CN106083200B - Dragon's fountain Song Dynasty brother's kiln celadon glaze and the method for making dragon's fountain Song Dynasty brother's kiln celadon product with the glaze - Google Patents
Dragon's fountain Song Dynasty brother's kiln celadon glaze and the method for making dragon's fountain Song Dynasty brother's kiln celadon product with the glaze Download PDFInfo
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- CN106083200B CN106083200B CN201610396776.9A CN201610396776A CN106083200B CN 106083200 B CN106083200 B CN 106083200B CN 201610396776 A CN201610396776 A CN 201610396776A CN 106083200 B CN106083200 B CN 106083200B
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- glaze
- kiln
- parts
- glazing
- fountain
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Classifications
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/52—Multiple coating or impregnating multiple coating or impregnating with the same composition or with compositions only differing in the concentration of the constituents, is classified as single coating or impregnation
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/04—Clay; Kaolin
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/32—Burning methods
- C04B33/34—Burning methods combined with glazing
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
Abstract
The invention belongs to porcelain field, in particular to a kind of dragon's fountain Song Dynasty brother's kiln celadon glaze and the method with glaze production dragon's fountain Song Dynasty brother's kiln celadon product.A kind of dragon's fountain Song Dynasty brother's kiln celadon glaze, including tire material and glaze, in which: the tire material is mainly made of raw material from the following weight: 80-90 parts of Zijin soil, 10-20 parts of western source china clay, yellow 10-20 parts of altar china clay；The glaze is mainly made of raw material from the following weight: 32-35 parts of ridge root glaze soil, 25-30 parts of quick lime, 3-5 parts of quartz, 3-5 parts of troilite, 11-13 parts of Dayao Zijin soil.Product produced by the present invention can realize the glaze paint of cream-coloured glaze.
Description
Technical field
The invention belongs to porcelain field, in particular to a kind of dragon's fountain Song Dynasty brother's kiln celadon glaze and with the glaze make the dragon's fountain Song Dynasty
The method of brother's kiln celadon product.
Background technique
The tire color of dragon's fountain brother's kiln porcelain has a variety of colors such as dark-grey, light gray, grey black and colour of loess, glaze colours more have pale blue, it is bluish white,
The difference of putty, bluish yellow, and based on putty.It is mainly characterized by the line piece that glaze paint is covered with cracking, normally referred to as " hacking ".
This to be formed by piece line by fine cracks, size is different, the depth of crackle color is also different.
Song Dynasty brother's kiln crack glaze has stronger vitality as a kind of decoration of art pottery.Due to of the remote past, brother
Kiln porcelain formula and manufacturing process are lost already, to meet growing consumer demand, have tried to restore in recent years
Song Dynasty brother's kiln porcelain formula and manufacturing process, but effect is not fully up to expectations.
Summary of the invention
The present invention provides a kind of dragon's fountain Song Dynasty brother's kiln celadon glaze, and dragon's fountain Song Dynasty brother's kiln celadon product obtained can realize cream colour
The glaze paint of glaze.
The technical solution adopted by the present invention to solve the technical problems is:
A kind of dragon's fountain Song Dynasty brother's kiln celadon glaze, including tire material and glaze, in which: the tire material is mainly by following parts by weight
Raw material is made: 80-90 parts of Zijin soil, 10-20 parts of western source china clay, yellow 10-20 parts of altar china clay；The glaze is mainly by following weight
The raw material of part is made: 32-35 parts of ridge root glaze soil, 25-30 parts of quick lime, 3-5 parts of quartz, 3-5 parts of troilite and Dayao Zijin soil
11-13 parts.
With the characteristics of cyan is presented in this project under high temperature reducing atmospheres, using iron oxide under high temperature reducing atmospheres, with more
Kind china clay mineral are raw material, and dragon's fountain Song Dynasty brother's kiln celadon product appearance obtained and the black tire brother kiln celadon pole of the Southern Song Dynasty are seemingly.
