CN1060951C - Antiviral veterinary injection and preparation method thereof - Google Patents
Antiviral veterinary injection and preparation method thereof Download PDFInfo
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- CN1060951C CN1060951C CN97116309A CN97116309A CN1060951C CN 1060951 C CN1060951 C CN 1060951C CN 97116309 A CN97116309 A CN 97116309A CN 97116309 A CN97116309 A CN 97116309A CN 1060951 C CN1060951 C CN 1060951C
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- 238000002347 injection Methods 0.000 title claims abstract description 28
- 239000007924 injection Substances 0.000 title claims abstract description 28
- 230000000840 anti-viral effect Effects 0.000 title claims abstract description 15
- 238000002360 preparation method Methods 0.000 title claims abstract description 7
- 239000003814 drug Substances 0.000 claims abstract description 32
- 238000001914 filtration Methods 0.000 claims abstract description 28
- 239000000706 filtrate Substances 0.000 claims abstract description 17
- 238000000034 method Methods 0.000 claims abstract description 10
- 241000208340 Araliaceae Species 0.000 claims abstract description 6
- 241000222336 Ganoderma Species 0.000 claims abstract description 6
- 235000005035 Panax pseudoginseng ssp. pseudoginseng Nutrition 0.000 claims abstract description 6
- 235000003140 Panax quinquefolius Nutrition 0.000 claims abstract description 6
- 241001506047 Tremella Species 0.000 claims abstract description 6
- 235000008434 ginseng Nutrition 0.000 claims abstract description 6
- 239000000203 mixture Substances 0.000 claims abstract description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 66
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 25
- 238000004321 preservation Methods 0.000 claims description 18
- 229940079593 drug Drugs 0.000 claims description 13
- 238000001816 cooling Methods 0.000 claims description 12
- 239000007788 liquid Substances 0.000 claims description 12
- 239000012567 medical material Substances 0.000 claims description 10
- 238000000247 postprecipitation Methods 0.000 claims description 9
- 239000002244 precipitate Substances 0.000 claims description 9
- 238000009835 boiling Methods 0.000 claims description 8
- 238000004061 bleaching Methods 0.000 claims description 6
- 229910052799 carbon Inorganic materials 0.000 claims description 6
- 238000011049 filling Methods 0.000 claims description 6
- 238000001179 sorption measurement Methods 0.000 claims description 6
- 230000001954 sterilising effect Effects 0.000 claims description 6
- 238000004659 sterilization and disinfection Methods 0.000 claims description 6
- 238000012546 transfer Methods 0.000 claims description 6
- 239000008215 water for injection Substances 0.000 claims description 6
- 239000009636 Huang Qi Substances 0.000 claims description 5
- 239000010231 banlangen Substances 0.000 claims description 5
- 238000005303 weighing Methods 0.000 claims description 5
- 239000012141 concentrate Substances 0.000 claims description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 3
- 238000005352 clarification Methods 0.000 claims description 3
- 230000006837 decompression Effects 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims description 3
- 238000007654 immersion Methods 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- 239000000843 powder Substances 0.000 claims description 3
- 238000001556 precipitation Methods 0.000 claims description 3
- 238000007639 printing Methods 0.000 claims description 3
- 238000012545 processing Methods 0.000 claims description 3
- 238000012216 screening Methods 0.000 claims description 3
- 239000003651 drinking water Substances 0.000 claims description 2
- 235000020188 drinking water Nutrition 0.000 claims description 2
- 238000010298 pulverizing process Methods 0.000 claims description 2
- 239000002994 raw material Substances 0.000 claims description 2
- 238000011084 recovery Methods 0.000 claims 1
- 208000000655 Distemper Diseases 0.000 abstract description 6
- 208000002979 Influenza in Birds Diseases 0.000 abstract description 6
- 206010037660 Pyrexia Diseases 0.000 abstract description 6
- 241000282898 Sus scrofa Species 0.000 abstract description 6
- 201000010099 disease Diseases 0.000 abstract description 4
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 abstract description 4
- 230000003612 virological effect Effects 0.000 abstract description 4
- 208000014058 canine distemper Diseases 0.000 abstract description 3
- 239000000273 veterinary drug Substances 0.000 abstract 2
- 241000282324 Felis Species 0.000 abstract 1
- 241000334160 Isatis Species 0.000 abstract 1
- 229940107666 astragalus root Drugs 0.000 abstract 1
- 231100000956 nontoxicity Toxicity 0.000 abstract 1
- 238000002791 soaking Methods 0.000 abstract 1
- 241001465754 Metazoa Species 0.000 description 5
- 241000700605 Viruses Species 0.000 description 5
- 241000282326 Felis catus Species 0.000 description 2
- 206010035148 Plague Diseases 0.000 description 2
- 241000607479 Yersinia pestis Species 0.000 description 2
- 230000002155 anti-virotic effect Effects 0.000 description 2
