly due to root system development, takes root not deep, and secondary root is few and thin and delicate, aerial parts of giving away Weight and occur.It is the most shallow that generation is primarily due to arable layer, wholely, seeding quality poor etc., cause root system development Bad, bury shallower, or because early stage is not watered, later stage irrigation amount is excessive, soil layer is wet soft, then meets wind and rain and the lodging that causes.Stem Lodging is owing to the mechanical tissue of basal part of stem is undeveloped, and first and second internode is long to be caused.Usual reason is because of application rate mistake Greatly, rich water is sufficient, and particularly nitrogen application is too much, miscarriage, and causes tiller too much, and colony is excessive, and polarization is slow, field Between strongly fragrant cover, illumination is the most not enough, and basal internode is long, and stalk wall is thin and unreal, and dry-matter accumulation is few, meets wind and rain invasion and attack, the lower portion of the stem Bend or fracture and cause.
Plant growth regulator, is the class pesticide grown for coordinate plant growth, has sky including synthetic The so compound of phytohormone similar action and natural phytohormone of extracting from biology.For target plant, plant is raw Long regulator is the non-nutritive chemical substance of external source, generally can conduct in plant to site of action, with the lowest concentration Just can promote or suppress some link of its life process, be allowed to the needs to meeting the mankind and develop.
According to the difference of water consumption, pesticide spray can be divided into again Large Copacity spraying (every mu of use water 50~100kg), middle appearance (every mu of use water is few for amount spraying (every mu of use water 10~30kg), low-gallonage spraying (every mu of use water 1~10kg) and ultra-low volume spray In 1kg).Conventional dispenser typically uses medium volume spraying.
Along with the development of unmanned air vehicle technique, the unmanned plane during flying dispenser risen in plant protection field, to the use of pesticide Bring new revolution.Unmanned plane dispenser has the advantages that effect is high, expenses for prevention and control is low, dosage is few, especially executes in paddy field Medicine, extreme terrain dispenser, concentration Unifying control dispenser field, compared with traditional insecticide-applying way, have obvious advantage.But nothing Another feature of man-machine dispenser is that water consumption is few, when conventional pesticide is used for unmanned plane dispenser, and low-gallonage spraying to be used, this Time drug effect be difficult to ensure.Droplet drift, droplet when frequently resulting in the drug effect reduction of medicament, dispenser volatilize, rotation oar gas The problems such as stream impact.
Existing plant growth regulator formulations mainly includes powder, water preparation etc., and plant growth regulator is ultralow Volume sprays liquor has no report both at home and abroad.
Typically by screening, volatility is low, lightning is high, molten to crop safety good to former medicine dissolubility for ultra low volume liquids Agent, is not watered during dispenser, but straight with ultra low volume sprayer tool, low-gallonage spraying apparatus or ultra-low volume electrostatic spray apparatus Connect and use.Ultra-low volume spray is owing to spraying from leaving aerosol apparatus without high volatile ingredient, its size of medicinal liquid and quality in droplet Head does not has significant change during arriving target, decreases volatilization and the drift of medicament.Droplet is tiny and uniform, it is possible to notable Improve the deposition of medicinal liquid.Owing to using without being watered, ultra-low volume spray liquor is suitable for water resource shortage, pest and disease damage collection Middle fulminant large area occurs and dispenser on a large scale in needing the short time, and specialized Unifying control dispenser, the most ultralow Volume sprays significantly reduces the labor intensity of operator.
The conventional spraying methods spraying commonly used regular dosage form of current domestic plant growth regulator, is that plant is raw Long regulator preparation carries out medicament sprinkling after diluting with a large amount of water, and this prevention and controls exists various problems:
1. conventional spraying work efficiency is low, and work efficiency is only 2~5 mus/day the most per capita, it is difficult to meet the needs of implantation in large scale, Along with domestic land transformation policy is to implement, soil presents the trend of intensive management, occurs that increasing agricultural planting is big Family, crop contiguous plant area increases;And along with China's aged tendency of population and the appearance of recruitment famine, labour force is increasingly becoming dilute Lacking resource, human cost improves constantly, and agriculture production cost continues to increase, and adds the seasonal obvious of agricultural production, medicament Sprinkling generally requires uses substantial amounts of manpower at short notice.
