CN106049098B - A kind of environment-friendly type wollen fabrics dyeing method - Google Patents

A kind of environment-friendly type wollen fabrics dyeing method Download PDF

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CN106049098B
CN106049098B CN201610513295.1A CN201610513295A CN106049098B CN 106049098 B CN106049098 B CN 106049098B CN 201610513295 A CN201610513295 A CN 201610513295A CN 106049098 B CN106049098 B CN 106049098B
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environment
accelerant
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expanded vermiculite
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CN106049098A (en
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何时荣
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Huzhou New Jiayi Silk Printing Co Ltd
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    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/38General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using reactive dyes
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/445Use of auxiliary substances before, during or after dyeing or printing
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/46General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing natural macromolecular substances or derivatives thereof
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/46General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing natural macromolecular substances or derivatives thereof
    • D06P1/48Derivatives of carbohydrates
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/52General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing synthetic macromolecular substances
    • D06P1/5207Macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • D06P1/525Polymers of unsaturated carboxylic acids or functional derivatives thereof
    • D06P1/5257(Meth)acrylic acid
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/62General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds with sulfate, sulfonate, sulfenic or sulfinic groups
    • D06P1/621Compounds without nitrogen
    • D06P1/622Sulfonic acids or their salts
    • D06P1/625Aromatic
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/64General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
    • D06P1/651Compounds without nitrogen
    • D06P1/65106Oxygen-containing compounds
    • D06P1/65131Compounds containing ether or acetal groups
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/673Inorganic compounds
    • D06P1/67383Inorganic compounds containing silicon
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P3/00Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
    • D06P3/008Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated using reactive dyes
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P3/00Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
    • D06P3/58Material containing hydroxyl groups
    • D06P3/60Natural or regenerated cellulose
    • D06P3/66Natural or regenerated cellulose using reactive dyes

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Molecular Biology (AREA)
  • Inorganic Chemistry (AREA)
  • Coloring (AREA)

Abstract

A kind of environment-friendly type wollen fabrics dyeing method, by the way of expanded vermiculite powder, gelatin, guar gum cooperation organic acid, it is prepared for the rush dye drug with good result, the hydrauture of reactive dye can effectively be reduced, when in use, anhydrous sodium sulphate can be replaced completely, greatly reduce the salt usage amount in dyeing process, the usage amount for reducing water and soda ash simultaneously, is good for the environment.

