CN106084972A - A kind of interior wall mildew-proof water-resistant powder of lacquer putty for use on - Google Patents
A kind of interior wall mildew-proof water-resistant powder of lacquer putty for use on Download PDFInfo
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- CN106084972A CN106084972A CN201610726337.XA CN201610726337A CN106084972A CN 106084972 A CN106084972 A CN 106084972A CN 201610726337 A CN201610726337 A CN 201610726337A CN 106084972 A CN106084972 A CN 106084972A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/34—Filling pastes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Plant Pathology (AREA)
- Adhesives Or Adhesive Processes (AREA)
- Paints Or Removers (AREA)
Abstract
The invention provides a kind of interior wall mildew-proof water-resistant powder of lacquer putty for use on and preparation method thereof.Preparation method is as follows: (1), by dicalcium powder, light calcium carbonate powder, ash calcium, Pulvis Talci, flyash, silicic acid hargil, mix homogeneously, is ground, crossed 300 400 mesh sieves;(2) by silica flour, through 2,000 3500 revs/min of speed lappings 20 35 minutes, dry and pulverize, cross 80 120 mesh sieves;(3) material step (1) and step (2) obtained adds water making beating and makes serosity;(4) add hydroxypropyl methyl cellulose, polyvinyl alcohol cold water instant dissolving glue powder, solid-state methane-siliconic acid, Cortex cinnamomi japonici (Ramulus Cinnamomi) 100% ethanol extraction, the Cortex Eucommiae 100% ethanol extraction, stir 60 120 minutes, filtering drying, pulverize finely ground, cross 300 400 mesh sieves.This interior wall mildew-proof water-resistant powder of lacquer putty for use on, has good resistance to water, is chronically under steam, and antimildew and antibacterial persistency is good.
Description
Technical field
The present invention relates to building material field, be specifically related to a kind of interior wall mildew-proof water-resistant powder of lacquer putty for use on.
Background technology
Before putty is paint class construction, construction surface is carried out a kind of surface packing material of pretreatment, it is therefore intended that fill and execute
The hole in work face and the curve deviation of rectification construction surface, for obtaining uniformly, smooth lacquer painting is laid a solid foundation, therefore should be possessed good
Adhesion strength and resistance to water, with ensure water vapour in atmosphere long-term corrode under not have hollowing, peeling, cracking etc. existing
As and remain able to combine closely with matrix, play good decoration and protective effect.Long-term due to building bathroom interior wall etc.
Being under water vapour, protected from environmental bigger, architectural engineering is for the resistance to water of inner wall putty, antimildew and antibacterial, cold-hot
Variations in temperature, adhesion strength and splitting resistance etc. are had higher requirement.Presently commercially available powder of lacquer putty for use on, poor adhesive force, no
Water-fast, service life is short.Often there is peeling, falls the phenomenon such as slag, shedding, more seriously in the house using this material to fit up
At above-mentioned powder of lacquer putty for use on after the time of one, metope mouldy can have mildew, has a strong impact on the attractive in appearance of indoor, and have even can release
Put harmful substance, be the polluter of indoor environment, be directly detrimental to health.
Summary of the invention
Solve the technical problem that: it is an object of the invention to provide a kind of interior wall mildew-proof water-resistant powder of lacquer putty for use on, have very well
Resistance to water, be chronically under steam, antimildew and antibacterial persistency is good.
Technical scheme: a kind of interior wall mildew-proof water-resistant powder of lacquer putty for use on, is prepared from by weight by following component: dicalcium powder
60-80 part, light calcium carbonate powder 15-25 part, ash calcium 40-45 part, Pulvis Talci 15-25 part, flyash 10-20 part, silicic acid hargil 10-15
Part, silica flour 15-25 part, hydroxypropyl methyl cellulose 15-24 part, polyvinyl alcohol cold water instant dissolving glue powder 6-12 part, solid-state methyl
Silicic acid 3.5-7.5 part, Cortex cinnamomi japonici (Ramulus Cinnamomi) 100% ethanol extraction 2.5-6.5 part, the Cortex Eucommiae 100% ethanol extraction 2.5-6.5 part, water 180-
220 parts.
