CN106046906A - Preparation method of environmentally friendly interior wall waterproof putty powder - Google Patents
Preparation method of environmentally friendly interior wall waterproof putty powder Download PDFInfo
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- CN106046906A CN106046906A CN201610672650.XA CN201610672650A CN106046906A CN 106046906 A CN106046906 A CN 106046906A CN 201610672650 A CN201610672650 A CN 201610672650A CN 106046906 A CN106046906 A CN 106046906A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/34—Filling pastes
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Materials Applied To Surfaces To Minimize Adherence Of Mist Or Water (AREA)
Abstract
The invention relates to a preparation method of an environmentally friendly interior wall waterproof putty powder, and belongs to the technical field of preparation of putty powder. The preparation method comprises the steps: firstly, crushing cactus, distilled water, scutellaria baicalensis and other substances, then putting the crushed mixture into a fermentation tank, adding lactic acid bacteria, and fermenting; then carrying out mixing heating reflux of the fermented mixture with an ethanol solution, to obtain a filtrate; refrigerating the filtrate, and carrying out centrifugal separation, to obtain a supernatant; then mixing and heating the supernatant, vermiculite, diatom mud and other substances, and freezing, to obtain a frozen material; and finally, mixing and stirring the frozen material with heavy calcium carbonate and other substances, to obtain the environmentally friendly interior wall waterproof putty powder. The prepared environmentally friendly interior wall waterproof putty powder plays a role in purifying indoor air, and has the formaldehyde removal rate reaching 94% or more and the toluene removal rate reaching 42% or more in 22-24 h; and the environmentally friendly interior wall waterproof putty powder has the advantages of environmental friendliness, no toxicity, and good water resistance, and resists water for 96 h without abnormalities.
Description
Technical field
The present invention relates to the preparation method of a kind of environment-friendly type inner wall water-proof putty powder, belong to powder of lacquer putty for use on preparing technical field.
Background technology
Harmful minimum gas of release in constructional ornamental material and furniture, the abnormal flavour etc. produced such as formaldehyde, ammonia, benzene and human body
Swimming in aerial, its occurrence status and form are complicated and diversified, with the presence of with free gas molecule form, some quilts
The absorption of substantial amounts of positive charge, encirclement floating in air form cation, and some minimum gas molecules are at already present particle table
Deposit on face, be condensed into aerosol system etc..Just because of above cation or aerocolloidal existence, cause and newly fit up indoor
Serious air, without dye, causes harm greatly to health.
Before putty is paint class construction, construction surface is carried out a kind of surface packing material of pretreatment, it is therefore intended that fill and execute
The hole in work face and the curve deviation of rectification construction surface, for obtaining uniformly, smooth lacquer painting is laid a solid foundation, therefore should be possessed good
Adhesion strength and resistance to water, with ensure water vapour in atmosphere long-term corrode under not have hollowing, peeling, cracking etc. existing
As and remain able to combine closely with matrix, play good decoration and protective effect.Due to inner wall of building and human contact
Time is long, big on the impact of health, and therefore architectural engineering is for the resistance to water of inner wall putty, aesthetic property, safety, environmental protection
Property etc. is had higher requirement.
Tradition powder of lacquer putty for use on have employed and can go out the tourmaline powder of anion, one type be must join with rare earth material
Activate tourmaline powder, but this powder of lacquer putty for use on has the danger that radioactivity exceeds standard；Equations of The Second Kind is addition dioxy in powder of lacquer putty for use on
Change titanium material, form Photocatalyst anion material, but the condition that this materials purification air obtains is must to be excited by light energy source
Just can work.People all can not be made satisfied it addition, existing powder of lacquer putty for use on obtains water resistance.
Summary of the invention
The technical problem to be solved: exceed standard material containing radioactivity in existing powder of lacquer putty for use on, dangerous,
Not environmentally, and add titanium dioxide, then exist and must be excited the problem that just can play air purification effect, the present invention by light energy source
First after the materials such as Radix et Caulis Opuntiae Dillenii, distilled water and Radix Scutellariae being pulverized, put in fermentation tank, add lactic acid bacteria and ferment, then
After fermenting mixture and ethanol solution are carried out Hybrid Heating backflow, obtain filtrate, after its cold preservation, centrifugation, obtain
Supernatant, after then the materials such as supernatant, Vermiculitum and diatom ooze being carried out Hybrid Heating, freezing, obtain cold animal, finally by it
Carry out mix and blend with materials such as ground calcium carbonate, obtain environment-friendly type inner wall water-proof putty powder.Interior wall prepared by the present invention is water-fast
Powder of lacquer putty for use on do not contains noxious substance, environmental protection, in use, and will not be protected from environmental, can reach to purify the effect of air.
