CN105997628A

CN105997628A - Moisturizing and anti-aging cosmetic containing agaric extract and preparation method of cosmetic

Info

Publication number: CN105997628A
Application number: CN201610345909.XA
Authority: CN
Inventors: 杨广群; 李菊芳; 陈鹏辉
Original assignee: Guangzhou Danqi Daily Chemical Co Ltd
Current assignee: Guangzhou Danqi Daily Chemical Co Ltd
Priority date: 2016-05-21
Filing date: 2016-05-21
Publication date: 2016-10-12

Abstract

The invention relates to the field of cosmetics, in particular to a moisturizing and anti-aging cosmetic containing an agaric extract and a preparation method of the cosmetic. The cosmetic is prepared from the following components: 5 to 15 parts of agaric extract, 0.6 to 3.2 parts of vitamin, 1 to 5 parts of antioxidant, 3 to 12 parts of anti-wrinkle activator, 1 to 3 parts of sun-screening agent, 0.5 to 2 parts of anti-allergy agent, 2.5 to 6 parts of skin whitening agent, 2 to 12 parts of moisturizing agent, 0.03 to 0.2 part of potassium hydroxide, 0.5 to 2 parts of acer truncatum seed oil, 0.3 to 1.2 parts of chelating agent, 0.1 to 0.3 part of thickening agent, 1.5 to 5.8 parts of emulgator, 0.2 to 1 part of preservative and 40 to 80 parts of deionized water. The cosmetic may be specifically prepared into repairing cream, repairing emulsion, essence cream or other products. The cosmetic disclosed by the invention has the beneficial effects of effectively improving the skin elasticity, delaying skin aging, improving skin color to achieve a skin whitening effect after insisting on using, preventing an allergy phenomenon with the addition of the anti-allergy agent, eliminating heavy metal pollution by chelation of heavy metal, relieving wrinkles, improving the skin and improving the brightness and the whitening degree of skin.

Description

Moisturizing defying age class cosmetics containing Auricularia extract and preparation method thereof

Technical field

The present invention relates to cosmetic field, be specially containing Auricularia extract moisturizing defying age class cosmetics and Preparation method.

Background technology

Aging is a kind of naturally process, and this was made explaining of comparison system by the natural-crosslinked theory of biomolecule State.This theory is pointed out when proving the molecular mechanism of Systemic aging: organism is a unstable chemistry System, belongs to dissipative structure.In system, various biomolecule have substantial amounts of reactive group, they inevitable phases Interaction generation chemical reaction makes biomolecule slowly cross-link to tend to chemically active stable.Over time Passage, crosslinking degree is continuously increased, and the reactive group of biomolecule constantly consumes minimizing, and original molecule is tied Structure gradually changes, and the accumulation Hui Shi biological tissue of these changes engenders aging phenomenon.Heavy metal is skin The first old and feeble killer is accelerated with health.The most a lot of cosmetic kinds are all added with smoothing wrinkle aging ingredient.

Chinese patent storehouse discloses preparation method and the whitening anti-aging of a kind of Cistanche Tubulosa extract Cosmetic (CN201210064589.2), the preparation method of described Cistanche Tubulosa extract includes pulverizing, slightly Extract, be centrifuged crude extract collecting and eluting, drying after standing, obtain Cistanche Tubulosa and carry Take thing.This preparation method is simple and pollution-free, content >=25% of the echinacoside of described extract, Mao Rui Content >=55% of flower glucosides, total glycosides content >=80%；The Cistanche Tubulosa extract warp that the method is prepared After crossing the test of antioxidant activity etc., it was demonstrated that Cistanche Tubulosa extract has an antioxidation, whitening, anti-ageing Old effect.It is added to cosmetics and prepares whitening anti-aging cosmetics, and cosmetics are carried out cell toxicant Property and the test such as safety, demonstrate the safe and non-stimulating of cosmetics and there is good whitening effect.