- 239000003443 antiviral agent Substances 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 244000144977 poultry Species 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 238000009395 breeding Methods 0.000 description 1
- 230000001488 breeding effect Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000036737 immune function Effects 0.000 description 1
- 238000000338 in vitro Methods 0.000 description 1
- 230000009545 invasion Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 235000013372 meat Nutrition 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 235000020679 tap water Nutrition 0.000 description 1
- 230000001225 therapeutic effect Effects 0.000 description 1
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- Medicines Containing Plant Substances (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention relates to a novel antiviral veterinary drug injection and a preparation method thereof, wherein the novel antiviral veterinary drug injection is mainly prepared from ginseng, lucid ganoderma, isatis root, tremella and astragalus root through the steps of crushing, soaking, decocting, filtering, taking filtrate and the like. Compared with the prior art, the traditional Chinese medicine composition is safe and reliable, has no toxicity, harm and residue, simple process, low cost and strong practicability, and is an ideal medicine for treating viral diseases such as fowl plague, swine fever, canine distemper, feline distemper and the like.
Description
The present invention relates to a kind of antiviral veterinary medicine injection, relate to a kind of veterinary medicine injection for the treatment of viral diseases such as fowl plague, swine fever, canine distemper, cat distemper and preparation method thereof specifically.
At present, raising day by day along with living standards of the people, people are also more and more higher to the demand of meat, egg, fowl, also promoted greatly developing of animal husbandry thus, yet, domestic animal and poultry but are subjected to the invasion and attack of plague virus such as fowl plague, swine fever constantly in raising, have caused the death of large quantities of domestic animals and poultry, have brought enormous economic loss for the raising cause.
Pestilence such as well-known fowl plague, swine fever are viral disease, virus can only be in living cells growth and breeding, in experiment in vitro antivirus action excellent drug, in the body during experiment since living cells to the selective permeation effect of material, cause the drug level that enters living cells very low, be difficult to reach therapeutic effect.How just can make body produce specific antiviral substance in cell, kill intravital virus, the antiviral function that improves domestic animal is plague virus such as current treatment fowl plague, swine fever and development animal husbandry one the very problem of significant and research.
The object of the present invention is to provide a kind of antiviral veterinary medicine injection and preparation method thereof, utilize the present invention in cell, to synthesize antiviral substance and to suppress virus by rapid excitating organism, and the immune function of body is improved rapidly.
The object of the present invention is achieved like this: it is mainly by Radix Ginseng, Ganoderma, Radix Isatidis, Tremella, the Radix Astragali, through pulverizing, soak, decoct, filter, get filtrate etc., form antiviral veterinary medicine injection of the present invention, it is characterized in that the percentage by weight of raw material is:
Radix Ginseng: 10-30% Ganoderma: 10-20%
Radix Isatidis: 20-60% Tremella: 5-15%
The Radix Astragali: 15-40%
The preparation method of antiviral veterinary medicine injection of the present invention is:
1. be purchased the screening and the above-mentioned clean medical material of weighing, processing and fabricating under the dry airy environment of sanitation and hygiene arranged possessing,
2. pulverize
With above-mentioned medical material mixing, be processed into coarse powder,
3. soak
Is 1.5: 1 with the drinking water that meets state health standards by the weight ratio of water and medicine, mix, at room temperature soaked 2 hours,
4. decoct
After the immersion, decoct twice, be fried boiling 30 minutes at every turn,
The weight that adds for the first time water is 5-7 times of former weighing medical material weight, after being fried boiling 30 minutes, filters with the plate filter, gets filtrate, and is standby,
The weight that adds for the second time water is 4-6 times of former weighing medical material weight, after being fried boiling 30 minutes, filters with the plate filter, gets filtrate, and is standby,
5. concentrate
Above-mentioned twice standby filtrate merging decocted, filter, filtrate decompression is concentrated into 1/3 of crude drug in whole weight, and indoor natural cooling is standby
6. precipitate with ethanol is 3 times
With add ethanol 3 times, (contain alcohol amount be respectively 55%, 75%, 83%) of above-mentioned reserve liquid at every turn, left standstill 24 hours at every turn, precipitation, filter, reclaim ethanol each 3 times.
