CN106135213A - A kind of Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor and preparation and application thereof - Google Patents
A kind of Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor and preparation and application thereof Download PDFInfo
- Publication number
- CN106135213A CN106135213A CN201610512818.0A CN201610512818A CN106135213A CN 106135213 A CN106135213 A CN 106135213A CN 201610512818 A CN201610512818 A CN 201610512818A CN 106135213 A CN106135213 A CN 106135213A
- Authority
- CN
- China
- Prior art keywords
- lodging
- hot
- tritici aestivi
- semen tritici
- liquor
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
- A01N43/40—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom six-membered rings
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01G—HORTICULTURE; CULTIVATION OF VEGETABLES, FLOWERS, RICE, FRUIT, VINES, HOPS OR SEAWEED; FORESTRY; WATERING
- A01G7/00—Botany in general
- A01G7/06—Treatment of growing trees or plants, e.g. for preventing decay of wood, for tingeing flowers or wood, for prolonging the life of plants
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
- A01N25/04—Dispersions, emulsions, suspoemulsions, suspension concentrates or gels
- A01N25/06—Aerosols
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N33/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
- A01N33/02—Amines; Quaternary ammonium compounds
- A01N33/12—Quaternary ammonium compounds
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/10—Aromatic or araliphatic carboxylic acids, or thio analogues thereof; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
Abstract
The invention belongs to agricultural technology field, relate to a kind of Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor, Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor, each component mixes according to following parts by weight proportioning: active component 2 30%, solvent 5 15%, surfactant 2 6%, water 43 87.9%.Have the beneficial effects that with strong points, nontoxic pollution-free, low cost, easy to operate, effect stability is notable, can prevent and resist the harm of hot dry wind and lodging, make Semen Tritici aestivi normally be in the milk and obtain preferable yield and quality, and there is the functional characteristic of " having calamity mitigation, increase production without calamity ".
Description
Technical field
The invention belongs to agricultural technology field, relate to a kind of Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor and preparation thereof and use
Method.
Background technology
Hot dry wind also known as " dry wind ", " hot run test ", custom is referred to as " fire south wind " or " windburn ", after being Growth of Wheat
A kind of high temperature, low humidity the comprehensive agricultural meteorological disaster with certain wind-force that phase occurs, is northern China Winter Wheat Area Semen Tritici aestivi
One of meteorological disaster main in production.Hot dry wind is also the environmental stress factor of Semen Tritici aestivi, and Semen Tritici aestivi is during hot dry wind, rising
Intensity increases, and moisture supply-demand imbalance, normal physiological activity is suppressed or destroys, and promotes Wheat in Grain Filling Stage to shorten, mass of 1000 kernel
Decline, can make time serious Semen Tritici aestivi blue or green dry force ripe.General time hot dry wind can make wheat yield 10%~20%, the serious time underproduction
More than 30%.
After Semen Tritici aestivi is endangered by hot dry wind, showing as grain husk shell greyish white unglazed in formalness, awns point is withered to bleach, and the awn of wheat is opened
The angle opened is ascending, and boot leaf moves back Lu, wilting, and cane green grass or young crops is withered, and severe one Jiao's head explodes awns, and stem and leaf is gloomy unglazed.Hot dry wind disaster
Mainly having a three types: 1, the low wet type of high temperature: be characterized in high temperature, arid, have certain wind-force, wind exacerbates dry, hot shadow
Ringing, this weather makes that the dry point of Semen Tritici aestivi, plant be withered and yellow, wheat grain is done not plump and affected yield.It is the main class of wheat district, north hot dry wind
Type.2, dead ripeness type after rain: being characterized in after rain high temperature and the finest, Exposure to Sunlight is strong, and hot blast blows hard, and causes the blue or green withered and dead ripeness of Semen Tritici aestivi.
3, drought wind type: feature is that humidity is low, wind speed big, but daily maximum temperature is not necessarily higher than 30 degree.