A method of dragon's fountain Song Dynasty brother's kiln celadon product is made with dragon's fountain Song Dynasty brother's kiln celadon glaze, comprising the following steps:
A, it fires biscuit: all raw materials of the tire material being mixed with water, base mud is made, the base mud is formed
After drying, biscuit is made in kiln-firing；
B, it prepares ceramic glaze: the raw material in the glaze being mixed according to the proportion, after crushing, adds water for ball milling, be sieved
Afterwards up to ceramic glaze；
C, glazing: the ceramic glaze is imposed on the biscuit, forms glaze layer in homogeneous thickness after dry to get base
Body carries out second of glazing after green body is cooling；
D, fire: after the glaze layer on green body parches naturally, kiln-firing, kiln discharge is got product after firing；Wherein fire
Process successively passes through following several stages: the stage that is rapidly heated, slow temperature rise period and natural cooling.
Preferably, start-stop temperature is room temperature in firing, the heating rate in the stage that is rapidly heated is 2-3 DEG C/min, is delayed
The heating rate of slow temperature rise period is 0.3-0.5 DEG C/min.
Preferably, green body is first put into biscuiting in kiln and is carried out for the first time after its cooling and dedusting to 800 DEG C before glazing
Glaze is soaked, soaks the glaze time between 10s-15s；Later, roasting in kilns is put into 500 DEG C, is carried out after its cooling and dedusting second
Glazing.
Preferably, second of glazing uses spray glazing, biscuit is placed on turntable and is slowly rotated, pressure pump pair is used
It carries out glazing, stops glazing when glazed thickness and carcass thickness ratio are 1.3:1.
The beneficial effects of the present invention are: the present invention tests out tire, glaze formula using reasonable raw ore raw material, and high temperature also
The thick glaze celadon glaze paint that glaze layer is abundant, shows the cream-coloured glaze to whiten in Huang is burnt out in Primordial Qi atmosphere, such glaze colours can be by iron tire
Black quality be covered with comprehensively, it is beautiful that glaze paint color shows exquisite in texture, gentle class under the setting off of black tire.
Detailed description of the invention
Fig. 1 is process flow chart of the invention；
Fig. 2 is firing heating curve of the invention.
Specific embodiment
Below by specific embodiment, technical scheme of the present invention will be further explained in detail.It should be appreciated that this hair
Bright implementation is not limited by the following examples, and the accommodation in any form made to the present invention and/or changed will all be fallen
Enter the scope of the present invention.
In the present invention, if not refering in particular to, all parts, percentage are unit of weight, used equipment and raw material etc.
It is commercially available or commonly used in the art.Method in following embodiments is unless otherwise instructed the normal of this field
Rule method.
Embodiment 1:
A kind of dragon's fountain Song Dynasty brother's kiln celadon glaze, including tire material and glaze, in which: the tire material is mainly by following parts by weight
Raw material is made: 80 parts of Zijin soil, 18 parts of western source china clay, yellow 15 parts of china clay of altar；The glaze is mainly by the raw material of following parts by weight
It is made: 32 parts of ridge root glaze soil, 25 parts of quick lime, 5 parts of quartz, 5 parts of troilite, 13 parts of soil of Dayao Zijin.
A method of with dragon's fountain Song Dynasty brother's kiln celadon glaze make dragon's fountain Song Dynasty brother's kiln celadon product, process as shown in Figure 1,
The following steps are included:
A, it fires biscuit: all raw materials of the tire material being mixed with water, base mud is made, the base mud is formed
After drying, biscuit is made in kiln-firing；
B, it prepares ceramic glaze: the raw material in the glaze being mixed according to the proportion, after crushing, adds water for ball milling, be sieved
Afterwards up to ceramic glaze；
C, glazing: the ceramic glaze is imposed on the biscuit, forms glaze layer in homogeneous thickness after dry to get base
Body carries out second of glazing after green body is cooling；
D, fire: after the glaze layer on green body parches naturally, kiln-firing, kiln discharge is got product after firing；Wherein fire
Process successively passes through following several stages: the stage that is rapidly heated, slow temperature rise period and natural cooling.
Wherein, glazing process: it is mainly characterized in that thin tire thickness glaze with the black tire brother kiln hacking celadon of the Southern Song Dynasty, and glaze is thicker than tire, therefore,
Glazing process is particularly critical.The present embodiment mainly uses multiple glazing method, which is divided into leaching glaze and glaze spraying two parts.Glazing
Before, green body is first put into kiln biscuiting to 800 DEG C or so, leaching glaze for the first time is carried out after its cooling and dedusting, the leaching glaze time is
Between 10s -15s.Later, roasting in kilns is put into 500 DEG C, and second of glazing is carried out after its cooling and dedusting.Second of glazing
Using spray glazing, biscuit is placed on turntable and is slowly rotated, glazing is carried out to it using pressure pump, to glazed thickness and carcass
Thickness ratio stops glazing when being 1.3:1 or so.
