CN106120391A - A kind of environment-friendly type wollen fabrics printing and dyeing are with promoting dye and preparation method thereof - Google Patents
A kind of environment-friendly type wollen fabrics printing and dyeing are with promoting dye and preparation method thereof Download PDFInfo
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- CN106120391A CN106120391A CN201610513411.XA CN201610513411A CN106120391A CN 106120391 A CN106120391 A CN 106120391A CN 201610513411 A CN201610513411 A CN 201610513411A CN 106120391 A CN106120391 A CN 106120391A
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- dyeing
- environment
- dye
- friendly type
- expanded vermiculite
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67383—Inorganic compounds containing silicon
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/46—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing natural macromolecular substances or derivatives thereof
- D06P1/48—Derivatives of carbohydrates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/52—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing synthetic macromolecular substances
- D06P1/5207—Macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- D06P1/525—Polymers of unsaturated carboxylic acids or functional derivatives thereof
- D06P1/5257—(Meth)acrylic acid
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/58—Material containing hydroxyl groups
- D06P3/60—Natural or regenerated cellulose
- D06P3/66—Natural or regenerated cellulose using reactive dyes
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Molecular Biology (AREA)
- Coloring (AREA)
Abstract
A kind of environment-friendly type wollen fabrics printing and dyeing are with promoting dye and preparation method thereof, expanded vermiculite powder, gelatin, guar gum is used to coordinate the mode of organic acid, it is prepared for the rush dye with good result, can effectively reduce the degree of hydration of reactive dye, in use, Matrii Sulfas Exsiccatus can be replaced completely, greatly reduce the salt usage amount in dyeing process, reduce the usage amount of water, beneficially environmental protection simultaneously.
Description
Technical field
The present invention relates to technical field of textile printing, particularly relate to a kind of environment-friendly type wollen fabrics printing and dyeing rush contaminate and
Preparation method.
Background technology
Cotton fiber occupies an important position in textile industry, constitutes about the 65% of fiber total output.Apply at present in cotton
Dyestuff most important, most potential in terms of stock-dye is reactive dye.Reactive dye are combined by covalent bond with cotton fiber,
The problem fundamentally solving coloured fibre wet colour fastness difference.Simultaneously as reactive dye to have chromatograph complete, color and luster is fresh
Gorgeous, technique for applying is easy, and the suitability is strong, the advantages such as price is relatively cheap, yield during it has become cotton fiber dyestuff in recent years
The dyestuff maximum with the output value.In traditional reactive dyeing process, must be added to substantial amounts of sodium chloride or sodium sulfate, work as dye
After adding salt in bath, the degree of hydration of dyestuff reduces, and the tendency that such dyestuff is shifted to fiber surface by aqueous solution is increased by, balance
Upper dye amount just increases.
Salt pollution problem in elimination activity dyeing, currently mainly by two kinds of methods, one is from increasing reactive dye
Set about i.e. cotton fiber cationization with cotton fiber affinity, by method chemically and physically, cotton fiber is modified, makes fibre
Dimension table wears positive charge, is increased the affinity of fiber and dyestuff by the electrostatic interaction between positive and negative charge, reaches to promote the work of dye
With.But in place of this method Shortcomings, as do not recycled, the performance of fiber itself is had an impact, small organic agents
Consumption is big, and the toxic side effect having, and polymer reactant is unfavorable for dyestuff penetration, the problems such as coloured fibre coloured light is the most bright-coloured.
It two is salt substitute technology, i.e. applies compound pollution-free, environment amenable to substitute Matrii Sulfas Exsiccatus (chemical name
Claim: anhydrous sodium sulfate, another name: Matrii Sulfas Exsiccatus, thenardite), these compound great majority remain salt, therefore referred to as salt substitute.
People are known by research, and the salt effect of unary carboxylation is stronger than NaCl, and polybasic carboxylic acid is stronger than unary carboxylation, replaces with them
Sal and Matrii Sulfas Exsiccatus, salt consumption can greatly reduce, but these so-called same Sal of salt substitute price, Matrii Sulfas Exsiccatus compare reality at present
It is being the most expensive, the most also cannot promotion and application.
Chinese invention patent CN101560736A discloses the accelerant of a kind of novel replacement Matrii Sulfas Exsiccatus, and it can significantly drop
Salt consumption (using minimal amount of accelerant that Matrii Sulfas Exsiccatus just can be made to drop to the 50% of original consumption) in low cotton fiber reactive dye,
It is that one is not only improving environmental protection, the environment-friend auxiliaries of printing and dyeing enterprise production cost can be reduced again simultaneously, but be as China pair
Improving constantly of dyeing environmental requirement, in the urgent need to research and develop a kind of low cost, can substitute completely Matrii Sulfas Exsiccatus rush dye.