It is further preferred that described a kind of interior wall mildew-proof water-resistant powder of lacquer putty for use on, following component prepare by weight and
Become: dicalcium powder 65-75 part, light calcium carbonate powder 19-23 part, ash calcium 41-43 part, Pulvis Talci 18-22 part, flyash 12-18 part, silicic acid are white
Soil 11-14 part, silica flour 18-22 part, hydroxypropyl methyl cellulose 18-22 part, polyvinyl alcohol cold water instant dissolving glue powder 8-10 part, solid
State methane-siliconic acid 4.5-6.5 part, Cortex cinnamomi japonici (Ramulus Cinnamomi) 100% ethanol extraction 3.5-5.5 part, the Cortex Eucommiae 100% ethanol extraction 3.5-5.5 part,
Water 190-210 part.
The preparation method of above-mentioned interior wall mildew-proof water-resistant powder of lacquer putty for use on comprises the following steps:
(1) by dicalcium powder, light calcium carbonate powder, ash calcium, Pulvis Talci, flyash, silicic acid hargil, mix homogeneously, grind, cross 200-400 mesh
Sieve;
(2) by silica flour, through 2000-3500 rev/min of speed lapping 20-35 minute, dry and pulverize, cross 80-120 mesh sieve;
(3) material step (1) and step (2) obtained adds water making beating and makes serosity;
(4) addition hydroxypropyl methyl cellulose, polyvinyl alcohol cold water instant dissolving glue powder, solid-state methane-siliconic acid, Cortex cinnamomi japonici (Ramulus Cinnamomi) 100% ethanol carry
Take thing, the Cortex Eucommiae 100% ethanol extraction, stir 60-120 minute, filtering drying, pulverize finely ground, cross 300-400 mesh sieve.
Further, the preparation method of described a kind of interior wall mildew-proof water-resistant powder of lacquer putty for use on, mistake in described step (1)
200-300 mesh sieve.
Further, the preparation method of described a kind of interior wall mildew-proof water-resistant powder of lacquer putty for use on, described step (2) medium speed
For 2500-3500 rev/min, milling time is 25-30 minute, crosses 100 mesh sieves.
Further, the preparation method of described a kind of interior wall mildew-proof water-resistant powder of lacquer putty for use on, serosity in described step (3)
Concentration be 50%.
Further, the preparation method of described a kind of interior wall mildew-proof water-resistant powder of lacquer putty for use on, stirring in described step (4)
Time is 80-100 minute, crosses 300-350 mesh sieve.
Beneficial effect: interior wall mildew-proof water-resistant powder of lacquer putty for use on of the present invention has resistance to water and adhesion strength, the water proofing property of excellence
For 0.6g/10min, the highest adhesion strength reaches 2.0MPa, and after freeze-thaw cycle five times, adhesion strength is 1.1MPa, simultaneously this
Interior wall mildew-proof water-resistant powder of lacquer putty for use on also has good biocidal property, and it has reached 100% to colibacillary inhibition.
Detailed description of the invention
Embodiment 1
A kind of interior wall mildew-proof water-resistant powder of lacquer putty for use on, is prepared from weight portion by following component: dicalcium powder 80 parts, light calcium carbonate powder 25
Part, ash calcium 40 parts, Pulvis Talci 15 parts, 10 parts of flyash, silicic acid hargil 10 parts, silica flour 15 parts, hydroxypropyl methyl cellulose 15
Part, polyvinyl alcohol cold water instant dissolving glue powder 6 parts, solid-state methane-siliconic acid 3.5 parts, Cortex cinnamomi japonici (Ramulus Cinnamomi) 100% ethanol extraction 6.5 parts, the Cortex Eucommiae 100%
Ethanol extraction 2.5 parts, 220 parts of water.