Wheat lodging disaster refers to, gives birth to middle and late stage at Semen Tritici aestivi, because climate factor or cultivation step are improper, causes little
Wheat large area is toppled over, and has a strong impact on Semen Tritici aestivi ripe, reduces mass of 1000 kernel, causes a kind of phenomenon of the underproduction.Lodging is that Semen Tritici aestivi is close
Plant high-yield culturing and the serious significant obstacle factor reducing marketing quality.Data shows according to the study: Semen Tritici aestivi is in lodging meeting in boot stage
The underproduction 31%, the pustulation period lodging meeting underproduction 25%, kernel maturity stage lodging the underproduction 12%, even straw bending also can cause and subtract
Produce.
Wheat lodging is mainly affected by the factor of kind lodging resistance, cultivation step and natural disaster.Can be divided into root lodging with
Stem lodges.Root lodging is bad mainly due to root system development, takes root not deep, and secondary root is few and thin and delicate, aerial parts of giving away
Weight and occur.It is the most shallow that generation is primarily due to arable layer, wholely, seeding quality poor etc., cause root system development
Bad, bury shallower, or because early stage is not watered, later stage irrigation amount is excessive, soil layer is wet soft, then meets wind and rain and the lodging that causes.Stem
Lodging is owing to the mechanical tissue of basal part of stem is undeveloped, and first and second internode is long to be caused.Usual reason is because of application rate mistake
Greatly, rich water is sufficient, and particularly nitrogen application is too much, miscarriage, and causes tiller too much, and colony is excessive, and polarization is slow, field
Between strongly fragrant cover, illumination is the most not enough, and basal internode is long, and stalk wall is thin and unreal, and dry-matter accumulation is few, meets wind and rain invasion and attack, the lower portion of the stem
Bend or fracture and cause.
Plant growth regulator, is the class pesticide grown for coordinate plant growth, has sky including synthetic
The so compound of phytohormone similar action and natural phytohormone of extracting from biology.For target plant, plant is raw
Long regulator is the non-nutritive chemical substance of external source, generally can conduct in plant to site of action, with the lowest concentration
Just can promote or suppress some link of its life process, be allowed to the needs to meeting the mankind and develop.
According to the difference of water consumption, pesticide spray can be divided into again Large Copacity spraying (every mu of use water 50~100kg), middle appearance
(every mu of use water is few for amount spraying (every mu of use water 10~30kg), low-gallonage spraying (every mu of use water 1~10kg) and ultra-low volume spray
In 1kg).Conventional dispenser typically uses medium volume spraying.
Along with the development of unmanned air vehicle technique, the unmanned plane during flying dispenser risen in plant protection field, to the use of pesticide
Bring new revolution.Unmanned plane dispenser has the advantages that effect is high, expenses for prevention and control is low, dosage is few, especially executes in paddy field
Medicine, extreme terrain dispenser, concentration Unifying control dispenser field, compared with traditional insecticide-applying way, have obvious advantage.But nothing
Another feature of man-machine dispenser is that water consumption is few, when conventional pesticide is used for unmanned plane dispenser, and low-gallonage spraying to be used, this
Time drug effect be difficult to ensure.Droplet drift, droplet when frequently resulting in the drug effect reduction of medicament, dispenser volatilize, rotation oar gas
The problems such as stream impact.
Existing plant growth regulator formulations mainly includes powder, water preparation etc., and plant growth regulator is ultralow
Volume sprays liquor has no report both at home and abroad.
Typically by screening, volatility is low, lightning is high, molten to crop safety good to former medicine dissolubility for ultra low volume liquids
Agent, is not watered during dispenser, but straight with ultra low volume sprayer tool, low-gallonage spraying apparatus or ultra-low volume electrostatic spray apparatus
Connect and use.Ultra-low volume spray is owing to spraying from leaving aerosol apparatus without high volatile ingredient, its size of medicinal liquid and quality in droplet
Head does not has significant change during arriving target, decreases volatilization and the drift of medicament.Droplet is tiny and uniform, it is possible to notable
Improve the deposition of medicinal liquid.Owing to using without being watered, ultra-low volume spray liquor is suitable for water resource shortage, pest and disease damage collection
Middle fulminant large area occurs and dispenser on a large scale in needing the short time, and specialized Unifying control dispenser, the most ultralow
Volume sprays significantly reduces the labor intensity of operator.