Summary of the invention
In order to solve the problem in background technology, the present invention provide a kind of environment-friendly type wollen fabrics printing and dyeing rush to contaminate and
Preparation method.
A kind of environment-friendly type wollen fabrics printing and dyeing are with promoting dye, including the main component of following percentage by weight:
Expanded vermiculite powder 35-45%
Guar gum 8-15%
Gelatin 8-10%
Organic acid 15-20%
Emulsifying agent 5-8%
Dispersant surplus.
Preferably, described organic acid is kojic acid.
Preferably, described emulsifying agent is dodecylbenzene sodium sulfonate.
Preferably, described dispersant is sodium polyacrylate.
A kind of environment-friendly type wollen fabrics printing and dyeing promote the preparation method of dye, comprise the following steps:
Step one: expanded vermiculite is pulverized, and cross 120 mesh sieves, extracting screen underflow, use the mode of wet grinding, by expanded vermiculite
Powder is ground to 10-30 μm；
Step 2: by expanded vermiculite powder, is added to the water, and adds dispersant and dodecylbenzene sodium sulfonate, is heated to 45-50 DEG C,
Stir under the conditions of 350-400rpm；
Step 3: add gelatin and arabic gum, continues emulsifying 10-with high speed dispersor under conditions of 8000-10000rpm
15min, forms uniform milk；
Step 4: add organic acid, regulates pH value, makes gelatin produce cohesion, constant temperature 15-20min with arabic gum；
Step 5: through drying under reduced pressure or lyophilization, obtains promoting dye.
Preferably, in described step 4, pH value is adjusted to 4-5.5.
The present invention uses the system of gelatin and arabic gum parcel expanded vermiculite powder as promoting dye, adds after promoting dye,
The rapid imbibition of system, thus effectively reduce the degree of hydration of reactive dye, without adding Matrii Sulfas Exsiccatus in whole dyeing process, greatly
Reduce greatly the salt usage amount in dyeing process, reduce the usage amount of water, beneficially environmental protection simultaneously.
Addition kojic acid, except regulation pH value, makes gelatin produce outside the effect of cohesion with arabic gum, is also equipped with inhibition system
Middle melanin produces, fresh-keeping hyperchromic function.
Environment-friendly type wollen fabrics printing and dyeing of the present invention promote dye, use expanded vermiculite powder, gelatin, guar gum to coordinate
The mode of organic acid, is prepared for the rush dye with good result, can effectively reduce the degree of hydration of reactive dye, use
Time, Matrii Sulfas Exsiccatus can be replaced completely, greatly reduce the salt usage amount in dyeing process, reduce the usage amount of water, favorably simultaneously
In environmental protection.
Detailed description of the invention
Embodiment 1
A kind of environment-friendly type wollen fabrics printing and dyeing are with promoting dye, including the main component of following percentage by weight:
Expanded vermiculite powder 40%
Guar gum 10%
Gelatin 8%
Organic acid 16%
Emulsifying agent 6%
Dispersant surplus.
Described organic acid is kojic acid.
Described emulsifying agent is dodecylbenzene sodium sulfonate.
Described dispersant is sodium polyacrylate.
A kind of environment-friendly type wollen fabrics printing and dyeing promote the preparation method of dye, comprise the following steps:
Step one: expanded vermiculite is pulverized, and cross 120 mesh sieves, extracting screen underflow, use the mode of wet grinding, by expanded vermiculite
Powder is ground to 10-30 μm；
Step 2: by expanded vermiculite powder, is added to the water, and adds dispersant and dodecylbenzene sodium sulfonate, is heated to 48 DEG C,
Stir under the conditions of 380rpm；
Step 3: add gelatin and arabic gum, continues emulsifying 12min, shape with high speed dispersor under conditions of 10000rpm
Uniformly milk；
Step 4: adding organic acid, regulation pH value is 4.7, makes gelatin produce cohesion, constant temperature 12min with arabic gum；
Step 5: through drying under reduced pressure or lyophilization, obtains promoting dye.
Embodiment 2
A kind of environment-friendly type wollen fabrics printing and dyeing are with promoting dye, including the main component of following percentage by weight:
Expanded vermiculite powder 35%
Guar gum 15%
Gelatin 10%
Organic acid 20%
Emulsifying agent 8%
Dispersant surplus.
Described organic acid is kojic acid.
Described emulsifying agent is dodecylbenzene sodium sulfonate.
Described dispersant is sodium polyacrylate.