2. conventional spraying needs substantial amounts of water, and usual water consumption reaches 10~30kg, and is much lacking away from water source and arid The area of water, reduces water consumption spraying and can not reach preferable pharmacy effect effect.
3. conventional nebulization uses medicament lightning, volatility do not meet low-gallonage spraying dispenser requirement.
Summary of the invention
The technical problem to be solved is to provide a kind of Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor and preparation thereof And using method, with strong points, nontoxic pollution-free, low cost, easy to operate, effect stability notable, can prevent and resist dry Hot blast and the harm of lodging, make Semen Tritici aestivi normally be in the milk and obtain preferable yield and quality, and has " having calamity mitigation, increase production without calamity " Functional characteristic, to solve the defect of prior art.
The invention discloses Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor, each component is mixed according to following parts by weight proportioning Close: active component 2-30%, solvent 5-15%, surfactant 2-6%, water 43-87.9%.
Further, described active component be paclobutrazol (common name paclobutrazol, has another name called: neoprene azoles, PP333, MET), chlorocholine chloride (common name chlormequat, has another name called: CCC, monobutyltin trichloride choline, three Western regions), first piperazine (common name Mepiquatchloride, has another name called: methyl piperidine, regulation amine, mepiquat chloride, help strong element), TrinexAN_SNacethyl (common name trinexapac- Ethyl), 5 nitroguaiacol sodium, onitrophenol, sodium paranitrophenol, isopentenyl gland purine (common name Isoamyl Alkenyl adenine, oxyenadenine+enadenine), α-naphthaleneacidsodium, in tridecyl alcohol one or more arbitrarily than Example mixture;
Further, described solvent is methanol, ethanol, capryl alcohol, N-Methyl pyrrolidone, spectrasolv DMDA, N, In N-dimethyl acetylamide, jatropha curcas oil, soybean oil, Semen Maydis oil, Oleum Gossypii semen, Oleum Brassicae campestris, Oleum Ricini, Oleum Terebinthinae one or more Arbitrary proportion mixture.
Further, described surfactant is calcium dodecyl benzene sulfonate (agriculture breast 500#), fatty alcohol-polyoxyethylene ether AEO-5, fatty alcohol-polyoxyethylene ether AEO-7, fatty alcohol-polyoxyethylene ether AEO-9, castor oil polyoxyethylene ether EL-10, Semen Ricini Oil polyoxyethylene ether EL-20, castor oil polyoxyethylene ether EL-40, tristyrylphenol polyoxyethylene ether phosphate ester three ethanol The arbitrary proportion mixture of one or more in amine salt AP-3, emulsifying agent Emulson AG PE, emulsifying agent Emulson AG104.
Further, also include that thickening agent, described thickening agent are xanthan gum, Radix Acaciae senegalis, sodium alginate, Polyethylene Glycol In one or more arbitrary proportion mixture.
Further, also include that antifreezing agent, described antifreezing agent are one or more in ethylene glycol, propylene glycol, diethylene glycol Arbitrary proportion mixture.
The invention also discloses the preparation method of a kind of Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor, prepare as follows Form:
By described active component and described solvent according to formula proportion stirring and dissolving;
Described surfactant, described thickening agent, described antifreezing agent, water, low whipping speed is added according still further to formula proportion Under the conditions of 1500-5000r/min, stir 20-60min so that it is mix homogeneously, obtain Semen Tritici aestivi hot-dry wind tolerance spray liquid resistant to lodging Agent.
Further, the invention also discloses the using method of described Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor: medicament Mu spouting liquid is 1-1.5kg, in employing Direct spraying, ultra-low volume spray, low-gallonage spraying or ultra-low volume electrostatic spray extremely Few a kind of means are sprayed.
The beneficial effects of the present invention is following some:
The most with strong points, nontoxic pollution-free, low cost, easy to operate, effect stability is notable.
2. can prevent and resist the harm of hot dry wind and lodging, make Semen Tritici aestivi normally be in the milk and obtain preferable yield and product Matter.
3. there is the functional characteristic of " having calamity mitigation, increase production without calamity ".
Detailed description of the invention
Being further described the detailed description of the invention of the present invention below in conjunction with embodiment, following example are only used for more Clearly demonstrate the technical em-bodiments of the present invention, and can not limit the scope of the invention with this.
