CN106048783B - 一种高效制备钛基-碳三维卷曲纳米纤维的方法 - Google Patents
一种高效制备钛基-碳三维卷曲纳米纤维的方法 Download PDFInfo
- Publication number
- CN106048783B CN106048783B CN201610382590.8A CN201610382590A CN106048783B CN 106048783 B CN106048783 B CN 106048783B CN 201610382590 A CN201610382590 A CN 201610382590A CN 106048783 B CN106048783 B CN 106048783B
- Authority
- CN
- China
- Prior art keywords
- tio
- nanofiber
- polyacrylonitrile
- temperature
- carbon
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000002121 nanofiber Substances 0.000 title claims abstract description 76
- 239000010936 titanium Substances 0.000 title claims abstract description 28
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 title claims abstract description 14
- 229910052719 titanium Inorganic materials 0.000 title claims abstract description 14
- 229910052799 carbon Inorganic materials 0.000 title claims abstract description 13
- 238000000034 method Methods 0.000 title claims description 19
- 238000002360 preparation method Methods 0.000 title abstract description 18
- 229920002239 polyacrylonitrile Polymers 0.000 claims abstract description 45
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims abstract description 37
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 claims abstract description 34
- 238000009987 spinning Methods 0.000 claims abstract description 28
- 238000005516 engineering process Methods 0.000 claims abstract description 16
- 238000003763 carbonization Methods 0.000 claims abstract description 10
- 230000007797 corrosion Effects 0.000 claims abstract description 8
- 238000005260 corrosion Methods 0.000 claims abstract description 8
- 230000003068 static effect Effects 0.000 claims abstract description 7
- 230000005518 electrochemistry Effects 0.000 claims abstract description 6
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 17
- 238000010792 warming Methods 0.000 claims description 16
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 claims description 15
- 239000000835 fiber Substances 0.000 claims description 12
- 238000010041 electrostatic spinning Methods 0.000 claims description 10
- 239000007789 gas Substances 0.000 claims description 10
- 239000012300 argon atmosphere Substances 0.000 claims description 8
- 229960000583 acetic acid Drugs 0.000 claims description 7
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims description 6
- FPCJKVGGYOAWIZ-UHFFFAOYSA-N butan-1-ol;titanium Chemical compound [Ti].CCCCO.CCCCO.CCCCO.CCCCO FPCJKVGGYOAWIZ-UHFFFAOYSA-N 0.000 claims description 6
- 238000004090 dissolution Methods 0.000 claims description 6
- 239000012299 nitrogen atmosphere Substances 0.000 claims description 6
- 239000003960 organic solvent Substances 0.000 claims description 6
- 238000007146 photocatalysis Methods 0.000 claims description 6
- 230000001699 photocatalysis Effects 0.000 claims description 6
- -1 Alkene nitrile Chemical class 0.000 claims description 5
- 238000005457 optimization Methods 0.000 claims description 5
- 239000012362 glacial acetic acid Substances 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 4
- 229910052786 argon Inorganic materials 0.000 claims description 3
- 239000002070 nanowire Substances 0.000 claims description 3
- 230000001954 sterilising effect Effects 0.000 claims description 3
- 239000002351 wastewater Substances 0.000 claims description 3
- 239000012298 atmosphere Substances 0.000 claims description 2
- 230000003115 biocidal effect Effects 0.000 claims description 2
- 239000002537 cosmetic Substances 0.000 claims description 2
- 210000003298 dental enamel Anatomy 0.000 claims description 2
- 239000003814 drug Substances 0.000 claims description 2
- 239000004922 lacquer Substances 0.000 claims 1
- 239000000463 material Substances 0.000 abstract description 17
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract description 7
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 abstract description 5
- 238000006555 catalytic reaction Methods 0.000 abstract description 5
- 150000001875 compounds Chemical class 0.000 abstract description 5
- 230000032683 aging Effects 0.000 abstract description 3
- 239000004408 titanium dioxide Substances 0.000 abstract description 2
- 230000003647 oxidation Effects 0.000 abstract 1
- 238000007254 oxidation reaction Methods 0.000 abstract 1