A kind of environment-friendly type wollen fabrics printing and dyeing promote the preparation method of dye, comprise the following steps:
Step one: expanded vermiculite is pulverized, and cross 120 mesh sieves, extracting screen underflow, use the mode of wet grinding, by expanded vermiculite
Powder is ground to 10-30 μm；
Step 2: by expanded vermiculite powder, is added to the water, and adds dispersant and dodecylbenzene sodium sulfonate, is heated to 45 DEG C,
Stir under the conditions of 400rpm；
Step 3: add gelatin and arabic gum, continues emulsifying 10min, shape with high speed dispersor under conditions of 10000rpm
Uniformly milk；
Step 4: adding organic acid, regulation pH value is 5.2, makes gelatin produce cohesion, constant temperature 15min with arabic gum；
Step 5: through drying under reduced pressure or lyophilization, obtains promoting dye.
Embodiment 3
A kind of environment-friendly type wollen fabrics printing and dyeing are with promoting dye, including the main component of following percentage by weight:
Expanded vermiculite powder 45%
Guar gum 8%
Gelatin 9%
Organic acid 15%
Emulsifying agent 5%
Dispersant surplus.
Described organic acid is kojic acid.
Described emulsifying agent is dodecylbenzene sodium sulfonate.
Described dispersant is sodium polyacrylate.
A kind of environment-friendly type wollen fabrics printing and dyeing promote the preparation method of dye, comprise the following steps:
Step one: expanded vermiculite is pulverized, and cross 120 mesh sieves, extracting screen underflow, use the mode of wet grinding, by expanded vermiculite
Powder is ground to 10-30 μm；
Step 2: by expanded vermiculite powder, is added to the water, and adds dispersant and dodecylbenzene sodium sulfonate, is heated to 50 DEG C,
Stir under the conditions of 400rpm；
Step 3: add gelatin and arabic gum, continues emulsifying 10min under conditions of 8000rpm with high speed dispersor, is formed
Uniform milk；
Step 4: adding organic acid, regulation pH value is 4.5, makes gelatin produce cohesion, constant temperature 15min with arabic gum；
Step 5: through drying under reduced pressure or lyophilization, obtains promoting dye.
The above, the only present invention preferably detailed description of the invention, but protection scope of the present invention is not limited thereto,
Any those familiar with the art in the technical scope that the invention discloses, according to technical scheme and
Inventive concept equivalent or change in addition, all should contain within protection scope of the present invention.
Claims (7)
1. environment-friendly type wollen fabrics printing and dyeing are with promoting dye, it is characterised in that include the composition of following percentage by weight:
Expanded vermiculite powder 35-45%
Guar gum 8-15%
Gelatin 8-10%
Organic acid 15-20%
Emulsifying agent 5-8%
Dispersant surplus.
2. environment-friendly type wollen fabrics printing and dyeing as claimed in claim 1 are with promoting dye, it is characterised in that described organic acid is bent
Acid.
3. environment-friendly type wollen fabrics printing and dyeing as claimed in claim 1 are with promoting dye, it is characterised in that described emulsifying agent is ten
Dialkyl benzene sulfonic acids sodium.
4. environment-friendly type wollen fabrics printing and dyeing as claimed in claim 1 are with promoting dye, it is characterised in that described dispersant is poly-
Sodium acrylate.
5. the environment-friendly type wollen fabrics printing and dyeing preparation method promoting dye, it is characterised in that comprise the following steps:
Step one: expanded vermiculite is pulverized, and cross 120 mesh sieves, extracting screen underflow, use the mode of wet grinding, by expanded vermiculite
Powder is ground to 10-30 μm；
Step 2: by expanded vermiculite powder, is added to the water, and adds dispersant and dodecylbenzene sodium sulfonate, is heated to 45-50 DEG C,
Stir under the conditions of 350-400rpm；
Step 3: add gelatin and arabic gum, continues emulsifying 10-with high speed dispersor under conditions of 8000-10000rpm
15min, forms uniform milk；
Step 4: add organic acid, regulates pH value, makes gelatin produce cohesion, constant temperature 15-20min with arabic gum；
Step 5: through drying under reduced pressure or lyophilization, obtains promoting dye.
6. the environment-friendly type wollen fabrics printing and dyeing preparation method promoting dye as claimed in claim 5, it is characterised in that described
In step 4, pH value is adjusted to 4-5.5.