Embodiment 1
30% first piperazine isopentenyl gland purine Semen Tritici aestivi hot-dry wind tolerance ultra-low volume spray resistant to lodging liquor
Formula is by following weight proportion:
Component Percentage by weight
First piperazine 28%
Isopentenyl gland purine 2%
N-Methyl pyrrolidone 5%
Oleum Ricini 10%
Calcium dodecyl benzene sulfonate 2%
Fatty alcohol-polyoxyethylene ether AEO-7 4%
Xanthan gum 0.2%
Ethylene glycol 4%
Water 44.8%
Preparation method:
In the reactor of band high speed shear, first with solvent by after active component stirring and dissolving, add surfactant, Thickening agent, antifreezing agent and water, high speed shear 30 minutes, shear rate is 5000 revs/min, and temperature is room temperature.I.e. obtain 30% First piperazine isopentenyl gland purine Semen Tritici aestivi hot-dry wind tolerance ultra-low volume spray resistant to lodging liquor.
Further, described active component can also be paclobutrazol (common name paclobutrazol, has another name called: neoprene azoles, PP333, MET), chlorocholine chloride (common name chlormequat, has another name called: CCC, monobutyltin trichloride choline, three Western regions), first piperazine (common name Mepiquatchloride, has another name called: methyl piperidine, regulation amine, mepiquat chloride, help strong element), TrinexAN_SNacethyl (common name trinexapac- Ethyl), 5 nitroguaiacol sodium, onitrophenol, sodium paranitrophenol, isopentenyl gland purine (common name Isoamyl Alkenyl adenine, oxyenadenine+enadenine), α-naphthaleneacidsodium, arbitrary proportion mixing several in tridecyl alcohol Thing;
Further, described solvent can also be methanol, ethanol, capryl alcohol, N-Methyl pyrrolidone, N, N-dimethyl caprinoyl In amine, N,N-dimethylacetamide, jatropha curcas oil, soybean oil, Semen Maydis oil, Oleum Gossypii semen, Oleum Brassicae campestris, Oleum Ricini, Oleum Terebinthinae several Arbitrary proportion mixture.
Further, described surfactant can also be calcium dodecyl benzene sulfonate (agriculture breast 500#), fatty alcohol polyoxy Vinyl Ether AEO-5, fatty alcohol-polyoxyethylene ether AEO-7, fatty alcohol-polyoxyethylene ether AEO-9, castor oil polyoxyethylene ether EL- 10, castor oil polyoxyethylene ether EL-20, castor oil polyoxyethylene ether EL-40, tristyrylphenol polyoxyethylene ether phosphate ester Arbitrary proportion mixture several in triethanolamine salt AP-3, emulsifying agent Emulson AG PE, emulsifying agent Emulson AG104.
Further, described thickening agent can also be several in xanthan gum, Radix Acaciae senegalis, sodium alginate, Polyethylene Glycol Arbitrary proportion mixture.
Further, the arbitrary proportion mixture that described antifreezing agent is several in being ethylene glycol, propylene glycol, diethylene glycol.
Embodiment 2
32% chlorocholine chloride isopentenyl gland purine Semen Tritici aestivi hot-dry wind tolerance ultra-low volume spray resistant to lodging liquor
Formula is by following weight proportion:
Preparation method:
In the reactor of band high speed shear, first with solvent by after active component stirring and dissolving, add surfactant, Thickening agent, antifreezing agent and water, high speed shear 25 minutes, shear rate is 5000 revs/min, and temperature is room temperature.I.e. obtain 32% Chlorocholine chloride isopentenyl gland purine Semen Tritici aestivi hot-dry wind tolerance ultra-low volume spray resistant to lodging liquor.
Embodiment 3
48% first piperazine α-naphthaleneacidsodium Semen Tritici aestivi hot-dry wind tolerance ultra-low volume spray resistant to lodging liquor
Formula is by following weight proportion:
Preparation method:
In the reactor of band high speed shear, first with solvent by after active component stirring and dissolving, add surfactant, Thickening agent, antifreezing agent and water, high speed shear 30 minutes, shear rate is 5000 revs/min, and temperature is room temperature.I.e. obtain 48% First piperazine α-naphthaleneacidsodium Semen Tritici aestivi hot-dry wind tolerance ultra-low volume spray resistant to lodging liquor.