Chinese patent storehouse discloses a kind of defying age, wrinkle removing anti-wrinkle cosmetic composition (CN200810233779.6) it is, by Ganoderma extract, Radix Agrimoniae extract, Radix Arnebiae extract, Flos Camelliae Japonicae Flower extract, chamomile extract, Semen Ginkgo extrac and other cosmetic bases composition, above extract divides Not accounting for composition total weight proportioning is 1%-20%.The dosage form of compositions can select cosmetic water, skin moistening Emulsion, cream, essence, massage cream, eye cream, gelatinous product.The present invention is to select safety non-pollution Green cosmetic material, there is natural, nontoxic, nonirritant, have no side effect and effectively defying age, go Wrinkle crease-resistant effect, meet people's requirement to cosmetics safety.

At present, the smoothing wrinkle anti-aging effects of moisturizing defying age class cosmetics is inconspicuous on the market, and improper use Easily accelerate wrinkle to occur.Therefore, select which kind of plant, and by its safety be applied in cosmetics reach Preferably prevent and treat acne effect, be problem demanding prompt solution.

Summary of the invention

For the problems referred to above, it is an object of the invention to provide the moisturizing defying age class cosmetics containing Auricularia extract And preparation method thereof, by Auricularia extract, vitamin, sunscreen, antioxidant, crease-resistant activating agent, resist Quick dose, whitening agent, wetting agent, PH conditioner, thickening agent, chelating agen, emulsifying agent, preservative and water are logical Cross series of process flow process and be formed with the cosmetic combinations of good moisturizing defying age effectiveness, specifically can be made into reparation The products such as frost, reparation breast, essence cream.

To achieve these goals, the present invention uses below scheme

According to the first aspect of the invention, it is provided that the moisturizing defying age class cosmetics containing Auricularia extract, by weight Amount part meter, including following components: Auricularia extract 5-15 part, vitamin 0.6-3.2 part, antioxidant 1-5 Part, crease-resistant activating agent 3-12 part, sunscreen 1-3 part, anti-sensitizer 0.5-2 part, whitening agent 2.5-6 part, guarantor Humectant 2-12 part, potassium hydroxide 0.03-0.2 part, Acer Truncatum Buge seed oil 0.5-2 part, chelating agen 0.3-1.2 part, Thickening agent 0.1-0.3 part, emulsifying agent 1.5-5.8 part, preservative 0.2-1 part, deionized water 40-80 part.

Preferably, described antioxidant be weight part ratio be (1-3): the tocopherol of (2-5) and tea-seed The mixture of oil.

Preferably, described crease-resistant activating agent be weight part ratio be (1-3): (1-2.5): (0.6-1.8): (1-3.5) polysaccharide/hydrolytic collagen, beta glucan, Semen Vitis viniferae extracting solution and the mixture of red wine polyphenols.

Preferably, described sunscreen be weight part ratio be (1-3): (2-4): the adjacent ammonia of (1.5-4) The mixture of yl benzoic acid ester, cinnamate derivative and camphor derivative.

Preferably, described anti-sensitizer be weight part ratio be (1-2.5): the glycyrrhizic acid dipotassium of (1.5-4), The mixture of tea tree ethereal oil.

Preferably, described whitening agent be weight part ratio be (1-2.5): (2-4): (0.3-1.2): (0.5-2.4) licoflavone, phloretin, Semen Citri grandis extract and the mixture of Folium Mori extract.

Preferably, described wetting agent be weight part ratio be (3-10): (2-8): (0.1-3): (0.1-0.6) Glycerol, Semen Maydis propylene glycol, reed fragrant plant oil and the mixture of oligofructose.

Preferably, described emulsifying agent be weight part ratio be (1-3): (1-3): (0.5-3): (0.8-3) Glyceryl stearate/PEG-100 stearate, cetearyl alcohol olive oil acid esters/Pyrusussuriensis smooth Fructus Canarii albi oleic acid Ester, methyl sesquistearate and acrylic acid (ester) class/C10-30 alcohol acrylate crosspolymers potassium The mixture of salt.

Preferably, described preservative be weight part ratio be (3-5): the sodium benzoate of (2-4), oxybenzene third Ester admixture.

