CN106116549A - A kind of ceramic ware for daily use with health care - Google Patents
A kind of ceramic ware for daily use with health care Download PDFInfo
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- CN106116549A CN106116549A CN201610460748.9A CN201610460748A CN106116549A CN 106116549 A CN106116549 A CN 106116549A CN 201610460748 A CN201610460748 A CN 201610460748A CN 106116549 A CN106116549 A CN 106116549A
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/16—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silicates other than clay
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/62204—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products using waste materials or refuse
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/52—Multiple coating or impregnating multiple coating or impregnating with the same composition or with compositions only differing in the concentration of the constituents, is classified as single coating or impregnation
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/89—Coating or impregnation for obtaining at least two superposed coatings having different compositions
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3205—Alkaline earth oxides or oxide forming salts thereof, e.g. beryllium oxide
- C04B2235/3213—Strontium oxides or oxide-forming salts thereof
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/349—Clays, e.g. bentonites, smectites such as montmorillonite, vermiculites or kaolines, e.g. illite, talc or sepiolite
Abstract
The invention discloses a kind of ceramic ware for daily use with health care, be made up of the raw material of following weight portion: tourmaline 16 18, celestite 13 15, potassium feldspar 17 20, albite 9 11, strontium carbonate 34, montmorillonite 10 13, Ludox 34, propenyl 12, flyash 40 45, white glaze ball 35 40, cullet 68, Maifanitum 10 14, green tea 21 25, Pericarpium citri sinensis 14 17, conch meal 68, shrimp shell meal 46, polyvinyl alcohol 0.2 0.3, tributyl phosphate 0.2 0.3, deionized water are appropriate;The domestic ceramics formula dispensing low cost of the present invention, serviceability is good, and firing time is short, and temperature is low, saves the energy, has obvious economic benefit and a social benefit, and has good antibacterial, sterilization, health-care effect, can in Shi porcelain industry wide popularization and application.
Description
Technical field
The present invention relates to domestic ceramics technical field, particularly relate to a kind of ceramic ware for daily use with health care.
Background technology
China's not only rich in mineral resources, is also coal production state maximum in the world and consumption of coal state, in recent years simultaneously
Coming, China's thermal power generation quickly grows, and wherein great majority are with coal as fuel, and generated energy reaches 1.3 hundred million kW h, shared by thermal power generation
Ratio has reached 79.6%, thus causes flyash discharge capacity to increase year by year.In the end of the year 2010, discharge capacity reaches nearly 300,000,000 tons, in a large number
The discharge of flyash have received to be paid close attention to the most widely.China started just to how utilizing flyash as resource from 1987
The breach of comprehensive utilization, comprehensively utilizes it, becomes a long-range policy of economy and social development.Cullet class thing
Its chemical stability of matter is extremely strong, without putrefaction, does not burns, can not degrade, and substantial amounts of cullet both took up an area, and polluted again environment, reclaimed
Being to save the energy, the optimal path of protection environment with utilizing, and have good economy, the main component of glass is dioxy
SiClx, it is possible to promote the sintering of pottery.In Production of Ceramics, firing temperature is the highest, and firing time is the longest, and energy consumption is the highest, according to
Heat Balance Calculation, firing temperature often reduces by 100 DEG C, then unit product heat consumption can reduce by more than 10%, and firing time often shortens 10%,
Then yield increases by 10%, and heat consumption reduces by 4%, so reduction firing temperature and time have significant energy-saving and emission-reduction social meaning.
Over nearly 20 years, ceramic industry enters developmental stage with rapid changepl. never-ending changes and improvements, new technique, a large amount of uses of new equipment, pottery
Porcelain yield also increases by a fairly big margin.New ceramics, as a kind of new material, solely sets one with the performance of its excellence at Material Field
Flag, is paid much attention to by people.Domestic ceramics occupies an important position at Material Field as traditional ceramics material, because it
Relating to the every aspect of people's life, the development of domestic ceramics is more wanted along with the raising of people's living standard proposes
Asking, the most antibacterial is to propose most common requirement at present.Due to the wilderness demand of porcelain, a large amount of exploitations of china clay resource are just with frightened
The speed of people reduces, and is non-renewable resources, if can not find alternate resources, it is likely that can face No Assets later
The difficult situation that can adopt.Yang Yuwei et al. is at " utilizing the industrial wastes such as flyash to prepare the research of a domestic ceramics " literary composition middle finger
Go out, utilize the flyash of power plant emission, a large amount of useless saggars of ceramic industry generation, useless porcelain powder to utilize Orthogonal Experiment and Design to join
Side, develops cleaning and produces the formula of domestic ceramics, wherein flyash, useless saggar, the content of useless porcelain powder be 10% respectively, 10%,
8%, applying this technology can be that enterprise brings considerable economic benefit, and the recycling for flyash finds an exit, although carry
High Social benefit and economic benefit, but a lot of performance is not reaching to the requirement of people, the most antibacterial, high temperature resistance, freeze proof etc.
