CN108193518A - A kind of true color spray ink disperse dye ink of the anhydrous printing of terylene chemical fibre ground cushion - Google Patents
A kind of true color spray ink disperse dye ink of the anhydrous printing of terylene chemical fibre ground cushion Download PDFInfo
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- CN108193518A CN108193518A CN201711495749.8A CN201711495749A CN108193518A CN 108193518 A CN108193518 A CN 108193518A CN 201711495749 A CN201711495749 A CN 201711495749A CN 108193518 A CN108193518 A CN 108193518A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/16—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
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- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/445—Use of auxiliary substances before, during or after dyeing or printing
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- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/60—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing polyethers
- D06P1/613—Polyethers without nitrogen
- D06P1/6131—Addition products of hydroxyl groups-containing compounds with oxiranes
- D06P1/6133—Addition products of hydroxyl groups-containing compounds with oxiranes from araliphatic or aliphatic alcohols
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- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/60—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing polyethers
- D06P1/613—Polyethers without nitrogen
- D06P1/6138—Polymerisation products of glycols, e.g. Carbowax, Pluronics
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- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/642—Compounds containing nitrogen
- D06P1/649—Compounds containing carbonamide, thiocarbonamide or guanyl groups
- D06P1/6495—Compounds containing carbonamide -RCON= (R=H or hydrocarbons)
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- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/651—Compounds without nitrogen
- D06P1/65106—Oxygen-containing compounds
- D06P1/65118—Compounds containing hydroxyl groups
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- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/651—Compounds without nitrogen
- D06P1/65106—Oxygen-containing compounds
- D06P1/65131—Compounds containing ether or acetal groups
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- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/651—Compounds without nitrogen
- D06P1/65168—Sulfur-containing compounds
- D06P1/65187—Compounds containing sulfide or disulfide groups
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67333—Salts or hydroxides
- D06P1/6735—Salts or hydroxides of alkaline or alkaline-earth metals with anions different from those provided for in D06P1/67341
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- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/34—Material containing ester groups
- D06P3/52—Polyesters
- D06P3/54—Polyesters using dispersed dyestuffs
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- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/30—Ink jet printing
Abstract
The present invention relates to field of printing and dyeing, particularly a kind of true color spray ink disperse dye ink of the anhydrous printing of terylene chemical fibre ground cushion.Faster, color sensation is more preferable for printing and dyeing colouring, and the color service life can be long.Ingredient includes:Disperse dye ink content 22 ~ 35%, agent content 3 ~ 7% of sizing mixing, level dyeing agent content 4 ~ 9%, moisture absorption agent content 2%；Lubricant content % softens agent content 1 ~ 3%, finish content 1 ~ 3%, including blast reason auxiliary agent 0.7 ~ 1.2%, fixation auxiliary agent 1 ~ 1.2%, printing assistant 1.3 ~ 1.6%；Deionized water 28 ~ 40%, chelating agent 0.5%；Levelling agent is mainly acid system levelling agent and cationic system levelling agent, the beneficial effects of the invention are as follows：It overcomes in the case where agent of sizing mixing, the dispersion liquid of disperse dye ink, deionized water total content are higher, the situation that the fixing degree of dyestuff can reduce, the adsorption capacity of entire dye ions can be increased by adding when chelating agent is carried out reconciling when in use once into steam colo(u)r printing process, overcome terylene color fastness is low in exhausting dye method dyeing course the shortcomings that, increase color fastness, homogenized diet is good.
Description
Technical field
The present invention relates to field of printing and dyeing, particularly a kind of true color spray ink disperse dyes ink of the anhydrous printing of terylene chemical fibre ground cushion
Water.
Background technology
Natural carpet dyeing, making are all very complicated so the expensive feelings for being even up to tens thousand of one square metre in carpet
Condition so industrialized production produces the carpet of textile of chemical fibre material, reduces the production prices of carpet, chemical fibre carpet is generally using drawing
Suede or establishment, in existing industrial textile using ink be mostly reactive dye (also known as chemically-reactive dyes), acid dyes or
Disperse dye ink, wherein reactive dye pH values easily increase, and hydrolysis or alcoholysis easily occur in water, so as to reduce weaving
The color fastness of product stamp, the coloring service life is too low, and color fastness decreased speed is very fast, not so washing and soaked fugitive color, and ink holds
It easily decomposes, a large amount of water is needed to print and dye, and dry making again, manufacture craft is expensive, it is impossible to it is long-term to preserve, additionally, due to
Contain impurity more, easily block nozzle, be increasingly not suitable for for the ink-jet cloth printing machine increasingly evolved.
