CN106045781A - Method for preparing liquid fertilizers from pig-farm cultivating waste liquid - Google Patents

Method for preparing liquid fertilizers from pig-farm cultivating waste liquid Download PDF

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Publication number
CN106045781A
CN106045781A CN201610387051.3A CN201610387051A CN106045781A CN 106045781 A CN106045781 A CN 106045781A CN 201610387051 A CN201610387051 A CN 201610387051A CN 106045781 A CN106045781 A CN 106045781A
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CN
China
Prior art keywords
liquid
pig farm
waste liquid
fertilizer
cultivation
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Pending
Application number
CN201610387051.3A
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Chinese (zh)
Inventor
沈建平
钟哲科
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ZHEJIANG HUATENG ANIMAL HUSBANDRY Ltd Co
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ZHEJIANG HUATENG ANIMAL HUSBANDRY Ltd Co
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Priority to CN201610387051.3A priority Critical patent/CN106045781A/en
Publication of CN106045781A publication Critical patent/CN106045781A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05FORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F17/00Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05FORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F11/00Other organic fertilisers
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/80Soil conditioners
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/40Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Soil Sciences (AREA)
  • Biochemistry (AREA)
  • Biotechnology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Microbiology (AREA)
  • Molecular Biology (AREA)
  • Fertilizers (AREA)

Abstract

The invention discloses a method for preparing liquid fertilizers from pig-farm cultivating waste liquid. The method includes the following steps that the pig-farm cultivating waste liquid obtained after dry-wet separation is collected, and liquid with the chemical oxygen demand smaller than 1,800 mg/l and the dry basis content smaller than or equal to 3% is obtained with a flocculence method; molasses with the weight accounting for 2% to 6% of the weight of the liquid is added into the liquid, and the pH value is adjusted to be 6 to 7.5; a fermenting functional bacterium solution is added, the mixture is stirred to be even, placed into a sealed container and placed into an incubator at the temperature of 35 DEG C, cultivating is carried out for 1 week to 2 weeks, a cover of the sealed container is opened once a day for ventilation and stirred till the pH is reduced to be smaller than 4, and fermented liquid is obtained; the fermented liquid is filtered and sieved with a 300-mesh sieve, and filtration liquid is kept; KOH of 0.1% to 0.3% is added to adjust the pH of the liquid to be 6 to 7. Due to the fermenting method, sundry bacteria are killed through beneficial microorganism populations; meanwhile, the characteristic that nutrient elements of nitrogen, phosphorus and the like contained in the cultivating waste liquid are high is sufficiently used, the liquid fertilizers are prepared, the treating cost is low, and effects are good.

