CN106084967B - Specimens of one's blood and preparation method thereof for ancient building material - Google Patents
Specimens of one's blood and preparation method thereof for ancient building material Download PDFInfo
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- CN106084967B CN106084967B CN201610622718.3A CN201610622718A CN106084967B CN 106084967 B CN106084967 B CN 106084967B CN 201610622718 A CN201610622718 A CN 201610622718A CN 106084967 B CN106084967 B CN 106084967B
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/34—Filling pastes
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Abstract
The present invention provides the specimenss of one's blood and preparation method thereof for ancient building material.Specimens of one's blood is by including that the raw material of following parts by weight is made: Swine plasma, lime water, active carbon, light calcium carbonate powder and hypocrellin.Preparation method: preparing each raw material, after active carbon and light calcium carbonate powder are ground load, is added in Swine plasma；Hypocrellin is added in lime water；The two is mixed again, stands, obtains specimens of one's blood.Obtained specimens of one's blood can play good Organic-inorganic composite effect with putty oil and brick dust, play excellent adhesive effect in the application for preparing grey oil loam.The pulling force for the grey oil loam being mixed to get using specimens of one's blood of the present invention is enhanced, it does not crack after smearing drying, it is easy to polish, also there is excellent waterproof and anticorrosion antibiotic property, repairing and filling especially suitable for ancient building material, in particular for ancient architecture timber, play the role of excellent filling timber, while waterproof and anticorrosion antibacterial.
Description
Technical field
The present invention relates to construction material specimens of one's blood technical fields, the more particularly, to specimens of one's blood of ancient building material and its preparation
Method.
Background technique
A kind of specimens of one's blood, coating made of domestic animal blood, there is adhesive effect, and there are also moisture-proof and insect prevention effects.Currently, traditional blood
The production method of material are as follows: soak diluter lime white with air hardening lime, after crossing wire gauze grate, it is poured into watery blood bucket on a small quantity
It is interior, slightly stir at any time, in one or two hour, watery blood changes, generate foam and go up, at meat jelly shape, i.e., specimens of one's blood hair at.Specimens of one's blood
Main application be that the material mixings such as itself and putty oil, brick dust are obtained into grey oil loam, for the repairing or filling of ancient architecture material,
In particular for the filling of ancient architecture timber, anti-corrosive properties are improved.Wherein, effect of the specimens of one's blood in grey oil loam is to play bonding to make
With.But existing specimens of one's blood ingredient is single, viscosity not enough, cannot play good adhesive effect, frequently can lead to smear drying
Grey oil loam cracking afterwards even falls off, and causes the repairing or filling failure of ancient building material.
Summary of the invention
In view of the above drawbacks of the prior art and problem, the object of the present invention is to provide for ancient building material specimens of one's blood and
Preparation method.Solve that existing specimens of one's blood ingredient is single, the inadequate technical problem of viscosity.
In order to achieve the above object, the invention provides the following technical scheme:
Specimens of one's blood for ancient building material of the invention, be made of the raw material for including following parts by weight: moisture content is low
In 50% 85-95 parts of Swine plasma, 8-15 parts of lime water, 12-18 parts of active carbon, 8-15 parts of light calcium carbonate powder and hypocrellin 1-3
Part.
Preferably, the specimens of one's blood is by including that the raw material of following parts by weight is made: moisture content is lower than 50% Swine plasma
90 parts, 10 parts of lime water, 15 parts of active carbon, 10 parts of light calcium carbonate powder and 2 parts of hypocrellin.
Further, in parts by weight, the raw material of the specimens of one's blood further includes 5-10 parts of aerogel powder.Preferably, it also wraps
Include 8 parts of aerogel powder.
Specifically, the aerogel powder uses silicon systems aerogel powder.
Preferably, the partial size of the active carbon is 1-10 μm, and the partial size of the light calcium carbonate powder is 200-800nm, the airsetting
The partial size at rubber powder end is 20-50 μm.
Further, the lime water is the ratio for being 1 ﹕ 8-10 according to the mass ratio of quick lime and water, by quick lime
It is added to the water what dissolution obtained.
Preferably, the lime water is the ratio for being 1 ﹕ 9 according to the mass ratio of quick lime and water, and water is added in quick lime
What middle dissolution obtained.