Invention content
The purpose of the invention is to invent a kind of true color spray ink disperse dyes of the anhydrous printing of terylene chemical fibre ground cushion
Ink, faster, color sensation is more preferable for printing and dyeing colouring, and the color service life can be long.
The present invention is achieved through the following technical solutions：A kind of true color spray ink dispersion of the anhydrous printing of terylene chemical fibre ground cushion
Dye ink, ingredient include:
Disperse dye ink content 22 ~ 35%,
It sizes mixing agent content 3 ~ 7%,
Level dyeing agent content 4 ~ 9%,
Moisture absorption agent content 2%；
Lubricant content %,
Soften agent content 1 ~ 3%,
Finish content 1 ~ 3%, including blast reason auxiliary agent 0.7 ~ 1.2%, fixation auxiliary agent 1 ~ 1.2%, printing assistant 1.3 ~ 1.6%；
Deionized water 28 ~ 40%,
Chelating agent 0.5%；
Disperse dye ink includes at least following color：
C.I. disperse yellow 7,54,64,70,71,100,242；
C.I. disperse orange 25,37,119；
C.I. disperse red 50,60,65,146,239；
C.I. disperse blue 26,35,55,56,81：1、91、366；
C.I. disperse violet 26,27,57,106；
Agent of sizing mixing includes thiodiglycol liquid, ethylene glycol liquid, sweet glycol liquid；
Levelling agent is mainly acid system levelling agent and cationic system levelling agent, including at least triphenyl vinyl phenol polyoxyethylene sulfonic acid
Ammonium, glycerine polyoxyethylene oleic acid ester, nonylphenol polyoxyethylene ether, nonylphenol polyoxyethylene ether sulfuric ester, dodecyl gather
At least one in ethylene oxide ether sulfuric ester, sodium metnylene bis-naphthalene sulfonate, sodium lignin sulfonate and benzyl naphthalene sulfonic acid-formaldehyde condensation product
Kind；
Hygroscopic agent includes polyethylene glycol liquid, ethylene glycol, oxo diethylene glycol, butyrolactam, n-methyl-2-pyrrolidone, 2- first
Base -3- hydroxyls-pyrokomane, in 4- butanediol 1,5-PDs；
Lubricant includes fatty acid loss water sorbit ester and fatty alcohol polyoxyethylene ether；
Softening agent includes calgon, isopropanol；
Suspended particulate as the preferred dispersion liquid is no more than 1 ~ 1.3 μm.
As the inorganic oxide source solution for also containing %0.3 ~ 0.4 in the preferred finishing agent, including methyl-
4- isothiazoline -3- ketone, hydrocortisone butyrate.
The beneficial effects of the invention are as follows：It overcomes in agent of sizing mixing, the dispersion liquid of disperse dye ink, deionized water total content
Compare it is high in the case of, situation that the fixing degree of dyestuff can reduce adds chelating agent and is reconciled when in use once
The adsorption capacity of entire dye ions can be increased when into steam colo(u)r printing process, overcome the terylene in dye method dyeing course is exhausted
The shortcomings that color fastness is low, increases color fastness, and homogenized diet is good；Toner and brightener demand are few, cooperation inherently terylene light
The higher situation of brightness, can reach other chemical fibre brightening degree highers, and dull fading time is longer；
Sizing mixing, agent will not can rise because of the content of demand viscosity and consistency harmful substance particularly aldehyde, using the glue that can be controlled
Body silica composition color fixing agent carries out fixation and control viscosity；
The surface tension of fabric determines the trend that the dot shape to be formed is relatively round, spreads around after ink is sprayed by ink jet printer
It is smaller, higher stamp fineness is can be obtained by if can quickly be absorbed by fabric, fixation reaction and dyestuff have preferably
Degree of fixation
With good depth of color；
Color has promotion, and for previous disperse dye ink after the addition of multiple additives, hydrophily can be almost insoluble worse and worse
Yu Shui.It can only significantly be added after dyestuff microparticle suspending liquid is cladded, be dispersed in water by means of anionic dispersing agents, it is this
Degree of control allotment is extremely complex, and production technology and cost of manufacture are very high, so that the advanced printing and dyeing disperse dye ink in China is all
It is import, this dyestuff is under the action of the multiple factors of cationic system levelling agent and chelating agent and ionized water, isolation as possible
Ions binding, " cladding energy " between dispersant molecule and dyestuff microparticle suspending liquid can be reduced, can will not again be gathered because of temperature
The dye granule of integrated bigger, general carpet blank material temperature degree surface can reach 100 degree of first spray in the case of steam process
Effect of the cladded dyestuff microparticle suspending liquid separate out docile of ink dye on printing product is more preferable, and color is more bright-coloured, decoloration
Phenomenon is less；
Dispersant dosage is more, and dye solubilization amount is bigger, and dyestuff is precipitated also more when temperature reduces, and dye granule is caused to increase
Seriously, what this product can repeat can carry out including the situation that reduction particle may polymerize again using aforementioned cladding, have and locate in advance
The situation of reason, improves the staining performance of polyester carpet, this ratio dosage of this ink and nonionic surfactant can be shown
When writing the high-temperature stability for improving dispersion, disperse dyes can be aggravated, dacron staining contaminates dispersion at 60 ~ 130 DEG C
The solubilising of material and there is positive impact to the high dispersion stability of dispersion.