Description

A kind of method utilizing pig farm cultivation waste liquid to make Liquid Fertilizer
Technical field
The present invention relates to a kind of pig farm breeding waste processing method, utilize pig farm cultivation waste liquid to make particularly to one The method of Liquid Fertilizer.
Background technology
Pig-breeding industry is in a flourish stage, and current China has evolved into Carnis Sus domestica big producing country of the world One of.China intensive industrialized piggery high speed development, if but aquaculture produce a large amount of garbages fail to deal carefully with in time, exceed Around, the detergent power of natural environment, it is possible to a series of problem of environmental pollution occurs.Livestock and poultry cultivation produces produced dirty Dye thing discharge has become one of most important agricultural pollution source of China, and production, living environment to plant's periphery cause pole Big harm.
The warps such as excrement that pig farm garbage generally refers to produce during pig-breeding, urine, sewage, residual feed, bedding and padding The liquid portion obtained after crossing separating dry space from moist space equipment contains higher antibacterial, virus, and the risk of environmental pollution is big, and processing cost is high.
Summary of the invention
The present invention is to solve defect and deficiency that above-mentioned prior art exists, it is provided that one utilizes pig farm to cultivate waste liquid The method making Liquid Fertilizer, uses the way of fermentation, utilizes beneficial microbe population to kill miscellaneous bacteria, meanwhile, make full use of cultivation The feature that in waste liquid, the nutrient element such as nitrogenous, phosphorus is higher, makes Liquid Fertilizer, and processing cost is low, effective.
The technical solution adopted for the present invention to solve the technical problems is: one utilizes pig farm cultivation waste liquid to make Liquid Fertilizer Method, comprise the following steps:
A, by pig farm breeding waste separating dry space from moist space, collect the cultivation of the pig farm after separating dry space from moist space waste liquid, use flocculation Method obtains COD less than 1800mg/l, the contents on dry basis liquid less than 3%;
B, add in aforesaid liquid and account for the molasses of liquid weight 2-6%, regulation pH value to 6-7.5;
C, addition Fermentation Function bacterium solution, stir, and is placed in sealing container, is placed in 35 DEG C of incubators cultivation 1-2 In week, the venting of sealing article handling once and is stirred, until pH drops to less than 4, is obtained fermentation liquid by every day;
D, above-mentioned fermentation liquid filter, and cross 300 mesh sieves, stay cleaner liquid, using the solid portion of separation as SOLID ORGANIC Fertilizer, the liquid portion of separation is through high temperature sterilize;
E, add the KOH of 0.1-0.3%, the pH to 6-7 of regulation liquid;
F, the above-mentioned liquid through KOH regulation both can be directly used as Liquid Fertilizer, it is also possible to as one of Liquid Fertilizer raw material, add Add other nutrient element, make various Liquid Fertilizer.
The innovative point of the present invention is: 1. using molasses regulation pH, play multi-effect, the pH of stock solution is typically at 8.5- 10.5, be not suitable for doing liquid fertilizer, and cane molasses pH is less than 6, therefore, is good regulator;2, cane molasses self has very Many nutritional labelings, can do Liquid Fertilizer;3. cane molasses can promote the Fast-propagation of EM, uses the method for EM fermentation to kill through a step Extremely, contain some pathogenic bacterias, worm's ovum, manufacture clean nutritional solution, increase available nutrient content in liquid;4. use doing of fermentation Method, utilizes beneficial microbe population to kill miscellaneous bacteria, meanwhile, makes full use of the nutrient element such as nitrogenous, phosphorus in cultivation waste liquid higher Feature, makes Liquid Fertilizer, and processing cost is low, effective.
As preferably, the flocculant that described flocculence uses is PAMC, and consumption accounts for pig farm cultivation waste liquid The 0.01-0.05% of weight.
As preferably, described molasses are cane molasses, and pH value is 4-6.
As preferably, Fermentation Function bacterium solution is EM bacterium solution, and bacterium solution bacterium number content is no less than 1,000,000,000/milliliter, and addition is The 0.3-0.5% of total liquid volume.
The invention has the beneficial effects as follows: use the way of fermentation, utilize beneficial microbe population to kill miscellaneous bacteria, fill meanwhile Point utilizing the feature that in cultivation waste liquid, the nutrient element such as nitrogenous, phosphorus is higher, make Liquid Fertilizer, processing cost is low, effective.
Detailed description of the invention
The detailed description of the invention of the present invention is as follows:
Embodiment 1: a kind of method utilizing pig farm cultivation waste liquid to make Liquid Fertilizer, comprises the following steps:
A, by pig farm breeding waste separating dry space from moist space, collect the cultivation of the pig farm after separating dry space from moist space waste liquid, use flocculation Method obtains COD less than 1800mg/l, contents on dry basis be 3% the flocculant that uses of liquid wherein flocculence for sun from Sub-polyacrylamide, consumption accounts for the 0.02% of pig farm cultivation waste liquid weight;
B, adding account for the cane molasses of liquid weight 2% in aforesaid liquid, regulation pH value is to 6;
C, addition EM bacterium solution, stir, and is placed in sealing container, is placed in 35 DEG C of incubators cultivation 1-2 week, every day The venting of sealing article handling once and being stirred, until pH drops to less than 4, obtain fermentation liquid, wherein EM bacterium solution bacterium number content is not Less than 1,000,000,000/milliliter, addition is the 0.3-0.5% of total liquid volume;
D, above-mentioned fermentation liquid filter, and cross 300 mesh sieves, stay cleaner liquid, using the solid portion of separation as SOLID ORGANIC Fertilizer, the liquid portion of separation is through high temperature sterilize;
E, the KOH adding 0.1%, the pH to 6-7 of regulation liquid;
F, the above-mentioned liquid through KOH regulation both can be directly used as Liquid Fertilizer, it is also possible to as one of Liquid Fertilizer raw material, add Add other nutrient element, make various Liquid Fertilizer.
Embodiment 2: a kind of method utilizing pig farm cultivation waste liquid to make Liquid Fertilizer, comprises the following steps:
A, by pig farm breeding waste separating dry space from moist space, collect the cultivation of the pig farm after separating dry space from moist space waste liquid, use flocculation Method obtains COD less than 1800mg/l, contents on dry basis be 2% the flocculant that uses of liquid wherein flocculence for sun from Sub-polyacrylamide, consumption accounts for the 0.05% of pig farm cultivation waste liquid weight;
B, adding account for the cane molasses of liquid weight 6% in aforesaid liquid, regulation pH value is to 7.5;
C, addition EM bacterium solution, stir, and is placed in sealing container, is placed in 35 DEG C of incubators cultivation 1-2 week, every day The venting of sealing article handling once and being stirred, until pH drops to less than 4, obtain fermentation liquid, wherein EM bacterium solution bacterium number content is not Less than 1,000,000,000/milliliter, addition is the 0.3-0.5% of total liquid volume;
D, above-mentioned fermentation liquid filter, and cross 300 mesh sieves, stay cleaner liquid, using the solid portion of separation as SOLID ORGANIC Fertilizer, the liquid portion of separation is through high temperature sterilize;
E, the KOH adding 0.3%, the pH to 6-7 of regulation liquid;
F, the above-mentioned liquid through KOH regulation both can be directly used as Liquid Fertilizer, it is also possible to as one of Liquid Fertilizer raw material, add Add other nutrient element, make various Liquid Fertilizer.
Embodiment 3: a kind of method utilizing pig farm cultivation waste liquid to make Liquid Fertilizer, comprises the following steps:
A, by pig farm breeding waste separating dry space from moist space, collect the cultivation of the pig farm after separating dry space from moist space waste liquid, use flocculation Method obtains COD less than 1800mg/l, contents on dry basis be 3% the flocculant that uses of liquid wherein flocculence for sun from Sub-polyacrylamide, consumption accounts for the 0.03% of pig farm cultivation waste liquid weight;
B, adding account for the cane molasses of liquid weight 4% in aforesaid liquid, regulation pH value is to 7;
C, addition EM bacterium solution, stir, and is placed in sealing container, is placed in 35 DEG C of incubators cultivation 1-2 week, every day The venting of sealing article handling once and being stirred, until pH drops to less than 4, obtain fermentation liquid, wherein EM bacterium solution bacterium number content is not Less than 1,000,000,000/milliliter, addition is the 0.3-0.5% of total liquid volume;
D, above-mentioned fermentation liquid filter, and cross 300 mesh sieves, stay cleaner liquid, using the solid portion of separation as SOLID ORGANIC Fertilizer, the liquid portion of separation is through high temperature sterilize;
E, the KOH adding 0.2%, the pH to 6-7 of regulation liquid;
F, the above-mentioned liquid through KOH regulation both can be directly used as Liquid Fertilizer, it is also possible to as one of Liquid Fertilizer raw material, add Add other nutrient element, make various Liquid Fertilizer.
The Liquid Fertilizer product composition of the present invention is analyzed as follows:
Through inspection in product, without pathogenic bacteria and worm's ovum.
Embodiment described above is the one preferably scheme of the present invention, not makees the present invention any pro forma Limit, on the premise of without departing from the technical scheme described in claim, also have other variant and remodeling.