- 239000002994 raw material Substances 0.000 abstract 1
- 239000000243 solution Substances 0.000 description 30
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 7
- 229920000036 polyvinylpyrrolidone Polymers 0.000 description 7
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 description 7
- 239000000126 substance Substances 0.000 description 7
- 229920000642 polymer Polymers 0.000 description 6
- 239000001267 polyvinylpyrrolidone Substances 0.000 description 6
- 229920000049 Carbon (fiber) Polymers 0.000 description 5
- 239000004917 carbon fiber Substances 0.000 description 5
- 239000002131 composite material Substances 0.000 description 5
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 4
- 239000002134 carbon nanofiber Substances 0.000 description 4
- 238000001878 scanning electron micrograph Methods 0.000 description 4
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 3
- 230000003197 catalytic effect Effects 0.000 description 3
- 230000008859 change Effects 0.000 description 3
- 239000011248 coating agent Substances 0.000 description 3
- 238000000576 coating method Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000002347 injection Methods 0.000 description 3
- 239000007924 injection Substances 0.000 description 3
- 239000002086 nanomaterial Substances 0.000 description 3
- 230000000704 physical effect Effects 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- ZHNUHDYFZUAESO-UHFFFAOYSA-N Formamide Chemical compound NC=O ZHNUHDYFZUAESO-UHFFFAOYSA-N 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 238000001354 calcination Methods 0.000 description 2
- 239000000919 ceramic Substances 0.000 description 2
- 239000004020 conductor Substances 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 230000018109 developmental process Effects 0.000 description 2
- 239000007772 electrode material Substances 0.000 description 2
- 239000012530 fluid Substances 0.000 description 2
- 229910021389 graphene Inorganic materials 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 2
- 230000005476 size effect Effects 0.000 description 2
- 230000003075 superhydrophobic effect Effects 0.000 description 2
- 238000003786 synthesis reaction Methods 0.000 description 2
- 230000005642 Aharonov-Bohm effect Effects 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- FXHOOIRPVKKKFG-UHFFFAOYSA-N N,N-Dimethylacetamide Chemical compound CN(C)C(C)=O FXHOOIRPVKKKFG-UHFFFAOYSA-N 0.000 description 1
- SECXISVLQFMRJM-UHFFFAOYSA-N N-Methylpyrrolidone Chemical compound CN1CCCC1=O SECXISVLQFMRJM-UHFFFAOYSA-N 0.000 description 1
- 241000209094 Oryza Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 239000004697 Polyetherimide Substances 0.000 description 1
- 239000002202 Polyethylene glycol Substances 0.000 description 1
- 239000004642 Polyimide Substances 0.000 description 1
- 239000004743 Polypropylene Substances 0.000 description 1
- 239000004793 Polystyrene Substances 0.000 description 1
- 239000004372 Polyvinyl alcohol Substances 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- NRTOMJZYCJJWKI-UHFFFAOYSA-N Titanium nitride Chemical compound [Ti]#N NRTOMJZYCJJWKI-UHFFFAOYSA-N 0.000 description 1
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 description 1
- 229920006221 acetate fiber Polymers 0.000 description 1
- CSCPPACGZOOCGX-UHFFFAOYSA-N acetone Substances CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- YHWCPXVTRSHPNY-UHFFFAOYSA-N butan-1-olate;titanium(4+) Chemical compound [Ti+4].CCCC[O-].CCCC[O-].CCCC[O-].CCCC[O-] YHWCPXVTRSHPNY-UHFFFAOYSA-N 0.000 description 1
- 238000005256 carbonitriding Methods 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 238000003486 chemical etching Methods 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000009749 continuous casting Methods 0.000 description 1
- 230000001351 cycling effect Effects 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 229910003460 diamond Inorganic materials 0.000 description 1
- 239000010432 diamond Substances 0.000 description 1
- KPUWHANPEXNPJT-UHFFFAOYSA-N disiloxane Chemical class [SiH3]O[SiH3] KPUWHANPEXNPJT-UHFFFAOYSA-N 0.000 description 1
- 230000002500 effect on skin Effects 0.000 description 1
- 239000010411 electrocatalyst Substances 0.000 description 1
- 238000001523 electrospinning Methods 0.000 description 1