The conventional spraying methods spraying commonly used regular dosage form of current domestic plant growth regulator, is that plant is raw
Long regulator preparation carries out medicament sprinkling after diluting with a large amount of water, and this prevention and controls exists various problems:
1. conventional spraying work efficiency is low, and work efficiency is only 2~5 mus/day the most per capita, it is difficult to meet the needs of implantation in large scale,
Along with domestic land transformation policy is to implement, soil presents the trend of intensive management, occurs that increasing agricultural planting is big
Family, crop contiguous plant area increases;And along with China's aged tendency of population and the appearance of recruitment famine, labour force is increasingly becoming dilute
Lacking resource, human cost improves constantly, and agriculture production cost continues to increase, and adds the seasonal obvious of agricultural production, medicament
Sprinkling generally requires uses substantial amounts of manpower at short notice.
2. conventional spraying needs substantial amounts of water, and usual water consumption reaches 10~30kg, and is much lacking away from water source and arid
The area of water, reduces water consumption spraying and can not reach preferable pharmacy effect effect.
3. conventional nebulization uses medicament lightning, volatility do not meet low-gallonage spraying dispenser requirement.
Summary of the invention
The technical problem to be solved is to provide a kind of Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor and preparation thereof
And using method, with strong points, nontoxic pollution-free, low cost, easy to operate, effect stability notable, can prevent and resist dry
Hot blast and the harm of lodging, make Semen Tritici aestivi normally be in the milk and obtain preferable yield and quality, and has " having calamity mitigation, increase production without calamity "
Functional characteristic, to solve the defect of prior art.
The invention discloses Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor, each component is mixed according to following parts by weight proportioning
Close: active component 2-30%, solvent 5-15%, surfactant 2-6%, water 43-87.9%.
Further, described active component be paclobutrazol (common name paclobutrazol, has another name called: neoprene azoles, PP333,
MET), chlorocholine chloride (common name chlormequat, has another name called: CCC, monobutyltin trichloride choline, three Western regions), first piperazine (common name
Mepiquatchloride, has another name called: methyl piperidine, regulation amine, mepiquat chloride, help strong element), TrinexAN_SNacethyl (common name trinexapac-
Ethyl), 5 nitroguaiacol sodium, onitrophenol, sodium paranitrophenol, isopentenyl gland purine (common name Isoamyl
Alkenyl adenine, oxyenadenine+enadenine), α-naphthaleneacidsodium, in tridecyl alcohol one or more arbitrarily than
Example mixture;
Further, described solvent is methanol, ethanol, capryl alcohol, N-Methyl pyrrolidone, spectrasolv DMDA, N,
In N-dimethyl acetylamide, jatropha curcas oil, soybean oil, Semen Maydis oil, Oleum Gossypii semen, Oleum Brassicae campestris, Oleum Ricini, Oleum Terebinthinae one or more
Arbitrary proportion mixture.
Further, described surfactant is calcium dodecyl benzene sulfonate (agriculture breast 500#), fatty alcohol-polyoxyethylene ether
AEO-5, fatty alcohol-polyoxyethylene ether AEO-7, fatty alcohol-polyoxyethylene ether AEO-9, castor oil polyoxyethylene ether EL-10, Semen Ricini
Oil polyoxyethylene ether EL-20, castor oil polyoxyethylene ether EL-40, tristyrylphenol polyoxyethylene ether phosphate ester three ethanol
The arbitrary proportion mixture of one or more in amine salt AP-3, emulsifying agent Emulson AG PE, emulsifying agent Emulson AG104.
Further, also include that thickening agent, described thickening agent are xanthan gum, Radix Acaciae senegalis, sodium alginate, Polyethylene Glycol
In one or more arbitrary proportion mixture.
Further, also include that antifreezing agent, described antifreezing agent are one or more in ethylene glycol, propylene glycol, diethylene glycol
Arbitrary proportion mixture.
The invention also discloses the preparation method of a kind of Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor, prepare as follows
Form:
By described active component and described solvent according to formula proportion stirring and dissolving;
Described surfactant, described thickening agent, described antifreezing agent, water, low whipping speed is added according still further to formula proportion
Under the conditions of 1500-5000r/min, stir 20-60min so that it is mix homogeneously, obtain Semen Tritici aestivi hot-dry wind tolerance spray liquid resistant to lodging
Agent.