Claims (4)

1. one kind utilizes the method that pig farm cultivation waste liquid makes Liquid Fertilizer, it is characterised in that comprise the following steps:
A, by pig farm breeding waste separating dry space from moist space, collect the cultivation of the pig farm after separating dry space from moist space waste liquid, use flocculence to obtain To COD less than 1800mg/l, the contents on dry basis liquid less than 3%;
B, add in aforesaid liquid and account for the molasses of liquid weight 2-6%, regulation pH value to 6-7.5;
C, addition Fermentation Function bacterium solution, stir, and is placed in sealing container, is placed in 35 DEG C of incubators cultivation 1-2 week, often The venting of sealing article handling once and is stirred by it, until pH drops to less than 4, obtains fermentation liquid;
D, above-mentioned fermentation liquid filter, and cross 300 mesh sieves, stay cleaner liquid, using the solid portion of separation as solid organic fertilizer, point From liquid portion through high temperature sterilize;
E, add the KOH of 0.1-0.3%, the pH to 6-7 of regulation liquid;
F, the above-mentioned liquid through KOH regulation both can be directly used as Liquid Fertilizer, it is also possible to as one of Liquid Fertilizer raw material, add it Its nutrient element, makes various Liquid Fertilizer.
A kind of method utilizing pig farm cultivation waste liquid to make Liquid Fertilizer the most according to claim 1, it is characterised in that described The flocculant that flocculence uses is PAMC, and consumption accounts for the 0.01-0.05% of pig farm cultivation waste liquid weight.
A kind of method utilizing pig farm cultivation waste liquid to make Liquid Fertilizer the most according to claim 1, it is characterised in that described Molasses are cane molasses, and pH value is 4-6.
A kind of method utilizing pig farm cultivation waste liquid to make Liquid Fertilizer the most according to claim 1, it is characterised in that fermentation Function bacterium solution is EM bacterium solution, and bacterium solution bacterium number content is no less than 1,000,000,000/milliliter, and addition is the 0.3-0.5% of total liquid volume.
CN201610387051.3A 2016-06-01 2016-06-01 Method for preparing liquid fertilizers from pig-farm cultivating waste liquid Pending CN106045781A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111646832A (en) * 2020-06-30 2020-09-11 郭云征 Biological organic liquid manure reaction tank, treatment system and treatment method

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1912102A (en) * 2006-08-28 2007-02-14 山东西王糖业有限公司 Method for producing fodde yeast using corn soaking water
CN101974428A (en) * 2010-09-30 2011-02-16 北京意科乐生态科技有限公司 Complex microbial preparation capable of resisting replant obstacle resistance and preparation method thereof
CN105503282A (en) * 2016-01-05 2016-04-20 国家林业局竹子研究开发中心 Method for preparing liquid manure from piggery cultivation waste in zero-release mode

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1912102A (en) * 2006-08-28 2007-02-14 山东西王糖业有限公司 Method for producing fodde yeast using corn soaking water
CN101974428A (en) * 2010-09-30 2011-02-16 北京意科乐生态科技有限公司 Complex microbial preparation capable of resisting replant obstacle resistance and preparation method thereof
CN105503282A (en) * 2016-01-05 2016-04-20 国家林业局竹子研究开发中心 Method for preparing liquid manure from piggery cultivation waste in zero-release mode

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111646832A (en) * 2020-06-30 2020-09-11 郭云征 Biological organic liquid manure reaction tank, treatment system and treatment method

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Application publication date: 20161026

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