- 235000019441 ethanol Nutrition 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 239000002657 fibrous material Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 238000005087 graphitization Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000001307 helium Substances 0.000 description 1
- 229910052734 helium Inorganic materials 0.000 description 1
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 239000007777 multifunctional material Substances 0.000 description 1
- 239000010813 municipal solid waste Substances 0.000 description 1
- 150000004767 nitrides Chemical class 0.000 description 1
- 150000002825 nitriles Chemical class 0.000 description 1
- 230000033116 oxidation-reduction process Effects 0.000 description 1
- 229910052697 platinum Inorganic materials 0.000 description 1
- 229920003229 poly(methyl methacrylate) Polymers 0.000 description 1
- 229920006260 polyaryletherketone Polymers 0.000 description 1
- 229920001601 polyetherimide Polymers 0.000 description 1
- 229920001223 polyethylene glycol Polymers 0.000 description 1
- 229920001721 polyimide Polymers 0.000 description 1
- 239000004926 polymethyl methacrylate Substances 0.000 description 1
- 229920001155 polypropylene Polymers 0.000 description 1
- 229920002223 polystyrene Polymers 0.000 description 1
- 229920002451 polyvinyl alcohol Polymers 0.000 description 1
- 238000006722 reduction reaction Methods 0.000 description 1
- 230000002207 retinal effect Effects 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 239000004065 semiconductor Substances 0.000 description 1
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 description 1
- 229910010271 silicon carbide Inorganic materials 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- HXJUTPCZVOIRIF-UHFFFAOYSA-N sulfolane Chemical compound O=S1(=O)CCCC1 HXJUTPCZVOIRIF-UHFFFAOYSA-N 0.000 description 1
- 238000010301 surface-oxidation reaction Methods 0.000 description 1
- 230000001225 therapeutic effect Effects 0.000 description 1
- VXUYXOFXAQZZMF-UHFFFAOYSA-N titanium(IV) isopropoxide Chemical compound CC(C)O[Ti](OC(C)C)(OC(C)C)OC(C)C VXUYXOFXAQZZMF-UHFFFAOYSA-N 0.000 description 1
- 229910052723 transition metal Inorganic materials 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
- D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
- D01F9/12—Carbon filaments; Apparatus specially adapted for the manufacture thereof
- D01F9/14—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments
- D01F9/20—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products
- D01F9/21—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products from macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D01F9/22—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products from macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds from polyacrylonitriles
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
- D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
- D01F9/12—Carbon filaments; Apparatus specially adapted for the manufacture thereof
- D01F9/14—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments
- D01F9/20—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products
- D01F9/21—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products from macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Textile Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Inorganic Fibers (AREA)
- Artificial Filaments (AREA)
- Nonwoven Fabrics (AREA)
Abstract
Description
Claims (2)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201610382590.8A CN106048783B (zh) | 2016-05-30 | 2016-05-30 | 一种高效制备钛基-碳三维卷曲纳米纤维的方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201610382590.8A CN106048783B (zh) | 2016-05-30 | 2016-05-30 | 一种高效制备钛基-碳三维卷曲纳米纤维的方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN106048783A CN106048783A (zh) | 2016-10-26 |
CN106048783B true CN106048783B (zh) | 2019-01-22 |
Family
ID=57171902
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201610382590.8A Expired - Fee Related CN106048783B (zh) | 2016-05-30 | 2016-05-30 | 一种高效制备钛基-碳三维卷曲纳米纤维的方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN106048783B (zh) |
Families Citing this family (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106693557B (zh) * | 2016-12-02 | 2020-01-21 | 清华大学 | Pm2.5过滤膜、制备方法以及pm2.5过滤纱窗 |
CN106782747B (zh) * | 2017-01-09 | 2019-08-09 | 清华大学 | 银纳米纤维薄膜及其制备方法和设备以及电子器件 |