The preparation method of above-mentioned interior wall mildew-proof water-resistant powder of lacquer putty for use on is: (1) by dicalcium powder, light calcium carbonate powder, ash calcium, Pulvis Talci,
Flyash, silicic acid hargil, mix homogeneously, grinds, crosses 200 mesh sieves;(2) by silica flour, through 2000 revs/min of speed lappings 35 points
Clock, dries and pulverizes, and crosses 120 mesh sieves;(3) material step (1) and step (2) obtained adds water making beating and makes serosity;(4) add
Enter hydroxypropyl methyl cellulose, polyvinyl alcohol cold water instant dissolving glue powder, solid-state methane-siliconic acid, Cortex cinnamomi japonici (Ramulus Cinnamomi) 100% ethanol extraction, the Cortex Eucommiae
100% ethanol extraction, stirs 60 minutes, filtering drying, pulverizes finely ground, crosses 300 mesh sieves.
Embodiment 2
A kind of interior wall mildew-proof water-resistant powder of lacquer putty for use on, is prepared from weight portion by following component: dicalcium powder 60 parts, light calcium carbonate powder 15
Part, ash Ca45 part, Pulvis Talci 25 parts, 20 parts of flyash, silicic acid hargil 15 parts, silica flour 25 parts, hydroxypropyl methyl cellulose 24
Part, polyvinyl alcohol cold water instant dissolving glue powder 12 parts, solid-state methane-siliconic acid 7.5 parts, Cortex cinnamomi japonici (Ramulus Cinnamomi) 100% ethanol extraction 2.5 parts, the Cortex Eucommiae
100% ethanol extraction 6.5 parts, 180 parts of water.
The preparation method of above-mentioned interior wall mildew-proof water-resistant powder of lacquer putty for use on is: (1) by dicalcium powder, light calcium carbonate powder, ash calcium, Pulvis Talci,
Flyash, silicic acid hargil, mix homogeneously, grinds, crosses 400 mesh sieves;(2) by silica flour, through 3500 revs/min of speed lappings 20 points
Clock, dries and pulverizes, and crosses 80 mesh sieves;(3) material step (1) and step (2) obtained adds water making beating and makes serosity;(4) add
Enter hydroxypropyl methyl cellulose, polyvinyl alcohol cold water instant dissolving glue powder, solid-state methane-siliconic acid, Cortex cinnamomi japonici (Ramulus Cinnamomi) 100% ethanol extraction, the Cortex Eucommiae
100% ethanol extraction, stirs 120 minutes, filtering drying, pulverizes finely ground, crosses 400 mesh sieves.
Embodiment 3
A kind of interior wall mildew-proof water-resistant powder of lacquer putty for use on, is prepared from weight portion by following component: dicalcium powder 65 parts, light calcium carbonate powder 19
Part, ash calcium 41 parts, Pulvis Talci 22 parts, 12 parts of flyash, silicic acid hargil 11 parts, silica flour 22 parts, hydroxypropyl methyl cellulose 18
Part, polyvinyl alcohol cold water instant dissolving glue powder 10 parts, solid-state methane-siliconic acid 4.5 parts, Cortex cinnamomi japonici (Ramulus Cinnamomi) 100% ethanol extraction 5.5 parts, the Cortex Eucommiae
100% ethanol extraction 3.5 parts, 210 parts of water.
The preparation method of above-mentioned interior wall mildew-proof water-resistant powder of lacquer putty for use on is: (1) by dicalcium powder, light calcium carbonate powder, ash calcium, Pulvis Talci,
Flyash, silicic acid hargil, mix homogeneously, grinds, crosses 200 mesh sieves;(2) by silica flour, through 2500 revs/min of speed lappings 25 points
Clock, dries and pulverizes, and crosses 100 mesh sieves;(3) material step (1) and step (2) obtained adds water making beating and makes serosity;(4) add
Enter hydroxypropyl methyl cellulose, polyvinyl alcohol cold water instant dissolving glue powder, solid-state methane-siliconic acid, Cortex cinnamomi japonici (Ramulus Cinnamomi) 100% ethanol extraction, the Cortex Eucommiae
100% ethanol extraction, stirs 80 minutes, filtering drying, pulverizes finely ground, crosses 300 mesh sieves.