Description

A kind of environment-friendly type wollen fabrics dyeing method
Technical field
The present invention relates to technical field of textile printing more particularly to a kind of environment-friendly type wollen fabrics dyeing methods.
Background technology
Cotton fiber occupies an important position in textile industry, accounts about the 65% of fiber total output.It applies at present in cotton Most important, most potential dyestuff in terms of stock-dye is reactive dye.Reactive dye and cotton fiber by Covalent bonding together, Fundamentally solve the problems, such as that coloured fibre wet colour fastness is poor.Simultaneously as reactive dye have chromatography complete, color and luster is fresh Gorgeous, the advantages that technique for applying is easy, strong applicability, price is relatively cheap, it had become yield in cotton fiber dyestuff in recent years With the maximum dyestuff of the output value.It must be added to a large amount of sodium chloride or sodium sulphate in traditional reactive dyeing process, work as dye After salt is added in bath, the hydrauture of dyestuff reduces, and the tendency that such dyestuff is shifted from aqueous solution to fiber surface is increased by, and balances Upper dye amount just increases.
Salt pollution problem in elimination activity dyeing, at present mainly by two methods, first, from reactive dye are increased Set about i.e. cotton fiber cationization with cotton fiber affinity, cotton fiber is modified by method chemically and physically, makes fibre Dimension table face is positively charged, increases the affinity of fiber and dyestuff by the electrostatic interaction between positive and negative charge, reaches the work for promoting dye With.But in place of this method Shortcomings, it cannot such as recycle, have an impact to the performance of fiber itself, small organic agents The problems such as dosage is big, and the toxic side effect having, and polymer reactant is unfavorable for dyestuff penetration, and coloured fibre coloured light is not bright-coloured.
The second is salt substitute technology, i.e., substitute anhydrous sodium sulphate (chemical name using pollution-free, environment amenable compound Claim:Anhydrous sodium sulfate, alias:Anhydrous sodium sulphate, thenardite), most of these compounds are still salt, therefore referred to as salt substitute. People know that the salt effect ratio NaCl of unary carboxylation is strong, and polybasic carboxylic acid is stronger than unary carboxylation, is replaced with them by research Salt and anhydrous sodium sulphate, salt dosage can greatly reduce, but the same salt of these so-called salt substitute prices, anhydrous sodium sulphate compare reality at present It is being too expensive, therefore also can not promotion and application.
Chinese invention patent CN101560736A discloses a kind of accelerant of novel replacement anhydrous sodium sulphate, it can significantly be dropped Salt dosage (anhydrous sodium sulphate can be made to drop to the 50% of original dosage using minimal amount of accelerant) in low cotton fiber reactive dye, It is that one kind not only improving environmental protection, while can reduce the environment-friend auxiliaries of printing and dyeing enterprise production cost again.
But the continuous improvement with China to dyeing environmental requirement, there is an urgent need to research and develop it is a kind of it is at low cost, can be complete The full accelerant for substituting anhydrous sodium sulphate, come the usage amount of salt component when reducing printing and dyeing.
Invention content
In order to solve the problems in background technology, the present invention provides a kind of environment-friendly type wollen fabrics dyeing method.
A kind of environment-friendly type wollen fabrics dyeing method, includes the following steps:
A, reactive dye are added in water and the mixed solution of accelerant, obtain reactive dye dye liquor;
B, cotton fabric is put into above-mentioned reactive dye dye liquor, bath raio 1:10-20, then with the speed of 1-2 DEG C/min It is warming up to 60-80 DEG C and keeps the temperature 20-40min, 0.2-0.5g/L soda ash is added, is warming up to 85-100 DEG C and keeps the temperature 15-25min, By fabric washing, drying after heat preservation, you can.
The accelerant includes the main component of following weight percent:
Preferably, the organic acid is kojic acid.
Preferably, the emulsifier is neopelex.
Preferably, the dispersant is Sodium Polyacrylate.
The preparation method of the accelerant, includes the following steps:
Step 1:Expanded vermiculite is crushed, and crosses 120 mesh sieve, extracting screen underflow will be expanded by the way of wet grinding Vermiculite power is ground to 10-30 μm;
Step 2:By expanded vermiculite powder, it is added to the water, dispersant and emulsifier is added, 45-50 DEG C is heated to, in 350- It is stirred evenly under the conditions of 400rpm;
Step 3:Gelatin and Arabic gum is added, is persistently emulsified under conditions of 8000-10000rpm with high speed dispersor 10-15min forms uniform milk;
Step 4:Organic acid is added, adjusts pH value, gelatin is made to generate cohesion, constant temperature 15-20min with Arabic gum;
Step 5:Through being dried under reduced pressure or being freeze-dried, accelerant is obtained.
Preferably, in the step four, pH value is adjusted to 4-5.5.
The present invention using gelatin and Arabic gum package expanded vermiculite powder system be used as accelerant, addition accelerant after, The rapid water swelling of system is not necessarily to that anhydrous sodium sulphate is added in entire dyeing process, greatly to effectively reduce the hydrauture of reactive dye The big salt usage amount reduced in dyeing process, while the usage amount of water and soda ash is reduced, it is good for the environment.