For solving above-mentioned technical problem, the technical solution used in the present invention is:
(1) count by weight, take 43～46 parts of Radix et Caulis Opuntiae Dilleniis, 30～32 parts of distilled water, 22～24 parts of Radix Scutellariaes, 10～13 parts of Fructus Persicae
Glue, 7～9 parts of caseins and 8～11 parts of distiller grains, put in pulverizer, pulverizes 40～50min with 1200～1500r/min, collects
Crushed mixture is put in fermentation tank, adds crushed mixture quality 4～the lactobacillus powder of 8%, stirs, design temperature
Being 35～38 DEG C, sealing and fermenting tank, with 110r/min stirring fermentation 2～3 days；
(2) after above-mentioned fermentation ends, the fermenting mixture in fermentation tank is collected, and by solid-to-liquid ratio 1:4, with mass fraction 65%
Ethanol solution mix homogeneously, then be placed in reflux, at 62～66 DEG C of backflows 1～3h, filtration under diminished pressure the most while hot, collected
Filtrate, is placed in cold room, stands 30～50min at 5～10 DEG C, and the filtrate after standing is put in centrifuge, with
2000r/min centrifugation 10～15min, collects supernatant；
(3) count by weight, take 50～55 parts of above-mentioned supernatant, 31～33 parts of Vermiculitums, 22～24 parts of diatom oozes and 8～10 parts
Cellulose ether, stirs, and heats it, is heated to 70～90 DEG C, with 130r/min agitating heating 4～8h, natural subsequently
Being cooled to room temperature, place in liquid nitrogen flash freezer machine, design temperature is-20～-10 DEG C, freezing processing 4～6min, collects freezing
Thing；
(4) count by weight, take 40～45 parts of above-mentioned frozen materials, 12～14 parts of ground calcium carbonate, 2～5 parts of solid contents are
The polyvinyl acetate emulsion of 10%, 1～3 part of water and 1～2 part of Carboxymethyl cellulose sodium, stir, and stands at 35～40 DEG C
1～2h, environment-friendly type inner wall water-proof putty powder.
The application process of the present invention: by solid-to-liquid ratio 20:7, the Internal wall water-fast putty powder of above-mentioned preparation is stirred with water
Mixing, after standing 5～10min, is stirred for 1～2min, can criticize and scrape use, criticizes and scrapes on the interior wall after cleaning out, blade coating
Amount be 0.6～0.8kg/m2, after painting to be doctored completes so that it is natural air drying, and it is detected, 22～24h, it is to first
The clearance of aldehyde reaches more than 94%, and the clearance of toluene reaches more than 42%, and its resistance to water (96h) is without exception.
The present invention is compared with additive method, and Advantageous Effects is:
(1) room air is played the effect of purification by the environment-friendly type inner wall water-proof putty powder that prepared by the present invention, and it is 22～24h
Time, the clearance of PARA FORMALDEHYDE PRILLS(91,95) reaches more than 94%, and the clearance of toluene reaches more than 42%；
(2) to prepare environment-friendly type inner wall water-proof putty powder water resistance good for the present invention, and resistance to water (96h) is without exception.