Embodiment 4
A kind of interior wall mildew-proof water-resistant powder of lacquer putty for use on, is prepared from weight portion by following component: dicalcium powder 75 parts, light calcium carbonate powder 23
Part, ash calcium 43 parts, Pulvis Talci 18 parts, 18 parts of flyash, silicic acid hargil 14 parts, silica flour 18 parts, hydroxypropyl methyl cellulose 22
Part, polyvinyl alcohol cold water instant dissolving glue powder 8 parts, solid-state methane-siliconic acid 6.5 parts, Cortex cinnamomi japonici (Ramulus Cinnamomi) 100% ethanol extraction 3.5 parts, the Cortex Eucommiae 100%
Ethanol extraction 5.5 parts, 190 parts of water.
The preparation method of above-mentioned interior wall mildew-proof water-resistant powder of lacquer putty for use on is: (1) by dicalcium powder, light calcium carbonate powder, ash calcium, Pulvis Talci,
Flyash, silicic acid hargil, mix homogeneously, grinds, crosses 300 mesh sieves;(2) by silica flour, through 3500 revs/min of speed lappings 30 points
Clock, dries and pulverizes, and crosses 100 mesh sieves;(3) material step (1) and step (2) obtained adds water making beating and makes serosity;(4) add
Enter hydroxypropyl methyl cellulose, polyvinyl alcohol cold water instant dissolving glue powder, solid-state methane-siliconic acid, Cortex cinnamomi japonici (Ramulus Cinnamomi) 100% ethanol extraction, the Cortex Eucommiae
100% ethanol extraction, stirs 100 minutes, filtering drying, pulverizes finely ground, crosses 350 mesh sieves.
Embodiment 5
A kind of interior wall mildew-proof water-resistant powder of lacquer putty for use on, is prepared from weight portion by following component: dicalcium powder 70 parts, light calcium carbonate powder 21
Part, ash calcium 42 parts, Pulvis Talci 20 parts, 15 parts of flyash, silicic acid hargil 13 parts, silica flour 20 parts, hydroxypropyl methyl cellulose 20
Part, polyvinyl alcohol cold water instant dissolving glue powder 9 parts, solid-state methane-siliconic acid 5.5 parts, Cortex cinnamomi japonici (Ramulus Cinnamomi) 100% ethanol extraction 4.5 parts, the Cortex Eucommiae 100%
Ethanol extraction 4.5 parts, 200 parts of water.
The preparation method of above-mentioned interior wall mildew-proof water-resistant powder of lacquer putty for use on is: (1) by dicalcium powder, light calcium carbonate powder, ash calcium, Pulvis Talci,
Flyash, silicic acid hargil, mix homogeneously, grinds, crosses 200 mesh sieves;(2) by silica flour, through 3000 revs/min of speed lappings 28 points
Clock, dries and pulverizes, and crosses 100 mesh sieves;(3) material step (1) and step (2) obtained adds water making beating and makes serosity;(4) add
Enter hydroxypropyl methyl cellulose, polyvinyl alcohol cold water instant dissolving glue powder, solid-state methane-siliconic acid, Cortex cinnamomi japonici (Ramulus Cinnamomi) 100% ethanol extraction, the Cortex Eucommiae
100% ethanol extraction, stirs 90 minutes, filtering drying, pulverizes finely ground, crosses 325 mesh sieves.