CN108525527B (zh) * | 2018-02-27 | 2021-06-01 | 北京市水科学技术研究院 | 碳纤维催化臭氧氧化复合分离膜及其制备方法和应用 |
CN110656402A (zh) * | 2019-01-21 | 2020-01-07 | 深圳维度新材料有限公司 | 一种无机纳米纤维制备方法及设备 |
CN110170282B (zh) * | 2019-05-07 | 2020-07-14 | 清华大学 | 一种各向异性层状无机纤维气凝胶材料及其制备方法 |
CN110184683B (zh) * | 2019-05-07 | 2020-06-19 | 清华大学 | 一种各向异性层状碳纤维基气凝胶材料及其制备方法 |
CN110424067A (zh) * | 2019-07-08 | 2019-11-08 | 清华大学 | 一种柔性二氧化硅纤维气凝胶材料及其制备方法 |
TWI770469B (zh) * | 2020-02-18 | 2022-07-11 | 國立臺灣大學 | 一種製備含奈米顆粒的高導電性碳纖維之方法及其用途 |
CN111682169B (zh) * | 2020-05-12 | 2021-08-20 | 湖北大学 | 一种三维导电网络结构复合材料及其制备方法和应用 |
CN115011971A (zh) * | 2022-06-28 | 2022-09-06 | 刘优昌 | 一种TiO2/TiC/C电催化剂及其制备方法 |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101428852A (zh) * | 2008-12-05 | 2009-05-13 | 中国科学院化学研究所 | 静电纺丝制备超疏水二氧化钛膜的方法 |
CN104451911A (zh) * | 2014-11-21 | 2015-03-25 | 天津工业大学 | 一种静电辅助溶液喷射纺丝装置及纺丝方法 |
CN104835949A (zh) * | 2014-07-28 | 2015-08-12 | 北汽福田汽车股份有限公司 | Si-TiO2-C纳米纤维复合薄膜及其制备方法和应用 |
CN105170181A (zh) * | 2015-09-25 | 2015-12-23 | 天津工业大学 | 一种优化碳/二氧化钛复合纤维膜催化性能的方法 |
CN105401339A (zh) * | 2015-09-06 | 2016-03-16 | 天津工业大学 | 一种聚芳醚砜基微/纳米纤维的制备方法 |
-
2016
- 2016-05-30 CN CN201610382590.8A patent/CN106048783B/zh not_active Expired - Fee Related
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101428852A (zh) * | 2008-12-05 | 2009-05-13 | 中国科学院化学研究所 | 静电纺丝制备超疏水二氧化钛膜的方法 |
CN104835949A (zh) * | 2014-07-28 | 2015-08-12 | 北汽福田汽车股份有限公司 | Si-TiO2-C纳米纤维复合薄膜及其制备方法和应用 |
CN104451911A (zh) * | 2014-11-21 | 2015-03-25 | 天津工业大学 | 一种静电辅助溶液喷射纺丝装置及纺丝方法 |
CN105401339A (zh) * | 2015-09-06 | 2016-03-16 | 天津工业大学 | 一种聚芳醚砜基微/纳米纤维的制备方法 |
CN105170181A (zh) * | 2015-09-25 | 2015-12-23 | 天津工业大学 | 一种优化碳/二氧化钛复合纤维膜催化性能的方法 |
Also Published As
Publication number | Publication date |
---|---|
CN106048783A (zh) | 2016-10-26 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN106048783B (zh) | 一种高效制备钛基-碳三维卷曲纳米纤维的方法 | |
Huang et al. | Fabrication of porous fibers via electrospinning: strategies and applications | |
Li et al. | Fabrication of titania nanofibers by electrospinning | |
Li et al. | Research progress of ultrafine alumina fiber prepared by sol-gel method: A review | |
Jia et al. | Flexible ceramic fibers: Recent development in preparation and application | |
WO2021068737A1 (zh) | 柔性莫来石纤维气凝胶材料及其制备方法 | |
Xu et al. | Electrospun TiO2‐based photocatalysts | |
Li et al. | Direct fabrication of composite and ceramic hollow nanofibers by electrospinning | |
Song et al. | Advances in electrospun TiO2 nanofibers: Design, construction, and applications | |
Zhang et al. | A review: carbon nanofibers from electrospun polyacrylonitrile and their applications | |
Shui et al. | Platinum nanowires produced by electrospinning | |
CN102683710A (zh) | 碳纳米纤维负载二氧化钛薄膜负极材料及其制备方法 | |
CN102658108A (zh) | 电纺法制备基于石墨烯/半导体光催化滤膜的方法 | |
CN111074380B (zh) | 一种氧化石墨烯/聚丙烯酸钠的拉伸流体及其在制备石墨烯中的应用 | |
CN104332640A (zh) | 全钒液流电池用热还原氧化石墨烯/纳米碳纤维复合电极制备方法 | |
Chen et al. | Status and strategies for fabricating flexible oxide ceramic micro-nanofiber materials | |
CN106637506B (zh) | 一种液态金属/二氧化钛纳米连续纤维及其制备方法 | |
CN101876095A (zh) | 一种多孔碳化硅纤维及其制备方法 | |
CN102701163B (zh) | 一种具有三维连通孔道结构的氮化钛纳米材料及制备方法 | |
CN105401335A (zh) | 一种聚芳醚酮基微/纳米纤维的制备方法 | |
CN103628182B (zh) | 一种碳基纳米纤维的制备方法 | |
CN107008240A (zh) | 氧化铝开孔泡沫陶瓷负载Si掺杂的纳米晶二氧化钛光催化剂及其制备方法 | |
CN107029693B (zh) | 一种碳点掺杂二氧化钛复合微管及其制备方法 | |
Zhang et al. | Facile fabrication of large scale microtubes with a natural template—Kapok fiber | |
CN106390766A (zh) | 一种具有自清洁功能的仿鼻腔纤毛结构过滤材料 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
GR01 | Patent grant | ||
GR01 | Patent grant | ||
TR01 | Transfer of patent right |
Effective date of registration: 20210508 Address after: 215505 No.7 Fuchunjiang Road, Changshu high tech Industrial Development Zone, Suzhou City, Jiangsu Province Patentee after: Suzhou wuchuangzhi New Material Technology Co.,Ltd. Address before: No. 399 Bingshui Road, Xiqing District, Tianjin, Tianjin Patentee before: TIANJIN POLYTECHNIC University |
|
TR01 | Transfer of patent right | ||
DD01 | Delivery of document by public notice |
Addressee: Han Chunmei Document name: payment instructions |
|
DD01 | Delivery of document by public notice | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20190122 |
|
CF01 | Termination of patent right due to non-payment of annual fee |