Firing process: in order to guarantee products appearance effect and improve yield rate, the present embodiment is slowly burnt into using shuttle kiln,
Enter the strong reductive firing stages in 1080 DEG C, and switchs in 1200 DEG C weak to be restored to 1320 DEG C of only fire, the nearly 18h of total time-consuming.It burns
It is as shown in Figure 2 at curve.Start-stop temperature is room temperature in firing, and the heating rate in the stage that is rapidly heated is 2-3 DEG C/min, slowly
The heating rate of temperature rise period is 0.3-0.5 DEG C/min.
Embodiment 2:
A kind of dragon's fountain Song Dynasty brother's kiln celadon glaze, including tire material and glaze, in which: the tire material is mainly by following parts by weight
Raw material is made: 90 parts of Zijin soil, 15 parts of western source china clay, yellow 20 parts of china clay of altar；The glaze is mainly by the raw material of following parts by weight
It is made: 35 parts of ridge root glaze soil, 25 parts of quick lime, 3 parts of quartz, 3 parts of troilite, 11 parts of soil of Dayao Zijin.Brother's kiln hacking celadon system
Technique is made with embodiment 1.
Embodiment 3:
A kind of dragon's fountain Song Dynasty brother's kiln celadon glaze, including tire material and glaze, in which: the tire material is mainly by following parts by weight
Raw material is made: 85 parts of Zijin soil, 16 parts of western source china clay, yellow 18 parts of china clay of altar；The glaze is mainly by the raw material of following parts by weight
It is made: 32-35 parts of ridge root glaze soil, 25-30 parts of quick lime, 3 parts of quartz, 5 parts of troilite, 12 parts of soil of Dayao Zijin.Brother's kiln hacking
Celadon manufacturing process is the same as embodiment 1.
The present invention has made black tire brother kiln hacking celadon tire material by many experiments, such tire material has preferable mouldability
Can, at 1300 DEG C --- black is presented when 1320 DEG C of firings.To burn out and the black tire brother kiln hacking celadon glaze paint appearance effect of the Southern Song Dynasty
Celadon as fruit obtains rational formula by many experiments, and it is beautiful refined finally to burn out glaze paint exquisite in texture, gentle class jade, victory
It causes, glaze colours is simple and elegant, the cream-coloured glaze to whiten in Huang.
Above-mentioned embodiment is only a preferred solution of the present invention, not the present invention is made in any form
Limitation, there are also other variations and modifications on the premise of not exceeding the technical scheme recorded in the claims.
Claims (2)
1. a kind of dragon's fountain Song Dynasty brother's kiln celadon glaze, it is characterised in that: including tire material and glaze, in which: the tire material mainly by with
The raw material of lower parts by weight is made: 80-90 parts of Zijin soil, 10-20 parts of western source china clay, yellow 10-20 parts of altar china clay；The glaze
It is mainly made of raw material from the following weight: 32-35 parts of ridge root glaze soil, 25-30 parts of quick lime, 3-5 parts of quartz, troilite 3-
5 parts and 11-13 parts of Dayao Zijin soil；
The method of dragon's fountain Song Dynasty brother's kiln celadon glaze production dragon's fountain Song Dynasty brother's kiln celadon product the following steps are included:
A, it fires biscuit: all raw materials of the tire material being mixed with water, base mud is made, by the base mud shaping and drying
Afterwards, biscuit is made in kiln-firing；
B, it prepares ceramic glaze: the raw material in the glaze being mixed according to the proportion, after crushing, adds water for ball milling, after sieving i.e.
Obtain ceramic glaze；
C, glazing: the ceramic glaze is imposed on the biscuit, forms glaze layer in homogeneous thickness after dry to get green body, base
Second of glazing is carried out after body is cooling；
Before glazing, green body is first put into biscuiting in kiln and carries out leaching glaze for the first time after its cooling and dedusting to 800 DEG C, soaks the glaze time
Between 10s-15s；Later, roasting in kilns is put into 500 DEG C, and second of glazing is carried out after its cooling and dedusting；
Second of glazing uses spray glazing, and biscuit is placed on turntable and is slowly rotated, carries out glazing to it using pressure pump, to
Glazed thickness and carcass thickness ratio stop glazing when being 1.3:1；
D, fire: after the glaze layer on green body parches naturally, kiln-firing, kiln discharge is got product after firing；Wherein sintering procedure
Successively by following several stages: the stage that is rapidly heated, slow temperature rise period and natural cooling；Start-stop temperature is room in firing
Temperature, the heating rate in the stage that is rapidly heated are 2-3 DEG C/min, and the heating rate of slow temperature rise period is 0.3-0.5 DEG C/min.