Not blocking sprayer, this dyestuff will not cause excessive coke in ink jet process with oligomer, the finish accumulated in the past
Oiling object, the dispersing uniformity requirement of dye liquor is very high, so the nozzle of ink-jet cloth printing machine will not be blocked；In heating or temperature-fall period
Middle lubricant cooperation printing assistant makes the dye liquor generation collection that will not cause to meet again existing, as its heat-coagulation is small, further alleviates
Dyeing defect mess code and color stain；
Fungi-proofing effect is more preferable, and most strains of carpet are dermatitis bacterium and fungi, can generate allergic dermatitis and other respectively
Such as tinea pedis skin disease, the pile structure of these carpets, which can be also attached to, grows acarid, contains inorganic oxide in dyestuff
Source solution has the growth that certain sterilization and bacteriostasis effect inhibits allergy and fungi.
Specific embodiment
Below by embodiment, the technical solutions of the present invention will be further described：
The present invention is achieved through the following technical solutions：A kind of true color spray ink disperse dyes of the anhydrous printing of terylene chemical fibre ground cushion
Ink, ingredient include:
Disperse dye ink content 22 ~ 35%,
It sizes mixing agent content 3 ~ 7%,
Level dyeing agent content 4 ~ 9%,
Moisture absorption agent content 2%；
Lubricant content %,
Soften agent content 1 ~ 3%,
Finish content 1 ~ 3%, including blast reason auxiliary agent 0.7 ~ 1.2%, fixation auxiliary agent 1 ~ 1.2%, printing assistant 1.3 ~ 1.6%；
Deionized water 28 ~ 40%,
Chelating agent 0.5%；
Disperse dye ink includes at least following color：
C.I. disperse yellow 7,54,64,70,71,100,242；
C.I. disperse orange 25,37,119；
C.I. disperse red 50,60,65,146,239；
C.I. disperse blue 26,35,55,56,81：1、91、366；
C.I. disperse violet 26,27,57,106；
Agent of sizing mixing includes thiodiglycol liquid, ethylene glycol liquid, sweet glycol liquid；
Levelling agent is mainly acid system levelling agent and cationic system levelling agent, including at least triphenyl vinyl phenol polyoxyethylene sulfonic acid
Ammonium, glycerine polyoxyethylene oleic acid ester, nonylphenol polyoxyethylene ether, nonylphenol polyoxyethylene ether sulfuric ester, dodecyl gather
At least one in ethylene oxide ether sulfuric ester, sodium metnylene bis-naphthalene sulfonate, sodium lignin sulfonate and benzyl naphthalene sulfonic acid-formaldehyde condensation product
Kind；
Hygroscopic agent includes polyethylene glycol liquid, ethylene glycol, oxo diethylene glycol, butyrolactam, n-methyl-2-pyrrolidone, 2- first
Base -3- hydroxyls-pyrokomane, in 4- butanediol 1,5-PDs；
Blast reason auxiliary agent is non-newborn silicone oil series or modified hydrophilic silicone oil series；
Fixation auxiliary agent is：Colloidal silicon dioxide component 3% ~ 11
Lubricant includes fatty acid loss water sorbit ester and fatty alcohol polyoxyethylene ether；
Softening agent includes calgon, isopropanol；
Suspended particulate as the preferred dispersion liquid is no more than 1 ~ 1.3 μm.
As in the preferred finishing agent, also the inorganic oxide source containing %0.3 ~ 0.4 is in solution, including first
Base -4- isothiazoline -3- ketone, hydrocortisone butyrate.