Further, the invention also discloses the using method of described Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor: medicament
Mu spouting liquid is 1-1.5kg, in employing Direct spraying, ultra-low volume spray, low-gallonage spraying or ultra-low volume electrostatic spray extremely
Few a kind of means are sprayed.
The beneficial effects of the present invention is following some:
The most with strong points, nontoxic pollution-free, low cost, easy to operate, effect stability is notable.
2. can prevent and resist the harm of hot dry wind and lodging, make Semen Tritici aestivi normally be in the milk and obtain preferable yield and product
Matter.
3. there is the functional characteristic of " having calamity mitigation, increase production without calamity ".
Detailed description of the invention
Being further described the detailed description of the invention of the present invention below in conjunction with embodiment, following example are only used for more
Clearly demonstrate the technical em-bodiments of the present invention, and can not limit the scope of the invention with this.
Embodiment 1
30% first piperazine isopentenyl gland purine Semen Tritici aestivi hot-dry wind tolerance ultra-low volume spray resistant to lodging liquor
Formula is by following weight proportion:
Component | Percentage by weight |
First piperazine | 28% |
Isopentenyl gland purine | 2% |
N-Methyl pyrrolidone | 5% |
Oleum Ricini | 10% |
Calcium dodecyl benzene sulfonate | 2% |
Fatty alcohol-polyoxyethylene ether AEO-7 | 4% |
Xanthan gum | 0.2% |
Ethylene glycol | 4% |
Water | 44.8% |
Preparation method:
In the reactor of band high speed shear, first with solvent by after active component stirring and dissolving, add surfactant,
Thickening agent, antifreezing agent and water, high speed shear 30 minutes, shear rate is 5000 revs/min, and temperature is room temperature.I.e. obtain 30%
First piperazine isopentenyl gland purine Semen Tritici aestivi hot-dry wind tolerance ultra-low volume spray resistant to lodging liquor.
Further, described active component can also be paclobutrazol (common name paclobutrazol, has another name called: neoprene azoles,
PP333, MET), chlorocholine chloride (common name chlormequat, has another name called: CCC, monobutyltin trichloride choline, three Western regions), first piperazine (common name
Mepiquatchloride, has another name called: methyl piperidine, regulation amine, mepiquat chloride, help strong element), TrinexAN_SNacethyl (common name trinexapac-
Ethyl), 5 nitroguaiacol sodium, onitrophenol, sodium paranitrophenol, isopentenyl gland purine (common name Isoamyl
Alkenyl adenine, oxyenadenine+enadenine), α-naphthaleneacidsodium, arbitrary proportion mixing several in tridecyl alcohol
Thing;
Further, described solvent can also be methanol, ethanol, capryl alcohol, N-Methyl pyrrolidone, N, N-dimethyl caprinoyl
In amine, N,N-dimethylacetamide, jatropha curcas oil, soybean oil, Semen Maydis oil, Oleum Gossypii semen, Oleum Brassicae campestris, Oleum Ricini, Oleum Terebinthinae several
Arbitrary proportion mixture.
Further, described surfactant can also be calcium dodecyl benzene sulfonate (agriculture breast 500#), fatty alcohol polyoxy
Vinyl Ether AEO-5, fatty alcohol-polyoxyethylene ether AEO-7, fatty alcohol-polyoxyethylene ether AEO-9, castor oil polyoxyethylene ether EL-
10, castor oil polyoxyethylene ether EL-20, castor oil polyoxyethylene ether EL-40, tristyrylphenol polyoxyethylene ether phosphate ester
Arbitrary proportion mixture several in triethanolamine salt AP-3, emulsifying agent Emulson AG PE, emulsifying agent Emulson AG104.
Further, described thickening agent can also be several in xanthan gum, Radix Acaciae senegalis, sodium alginate, Polyethylene Glycol
Arbitrary proportion mixture.
Further, the arbitrary proportion mixture that described antifreezing agent is several in being ethylene glycol, propylene glycol, diethylene glycol.