The shortcoming that performance is the highest, service life is not grown.
Summary of the invention
The object of the invention is contemplated to make up the defect of prior art, it is provided that a kind of domestic ceramics system with health care
Product.
The present invention is achieved by the following technical solutions:
A kind of ceramic ware for daily use with health care, is made up of the raw material of following weight portion: tourmaline 16-18, sky
Cordierite 13-15, potassium feldspar 17-20, albite 9-11, strontium carbonate 3-4, montmorillonite 10-13, Ludox 3-4, propenyl 1-2, powder
Coal ash 40-45, white glaze ball 35-40, cullet 6-8, Maifanitum 10-14, green tea 21-25, Pericarpium citri sinensis 14-17, conch meal 6-8,
Shrimp shell meal 4-6, polyvinyl alcohol 0.2-0.3, tributyl phosphate 0.2-0.3, deionized water are appropriate.
Described a kind of ceramic ware for daily use with health care, is made up of following concrete steps:
(1) Ludox, montmorillonite and propenyl are stirred, add concentration and be the copper nitrate of 0.2mol/L, silver nitrate
Solution, wherein montmorillonite and copper nitrate, silver nitrate solid-to-liquid ratio are 1:2-3:1-2, rise high-temperature and stir under the conditions of 50-60 DEG C instead
Answer 2-3h, continue to rise high-temperature at 60-70 DEG C, keep 30-40min, be then dried, grind, wash, filter the most after drying
Standby;
(2) by Maifanitum clean dry after wear into fine powder, by green tea, Pericarpium citri sinensis, conch meal, shrimp shell meal mixing be added to 75% second
In alcoholic solution, decoct 20-30min when 50-60 DEG C, be continuously heating to when 90-100 DEG C decoct 10-20min, be cooled to room temperature
After carry out centrifugation, take after its supernatant concentration and polyvinyl alcohol, medical stone powder, tributyl phosphate ball milling 30-40min, knot
While being stirred continuously slurry with direct current drive blender after bundle, it is standby that spray drying makes nano medical stone microsphere;
(3) cullet is cleaned up post-drying to crush, be then added to ground 100-200 mesh sieve in colloid mill, by glass
Glass powder and flyash, tourmaline, celestite, potassium feldspar are mixed to get dry material, add and account for going of dry material gross mass 40-50%
Ionized water, obtained the slurry of 300-400 mesh through ball mill pulverizing;
(4) the slurry magnetic separator that step (3) obtains is carried out iron removal by magnetic separation, make content≤0.2% of ferrum in slurry, by slurry
It is added to drying and moulding in forming machine and obtains base substrate, base substrate is put in the sintering furnace that in-furnace temperature is 100-200 DEG C, at 1200-
Carrying out at a temperature of 1280 DEG C calcining 5-7h, after being cooled to room temperature, polishing is scraped standby;
(5) antibacterial mixing white glaze ball, strontium carbonate, albite and step (1) obtained, is added in ball mill carry out wet method ball
Mill, adds the deionized water of material gross weight 45-55%, the glaze slip after ball milling is crossed 200 mesh, 300 mesh sieves respectively, goes the removal of impurity
And coarse granule, obtain thin glaze slip, by glaze slip glazing on biscuit prepared by step (4), at 1100-1180 DEG C, sinter 4-5h;
(6) nano medical stone microsphere and the phosphoric acid hydrogen al binder step (2) prepared mix according to 2-3:1 ratio, are coated in
Ceramic surface prepared by step (5), after drying in the shade, at 120-140 DEG C, constant temperature 2h is the most available.
The invention have the advantage that the present invention utilizes waste resource flyash as Ceramic Material, reduce the dirt to environment
Dye, and wherein silicon oxide, alumina content are higher, and specific grain surface is long-pending big in loose structure, easily grinds, can reduce system
The firing temperature of product, reaches energy-conservation purpose, and discarded glass, with flyash sintering process, melts at low temperatures, is formed
Glass phase, plays the effect of bonding agent, reduces firing temperature, and it is smooth, freeze proof, easy to clean, anti-to improve ceramic surface
The performance of the aspects such as impact, by the antibacterial of synthesis and glaze mixing glazing on biscuit of ceramics surface, improves ceramic antibacterial
Performance, reduces the danger coefficient that the mankind are ill, and uses the decoction of green tea, Pericarpium citri sinensis, conch meal, shrimp shell meal to extract trace
Element Maifanitum cladding forms nano medical stone microsphere, utilizes binding agent to be bonded in ceramic surface, solvable by being heated for a long time
Going out the multiple trace element useful to human body, the body for people provides nutrition, building body, regulates metabolism, to human body
Benefiting, the domestic ceramics formula dispensing low cost of the present invention, serviceability is good, and firing time is short, and temperature is low, saves energy
Source, has obvious economic benefit and a social benefit, and has good antibacterial, sterilization, health-care effect, can be in Shi porcelain industry
Wide popularization and application.