A kind of true color spray ink disperse dye ink of the anhydrous printing of terylene chemical fibre ground cushion is prepared and method：
Embodiment 1：
It is made according to weight percent including following components：
1. dyestuff dry powder filter cake be ground into less than 0.6 μm hybrid particles carry out pre-production become dyestuff microparticle suspending liquid or
Thick dose of C.I. disperse yellow 144% of dyestuff, manufacturing process is as follows, every gram of 0.6 μm of dyestuff dry powder carry out add in dispersant for N systems with
MF systems, nonionic surface active agent 9~14.5%；Water-soluble nonionic surfactant 0.1~5%；Non-ionic increasing
Thick dose of 2-11%, other are presetting for water and the progress of other dye additives；
2. after the completion of thick dose of C.I. disperse yellow 144% of step 1 dyestuff microparticle suspending liquid or dyestuff, add polyethylene glycol liquid,
Ethylene glycol, oxo diethylene glycol, butyrolactam, n-methyl-2-pyrrolidone, 2- methyl -3- hydroxyls-pyrokomane, 4- fourths two
Alcohol 1,5-PD；
3. add in thiodiglycol liquid, ethylene glycol liquid, sweet glycol liquid one or more of which；
4. adding in levelling agent, it is added according to practical terylene model or blended type, color requirements；
5. add in calgon, isopropanol；
6. component is 45 DEG C in temperature on, and rotating speed is sufficiently stirred 2 hours under the conditions of being 150 turns/min, must be mixed molten
Liquid；
7. deionized water, fatty acid loss water sorbit ester and fatty alcohol polyoxyethylene ether are individually added into, finish content 1 ~ 3%, packet
Blast reason auxiliary agent 0.7 ~ 1.2%, fixation auxiliary agent 1 ~ 1.2%, printing assistant 1.3 ~ 1.6% are included, is stirred to obtain mixing suspension；
8. by the mixing mixing suspension steps for importing 1-6 mixed liquors of step 7；
9. add in ionized water and chelating agent；
10. importing finishing agent, continue to be stirred, finally obtain consistency Tack values less than 17 ~ 5mps, fluidity 36 ~
70mm, viscosity 8-12mPas；
11. by being cooled to room temperature with the mixed solution that step obtains by cooler, mixed solution after cooling is passed through successively
The millipore filter that aperture is 0.45 μm and 0.20 μm filters, and polyester carpet yellow anhydrous printing true color spray ink point can be made
Dissipate dye ink.
12. it is first immersed in advance in pre- soft water using preceding addition terylene chemical fibre ground cushion original dye body and carries out pre- bubble processing, pre- soft water
Including distilled water, 1.3 ~ 1.5g/L of ammonium sulfate, sodium hydrosulfite 1g/L is warming up to 90 DEG C for every 2 DEG C/min under room temperature, impregnates 10 minutes
→ 1 DEG C/min is warming up to 130 DEG C, impregnates 50 minutes → 3 DEG C/min, cools to 60 DEG C → taking-up and carries out restocking, ink jet printer is led
Enter true color spray ink disperse dye ink and carry out ink-jet cloth printing.
Preparation method is taken out remaining nonstandard chemicals step again after step 13, is put into deionized water and adjusts gross mass
Hot iron is carried out after being moistened in the water of a concentration of 10 ± 1Wt.%, 10 ~ 14 parts of absolute ethyl alcohol, glacial acetic acid or member are added in during blanching
Bright 20 parts of powder suspension, 3 ~ 8 parts of emulsifier, 6 ~ 8 parts of dust-proofing agent, 10 parts of bleeding agent, other deionized waters；Bleeding agent at least mixes
There are sulfated castor oil, sodium alkyl sulfonate, alkyl sulfate sodium, secondary alkyl sulphate sodium, succinic acid alkyl ester sulfonate sodium；It is dust-proof
Agent is anhydrous sodium sulfate and dust proofing agent for dyestuff D series or Bayer Bitterfeld GmbH BAYER series.
Specific embodiment described herein is only an example for the spirit of the invention.Technology belonging to the present invention is led
The technical staff in domain can do various modifications or additions to described specific embodiment or replace in a similar way
In generation, however, it does not deviate from the spirit of the invention or beyond the scope of the appended claims.