Embodiment 2
32% chlorocholine chloride isopentenyl gland purine Semen Tritici aestivi hot-dry wind tolerance ultra-low volume spray resistant to lodging liquor
Formula is by following weight proportion:
Preparation method:
In the reactor of band high speed shear, first with solvent by after active component stirring and dissolving, add surfactant,
Thickening agent, antifreezing agent and water, high speed shear 25 minutes, shear rate is 5000 revs/min, and temperature is room temperature.I.e. obtain 32%
Chlorocholine chloride isopentenyl gland purine Semen Tritici aestivi hot-dry wind tolerance ultra-low volume spray resistant to lodging liquor.
Embodiment 3
48% first piperazine α-naphthaleneacidsodium Semen Tritici aestivi hot-dry wind tolerance ultra-low volume spray resistant to lodging liquor
Formula is by following weight proportion:
Preparation method:
In the reactor of band high speed shear, first with solvent by after active component stirring and dissolving, add surfactant,
Thickening agent, antifreezing agent and water, high speed shear 30 minutes, shear rate is 5000 revs/min, and temperature is room temperature.I.e. obtain 48%
First piperazine α-naphthaleneacidsodium Semen Tritici aestivi hot-dry wind tolerance ultra-low volume spray resistant to lodging liquor.
Embodiment 4
22% α-naphthaleneacidsodium isopentenyl gland purine Semen Tritici aestivi hot-dry wind tolerance ultra-low volume spray resistant to lodging liquor
Formula is by following weight proportion:
Component | Percentage by weight |
α-naphthaleneacidsodium | 20% |
Isopentenyl gland purine | 2% |
Capryl alcohol | 10% |
Semen Maydis oil | 2% |
Calcium dodecyl benzene sulfonate (agriculture breast 500#) | 3% |
Emulsifying agent Emulson AG PE | 3% |
Sodium alginate | 0.2% |
Propylene glycol | 4% |
Water | 26.8% |
Preparation method:
In the reactor of band high speed shear, first with solvent by after active component stirring and dissolving, add surfactant,
Thickening agent, antifreezing agent and water, high speed shear 30 minutes, shear rate is 5000 revs/min, and temperature is room temperature.I.e. obtain 22%
α-naphthaleneacidsodium isopentenyl gland purine Semen Tritici aestivi hot-dry wind tolerance ultra-low volume spray resistant to lodging liquor.
Product quality detection method
(1) viscosimetric analysis
DJ-1 type rotation r viscometer is used to measure, it is desirable to viscosity is 300~600cp, and this viscosity can make preparation stabilization.
(2) low-temperature stability test
Take in the sample addition centrifuge tube of 100, refrigerator is cooled to (0 ± 2) DEG C, allows centrifuge tube and content (0
± 2) keep 1h at DEG C, stir once every 15min therebetween, each 15s, check and record and analyse with or without solids or grease
Go out.Centrifuge tube is put back to refrigerator, at (0 ± 2) DEG C, continues to place 7d, centrifuge tube is taken out, room temperature (less than 20 DEG C)
The volume of lower standing 3h, centrifugation 15min (pipe top relative centrifugal force(RCF) is 500~600g) record tube bottom precipitate
(being accurate to 0.05mL).Precipitate is qualified less than 0.3mL.
(3) heat storage stability test
With syringe, about 30mL sample is injected in clean ampoule bottle (avoiding sample contacts bottleneck), put this ampoule bottle in
Cryosel bath is freezed, seals rapidly (avoiding solvent to volatilize) with thermal-flame, at least envelope 3 bottles, be cooled to room temperature and weigh.To seal
Ampoule bottle be placed in canister, then canister is put in 54 ± 2 DEG C of calorstats, places 14d, take out and be cooled to room
Temperature, by wiped clean outside ampoule bottle, weighs respectively, the sample that quality does not changes, and observes emulsion-stabilizing situation.
(4) product safety in utilization test
After dispenser 3 days, 7 days, investigate plant growth situation, pass judgment on each process community and blank community crop
Undermined symptom, to determine the medicament safety to Semen Tritici aestivi.