Detailed description of the invention
A kind of ceramic ware for daily use with health care, is made up of the raw material of following weight portion (kilogram): electrically
Stone 16, celestite 13, potassium feldspar 17, albite 9, strontium carbonate 3, montmorillonite 10, Ludox 3, propenyl 1, flyash 40, white glaze
Ball 35, cullet 6, Maifanitum 10, green tea 21, Pericarpium citri sinensis 14, conch meal 6, shrimp shell meal 4, polyvinyl alcohol 0.2, tributyl phosphate
0.2, deionized water is appropriate.
Described a kind of ceramic ware for daily use with health care, is made up of following concrete steps:
(1) Ludox, montmorillonite and propenyl are stirred, add concentration and be the copper nitrate of 0.2mol/L, silver nitrate
Solution, wherein montmorillonite and copper nitrate, silver nitrate solid-to-liquid ratio are 1:2:1, rise high-temperature and stir reaction 2h under the conditions of 50 DEG C, continue
High-temperature of continuing rising keeps 30min at 60 DEG C, be then dried, grind, wash, filter the most standby;
(2) by Maifanitum clean dry after wear into fine powder, by green tea, Pericarpium citri sinensis, conch meal, shrimp shell meal mixing be added to 75% second
In alcoholic solution, decoct 20min when 50 DEG C, when being continuously heating to 90 DEG C, decoct 10min, be centrifuged after being cooled to room temperature point
From, take after its supernatant concentration and polyvinyl alcohol, medical stone powder, tributyl phosphate ball milling 30min, after terminating, use unidirectional current
Slurry is stirred continuously by dynamic blender, and it is standby that spray drying makes nano medical stone microsphere;
(3) cullet is cleaned up post-drying to crush, be then added to ground 100 mesh sieves in colloid mill, by glass dust
It is mixed to get dry material with flyash, tourmaline, celestite, potassium feldspar, adds the deionized water accounting for dry material gross mass 40%,
The slurry of 300 mesh was obtained through ball mill pulverizing;
(4) the slurry magnetic separator that step (3) obtains is carried out iron removal by magnetic separation, make content≤0.2% of ferrum in slurry, by slurry
It is added to drying and moulding in forming machine and obtains base substrate, base substrate is put in the sintering furnace that in-furnace temperature is 100 DEG C, 1200 DEG C of temperature
Under carry out calcine 5h, after being cooled to room temperature polishing scrape standby;
(5) antibacterial mixing white glaze ball, strontium carbonate, albite and step (1) obtained, is added in ball mill carry out wet method ball
Mill, adds the deionized water of material gross weight 45%, and the glaze slip after ball milling is crossed 200 mesh, 300 mesh sieves respectively, goes the removal of impurity and thick
Granule, obtains thin glaze slip, by glaze slip glazing on biscuit prepared by step (4), sinters 4h at 1100 DEG C;
(6) nano medical stone microsphere and the phosphoric acid hydrogen al binder step (2) prepared mix according to 2:1 ratio, are coated in step
Suddenly the ceramic surface that prepared by (5), after drying in the shade, at 120 DEG C, constant temperature 2h is the most available.
Test data:
Product appearance is regular, and glaze is smooth;Thermal shock resistance test reaches heat exchange in 20 DEG C of water of 200 DEG C of inputs and does not splits;Machine
Tool intensity >=140mp2;Glaze vickers microhardness >=6.1GPa;Sunlight germicidal efficiency >=73% of lower 1 hour;Shock resistance is strong
Degree >=1.5J/cm2.
Claims (2)
1. a ceramic ware for daily use with health care, it is characterised in that be made up of the raw material of following weight portion: electricity
Gas stone 16-18, celestite 13-15, potassium feldspar 17-20, albite 9-11, strontium carbonate 3-4, montmorillonite 10-13, Ludox 3-4,
Propenyl 1-2, flyash 40-45, white glaze ball 35-40, cullet 6-8, Maifanitum 10-14, green tea 21-25, Pericarpium citri sinensis 14-
17, conch meal 6-8, shrimp shell meal 4-6, polyvinyl alcohol 0.2-0.3, tributyl phosphate 0.2-0.3, deionized water are appropriate.