Kojic acid is added in addition to adjusting pH value, so that gelatin is generated with Arabic gum outside the effect of cohesion, is also equipped with inhibition system Middle melanin production, fresh-keeping hyperchromic function.
Environment-friendly type wollen fabrics dyeing method of the present invention, is combined with using expanded vermiculite powder, gelatin, Arabic gum The mode of machine acid, is prepared for the accelerant with good result, can effectively reduce the hydrauture of reactive dye, when in use, Anhydrous sodium sulphate can be replaced completely, the salt usage amount in dyeing process is greatly reduced, while reducing the usage amount of water and soda ash, have Conducive to environmental protection.
Specific implementation mode
Embodiment 1
A kind of environment-friendly type wollen fabrics dyeing method, includes the following steps:
A, reactive dye are added in water and the mixed solution of accelerant, obtain reactive dye dye liquor;
B, cotton fabric is put into above-mentioned reactive dye dye liquor, bath raio 1:15, then heated up with the speed of 1.5 DEG C/min To 75 DEG C and keep the temperature 30min, be added 0.3g/L soda ash, be warming up to 95 DEG C and keep the temperature 20min, after heat preservation by fabric washing, Drying, you can.
The accelerant includes the main component of following weight percent:
The organic acid is kojic acid.
The emulsifier is neopelex.
The dispersant is Sodium Polyacrylate.
The preparation method of the accelerant, includes the following steps:
Step 1:Expanded vermiculite is crushed, and crosses 120 mesh sieve, extracting screen underflow will be expanded by the way of wet grinding Vermiculite power is ground to 10-30 μm;
Step 2:By expanded vermiculite powder, it is added to the water, dispersant and emulsifier is added, 48 DEG C are heated to, in 380rpm items It is stirred evenly under part;
Step 3:Gelatin and Arabic gum is added, is persistently emulsified under conditions of 10000rpm with high speed dispersor 12min forms uniform milk;
Step 4:Organic acid is added, it is 4.7 to adjust pH value, and gelatin is made to generate cohesion, constant temperature 12min with Arabic gum;
Step 5:Through being dried under reduced pressure or being freeze-dried, accelerant is obtained.
Embodiment 2
A kind of environment-friendly type wollen fabrics dyeing method, includes the following steps:
A, reactive dye are added in water and the mixed solution of accelerant, obtain reactive dye dye liquor;
B, cotton fabric is put into above-mentioned reactive dye dye liquor, bath raio 1:10, then it is warming up to the speed of 2 DEG C/min 60 DEG C and keep the temperature 40min, 0.2g/L soda ash be added, is warming up to 100 DEG C and keeps the temperature 15min, after heat preservation by fabric washing, dry It is dry, you can.
The accelerant includes the main component of following weight percent:
The organic acid is kojic acid.
The emulsifier is neopelex.
The dispersant is Sodium Polyacrylate.
The preparation method of the accelerant, includes the following steps:
Step 1:Expanded vermiculite is crushed, and crosses 120 mesh sieve, extracting screen underflow will be expanded by the way of wet grinding Vermiculite power is ground to 10-30 μm;
Step 2:By expanded vermiculite powder, it is added to the water, dispersant and emulsifier is added, 45 DEG C are heated to, in 400rpm items It is stirred evenly under part;
Step 3:Gelatin and Arabic gum is added, is persistently emulsified under conditions of 10000rpm with high speed dispersor 10min forms uniform milk;
Step 4:Organic acid is added, it is 5.2 to adjust pH value, and gelatin is made to generate cohesion, constant temperature 15min with Arabic gum;
Step 5:Through being dried under reduced pressure or being freeze-dried, accelerant is obtained.
Embodiment 3
A kind of environment-friendly type wollen fabrics dyeing method, includes the following steps:
A, reactive dye are added in water and the mixed solution of accelerant, obtain reactive dye dye liquor;
B, cotton fabric is put into above-mentioned reactive dye dye liquor, bath raio 1:20, then it is warming up to the speed of 1 DEG C/min 80 DEG C and keep the temperature 20min, 0.5g/L soda ash be added, is warming up to 85 DEG C and keeps the temperature 25min, after heat preservation by fabric washing, dry It is dry, you can.
The accelerant includes the main component of following weight percent:
The organic acid is kojic acid.
The emulsifier is neopelex.
The dispersant is Sodium Polyacrylate.
The preparation method of the accelerant, includes the following steps:
Step 1:Expanded vermiculite is crushed, and crosses 120 mesh sieve, extracting screen underflow will be expanded by the way of wet grinding Vermiculite power is ground to 10-30 μm;
Step 2:By expanded vermiculite powder, it is added to the water, dispersant and emulsifier is added, 50 DEG C are heated to, in 400rpm items It is stirred evenly under part;
Step 3:Gelatin and Arabic gum is added, 10min is persistently emulsified under conditions of 8000rpm with high speed dispersor, Form uniform milk;
Step 4:Organic acid is added, it is 4.5 to adjust pH value, and gelatin is made to generate cohesion, constant temperature 15min with Arabic gum;
Step 5:Through being dried under reduced pressure or being freeze-dried, accelerant is obtained.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto, Any one skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.