The present invention also provides the preparation methods of the specimens of one's blood for ancient building material, comprising the following steps:
Step 1: preparing the Swine plasma that moisture content is lower than 50%: pig blood being solidified, then filtering removal serum, obtains pig blood
Grumeleuse；Then it after pig blood grumeleuse being milled, then solidifies, refilters removal serum, so repeat to obtaining moisture content lower than 50%
Pig blood grumeleuse；Then pig blood grumeleuse is milled crushing, and crosses 200 meshes, obtain the Swine plasma that moisture content is lower than 50%；
Step 2: weighing Swine plasma of the moisture content lower than 50%, the life of step 1 according to each raw material dosage in above-mentioned specimens of one's blood
Limewash, active carbon, light calcium carbonate powder and hypocrellin；
Step 3: active carbon and light calcium carbonate powder are mixed, 30-50min is ground using planetary-type grinding machine, obtains load light calcium
Active carbon；The active carbon for loading light calcium is added in Swine plasma again, is mixed, 1.5-3 hours is stood, obtains pig blood pulp mixture；
Hypocrellin is added in lime water and is stirred and evenly mixed, lime water mixed solution is obtained；Then pig is added in lime water mixed solution
In plasma mixtures, stirs 40-60 minutes, obtain half paste specimens of one's blood, then stand 10-15 hours again, obtain specimens of one's blood.
Further, in step 2, when the raw material of the specimens of one's blood includes aerogel powder, in step 3, light calcium is loaded
Active carbon add in aerogel powder, using planetary-type grinding machine grind 30-50min, obtain composite load mixture；So
The composite load mixture is added in Swine plasma afterwards, mixes, obtains pig blood pulp mixture.
Further, in step 3, during the standing of half paste specimens of one's blood, half paste specimens of one's blood is placed on subnormal ambient
In.
Further, the pressure of the subnormal ambient is 0.05-0.08MPa.Preferably, 0.06MPa.
Specimens of one's blood for ancient building material of the invention, increases active carbon and light calcium carbonate powder, since specimens of one's blood needs in the application
It to be mixed with inorganic material brick dust, obtain the grey oil loam of inorganic-organic hybrid, therefore, the present invention increases suction in specimens of one's blood
The good light calcium carbonate powder of oiliness.But since light calcium carbonate powder stability is poor, Yi Chen, therefore, the present invention increase activity simultaneously in specimens of one's blood
Charcoal, on the activated carbon by easily heavy light calcium carbonate powder load, redisperse is into Swine plasma, good dispersion of the active carbon in Swine plasma,
To solve the dispersion of light calcium carbonate powder.The addition of hypocrellin improves the insect-proof fungicidal effect of specimens of one's blood.So that obtaining
Specimens of one's blood in the application for preparing grey oil loam, good Organic-inorganic composite effect can be played with putty oil and brick dust, is played excellent
Different adhesive effect.Aerogel powder is preferably increased in the present invention, it can the porous load as active carbon and light calcium carbonate powder
Body improves the dispersibility of active carbon and light calcium carbonate powder, can also play the role of enhancing specimens of one's blood bond properties.
The viscosity of specimens of one's blood for ancient building material of the invention is good, is obtained using the pulling force of its grey oil loam being mixed to get
To enhancing, do not crack after smearing drying, it is easy to polish, also there is excellent waterproof and anticorrosion insect prevention antibiotic property, especially suitable for ancient architecture
The repairing and filling of material are built, in particular for ancient architecture timber, plays the role of excellent filling timber, while waterproof and anticorrosion is anti-
Worm antibacterial.
Specific embodiment
Below in conjunction with the embodiment of the present invention, technical solution of the present invention is clearly and completely described, it is clear that
Described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based on the implementation in the present invention
Example, every other embodiment obtained by those of ordinary skill in the art without making creative efforts belong to
The scope of protection of the invention.
Embodiment 1
The specimens of one's blood for ancient building material of the embodiment of the present invention 1 is made of the raw material for including following parts by weight: containing
Swine plasma 90 part of the water rate lower than 50%, 10 parts of lime water, 15 parts of active carbon, 10 parts of light calcium carbonate powder and 2 parts of hypocrellin.It is described
The partial size of active carbon is 1-10 μm, and the partial size of the light calcium carbonate powder is 200-800nm.
Wherein, lime water is the ratio for being 1 ﹕ 9 according to the mass ratio of quick lime and water, and quick lime is added to the water dissolution
It obtains.