Detailed description of the invention
Count the most by weight, take 43～46 parts of Radix et Caulis Opuntiae Dilleniis, 30～32 parts of distilled water, 22～24 parts of Radix Scutellariaes, 10～13 parts of Fructus Persicae
Glue, 7～9 parts of caseins and 8～11 parts of distiller grains, put in pulverizer, pulverizes 40～50min with 1200～1500r/min, collects
Crushed mixture is put in fermentation tank, adds crushed mixture quality 4～the lactobacillus powder of 8%, stirs, design temperature
Being 35～38 DEG C, sealing and fermenting tank, with 110r/min stirring fermentation 2～3 days；After above-mentioned fermentation ends, collect in fermentation tank
Fermenting mixture, and by solid-to-liquid ratio 1:4, mix homogeneously with mass fraction 65% ethanol solution, then be placed in reflux,
62～66 DEG C of backflows 1～3h, filtration under diminished pressure the most while hot, collect filtrate, be placed in cold room, stand 30 at 5～10 DEG C
～50min, the filtrate after standing is put in centrifuge, with 2000r/min centrifugation 10～15min, collects supernatant；
Count the most by weight, take 50～55 parts of above-mentioned supernatant, 31～33 parts of Vermiculitums, 22～24 parts of diatom oozes and 8～10 parts of fibres
Dimension element ether, stirs, and heats it, be heated to 70～90 DEG C, with 130r/min agitating heating 4～8h, the coldest
But to room temperature, placing in liquid nitrogen flash freezer machine, design temperature is-20～-10 DEG C, freezing processing 4～6min, collects frozen material；
Finally count by weight, take 40～45 parts of above-mentioned frozen materials, 12～14 parts of ground calcium carbonate, 2～5 parts of solid contents are 10%
Polyvinyl acetate emulsion, 1～3 part of water and 1～2 part of Carboxymethyl cellulose sodium, stir, and stands 1～2h at 35～40 DEG C,
Environment-friendly type inner wall water-proof putty powder.
Example 1
Count the most by weight, take 46 parts of Radix et Caulis Opuntiae Dilleniis, 32 parts of distilled water, 24 parts of Radix Scutellariaes, 13 parts of Resina persicaes, 9 parts of caseins and 11
Part distiller grains, put in pulverizer, pulverize 50min with 1500r/min, collect crushed mixture and put in fermentation tank, add powder
The lactobacillus powder of broken mixture quality 8%, stirs, and design temperature is 38 DEG C, sealing and fermenting tank, sends out with 110r/min stirring
Ferment 3 days；After above-mentioned fermentation ends, collect the fermenting mixture in fermentation tank, and by solid-to-liquid ratio 1:4, with mass fraction 65%
Ethanol solution mix homogeneously, then be placed in reflux, at 66 DEG C of reflux 3h, the most while hot filtration under diminished pressure, collect filtrate, and
Being placed in cold room, stand 50min at 10 DEG C, the filtrate after standing is put in centrifuge, with 2000r/min centrifugation
15min, collects supernatant；Count the most by weight, take 55 parts of above-mentioned supernatant, 33 parts of Vermiculitums, 24 parts of diatom oozes and 10 parts
Cellulose ether, stirs, and heats it, is heated to 90 DEG C, with 130r/min agitating heating 8h, naturally cools to room subsequently
Temperature, places in liquid nitrogen flash freezer machine, and design temperature is-10 DEG C, freezing processing 6min, collects frozen material；The most by weight
Meter, takes 45 parts of above-mentioned frozen materials, 14 parts of ground calcium carbonate, 5 parts of solid contents are the polyvinyl acetate emulsion of 10%, 3 parts of water and 2 parts
Carboxymethyl cellulose sodium, stirs, at 40 DEG C stand 2h, environment-friendly type inner wall water-proof putty powder.
By solid-to-liquid ratio 20:7, it is stirred mixing with water by the Internal wall water-fast putty powder of above-mentioned preparation, after standing 7min, then
Stirring 2min, can criticize and scrape use, criticizes and scrapes on the interior wall after cleaning out, and the amount of blade coating is 0.7kg/m2, painting to be doctored completes
After so that it is natural air drying, and it is detected, when 23h, the clearance of its PARA FORMALDEHYDE PRILLS(91,95) reaches 95%, the clearance of toluene
Reach 43.5%, and its resistance to water (96h) is without exception.