Table 1 Semen Tritici aestivi is by poisoning grade scale
Rank | To Semen Tritici aestivi extent of injury |
1 | Growth is normal |
2 | Slight poisoning |
3 | Medium poisoning, can recover |
4 | Poisoning is heavier, it is difficult to recover |
5 | Poisoning is heavier, it is difficult to recover |
(5) volatility measures (filter paper enzyme): weigh 0.5g solution to be measured, drips in filter paper central authorities, weighs record and adds
Enter the quality before and after medicinal liquid, be repeated 3 times, be placed in ventilating kitchen, measure scraps of paper weight at 60min, 120min respectively.Calculate volatilization
Rate.
Result of the test
Table 2 Semen Tritici aestivi hot-dry wind tolerance ultra-low volume spray resistant to lodging liquor capability and performance testing result
Table 3 Semen Tritici aestivi hot-dry wind tolerance ultra-low volume spray resistant to lodging liquor volatility measurement result
Spray carrier | Volatility % (60min) | Volatility % (120min) | Evaluation of result |
Example 1 | 26.5 | 36.6 | Qualified |
Example 2 | 22.4 | 32.5 | Qualified |
Example 3 | 25.6 | 34.2 | Qualified |
Example 4 | 27.7 | 38.9 | Qualified |
Clear water CK | 88.5 | 100.0 | — |
The above is only the preferred embodiments of the present invention, it is noted that for the ordinary skill people of the art
For Yuan, on the premise of without departing from the technology of the present invention principle, it is also possible to make some improvements and modifications, these improvements and modifications
Also should be regarded as protection scope of the present invention.
Claims (8)
1. a Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor, it is characterised in that each component is mixed according to following parts by weight proportioning
Close: active component 2-30%, solvent 5-15%, surfactant 2-6%, water 43-87.9%.
2. Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor as claimed in claim 1, it is characterised in that described active component is many
Effect azoles, chlorocholine chloride, first piperazine, TrinexAN_SNacethyl, 5 nitroguaiacol sodium, onitrophenol, sodium paranitrophenol, isopentenyl gland
The arbitrary proportion mixture of one or more in purine, α-naphthaleneacidsodium, tridecyl alcohol.
3. Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor as claimed in claim 1, it is characterised in that described solvent be methanol,
Ethanol, capryl alcohol, N-Methyl pyrrolidone, spectrasolv DMDA, N,N-dimethylacetamide, jatropha curcas oil, soybean oil, jade
The arbitrary proportion mixture of one or more in Miyou, Oleum Gossypii semen, Oleum Brassicae campestris, Oleum Ricini, Oleum Terebinthinae.
4. Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor as claimed in claim 1, it is characterised in that described surfactant is
Calcium dodecyl benzene sulfonate, fatty alcohol-polyoxyethylene ether, fatty alcohol-polyoxyethylene ether, fatty alcohol-polyoxyethylene ether, Oleum Ricini are poly-
Oxygen vinyl Ether, castor oil polyoxyethylene ether, castor oil polyoxyethylene ether, tristyrylphenol polyoxyethylene ether phosphate ester three second
The arbitrary proportion mixture of one or more in alcohol amine salt, emulsifying agent Emulson AG PE, emulsifying agent Emulson AG104.
5. Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor as claimed in claim 1, it is characterised in that also include thickening agent, institute
Stating thickening agent is the arbitrary proportion mixture of one or more in xanthan gum, Radix Acaciae senegalis, sodium alginate, Polyethylene Glycol.
6. Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor as claimed in claim 1, it is characterised in that also include antifreezing agent, institute
Stating antifreezing agent is the arbitrary proportion mixture of one or more in ethylene glycol, propylene glycol, diethylene glycol.
7. the preparation method of a Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor, it is characterised in that be prepared from as follows:
By described active component and described solvent according to formula proportion stirring and dissolving;
Adding described surfactant, described thickening agent, described antifreezing agent, water according still further to formula proportion, low whipping speed is
Under the conditions of 1500-5000r/min, stir 20-60min so that it is mix homogeneously, obtain Semen Tritici aestivi hot-dry wind tolerance spray liquid resistant to lodging
Agent.