The preparation method of the specimens of one's blood for ancient building material of the present embodiment 1, comprising the following steps:
Step 1: preparing the Swine plasma that moisture content is lower than 50%: pig blood being solidified, then filtering removal serum, obtains pig blood
Grumeleuse；Then it after pig blood grumeleuse being milled, then solidifies, refilters removal serum, so repeat to obtaining moisture content lower than 50%
Pig blood grumeleuse；Then pig blood grumeleuse is milled crushing, and crosses 200 meshes, obtain the Swine plasma that moisture content is lower than 50%；
Step 2: weighing Swine plasma of the moisture content lower than 50%, the life of step 1 according to each raw material dosage in above-mentioned specimens of one's blood
Limewash, active carbon, light calcium carbonate powder and hypocrellin；
Step 3: active carbon and light calcium carbonate powder are mixed, 50min is ground using planetary-type grinding machine, obtains load light calcium
Active carbon；The active carbon for loading light calcium is added in Swine plasma again, is mixed, 2 hours is stood, obtains pig blood pulp mixture；Bamboo is red
Rhzomorph is added in lime water and stirs and evenly mixs, and obtains lime water mixed solution；Then lime water mixed solution addition Swine plasma is mixed
It closes in object, stirs 50 minutes, obtain half paste specimens of one's blood, half paste specimens of one's blood is then placed on the negative pressure ring that pressure is 0.06MPa
12 hours are stood in border, obtains specimens of one's blood.
Embodiment 2
The specimens of one's blood for ancient building material of the embodiment of the present invention 2 is made of the raw material for including following parts by weight: containing
Swine plasma 85 part of the water rate lower than 50%, 8 parts of lime water, 12 parts of active carbon, 8 parts of light calcium carbonate powder and 1 part of hypocrellin.The work
Property charcoal partial size be 1-10 μm, the partial size of the light calcium carbonate powder is 200-800nm.
Wherein, lime water is the ratio for being 1 ﹕ 8 according to the mass ratio of quick lime and water, and quick lime is added to the water dissolution
It obtains.
That the preparation method is the same as that of Example 1 is identical for the specimens of one's blood for ancient building material of the present embodiment 2.
Embodiment 3
The specimens of one's blood for ancient building material of the embodiment of the present invention 2 is made of the raw material for including following parts by weight: containing
Swine plasma 95 part of the water rate lower than 50%, 15 parts of lime water, 18 parts of active carbon, 15 parts of light calcium carbonate powder and 3 parts of hypocrellin.It is described
The partial size of active carbon is 1-10 μm, and the partial size of the light calcium carbonate powder is 200-800nm.
Wherein, lime water is the ratio for being 1 ﹕ 10 according to the mass ratio of quick lime and water, quick lime is added to the water molten
What solution obtained.
That the preparation method is the same as that of Example 1 is identical for the specimens of one's blood for ancient building material of the present embodiment 3.
Embodiment 4
The present embodiment 4 is increased in the raw material of specimens of one's blood on the basis of embodiment 1, embodiment 2 or embodiment 3
Aerogel powder, the parts by weight of aerogel powder are 5-10 parts, preferably 8 parts.
Specifically, the present embodiment 4 provides the specimens of one's blood for being preferably used in ancient building material, is by including following parts by weight
Raw material be made: moisture content lower than 50% 90 parts of Swine plasma, 10 parts of lime water, 15 parts of active carbon, 10 parts of light calcium carbonate powder, airsetting
8 parts and 2 parts of hypocrellin of rubber powder end.The partial size of the active carbon is 1-10 μm, and the partial size of the light calcium carbonate powder is 200-800nm,
The partial size of the aerogel powder is 20-50 μm.
The aerogel powder uses silicon systems aerogel powder.
The preparation method of the specimens of one's blood for ancient building material of the present embodiment 4 unlike the first embodiment, the behaviour of step 3
Make, specifically, in step 3, the active carbon for loading light calcium is added in aerogel powder, is ground using planetary-type grinding machine
30-50min is ground, composite load mixture is obtained；Then the composite load mixture is added in Swine plasma, mixes, obtains pig blood
Pulp mixture.Other steps and parameter are same as Example 1.
The above description is merely a specific embodiment, but scope of protection of the present invention is not limited thereto, any
Those familiar with the art in the technical scope disclosed by the present invention, can easily think of the change or the replacement, and should all contain
Lid is within protection scope of the present invention.Therefore, the protection scope of the present invention shall be subject to the protection scope of the claims.