Claims (5)
1. a kind of true color spray ink disperse dye ink of the anhydrous printing of terylene chemical fibre ground cushion, it is characterized in that ingredient includes:
Dispersion content 22 ~ 35%,
It sizes mixing agent content 3 ~ 7%,
Level dyeing agent content 4 ~ 9%,
Moisture absorption agent content 2%；
Lubricant content %,
Soften agent content 1 ~ 3%,
Finish content 1 ~ 3%, the finishing agent include blast reason auxiliary agent 0.7 ~ 1.2%, fixation auxiliary agent 1 ~ 1.2%, printing assistant
1.3~1.6%；
Chelating agent 0.5%；
Other are deionized water 28 ~ 40%,
The dispersion liquid of disperse dye ink includes at least following color：
C.I. disperse yellow 7,54,64,70,71,100,242；
C.I. disperse orange 25,37,119；
C.I. disperse red 50,60,65,146,239；
C.I. disperse blue 26,35,55,56,81：1、91、366；
C.I. disperse violet 26,27,57,106；
Agent of sizing mixing includes thiodiglycol liquid, ethylene glycol liquid, sweet glycol liquid；
Levelling agent includes acid system levelling agent and cationic system levelling agent；
Hygroscopic agent includes polyethylene glycol liquid, ethylene glycol, oxo diethylene glycol, butyrolactam, n-methyl-2-pyrrolidone, 2- first
Base -3- hydroxyls-pyrokomane, in 4- butanediol 1,5-PDs；
Blast reason auxiliary agent is non-newborn silicone oil series or modified hydrophilic silicone oil series；
Fixation auxiliary agent is：Colloidal silicon dioxide component 3% ~ 11
Lubricant includes fatty acid loss water sorbit ester and fatty alcohol polyoxyethylene ether；
Softening agent includes calgon, isopropanol.
2. according to a kind of true color spray ink disperse dye ink of the anhydrous printing of terylene chemical fibre ground cushion of claim 1, it is characterized in that:Institute
The suspended particulate for stating dispersion liquid is no more than 1 ~ 1.3 μm.
3. according to a kind of true color spray ink disperse dye ink of the anhydrous printing of terylene chemical fibre ground cushion of claim 1, it is characterized in that:Institute
The also inorganic oxide source containing %0.3 ~ 0.4 is stated in finishing agent in solution, including methyl -4- isothiazoline -3- ketone,
Hydrocortisone butyrate.
4. according to a kind of preparation method of the true color spray ink disperse dye ink of the anhydrous printing of terylene chemical fibre ground cushion of claim 1:
The disperse dye ink, other additives be organic solvent, glacial acetic acid and anhydrous sodium sulphate, Elements in Organic Solvents include ethylene glycol,
Diethylene glycol, triethylene glycol, propylene glycol, butanediol, ethylene glycol monoethyl ether, ethylene glycol monobutyl ether, diethylene glycol monobutyl ether, diethyl
2-ethoxyethanol, diethylene glycol monomethyl ether, glycerine, 2-Pyrrolidone, N- methyl-pyrrolidons, 1,3- dimethyl -2- imidazoles
The group that quinoline ketone and triethanolamine are formed；Wherein the content of organic solvent composition is 0.095~33.25 weight percent；Ice
Acetic acid content is 0.005~1.75 weight percent；The content of anhydrous sodium sulphate is 5~35 weight percent；And water；
1）Dyestuff dry powder filter cake be ground into less than 0.6 μm hybrid particles carry out pre-production become dyestuff microparticle suspending liquid or
Thick dose of C.I. disperse yellow 144% of dyestuff, manufacturing process is as follows, every gram of 0.6 μm of dyestuff dry powder carry out add in dispersant for N systems with
MF systems, nonionic surface active agent 9~14.5%；Water-soluble nonionic surfactant 0.1~5%；Non-ionic increasing
Thick dose of 2-11%, other are presetting for water and the progress of other dye additives；
2）After the completion of thick dose of C.I. disperse yellow 144% of step 1 dyestuff microparticle suspending liquid or dyestuff, add polyethylene glycol liquid,
Ethylene glycol, oxo diethylene glycol, butyrolactam, n-methyl-2-pyrrolidone, 2- methyl -3- hydroxyls-pyrokomane, 4- fourths two
Alcohol 1,5-PD；
3）Add in thiodiglycol liquid, ethylene glycol liquid, sweet glycol liquid one or more of which；
4）Levelling agent is added in, is added according to practical terylene model or blended type, color requirements；
5）Add in calgon, isopropanol；
6）Upper component is 45 DEG C in temperature, and rotating speed is sufficiently stirred 2 hours under the conditions of being 150 turns/min, must be mixed molten