For the first time, it is industrial alcohol 95% or more that above-mentioned reserve liquid is added the alcohol amount of containing, and making it contain that alcohol measures is 55%, left standstill again 24 hours, post precipitation, filtration, filter method is to use the bottle,suction sucking filtration, after reclaiming ethanol, add the injection water, the weight ratio of water for injection and crude drug in whole is 1: 1, indoor natural cooling, after being cooled to room temperature, cold preservation between 4-8 ℃ again, cold preservation 48 hours, standby
For the second time, the precipitate after filtering for the first time added to contain the alcohol amount be industrial alcohol 95% or more, making it contain that alcohol measures is 75%, left standstill again 24 hours, post precipitation, filtration, filter method is to use the bottle,suction sucking filtration, after reclaiming ethanol, add the injection water, the weight ratio of water for injection and crude drug in whole is 1: 1, indoor natural cooling, after being cooled to room temperature, cold preservation between 4-8 ℃ again, cold preservation 48 hours, standby
For the third time, the precipitate after filtering for the second time added to contain the alcohol amount be industrial alcohol 95% or more, making it contain that alcohol measures is 83%, left standstill again 24 hours, post precipitation, filtration, filter method is to use the bottle,suction sucking filtration, after reclaiming ethanol, add the injection water, the weight ratio of water for injection and crude drug in whole is 1: 1, indoor natural cooling, after being cooled to room temperature, cold preservation between 4-8 ℃ again, cold preservation 48 hours, standby
7. adsorption bleaching
Above-mentioned three times reserve liquid is added 0.3% active carbon stirring, be heated to 80 ℃, be 30 minutes heat time heating time, behind the adsorption bleaching, refilter,
8. allocate fine straining
In filtrate, transfer pH value, transfer to 5.5-7.0, add the injection water and contain crude drug in whole to every milliliter
1 gram is filtered to clarification with No. 4 filter sticks, promptly reaches till the printing opacity, filter with filter stick formula filter bulb,
9. fill
With filling machine with above-mentioned liquid medicine filling in the ampere bottle, the ampere bottle was placed in 100 ℃ the sterilization cabinet sterilization 30 minutes, promptly get antiviral veterinary medicine injection of the present invention.Have another name called the broad-spectrum high efficacy novel anti-virus
But veterinary drug-pestilence health injection.
The present invention compared with prior art, it is safe and reliable, nontoxic, harmless, noresidue, technology is simple, and is with low cost, practical, real is the ideal medicament of viral diseases such as current treatment fowl plague, swine fever, canine distemper, cat distemper.
Below in conjunction with embodiment the present invention is described, the scheme of embodiment described here, do not limit the present invention, one of skill in the art can make improvements and change according to spirit of the present invention, described these improvement and variation all should be considered as within the scope of the invention, and scope and spirit of the present invention are limited by claim.
Embodiment
1. be purchased screening and weigh clean medical material Radix Ginseng 20 grams, Ganoderma 15 grams, Radix Isatidis 40 grams, Tremella 10 grams
, the Radix Astragali 15 gram, amount to 100 grams processing and fabricating under the dry airy environment of sanitation and hygiene,
2. pulverize
With above-mentioned medical material mixing, be processed into coarse powder,
3. soak
Mix with the clean medical material of above-mentioned 100 grams with 150 gram tap waters, at room temperature soaked 2 hours,
4. decoct
After the immersion, decoct twice, be fried boiling 30 minutes at every turn,
Add for the first time water 600 grams, after being fried boiling 30 minutes, filter, get filtrate with the plate filter, standby,
Add for the second time water 500 grams, after being fried boiling 30 minutes, filter, get filtrate with the plate filter, standby,
5. concentrate
Above-mentioned twice standby filtrate merging is decocted, filters, filtrate decompression concentrate 33 gram concentrated solutions, indoor natural cooling, standby
6. precipitate with ethanol is 3 times
With add ethanol 3 times, (contain alcohol amount be respectively 55%, 75%, 83%) of above-mentioned reserve liquid at every turn, left standstill 24 hours at every turn, precipitation, filter, reclaim ethanol each 3 times.