Embodiment 4
22% α-naphthaleneacidsodium isopentenyl gland purine Semen Tritici aestivi hot-dry wind tolerance ultra-low volume spray resistant to lodging liquor
Formula is by following weight proportion:
Component Percentage by weight
α-naphthaleneacidsodium 20%
Isopentenyl gland purine 2%
Capryl alcohol 10%
Semen Maydis oil 2%
Calcium dodecyl benzene sulfonate (agriculture breast 500#) 3%
Emulsifying agent Emulson AG PE 3%
Sodium alginate 0.2%
Propylene glycol 4%
Water 26.8%
Preparation method:
In the reactor of band high speed shear, first with solvent by after active component stirring and dissolving, add surfactant, Thickening agent, antifreezing agent and water, high speed shear 30 minutes, shear rate is 5000 revs/min, and temperature is room temperature.I.e. obtain 22% α-naphthaleneacidsodium isopentenyl gland purine Semen Tritici aestivi hot-dry wind tolerance ultra-low volume spray resistant to lodging liquor.
Product quality detection method
(1) viscosimetric analysis
DJ-1 type rotation r viscometer is used to measure, it is desirable to viscosity is 300~600cp, and this viscosity can make preparation stabilization.
(2) low-temperature stability test
Take in the sample addition centrifuge tube of 100, refrigerator is cooled to (0 ± 2) DEG C, allows centrifuge tube and content (0 ± 2) keep 1h at DEG C, stir once every 15min therebetween, each 15s, check and record and analyse with or without solids or grease Go out.Centrifuge tube is put back to refrigerator, at (0 ± 2) DEG C, continues to place 7d, centrifuge tube is taken out, room temperature (less than 20 DEG C) The volume of lower standing 3h, centrifugation 15min (pipe top relative centrifugal force(RCF) is 500~600g) record tube bottom precipitate (being accurate to 0.05mL).Precipitate is qualified less than 0.3mL.
(3) heat storage stability test
With syringe, about 30mL sample is injected in clean ampoule bottle (avoiding sample contacts bottleneck), put this ampoule bottle in Cryosel bath is freezed, seals rapidly (avoiding solvent to volatilize) with thermal-flame, at least envelope 3 bottles, be cooled to room temperature and weigh.To seal Ampoule bottle be placed in canister, then canister is put in 54 ± 2 DEG C of calorstats, places 14d, take out and be cooled to room Temperature, by wiped clean outside ampoule bottle, weighs respectively, the sample that quality does not changes, and observes emulsion-stabilizing situation.
(4) product safety in utilization test
After dispenser 3 days, 7 days, investigate plant growth situation, pass judgment on each process community and blank community crop Undermined symptom, to determine the medicament safety to Semen Tritici aestivi.
Table 1 Semen Tritici aestivi is by poisoning grade scale
Rank To Semen Tritici aestivi extent of injury
1 Growth is normal
2 Slight poisoning
3 Medium poisoning, can recover
4 Poisoning is heavier, it is difficult to recover
5 Poisoning is heavier, it is difficult to recover
(5) volatility measures (filter paper enzyme): weigh 0.5g solution to be measured, drips in filter paper central authorities, weighs record and adds Enter the quality before and after medicinal liquid, be repeated 3 times, be placed in ventilating kitchen, measure scraps of paper weight at 60min, 120min respectively.Calculate volatilization Rate.
Result of the test
Table 2 Semen Tritici aestivi hot-dry wind tolerance ultra-low volume spray resistant to lodging liquor capability and performance testing result
Table 3 Semen Tritici aestivi hot-dry wind tolerance ultra-low volume spray resistant to lodging liquor volatility measurement result
Spray carrier Volatility % (60min) Volatility % (120min) Evaluation of result
Example 1 26.5 36.6 Qualified
Example 2 22.4 32.5 Qualified
Example 3 25.6 34.2 Qualified
Example 4 27.7 38.9 Qualified
Clear water CK 88.5 100.0
The above is only the preferred embodiments of the present invention, it is noted that for the ordinary skill people of the art For Yuan, on the premise of without departing from the technology of the present invention principle, it is also possible to make some improvements and modifications, these improvements and modifications Also should be regarded as protection scope of the present invention.