Comparative example 1
A kind of interior wall mildew-proof water-resistant powder of lacquer putty for use on, is prepared from weight portion by following component: dicalcium powder 80 parts, light calcium carbonate powder 25
Part, ash calcium 40 parts, silica flour 15 parts, hydroxypropyl methyl cellulose 15 parts, polyvinyl alcohol cold water instant dissolving glue powder 6 parts, solid-state methyl
Silicic acid 3.5 parts, Cortex cinnamomi japonici (Ramulus Cinnamomi) 100% ethanol extraction 6.5 parts, the Cortex Eucommiae 100% ethanol extraction 2.5 parts, 220 parts of water.
The preparation method of above-mentioned interior wall mildew-proof water-resistant powder of lacquer putty for use on is: (1) by dicalcium powder, light calcium carbonate powder, ash calcium, Pulvis Talci,
Mix homogeneously, grinds, and crosses 200 mesh sieves;(2) by silica flour, through 2000 revs/min of speed lappings 35 minutes, dry and pulverize, mistake
120 mesh sieves;(3) material step (1) and step (2) obtained adds water making beating and makes serosity;(4) hydroxypropyl methyl is added fine
Dimension element, polyvinyl alcohol cold water instant dissolving glue powder, solid-state methane-siliconic acid, Cortex cinnamomi japonici (Ramulus Cinnamomi) 100% ethanol extraction, the Cortex Eucommiae 100% ethanol extraction,
Stir 60 minutes, filtering drying, pulverize finely ground, cross 300 mesh sieves.
Comparative example 2
A kind of interior wall mildew-proof water-resistant powder of lacquer putty for use on, is prepared from weight portion by following component: dicalcium powder 60 parts, light calcium carbonate powder 15
Part, ash Ca45 part, Pulvis Talci 25 parts, 20 parts of flyash, silicic acid hargil 15 parts, silica flour 25 parts, hydroxypropyl methyl cellulose 24
Part, polyvinyl alcohol cold water instant dissolving glue powder 12 parts, solid-state methane-siliconic acid 7.5 parts, 180 parts of water.
The preparation method of above-mentioned interior wall mildew-proof water-resistant powder of lacquer putty for use on is: (1) by dicalcium powder, light calcium carbonate powder, ash calcium, Pulvis Talci,
Flyash, silicic acid hargil, mix homogeneously, grinds, crosses 400 mesh sieves;(2) by silica flour, through 3500 revs/min of speed lappings 20 points
Clock, dries and pulverizes, and crosses 80 mesh sieves;(3) material step (1) and step (2) obtained adds water making beating and makes serosity;(4) add
Enter hydroxypropyl methyl cellulose, polyvinyl alcohol cold water instant dissolving glue powder, solid-state methane-siliconic acid, stir 120 minutes, filtering drying, powder
Broken finely ground, cross 400 mesh sieves.
The property indices of material of the present invention see table, it may be seen that this interior wall mildew-proof water-resistant powder of lacquer putty for use on has
Excellent resistance to water and adhesion strength, water proofing property is 0.6g/10min, and the highest adhesion strength reaches 2.0MPa, freeze-thaw cycle five
After secondary, adhesion strength is 1.1MPa, and this interior wall mildew-proof water-resistant powder of lacquer putty for use on also has good biocidal property simultaneously, and it is to large intestine bar
The inhibition of bacterium has reached 100%.
The table 1 interior wall property indices of mildew-proof water-resistant powder of lacquer putty for use on
Note: this experiment is escherichia coli with antibacterial.
Claims (7)
1. an interior wall mildew-proof water-resistant powder of lacquer putty for use on, it is characterised in that be prepared from by weight by following component: dicalcium powder
60-80 part, light calcium carbonate powder 15-25 part, ash calcium 40-45 part, Pulvis Talci 15-25 part, flyash 10-20 part, silicic acid hargil 10-15
Part, silica flour 15-25 part, hydroxypropyl methyl cellulose 15-24 part, polyvinyl alcohol cold water instant dissolving glue powder 6-12 part, solid-state methyl
Silicic acid 3.5-7.5 part, Cortex cinnamomi japonici (Ramulus Cinnamomi) 100% ethanol extraction 2.5-6.5 part, the Cortex Eucommiae 100% ethanol extraction 2.5-6.5 part, water 180-
220 parts.