Claims (10)
1. being used for the specimens of one's blood of ancient building material, which is characterized in that the raw material including following parts by weight: moisture content is lower than 50%
85-95 parts of Swine plasma, 8-15 parts of lime water, 12-18 parts of active carbon, 8-15 parts of light calcium carbonate powder and 1-3 parts of hypocrellin,
The active carbon and light calcium carbonate powder mixing, grind 30-50min using planetary-type grinding machine, obtain the active carbon of load light calcium.
2. the specimens of one's blood according to claim 1 for ancient building material, which is characterized in that the specimens of one's blood includes following weight
The raw material of number: moisture content is lower than 50% 90 parts of Swine plasma, 10 parts of lime water, 15 parts of active carbon, 10 parts of light calcium carbonate powder and bamboo
2 parts of red rhzomorph.
3. the specimens of one's blood according to claim 1 or 2 for ancient building material, which is characterized in that in parts by weight, described
The raw material of specimens of one's blood further includes 5-10 parts of aerogel powder.
4. the specimens of one's blood according to claim 3 for ancient building material, which is characterized in that the partial size of the active carbon is 1-
10 μm, the partial size of the light calcium carbonate powder is 200-800nm, and the partial size of the aerogel powder is 20-50 μm.
5. the specimens of one's blood according to claim 3 for ancient building material, which is characterized in that the aerogel powder uses silicon
It is aerogel powder.
6. according to claim 1, being used for the specimens of one's blood of ancient building material described in 2,4 or 5, which is characterized in that the quick lime
Water is the ratio for being 1 ﹕ 8-10 according to the mass ratio of quick lime and water, and quick lime is added to the water what dissolution obtained.
7. the preparation method of the specimens of one's blood for ancient building material, which comprises the following steps:
Step 1: preparing the Swine plasma that moisture content is lower than 50%: pig blood being solidified, then filtering removal serum, obtains pig blood grumeleuse；
Then after pig blood grumeleuse being milled, then solidify, refilter removal serum, so repeat to obtain moisture content be lower than 50% pig blood
Grumeleuse；Then pig blood grumeleuse is milled crushing, and crosses 200 meshes, obtain the Swine plasma that moisture content is lower than 50%；
Step 2: weighing the aqueous of step 1 according to each raw material dosage in specimens of one's blood described in any one of the claims 1 to 6
Rate is lower than 50% Swine plasma, lime water, active carbon, light calcium carbonate powder and hypocrellin；
Step 3: the active carbon for loading light calcium is added in Swine plasma, mix, stands 1.5-3 hours, obtain pig blood pulp mixture；
Hypocrellin is added in lime water and is stirred and evenly mixed, lime water mixed solution is obtained；Then pig is added in lime water mixed solution
In plasma mixtures, stirs 40-60 minutes, obtain half paste specimens of one's blood, then stand 10-15 hours again, obtain specimens of one's blood.
8. the preparation method of the specimens of one's blood according to claim 7 for ancient building material, which is characterized in that in step 2,
When the raw material of the specimens of one's blood includes aerogel powder, in step 3, the active carbon for loading light calcium is added in aerogel powder,
30-50min is ground using planetary-type grinding machine, obtains composite load mixture；Then pig is added in the composite load mixture
In blood plasma, mixes, obtain pig blood pulp mixture.
9. the preparation method according to claim 7 or 8 for the specimens of one's blood of ancient building material, which is characterized in that step
In three, during the standing of half paste specimens of one's blood, half paste specimens of one's blood is placed in subnormal ambient.
10. the preparation method of the specimens of one's blood according to claim 9 for ancient building material, which is characterized in that the negative pressure
The pressure of environment is 0.05-0.08MPa.
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| CN201610622718.3A CN106084967B (en) | 2016-08-02 | 2016-08-02 | Specimens of one's blood and preparation method thereof for ancient building material |
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Effective date of registration: 20201012 Address after: 037000 No.3, North 1st Street, hydu, equipment Park, Datong Economic and Technological Development Zone, Shanxi Province Patentee after: Shanxi ancient architecture Group Engineering Co., Ltd Address before: 101102, Beijing Zhongguancun Tongzhou District science and Technology Park, Tongzhou Park Jinqiao technology industry base, 13 South four street, building 5, 5C Patentee before: BEIJING CHUZHIYUAN ENVIRONMENTAL PROTECTION TECHNOLOGY Co.,Ltd. |