8. the using method of a Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor, it is characterised in that use as follows: medicament
Mu spouting liquid is 1-1.5kg, in employing Direct spraying, ultra-low volume spray, low-gallonage spraying or ultra-low volume electrostatic spray extremely
Few a kind of means are sprayed.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201610512818.0A CN106135213A (en) | 2016-07-01 | 2016-07-01 | A kind of Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor and preparation and application thereof |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201610512818.0A CN106135213A (en) | 2016-07-01 | 2016-07-01 | A kind of Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor and preparation and application thereof |
Publications (1)
Publication Number | Publication Date |
---|---|
CN106135213A true CN106135213A (en) | 2016-11-23 |
Family
ID=57349694
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201610512818.0A Pending CN106135213A (en) | 2016-07-01 | 2016-07-01 | A kind of Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor and preparation and application thereof |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN106135213A (en) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107014709A (en) * | 2017-04-20 | 2017-08-04 | 山西省农业科学院小麦研究所 | Utilize intermission seeding identification water ground Wheat in Grain Filling Stage high temperature resistant dry heat resistance wind method |
CN109006264A (en) * | 2018-06-17 | 2018-12-18 | 河北省农林科学院旱作农业研究所 | New wheat breed dry heat resistance wind identification method and Special temp controlling canopy |
CN110881470A (en) * | 2019-09-27 | 2020-03-17 | 四川国光农化股份有限公司 | Suspending agent composition, suspending agent, and preparation process and application thereof |
CN115363027A (en) * | 2022-09-14 | 2022-11-22 | 四川国光农化股份有限公司 | Pesticide ultra-low volume liquid and preparation method and application thereof |
Citations (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0088631A1 (en) * | 1982-03-10 | 1983-09-14 | Lilly Industries Limited | Plant growth regulation method and composition |
CN1035941A (en) * | 1988-03-20 | 1989-10-04 | 冯宏章 | Withered spirit and preparation method thereof |
CN1080812A (en) * | 1992-07-06 | 1994-01-19 | 广西化工研究所 | Plant growth regulator |
CN1230340A (en) * | 1999-03-16 | 1999-10-06 | 新疆农业科学院微生物应用研究所 | Synergistic mepiquat chloride and its production |
CN1795723A (en) * | 2004-12-22 | 2006-07-05 | 郭勋斌 | Plant growth regulator and production process |
CN1911015A (en) * | 2005-08-11 | 2007-02-14 | 中国农业大学 | Compound microemulsion of plant growth regulator, prepn. method and use thereof |
CN101743954A (en) * | 2008-12-19 | 2010-06-23 | 唐浩 | Multi-effect azole suspending agent and method for preparing same |
CN101773128A (en) * | 2010-02-03 | 2010-07-14 | 中国科学院西双版纳热带植物园 | Special growth regulating agent for jatropha and application thereof |
CN103719105A (en) * | 2014-01-20 | 2014-04-16 | 四川国光农化股份有限公司 | Plant growth adjusting composition as well as preparation and application thereof |
CN105707089A (en) * | 2016-03-24 | 2016-06-29 | 河北上瑞化工有限公司 | Neutral water agent containing isopentennyladenine and preparation method of neutral water agent |
-
2016
- 2016-07-01 CN CN201610512818.0A patent/CN106135213A/en active Pending
Patent Citations (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0088631A1 (en) * | 1982-03-10 | 1983-09-14 | Lilly Industries Limited | Plant growth regulation method and composition |
CN1035941A (en) * | 1988-03-20 | 1989-10-04 | 冯宏章 | Withered spirit and preparation method thereof |
CN1080812A (en) * | 1992-07-06 | 1994-01-19 | 广西化工研究所 | Plant growth regulator |
CN1230340A (en) * | 1999-03-16 | 1999-10-06 | 新疆农业科学院微生物应用研究所 | Synergistic mepiquat chloride and its production |
CN1795723A (en) * | 2004-12-22 | 2006-07-05 | 郭勋斌 | Plant growth regulator and production process |
CN1911015A (en) * | 2005-08-11 | 2007-02-14 | 中国农业大学 | Compound microemulsion of plant growth regulator, prepn. method and use thereof |
CN101743954A (en) * | 2008-12-19 | 2010-06-23 | 唐浩 | Multi-effect azole suspending agent and method for preparing same |
CN101773128A (en) * | 2010-02-03 | 2010-07-14 | 中国科学院西双版纳热带植物园 | Special growth regulating agent for jatropha and application thereof |