A kind of interior wall mildew-proof water-resistant powder of lacquer putty for use on the most according to claim 1, it is characterised in that by following component by weight
Part is prepared from: dicalcium powder 65-75 part, light calcium carbonate powder 19-23 part, ash calcium 41-43 part, Pulvis Talci 18-22 part, flyash 12-18
Part, silicic acid hargil 11-14 part, silica flour 18-22 part, hydroxypropyl methyl cellulose 18-22 part, polyvinyl alcohol cold water instant dissolving glue powder
8-10 part, solid-state methane-siliconic acid 4.5-6.5 part, Cortex cinnamomi japonici (Ramulus Cinnamomi) 100% ethanol extraction 3.5-5.5 part, the Cortex Eucommiae 100% ethanol extraction
3.5-5.5 part, water 190-210 part.
3. an interior wall mildew-proof water-resistant powder of lacquer putty for use on, it is characterised in that: comprise the following steps:
(1) by dicalcium powder, light calcium carbonate powder, ash calcium, Pulvis Talci, flyash, silicic acid hargil, mix homogeneously, grind, cross 200-400 mesh
Sieve;
(2) by silica flour, through 2000-3500 rev/min of speed lapping 20-35 minute, dry and pulverize, cross 80-120 mesh sieve;
(3) material step (1) and step (2) obtained adds water making beating and makes serosity;
(4) addition hydroxypropyl methyl cellulose, polyvinyl alcohol cold water instant dissolving glue powder, solid-state methane-siliconic acid, Cortex cinnamomi japonici (Ramulus Cinnamomi) 100% ethanol carry
Take thing, the Cortex Eucommiae 100% ethanol extraction, stir 60-120 minute, filtering drying, pulverize finely ground, cross 300-400 mesh sieve.
A kind of interior wall mildew-proof water-resistant powder of lacquer putty for use on the most according to claim 3, it is characterised in that: mistake in described step (1)
200-300 mesh sieve.
A kind of interior wall mildew-proof water-resistant powder of lacquer putty for use on the most according to claim 3, it is characterised in that: described step (2) transfer
Speed is 2500-3500 rev/min, and milling time is 25-30 minute, crosses 100 mesh sieves.
A kind of interior wall mildew-proof water-resistant powder of lacquer putty for use on the most according to claim 3, it is characterised in that: slurry in described step (3)
The concentration of liquid is 50%.
A kind of interior wall mildew-proof water-resistant powder of lacquer putty for use on the most according to claim 3, it is characterised in that: described step is stirred in (4)
The time of mixing is 80-100 minute, crosses 300-350 mesh sieve.
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Cited By (3)
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CN109401413A (en) * | 2017-04-13 | 2019-03-01 | 刘义辉 | A kind of moisture-proof anti-crack mastic powder containing Chinese alpine rush component |
CN114213893A (en) * | 2021-12-31 | 2022-03-22 | 河南三棵树新材料科技有限公司 | Interior wall putty powder with water-resistant and mildew-proof functions and preparation method thereof |
CN115746611A (en) * | 2022-11-17 | 2023-03-07 | 江苏久诺新材科技股份有限公司 | Mildew-proof water-resistant putty for interior wall and preparation process thereof |
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Publication number | Priority date | Publication date | Assignee | Title |
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CN109401413A (en) * | 2017-04-13 | 2019-03-01 | 刘义辉 | A kind of moisture-proof anti-crack mastic powder containing Chinese alpine rush component |
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CN114213893A (en) * | 2021-12-31 | 2022-03-22 | 河南三棵树新材料科技有限公司 | Interior wall putty powder with water-resistant and mildew-proof functions and preparation method thereof |
CN115746611A (en) * | 2022-11-17 | 2023-03-07 | 江苏久诺新材科技股份有限公司 | Mildew-proof water-resistant putty for interior wall and preparation process thereof |
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