Example 2
Count the most by weight, take 43 parts of Radix et Caulis Opuntiae Dilleniis, 30 parts of distilled water, 22 parts of Radix Scutellariaes, 10 parts of Resina persicaes, 7 parts of caseins and 8 parts
Distiller grains, put in pulverizer, pulverize 40min with 1200r/min, collect crushed mixture and put in fermentation tank, add pulverizing
The lactobacillus powder of mixture quality 4%, stirs, and design temperature is 35 DEG C, sealing and fermenting tank, with 110r/min stirring fermentation
2 days；After above-mentioned fermentation ends, collect the fermenting mixture in fermentation tank, and by solid-to-liquid ratio 1:4, with mass fraction 65% second
Alcoholic solution mix homogeneously, then be placed in reflux, at 62 DEG C of reflux 1h, the most while hot filtration under diminished pressure, collect filtrate, juxtaposition
In cold room, standing 30min at 5 DEG C, the filtrate after standing is put in centrifuge, with 2000r/min centrifugation
10min, collects supernatant；Count the most by weight, take 50 parts of above-mentioned supernatant, 31 parts of Vermiculitums, 22 parts of diatom oozes and 8 parts of fibres
Dimension element ether, stirs, and heats it, be heated to 70 DEG C, with 130r/min agitating heating 8h, naturally cool to room subsequently
Temperature, places in liquid nitrogen flash freezer machine, and design temperature is-20 DEG C, freezing processing 4min, collects frozen material；The most by weight
Meter, takes 40 parts of above-mentioned frozen materials, 12 parts of ground calcium carbonate, 2 parts of solid contents are the polyvinyl acetate emulsion of 10%, 1 part of water and 1 part
Carboxymethyl cellulose sodium, stirs, at 35 DEG C stand 1h, environment-friendly type inner wall water-proof putty powder.
By solid-to-liquid ratio 20:7, it is stirred mixing with water by the Internal wall water-fast putty powder of above-mentioned preparation, after standing 10min,
Being stirred for 2min, can criticize and scrape use, criticize and scrape on the interior wall after cleaning out, the amount of blade coating is 0.8kg/m2, to be doctored it is painted with
Cheng Hou so that it is natural air drying, and it is detected, when 24h, the extraction efficiency of its PARA FORMALDEHYDE PRILLS(91,95) reaches 94.5%, going of toluene
Except rate reaches 43%, and its resistance to water (96h) is without exception.
Example 3
Count the most by weight, take 44 parts of Radix et Caulis Opuntiae Dilleniis, 31 parts of distilled water, 23 parts of Radix Scutellariaes, 12 parts of Resina persicaes, 8 parts of caseins and 10
Part distiller grains, put in pulverizer, pulverize 45min with 1300r/min, collect crushed mixture and put in fermentation tank, add powder
The lactobacillus powder of broken mixture quality 5%, stirs, and design temperature is 37 DEG C, sealing and fermenting tank, sends out with 110r/min stirring
Ferment 2 days；After above-mentioned fermentation ends, collect the fermenting mixture in fermentation tank, and by solid-to-liquid ratio 1:4, with mass fraction 65%
Ethanol solution mix homogeneously, then be placed in reflux, at 65 DEG C of reflux 2h, the most while hot filtration under diminished pressure, collect filtrate, and
Being placed in cold room, stand 35min at 7 DEG C, the filtrate after standing is put in centrifuge, with 2000r/min centrifugation
12min, collects supernatant；Count the most by weight, take 52 parts of above-mentioned supernatant, 32 parts of Vermiculitums, 23 parts of diatom oozes and 9 parts of fibres
Dimension element ether, stirs, and heats it, be heated to 80 DEG C, with 130r/min agitating heating 7h, naturally cool to room subsequently
Temperature, places in liquid nitrogen flash freezer machine, and design temperature is-15 DEG C, freezing processing 5min, collects frozen material；The most by weight
Meter, takes 42 parts of above-mentioned frozen materials, 13 parts of ground calcium carbonate, 3 parts of solid contents are the polyvinyl acetate emulsion of 10%, 2 parts of water and 1 part
Carboxymethyl cellulose sodium, stirs, at 37 DEG C stand 1h, environment-friendly type inner wall water-proof putty powder.
By solid-to-liquid ratio 20:7, it is stirred mixing with water by the Internal wall water-fast putty powder of above-mentioned preparation, after standing 5min, then
Stirring 1min, can criticize and scrape use, criticizes and scrapes on the interior wall after cleaning out, and the amount of blade coating is 0.6kg/m2, painting to be doctored completes
After so that it is natural air drying, and it is detected, when 22h, the clearance of its PARA FORMALDEHYDE PRILLS(91,95) reaches 94.8%, the removal of toluene
Rate reaches 43%, and its resistance to water (96h) is without exception.