Claims (8)

1. a Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor, it is characterised in that each component is mixed according to following parts by weight proportioning Close: active component 2-30%, solvent 5-15%, surfactant 2-6%, water 43-87.9%.
2. Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor as claimed in claim 1, it is characterised in that described active component is many Effect azoles, chlorocholine chloride, first piperazine, TrinexAN_SNacethyl, 5 nitroguaiacol sodium, onitrophenol, sodium paranitrophenol, isopentenyl gland The arbitrary proportion mixture of one or more in purine, α-naphthaleneacidsodium, tridecyl alcohol.
3. Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor as claimed in claim 1, it is characterised in that described solvent be methanol, Ethanol, capryl alcohol, N-Methyl pyrrolidone, spectrasolv DMDA, N,N-dimethylacetamide, jatropha curcas oil, soybean oil, jade The arbitrary proportion mixture of one or more in Miyou, Oleum Gossypii semen, Oleum Brassicae campestris, Oleum Ricini, Oleum Terebinthinae.
4. Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor as claimed in claim 1, it is characterised in that described surfactant is Calcium dodecyl benzene sulfonate, fatty alcohol-polyoxyethylene ether, fatty alcohol-polyoxyethylene ether, fatty alcohol-polyoxyethylene ether, Oleum Ricini are poly- Oxygen vinyl Ether, castor oil polyoxyethylene ether, castor oil polyoxyethylene ether, tristyrylphenol polyoxyethylene ether phosphate ester three second The arbitrary proportion mixture of one or more in alcohol amine salt, emulsifying agent Emulson AG PE, emulsifying agent Emulson AG104.
5. Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor as claimed in claim 1, it is characterised in that also include thickening agent, institute Stating thickening agent is the arbitrary proportion mixture of one or more in xanthan gum, Radix Acaciae senegalis, sodium alginate, Polyethylene Glycol.
6. Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor as claimed in claim 1, it is characterised in that also include antifreezing agent, institute Stating antifreezing agent is the arbitrary proportion mixture of one or more in ethylene glycol, propylene glycol, diethylene glycol.
7. the preparation method of a Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor, it is characterised in that be prepared from as follows:
By described active component and described solvent according to formula proportion stirring and dissolving;
Adding described surfactant, described thickening agent, described antifreezing agent, water according still further to formula proportion, low whipping speed is Under the conditions of 1500-5000r/min, stir 20-60min so that it is mix homogeneously, obtain Semen Tritici aestivi hot-dry wind tolerance spray liquid resistant to lodging Agent.
8. the using method of a Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor, it is characterised in that use as follows: medicament Mu spouting liquid is 1-1.5kg, in employing Direct spraying, ultra-low volume spray, low-gallonage spraying or ultra-low volume electrostatic spray extremely Few a kind of means are sprayed.
CN201610512818.0A 2016-07-01 2016-07-01 A kind of Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor and preparation and application thereof Pending CN106135213A (en)

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CN107014709A (en) * 2017-04-20 2017-08-04 山西省农业科学院小麦研究所 Utilize intermission seeding identification water ground Wheat in Grain Filling Stage high temperature resistant dry heat resistance wind method
CN109006264A (en) * 2018-06-17 2018-12-18 河北省农林科学院旱作农业研究所 New wheat breed dry heat resistance wind identification method and Special temp controlling canopy
CN110881470A (en) * 2019-09-27 2020-03-17 四川国光农化股份有限公司 Suspending agent composition, suspending agent, and preparation process and application thereof
CN115363027A (en) * 2022-09-14 2022-11-22 四川国光农化股份有限公司 Pesticide ultra-low volume liquid and preparation method and application thereof

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CN107014709A (en) * 2017-04-20 2017-08-04 山西省农业科学院小麦研究所 Utilize intermission seeding identification water ground Wheat in Grain Filling Stage high temperature resistant dry heat resistance wind method
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CN109006264A (en) * 2018-06-17 2018-12-18 河北省农林科学院旱作农业研究所 New wheat breed dry heat resistance wind identification method and Special temp controlling canopy
CN110881470A (en) * 2019-09-27 2020-03-17 四川国光农化股份有限公司 Suspending agent composition, suspending agent, and preparation process and application thereof
CN115363027A (en) * 2022-09-14 2022-11-22 四川国光农化股份有限公司 Pesticide ultra-low volume liquid and preparation method and application thereof

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