7. the environment-friendly type wollen fabrics printing and dyeing preparation method promoting dye as claimed in claim 5, it is characterised in that include with
Lower step:
Step one: expanded vermiculite is pulverized, and cross 120 mesh sieves, extracting screen underflow, use the mode of wet grinding, by expanded vermiculite
Powder is ground to 10-30 μm；
Step 2: by expanded vermiculite powder, is added to the water, and adds dispersant and dodecylbenzene sodium sulfonate, is heated to 48 DEG C,
Stir under the conditions of 380rpm；
Step 3: add gelatin and arabic gum, continues emulsifying 12min, shape with high speed dispersor under conditions of 10000rpm
Uniformly milk；
Step 4: adding organic acid, regulation pH value is 4.7, makes gelatin produce cohesion, constant temperature 12min with arabic gum；
Step 5: through drying under reduced pressure or lyophilization, obtains promoting dye；
Described environment-friendly type wollen fabrics printing and dyeing promote dye, including the main component of following percentage by weight:
Expanded vermiculite powder 40%
Guar gum 10%
Gelatin 8%
Kojic acid 16%
Dodecylbenzene sodium sulfonate 6%
Sodium polyacrylate surplus.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610513411.XA CN106120391B (en) | 2016-07-04 | 2016-07-04 | A kind of printing and dyeing of environment-friendly type cotton textiles are with accelerant and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610513411.XA CN106120391B (en) | 2016-07-04 | 2016-07-04 | A kind of printing and dyeing of environment-friendly type cotton textiles are with accelerant and preparation method thereof |
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| CN106120391A true CN106120391A (en) | 2016-11-16 |
| CN106120391B CN106120391B (en) | 2019-01-15 |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106368008A (en) * | 2016-08-31 | 2017-02-01 | 浙江正宇纺织印染基地有限公司 | Dyeing accelerant for printing and dyeing of silk-cotton blended fabric and preparation method thereof |
| CN109577041A (en) * | 2019-01-15 | 2019-04-05 | 梅丽玲 | A kind of preparation method of intelligent heat preserving dyestuff |
| CN110725143A (en) * | 2019-11-19 | 2020-01-24 | 湖州世合纺织有限公司 | Printing and dyeing method for salt-free cotton-polyester blended fabric |
| CN110846908A (en) * | 2019-11-19 | 2020-02-28 | 湖州世合纺织有限公司 | Accelerating agent suitable for natural dye and use method thereof |
| CN111676716A (en) * | 2020-05-13 | 2020-09-18 | 华南理工大学 | Method for preparing cotton fiber accelerating agent by using folic acid production wastewater |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1817972A (en) * | 2006-01-16 | 2006-08-16 | 大连理工大学 | Acid dye composition |
| CN101381963A (en) * | 2007-09-09 | 2009-03-11 | 胡红湘 | Salt free dyeing with reactive dye |
| CN105274871A (en) * | 2015-04-07 | 2016-01-27 | 时兴纺整(苏州)有限公司 | Invisible pattern surface treatment technology for cloth showing patterns meeting water |
-
2016
- 2016-07-04 CN CN201610513411.XA patent/CN106120391B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1817972A (en) * | 2006-01-16 | 2006-08-16 | 大连理工大学 | Acid dye composition |
| CN101381963A (en) * | 2007-09-09 | 2009-03-11 | 胡红湘 | Salt free dyeing with reactive dye |
| CN105274871A (en) * | 2015-04-07 | 2016-01-27 | 时兴纺整(苏州)有限公司 | Invisible pattern surface treatment technology for cloth showing patterns meeting water |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106368008A (en) * | 2016-08-31 | 2017-02-01 | 浙江正宇纺织印染基地有限公司 | Dyeing accelerant for printing and dyeing of silk-cotton blended fabric and preparation method thereof |
| CN109577041A (en) * | 2019-01-15 | 2019-04-05 | 梅丽玲 | A kind of preparation method of intelligent heat preserving dyestuff |
| CN109577041B (en) * | 2019-01-15 | 2021-11-09 | 台州市旭泓服饰有限公司 | Preparation method of intelligent heat-preservation dye |
| CN110725143A (en) * | 2019-11-19 | 2020-01-24 | 湖州世合纺织有限公司 | Printing and dyeing method for salt-free cotton-polyester blended fabric |
| CN110846908A (en) * | 2019-11-19 | 2020-02-28 | 湖州世合纺织有限公司 | Accelerating agent suitable for natural dye and use method thereof |
| CN111676716A (en) * | 2020-05-13 | 2020-09-18 | 华南理工大学 | Method for preparing cotton fiber accelerating agent by using folic acid production wastewater |
| CN111676716B (en) * | 2020-05-13 | 2021-05-14 | 华南理工大学 | Method for preparing cotton fiber accelerating agent by using folic acid production wastewater |
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| CN106120391B (en) | 2019-01-15 |
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Denomination of invention: The invention relates to an environment-friendly dye promoter for printing and dyeing of cotton textiles and a preparation method thereof Effective date of registration: 20210729 Granted publication date: 20190115 Pledgee: Zhejiang Deqing Rural Commercial Bank Co.,Ltd. Xinshi sub branch Pledgor: HUZHOU XINJIAYI SILK WEAVING PRINTING Co.,Ltd. Registration number: Y2021330001033 |