Claims (1)
1. the preparation method of an environment-friendly type inner wall water-proof putty powder, it is characterised in that concrete preparation process is:
(1) count by weight, take 43～46 parts of Radix et Caulis Opuntiae Dilleniis, 30～32 parts of distilled water, 22～24 parts of Radix Scutellariaes, 10～13 parts of Fructus Persicae
Glue, 7～9 parts of caseins and 8～11 parts of distiller grains, put in pulverizer, pulverizes 40～50min with 1200～1500r/min, collects
Crushed mixture is put in fermentation tank, adds crushed mixture quality 4～the lactobacillus powder of 8%, stirs, design temperature
Being 35～38 DEG C, sealing and fermenting tank, with 110r/min stirring fermentation 2～3 days；
(2) after above-mentioned fermentation ends, the fermenting mixture in fermentation tank is collected, and by solid-to-liquid ratio 1:4, with mass fraction 65%
Ethanol solution mix homogeneously, then be placed in reflux, at 62～66 DEG C of backflows 1～3h, filtration under diminished pressure the most while hot, collected
Filtrate, is placed in cold room, stands 30～50min at 5～10 DEG C, and the filtrate after standing is put in centrifuge, with
2000r/min centrifugation 10～15min, collects supernatant；
(3) count by weight, take 50～55 parts of above-mentioned supernatant, 31～33 parts of Vermiculitums, 22～24 parts of diatom oozes and 8～10 parts
Cellulose ether, stirs, and heats it, is heated to 70～90 DEG C, with 130r/min agitating heating 4～8h, natural subsequently
Being cooled to room temperature, place in liquid nitrogen flash freezer machine, design temperature is-20～-10 DEG C, freezing processing 4～6min, collects freezing
Thing；
(4) count by weight, take 40～45 parts of above-mentioned frozen materials, 12～14 parts of ground calcium carbonate, 2～5 parts of solid contents are
The polyvinyl acetate emulsion of 10%, 1～3 part of water and 1～2 part of Carboxymethyl cellulose sodium, stir, and stands at 35～40 DEG C
1～2h, environment-friendly type inner wall water-proof putty powder.
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| CN201610672650.XA CN106046906A (en) | 2016-08-16 | 2016-08-16 | Preparation method of environmentally friendly interior wall waterproof putty powder |
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| CN201610672650.XA CN106046906A (en) | 2016-08-16 | 2016-08-16 | Preparation method of environmentally friendly interior wall waterproof putty powder |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106905745A (en) * | 2017-03-28 | 2017-06-30 | 柳州智美装饰工程有限责任公司 | A kind of powder of lacquer putty for use on |
| CN108948885A (en) * | 2018-06-22 | 2018-12-07 | 安徽索亚装饰材料有限公司 | A kind of preparation method of high rigidity purification air wall paper-based membrane |
| CN110982310A (en) * | 2019-12-30 | 2020-04-10 | 贵州安凯达实业股份有限公司 | Method for preparing fireproof coating by taking construction waste as raw material |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1458202A (en) * | 2003-01-14 | 2003-11-26 | 上海大学 | Water inner wall mastic for building and its preparing method |
| CN105273483A (en) * | 2015-11-14 | 2016-01-27 | 苏州大乘环保建材有限公司 | Multi-model paste putty and preparation method thereof |
| CN105754396A (en) * | 2016-04-25 | 2016-07-13 | 李德新 | Putty powder and preparing method thereof |
-
2016
- 2016-08-16 CN CN201610672650.XA patent/CN106046906A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1458202A (en) * | 2003-01-14 | 2003-11-26 | 上海大学 | Water inner wall mastic for building and its preparing method |
| CN105273483A (en) * | 2015-11-14 | 2016-01-27 | 苏州大乘环保建材有限公司 | Multi-model paste putty and preparation method thereof |
| CN105754396A (en) * | 2016-04-25 | 2016-07-13 | 李德新 | Putty powder and preparing method thereof |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106905745A (en) * | 2017-03-28 | 2017-06-30 | 柳州智美装饰工程有限责任公司 | A kind of powder of lacquer putty for use on |
| CN108948885A (en) * | 2018-06-22 | 2018-12-07 | 安徽索亚装饰材料有限公司 | A kind of preparation method of high rigidity purification air wall paper-based membrane |
| CN110982310A (en) * | 2019-12-30 | 2020-04-10 | 贵州安凯达实业股份有限公司 | Method for preparing fireproof coating by taking construction waste as raw material |
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Application publication date: 20161026 |
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