A kind of ceramic ware for daily use with health care, it is characterised in that by following concrete step
Suddenly make:
(1) Ludox, montmorillonite and propenyl are stirred, add concentration and be the copper nitrate of 0.2mol/L, silver nitrate
Solution, wherein montmorillonite and copper nitrate, silver nitrate solid-to-liquid ratio are 1:2-3:1-2, rise high-temperature and stir under the conditions of 50-60 DEG C instead
Answer 2-3h, continue to rise high-temperature at 60-70 DEG C, keep 30-40min, be then dried, grind, wash, filter the most after drying
Standby;
(2) by Maifanitum clean dry after wear into fine powder, by green tea, Pericarpium citri sinensis, conch meal, shrimp shell meal mixing be added to 75% second
In alcoholic solution, decoct 20-30min when 50-60 DEG C, be continuously heating to when 90-100 DEG C decoct 10-20min, be cooled to room temperature
After carry out centrifugation, take after its supernatant concentration and polyvinyl alcohol, medical stone powder, tributyl phosphate ball milling 30-40min, knot
While being stirred continuously slurry with direct current drive blender after bundle, it is standby that spray drying makes nano medical stone microsphere;
(3) cullet is cleaned up post-drying to crush, be then added to ground 100-200 mesh sieve in colloid mill, by glass
Glass powder and flyash, tourmaline, celestite, potassium feldspar are mixed to get dry material, add and account for going of dry material gross mass 40-50%
Ionized water, obtained the slurry of 300-400 mesh through ball mill pulverizing;
(4) the slurry magnetic separator that step (3) obtains is carried out iron removal by magnetic separation, make content≤0.2% of ferrum in slurry, by slurry
It is added to drying and moulding in forming machine and obtains base substrate, base substrate is put in the sintering furnace that in-furnace temperature is 100-200 DEG C, at 1200-
Carrying out at a temperature of 1280 DEG C calcining 5-7h, after being cooled to room temperature, polishing is scraped standby;
(5) antibacterial mixing white glaze ball, strontium carbonate, albite and step (1) obtained, is added in ball mill carry out wet method ball
Mill, adds the deionized water of material gross weight 45-55%, the glaze slip after ball milling is crossed 200 mesh, 300 mesh sieves respectively, goes the removal of impurity
And coarse granule, obtain thin glaze slip, by glaze slip glazing on biscuit prepared by step (4), at 1100-1180 DEG C, sinter 4-5h;
(6) nano medical stone microsphere and the phosphoric acid hydrogen al binder step (2) prepared mix according to 2-3:1 ratio, are coated in
Ceramic surface prepared by step (5), after drying in the shade, at 120-140 DEG C, constant temperature 2h is the most available.
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CN201610460748.9A CN106116549A (en) | 2016-06-23 | 2016-06-23 | A kind of ceramic ware for daily use with health care |
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CN201610460748.9A CN106116549A (en) | 2016-06-23 | 2016-06-23 | A kind of ceramic ware for daily use with health care |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107663083A (en) * | 2017-09-30 | 2018-02-06 | 武汉马腾科技发展有限公司 | A kind of ceramics with high-wearing feature and antibiotic property and preparation method thereof |
CN109401632A (en) * | 2018-11-20 | 2019-03-01 | 吴江市格瑞福金属制品有限公司 | A kind of environment-friendly type polishing fluid and preparation method thereof for casting |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105084867A (en) * | 2015-08-05 | 2015-11-25 | 澧县新鹏陶瓷有限公司 | Antibiosis ceramic product with coal ash as main raw material and preparing method of antibiosis ceramic product |
-
2016
- 2016-06-23 CN CN201610460748.9A patent/CN106116549A/en not_active Withdrawn
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105084867A (en) * | 2015-08-05 | 2015-11-25 | 澧县新鹏陶瓷有限公司 | Antibiosis ceramic product with coal ash as main raw material and preparing method of antibiosis ceramic product |
Non-Patent Citations (1)
Title |
---|
王永康等: "《纳米材料科学与技术》", 31 March 2002, 浙江大学出版社 * |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107663083A (en) * | 2017-09-30 | 2018-02-06 | 武汉马腾科技发展有限公司 | A kind of ceramics with high-wearing feature and antibiotic property and preparation method thereof |
CN109401632A (en) * | 2018-11-20 | 2019-03-01 | 吴江市格瑞福金属制品有限公司 | A kind of environment-friendly type polishing fluid and preparation method thereof for casting |
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Application publication date: 20161116 |