Liquid；
7）It is individually added into deionized water, fatty acid loss water sorbit ester and fatty alcohol polyoxyethylene ether, finish content 1 ~ 3%, packet
Blast reason auxiliary agent 0.7 ~ 1.2%, fixation auxiliary agent 1 ~ 1.2%, printing assistant 1.3 ~ 1.6% are included, is stirred to obtain mixing suspension；
8）By the mixing mixing suspension steps for importing 1-6 mixed liquors of step 7；
9）Add in ionized water and chelating agent；
10）Finishing agent is imported, continues to be stirred, temperature is controlled at 35 DEG C hereinafter, continuing stirring 10 minutes after adding, stops
Only, reactor bottom material is released into 150-200kg, puts into reaction kettle again, then control 35 DEG C of temperature 40 minutes stirred below, most
After obtain consistency Tack values less than 17 ~ 5mps, 36 ~ 70mm of fluidity, viscosity 8-12mPas, dyeing process is in printing and dyeing temperature
70 ~ 110 DEG C of dispersibilities are in more than A/4, and for room temperature dispersibility in more than A/2,130 degree or more more than A/3, qualification export is not qualified
It is adjusted again；
11）It will be cooled to room temperature with the mixed solution that step obtains by cooler, mixed solution after cooling passed through successively
The millipore filter that aperture is 0.45 μm and 0.20 μm filters, and polyester carpet yellow anhydrous printing true color spray ink point can be made
Dissipate dye ink；
12）It is first immersed in advance in pre- soft water using preceding addition terylene chemical fibre ground cushion original dye body and carries out pre- bubble processing, pre- soft water includes
Distilled water, 1.3 ~ 1.5g/L of ammonium sulfate, sodium hydrosulfite 1g/L are warming up to 90 DEG C for every 2 DEG C/min under room temperature, impregnate 10 minutes → 1
DEG C/min be warming up to 130 DEG C, impregnate 50 minutes → 3 DEG C/min, cool to 60 DEG C → take out and carry out restocking, ink jet printer imports true
Color spray ink disperse dye ink carries out ink-jet cloth printing.
5. according to a kind of preparation method of the true color spray ink disperse dye ink of the anhydrous printing of terylene chemical fibre ground cushion of claim 4,
It is characterized in that:It is taken out remaining nonstandard chemicals step again after step 13, being put into deionized water adjusting total mass concentration is
Hot iron is carried out after being moistened in the water of 10 ± 1Wt.%, adds in 10 ~ 14 parts of absolute ethyl alcohol during blanching, glacial acetic acid or anhydrous sodium sulphate hang
20 parts of supernatant liquid, 3 ~ 8 parts of emulsifier, 6 ~ 8 parts of dust-proofing agent, 10 parts of bleeding agent, other deionized waters；Bleeding agent is at least mixed with sulfuric acid
Change castor oil, sodium alkyl sulfonate, alkyl sulfate sodium, secondary alkyl sulphate sodium, succinic acid alkyl ester sulfonate sodium；Dust-proofing agent is nothing
Aqueous sodium persulfate and dust proofing agent for dyestuff D series or Bayer Bitterfeld GmbH BAYER series.
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| CN109208345A (en) * | 2018-08-21 | 2019-01-15 | 聂志强 | A kind of colouring method of wear-resisting cloth bag |
| CN111945442A (en) * | 2020-09-05 | 2020-11-17 | 泰州利广瑞新材料科技有限公司 | Nanometer anhydrous dyeing material and technology for polyester fiber |
| CN112195664A (en) * | 2019-07-08 | 2021-01-08 | 南通鸿鼎威雅地毯有限公司 | Printed carpet production process without sewage discharge |
| CN112281513A (en) * | 2020-10-22 | 2021-01-29 | 于长德 | Carpet printing method |
| TWI754878B (en) * | 2019-12-03 | 2022-02-11 | 財團法人紡織產業綜合研究所 | Sprayable and hygroscopic ink for digital printing process for fabric and hygroscopic fabric |
| US20220298355A1 (en) * | 2019-11-29 | 2022-09-22 | Zhejiang Green Universe Textile Technology Co., Ltd. | Disperse Dye Color Paste for Waterless Dyeing, and Preparation Method and Application Thereof |
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| CN109208345A (en) * | 2018-08-21 | 2019-01-15 | 聂志强 | A kind of colouring method of wear-resisting cloth bag |
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| CN112281513A (en) * | 2020-10-22 | 2021-01-29 | 于长德 | Carpet printing method |
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