For the first time, it is industrial alcohol 95% or more that above-mentioned reserve liquid is added the alcohol amount of containing, and making it contain that alcohol measures is 55%, left standstill again 24 hours, post precipitation, filtration, filter method is to use the bottle,suction sucking filtration, after reclaiming ethanol, add injection water 100 gram, indoor natural cooling, be cooled to room temperature after, cold preservation between 4-8 ℃ again, cold preservation 48 hours, standby
For the second time, the precipitate after filtering for the first time added to contain the alcohol amount be industrial alcohol 95% or more, making it contain that alcohol measures is 75%, left standstill again 24 hours, post precipitation, filtration, filter method is to use the bottle,suction sucking filtration, after reclaiming ethanol, add injection water 100 gram, indoor natural cooling, be cooled to room temperature after, cold preservation between 4-8 ℃ again, cold preservation 48 hours, standby
For the third time, the precipitate after filtering for the second time added to contain the alcohol amount be industrial alcohol 95% or more, making it contain that alcohol measures is 83%, left standstill again 24 hours, post precipitation, filtration, filter method is to use the bottle,suction sucking filtration, after reclaiming ethanol, add injection water 100 gram, indoor natural cooling, be cooled to room temperature after, cold preservation between 4-8 ℃ again, cold preservation 48 hours, standby
7. adsorption bleaching
Above-mentioned three times reserve liquid is added 0.3% active carbon stirring, be heated to 80 ℃, be 30 minutes heat time heating time, behind the adsorption bleaching, refilter,
8. allocate fine straining
In filtrate, transfer pH value, transfer to 5.5-7.0, add the injection water and contain crude drug in whole 1 gram to every milliliter, be filtered to clarification, promptly reach till the printing opacity with No. 4 filter sticks, with the filtration of filter stick formula filter bulb,
9. fill
With filling machine with above-mentioned liquid medicine filling in the ampere bottle, the ampere bottle was placed in 100 ℃ the sterilization cabinet sterilization 30 minutes, promptly get antiviral veterinary medicine injection of the present invention.But have another name called broad-spectrum high efficacy antiviral veterinary medicine-pestilence health injection.
Claims (2)
1, a kind of antiviral veterinary medicine injection, it is mainly by Radix Ginseng, Ganoderma, Radix Isatidis, Tremella, the Radix Astragali, forms through pulverizing, soak, decoct, filter, get filtrate etc., it is characterized in that the percentage by weight of raw material is:
Radix Ginseng: 10-30% Ganoderma: 10-20%
Radix Isatidis: 20-60% Tremella: 5-15%
The Radix Astragali: 15-40%.