Claims (7)

1. a kind of environment-friendly type wollen fabrics dyeing method, which is characterized in that include the following steps:
A, reactive dye are added in water and the mixed solution of accelerant, obtain reactive dye dye liquor;
B, cotton fabric is put into above-mentioned reactive dye dye liquor, bath raio 1:Then 10-20 is heated up with the speed of 1-2 DEG C/min To 60-80 DEG C and 20-40min is kept the temperature, 0.2-0.5g/L soda ash is added, is warming up to 85-100 DEG C and keeps the temperature 15-25min, keeps the temperature After by fabric washing, drying, you can;
The accelerant includes the ingredient of following weight percent:
Expanded vermiculite powder 35-45%
Arabic gum 8-15%
Gelatin 8-10%
Organic acid 15-20%
Emulsifier 5-8%
Dispersant surplus.
2. environment-friendly type wollen fabrics dyeing method as described in claim 1, which is characterized in that the organic acid is kojic acid.
3. environment-friendly type wollen fabrics dyeing method as described in claim 1, which is characterized in that the emulsifier is dodecane Base benzene sulfonic acid sodium salt.
4. environment-friendly type wollen fabrics dyeing method as described in claim 1, which is characterized in that the dispersant is polypropylene Sour sodium.
5. environment-friendly type wollen fabrics dyeing method as described in claim 1, which is characterized in that the preparation side of the accelerant Method includes the following steps:
Step 1:Expanded vermiculite is crushed, and crosses 120 mesh sieve, extracting screen underflow, by the way of wet grinding, by expanded vermiculite Powder is ground to 10-30 μm;
Step 2:By expanded vermiculite powder, it is added to the water, dispersant and emulsifier is added, 45-50 DEG C is heated to, in 350- It is stirred evenly under the conditions of 400rpm;
Step 3:Gelatin and Arabic gum is added, 10- is persistently emulsified under conditions of 8000-10000rpm with high speed dispersor 15min forms uniform milk;
Step 4:Organic acid is added, adjusts pH value, gelatin is made to generate cohesion, constant temperature 15-20min with Arabic gum;
Step 5:Through being dried under reduced pressure or being freeze-dried, accelerant is obtained.
6. environment-friendly type wollen fabrics dyeing method as claimed in claim 5, which is characterized in that in the step four, by pH Value is adjusted to 4-5.5.
7. environment-friendly type wollen fabrics dyeing method as claimed in claim 5, which is characterized in that include the following steps:
A, reactive dye are added in water and the mixed solution of accelerant, obtain reactive dye dye liquor;
B, cotton fabric is put into above-mentioned reactive dye dye liquor, bath raio 1:15, then 75 are warming up to the speed of 1.5 DEG C/min DEG C and keep the temperature 30min, 0.3g/L soda ash is added, is warming up to 95 DEG C and keeps the temperature 20min, by fabric washing, drying after heat preservation, ;
The preparation method of the accelerant, includes the following steps:
Step 1:Expanded vermiculite is crushed, and crosses 120 mesh sieve, extracting screen underflow, by the way of wet grinding, by expanded vermiculite Powder is ground to 10-30 μm;
Step 2:By expanded vermiculite powder, it is added to the water, dispersant and emulsifier is added, 48 DEG C are heated to, under the conditions of 380rpm It stirs evenly;
Step 3:Gelatin and Arabic gum is added, 12min, shape are persistently emulsified under conditions of 10000rpm with high speed dispersor At uniform milk;
Step 4:Organic acid is added, it is 4.7 to adjust pH value, and gelatin is made to generate cohesion, constant temperature 12min with Arabic gum;
Step 5:Through being dried under reduced pressure or being freeze-dried, accelerant is obtained;
The accelerant includes the main component of following weight percent:
Expanded vermiculite powder 40%
Arabic gum 10%
Gelatin 8%
Kojic acid 16%
Neopelex 6%
Sodium Polyacrylate surplus.
CN201610513295.1A 2016-07-04 2016-07-04 A kind of environment-friendly type wollen fabrics dyeing method Active CN106049098B (en)

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CN109577041B (en) * 2019-01-15 2021-11-09 台州市旭泓服饰有限公司 Preparation method of intelligent heat-preservation dye
CN110725143A (en) * 2019-11-19 2020-01-24 湖州世合纺织有限公司 Printing and dyeing method for salt-free cotton-polyester blended fabric
CN112267313A (en) * 2020-11-05 2021-01-26 湖州金玺丝绸科技股份有限公司 Light-color printing process of washable silk fabric

Citations (3)

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Publication number Priority date Publication date Assignee Title
CN1817972A (en) * 2006-01-16 2006-08-16 大连理工大学 Acid dye composition
CN101381963A (en) * 2007-09-09 2009-03-11 胡红湘 Salt free dyeing with reactive dye
CN105274871A (en) * 2015-04-07 2016-01-27 时兴纺整(苏州)有限公司 Invisible pattern surface treatment technology for cloth showing patterns meeting water

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20150124175A (en) * 2014-04-28 2015-11-05 김기호 Functional natural dyeing method

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1817972A (en) * 2006-01-16 2006-08-16 大连理工大学 Acid dye composition
CN101381963A (en) * 2007-09-09 2009-03-11 胡红湘 Salt free dyeing with reactive dye
CN105274871A (en) * 2015-04-07 2016-01-27 时兴纺整(苏州)有限公司 Invisible pattern surface treatment technology for cloth showing patterns meeting water

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Denomination of invention: An environment-friendly cotton textile printing and dyeing method

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Pledgee: Zhejiang Deqing Rural Commercial Bank Co.,Ltd. Xinshi sub branch

Pledgor: HUZHOU XINJIAYI SILK WEAVING PRINTING Co.,Ltd.

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