CN103719105A (en) * | 2014-01-20 | 2014-04-16 | 四川国光农化股份有限公司 | Plant growth adjusting composition as well as preparation and application thereof |
CN105707089A (en) * | 2016-03-24 | 2016-06-29 | 河北上瑞化工有限公司 | Neutral water agent containing isopentennyladenine and preparation method of neutral water agent |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107014709A (en) * | 2017-04-20 | 2017-08-04 | 山西省农业科学院小麦研究所 | Utilize intermission seeding identification water ground Wheat in Grain Filling Stage high temperature resistant dry heat resistance wind method |
CN107014709B (en) * | 2017-04-20 | 2019-04-09 | 山西省农业科学院小麦研究所 | Using intermission seeding identification water Wheat in Grain Filling Stage high temperature resistant dry heat resistance wind method |
CN109006264A (en) * | 2018-06-17 | 2018-12-18 | 河北省农林科学院旱作农业研究所 | New wheat breed dry heat resistance wind identification method and Special temp controlling canopy |
CN110881470A (en) * | 2019-09-27 | 2020-03-17 | 四川国光农化股份有限公司 | Suspending agent composition, suspending agent, and preparation process and application thereof |
CN115363027A (en) * | 2022-09-14 | 2022-11-22 | 四川国光农化股份有限公司 | Pesticide ultra-low volume liquid and preparation method and application thereof |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN105010402B (en) | A kind of suspension type biological seed coat agent, its preparation method and purposes | |
CN106135213A (en) | A kind of Semen Tritici aestivi hot-dry wind tolerance spraying resistant to lodging liquor and preparation and application thereof | |
CN103864512B (en) | A kind of nano biological environment protection multifunctional organic bamboo vinegar medicine is fertile | |
CN104067869B (en) | Chemical cotton topping method for shine early cotton region | |
CN106172407A (en) | Ultra-low volume spray liquor containing brassin lactones and preparation and application thereof | |
CN104855412A (en) | Dispersible oil suspending agent containing spirotetramat and dinotefuran | |
CN103058775B (en) | Preparation for preventing citrus young fruits from physiological fruit drop and application method thereof | |
CN103416385A (en) | Closed weeding method for beet paper tube seedling seedbeds | |
CN106386811A (en) | Plant growth regulating composition, and preparation and application thereof | |
CN105475282A (en) | Polyamine composite agent enhancing wheat and corn drought resistance | |
CN109265235A (en) | Special fertilizer with insecticidal activity | |
CN106472506A (en) | A kind of compositionss of coordinate plant growth, preparation and its application | |
CN103719151B (en) | One cultivates peanut seed dressing and preparation method thereof and application | |
CN102976861B (en) | Preparation for promoting growth and development of wheat in weak light environment and preparation method thereof | |
CN108770872A (en) | The compound pesticide preparation and its preparation of a kind of carvacrol and Folium Isatidis extract and application | |
CN101524065B (en) | Prohexadione-calcium water-dispersible dropping pill as plant growth regulator, and preparation method thereof | |
CN108184875A (en) | A kind of composition containing copper rosinate and captan, preparation method and applications | |
CN107212018B (en) | A kind of composition pesticide of suitable trickle irrigation | |
CN110178844A (en) | A kind of dedicated flower and fruit protecting strengthening root composition of citrus and its application | |
CN104855384A (en) | Pesticide composition containing 2-(acetoxyl)benzoic acid and indolebutyric acid | |
CN103918656A (en) | Plant growth regulator composition and preparation thereof | |
CN104255734B (en) | The composition pesticide of a kind of containing chlorfenapyr and fluazinam | |
CN106212486A (en) | A kind of Brassica campestris L cracking resistance angle agent and application | |
CN106116904A (en) | Promote the composite assistant that boron element is absorbed by crop blade face | |
CN107318847B (en) | A kind of herbicidal composition containing fluorine chloropyridine ester and Acetochlor |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
RJ01 | Rejection of invention patent application after publication |
Application publication date: 20161123 |
|
RJ01 | Rejection of invention patent application after publication |