2, the preparation method of the described antiviral veterinary medicine injection of a kind of claim 1, its feature also is:
1. be purchased the screening and the above-mentioned clean medical material of weighing, processing and fabricating under the dry airy environment of sanitation and hygiene arranged possessing,
2. pulverize
With above-mentioned medical material mixing, be processed into coarse powder,
3. soak
Is 1.5: 1 with the drinking water that meets state health standards by the weight ratio of water and medicine, mix, at room temperature soaked 2 hours,
4. decoct
After the immersion, decoct twice, be fried boiling 30 minutes at every turn,
The weight that adds for the first time water is 5-7 times of former weighing medical material weight, after being fried boiling 30 minutes, filters with the plate filter, gets filtrate, and is standby,
5. concentrate
Above-mentioned twice standby filtrate merging decocted, filter, filtrate decompression is concentrated into 1/3 of crude drug in whole weight, and indoor natural cooling is standby,
6. precipitate with ethanol is 3 times
Above-mentioned reserve liquid is added ethanol 3 times, contain the alcohol amount at every turn and be respectively 55%, 75%, 83%, left standstill 24 hours at every turn, precipitation, filtration, recovery ethanol,
For the first time, it is industrial alcohol 95% or more that above-mentioned reserve liquid is added the alcohol amount of containing, and making it contain that alcohol measures is 55%, left standstill again 24 hours, post precipitation, filtration, filter method is to use the bottle,suction sucking filtration, after reclaiming ethanol, add the injection water, the weight ratio of water for injection and crude drug in whole is 1: 1, indoor natural cooling, after being cooled to room temperature, cold preservation between 4-8 ℃ again, cold preservation 48 hours, standby
For the second time, the precipitate after filtering for the first time added to contain the alcohol amount be industrial alcohol 95% or more, making it contain that alcohol measures is 75%, left standstill again 24 hours, post precipitation, filtration, filter method is to use the bottle,suction sucking filtration, after reclaiming ethanol, add the injection water, the weight ratio of water for injection and crude drug in whole is 1: 1, indoor natural cooling, after being cooled to room temperature, cold preservation between 4-8 ℃ again, cold preservation 48 hours, standby
For the third time, the precipitate after filtering for the second time added to contain the alcohol amount be industrial alcohol 95% or more, making it contain that alcohol measures is 83%, left standstill again 24 hours, post precipitation, filtration, filter method is to use the bottle,suction sucking filtration, after reclaiming ethanol, add the injection water, the weight ratio of water for injection and crude drug in whole is 1: 1, indoor natural cooling, after being cooled to room temperature, cold preservation between 4-8 ℃ again, cold preservation 48 hours, standby
7. adsorption bleaching
The active carbon of above-mentioned three times reserve liquid 0.3% is stirred, be heated to 80 ℃, be 30 minutes heat time heating time, behind the adsorption bleaching, refilter,
8. allocate fine straining
In filtrate, transfer pH value, transfer to 5.5-7.0, add the injection water and contain crude drug in whole 1 gram to every milliliter, be filtered to clarification, promptly reach till the printing opacity with No. 4 filter sticks, with the filtration of filter stick formula filter bulb,
9. fill
With filling machine with above-mentioned liquid medicine filling in the ampere bottle, the ampere bottle was placed in 100 ℃ the sterilization cabinet sterilization 30 minutes, promptly get antiviral veterinary medicine injection of the present invention.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN97116309A CN1060951C (en) | 1997-08-08 | 1997-08-08 | Antiviral veterinary injection and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN97116309A CN1060951C (en) | 1997-08-08 | 1997-08-08 | Antiviral veterinary injection and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1207911A CN1207911A (en) | 1999-02-17 |
| CN1060951C true CN1060951C (en) | 2001-01-24 |
Family
ID=5173754
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN97116309A Expired - Fee Related CN1060951C (en) | 1997-08-08 | 1997-08-08 | Antiviral veterinary injection and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1060951C (en) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2455151A (en) * | 2007-11-27 | 2009-06-03 | Phynova Ltd | An Astragalus extract as an antiviral for several genera of the Flaviviridae family |
| CN104288554A (en) * | 2014-09-30 | 2015-01-21 | 天津瑞贝特科技发展有限公司 | Traditional Chinese veterinary medicine injection for treating infectious bursal disease and preparation method thereof |
| CN104984014A (en) * | 2015-08-04 | 2015-10-21 | 山东新希望六和集团有限公司 | Medicine composition for treating feline panleukopenia and preparation method thereof |
| CN115381862A (en) * | 2022-09-04 | 2022-11-25 | 中国农业科学院蜜蜂研究所 | Preparation for inhibiting crawl bee syndrome caused by bee virus and preparation method and application thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1125618A (en) * | 1995-09-14 | 1996-07-03 | 吉林省生物制品厂生物药品研究所 | Oral liquid for treatment of chicken's Newcastle disease and Fabricius bursa disease |
-
1997
- 1997-08-08 CN CN97116309A patent/CN1060951C/en not_active Expired - Fee Related
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1125618A (en) * | 1995-09-14 | 1996-07-03 | 吉林省生物制品厂生物药品研究所 | Oral liquid for treatment of chicken's Newcastle disease and Fabricius bursa disease |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1207911A (en) | 1999-02-17 |
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