2. a kind of method of the production of dragon's fountain Song Dynasty brother's kiln celadon glaze according to claim 1 dragon's fountain Song Dynasty brother's kiln celadon product,
Characterized by comprising the following steps:
A, it fires biscuit: all raw materials of the tire material being mixed with water, base mud is made, by the base mud shaping and drying
Afterwards, biscuit is made in kiln-firing；
B, it prepares ceramic glaze: the raw material in the glaze being mixed according to the proportion, after crushing, adds water for ball milling, after sieving i.e.
Obtain ceramic glaze；
C, glazing: the ceramic glaze is imposed on the biscuit, forms glaze layer in homogeneous thickness after dry to get green body, base
Second of glazing is carried out after body is cooling；
Before glazing, green body is first put into biscuiting in kiln and carries out leaching glaze for the first time after its cooling and dedusting to 800 DEG C, soaks the glaze time
Between 10s-15s；Later, roasting in kilns is put into 500 DEG C, and second of glazing is carried out after its cooling and dedusting；
Second of glazing uses spray glazing, and biscuit is placed on turntable and is slowly rotated, carries out glazing to it using pressure pump, to
Glazed thickness and carcass thickness ratio stop glazing when being 1.3:1；
D, fire: after the glaze layer on green body parches naturally, kiln-firing, kiln discharge is got product after firing；Wherein sintering procedure
Successively by following several stages: the stage that is rapidly heated, slow temperature rise period and natural cooling；Start-stop temperature is room in firing
Temperature, the heating rate in the stage that is rapidly heated are 2-3 DEG C/min, and the heating rate of slow temperature rise period is 0.3-0.5 DEG C/min.
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| CN201610396776.9A CN106083200B (en) | 2016-06-06 | 2016-06-06 | Dragon's fountain Song Dynasty brother's kiln celadon glaze and the method for making dragon's fountain Song Dynasty brother's kiln celadon product with the glaze |
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| CN201610396776.9A CN106083200B (en) | 2016-06-06 | 2016-06-06 | Dragon's fountain Song Dynasty brother's kiln celadon glaze and the method for making dragon's fountain Song Dynasty brother's kiln celadon product with the glaze |
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| CN106083200A CN106083200A (en) | 2016-11-09 |
| CN106083200B true CN106083200B (en) | 2019-01-04 |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108373265A (en) * | 2018-02-06 | 2018-08-07 | 平顶山学院 | A kind of shrinkproof glaze handicraft of celadon and method |
| CN108751708A (en) * | 2018-06-04 | 2018-11-06 | 浙江上木木陶瓷文化有限公司 | The pure matting glaze of high temperature more kiln, using the matting glaze kiln secret colour ware and its method for cooking |
| CN110183248A (en) * | 2019-05-22 | 2019-08-30 | 李茂林 | Material, dragon's fountain porcelain and preparation method thereof is presented in Vermilion for dragon's fountain porcelain |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101734948A (en) * | 2008-11-04 | 2010-06-16 | 李邦强 | Longquan official ware celadon glaze of the Ming Dynasty and method for manufacturing Longquan official ware celadon product of the Ming Dynasty by using glaze |
-
2016
- 2016-06-06 CN CN201610396776.9A patent/CN106083200B/en active Active
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101734948A (en) * | 2008-11-04 | 2010-06-16 | 李邦强 | Longquan official ware celadon glaze of the Ming Dynasty and method for manufacturing Longquan official ware celadon product of the Ming Dynasty by using glaze |
Non-Patent Citations (2)
| Title |
|---|
| "南宋龙泉黑胎哥窑开片青瓷的复烧工艺研究";毛伟杰;《大众文艺》;20151030;第85页第1栏倒数第3行-第2栏第13行 |
| "黑胎哥窑青瓷的仿制";吴艳芳等;《丽水学院学报》;20160331;第38卷(第2期);第104-105页第2.3节和图5 |
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