According to the second aspect of the invention, it is provided that the preparation of the moisturizing defying age class cosmetics containing Auricularia extract Method, it comprises the following steps:

(1) emulsifying agent, antioxidant and Acer Truncatum Buge seed oil are put in oil phase pot successively, be heated to 70-85 DEG C, wait all components to be incubated after melting, prepare A phase；

(2) by vitamin, crease-resistant activating agent, sunscreen, anti-sensitizer, whitening agent, wetting agent, chelating Agent, thickening agent and deionized water put in emulsifying pot successively, are heated to 70-85 DEG C, and insulation 15-30m makes it Fully dissolve, prepare B phase；

(3) the B phase that A phase step (1) prepared and step (2) prepare is pumped in homogenizer successively, Homogenizing 5-15 minute, stir speed (S.S.) is 2000-4000rpm, then insulated and stirred 15-45m, and stir speed (S.S.) is 30-50rpm；

(4) emulsion in step (3) is cooled to 40-45 DEG C, adds potassium hydroxide, stir；

(5) add Auricularia extracting solution and preservative, stir, obtain moisturizing defying age class cosmetics group Compound.

The invention has the beneficial effects as follows: be effectively improved skin elasticity, delay skin aging；Improve the colour of skin, Adhere to that use has whitening effect；Increase anti-sensitizer, prevent allergic phenomena；Chelating heavy metal, eliminates heavy metal Pollute；Releive wrinkle, improve skin, improve brightness and the fairness of skin.

Detailed description of the invention

For the problems referred to above, it is an object of the invention to provide the moisturizing defying age class cosmetics containing Auricularia extract And preparation method thereof, by Auricularia extract, vitamin, sunscreen, antioxidant, crease-resistant activating agent, resist Quick dose, whitening agent, wetting agent, PH conditioner, chelating agen, thickening agent, emulsifying agent, preservative and water are logical Cross series of process flow process and be formed with the cosmetic combinations of good moisturizing defying age effectiveness, specifically can be made into reparation The products such as frost, reparation breast, essence cream.

To achieve these goals, the present invention uses below scheme

Auricularia can reduce the formation of lipid peroxidation product lipofuscin by fall plasma cholesterol, thin to safeguard The homergy of born of the same parents, shows delaying senility function.Use chemiluminometry, have studied 2.5% black wood Ear water extract 50 μ l, 800 μ l, 1000 μ l are to H2O2 or by enzyme system and the super oxygen of non-enzyme system generation Compound free radical (O-2) has scavenging action, in dose-effect relationship between Scavenging activity and consumption, shows black wood Ear water extract contains the composition of Wheat Protein.

For the technical scheme making those skilled in the art be better understood from the application, below in conjunction with reality Execute example technical scheme is clearly and completely described, it is clear that described embodiment is only Being only a part of embodiment of the application, based on the embodiment in the application, those of ordinary skill in the art exist Do not make the every other embodiment obtained under creative work premise, all should belong to the application protection Scope.

Embodiment 1

Moisturizing defying age class cosmetics containing Auricularia extract, by weight, including following components: Auricularia Extract 5 parts, vitamin 1.2 parts, tocopherol 0.6 part, tea-seed oil 1.5 parts, polysaccharide/hydrolytic collagen 1.8 Part, beta glucan 2.3 parts, Semen Vitis viniferae extracting solution 1.2 parts, red wine polyphenols 2 parts, o-aminobenzoa 0.8 Part, cinnamate derivative 1.5 parts, camphor derivative 0.8 part, glycyrrhizic acid dipotassium 0.4 part, tea tree ethereal oil 0.6 Part, licoflavone 1.5 parts, phloretin 2 parts, Semen Citri grandis extract 0.8 part, Folium Mori extract 1.2 parts, glycerol 5 parts, Semen Maydis propylene glycol 4 parts, reed fragrant plant oil 2.6 parts, oligofructose 0.05 part, potassium hydroxide 0.15 part, unit Precious maple seed oil 0.7 part, chelating agen 0.5 part, thickening agent 0.15 part, glyceryl stearate/PEG-100 stearic acid Ester 1.5 parts, cetearyl alcohol olive oil acid esters/Pyrusussuriensis smooth olive oil acid esters 1.6 parts, methyl times semihard Fat acid ester 2 parts, acrylic acid (ester) class/C10-30 alcohol acrylate crosspolymers potassium salt 0.8 part, benzoic acid 0.3 part of sodium, propyl hydroxybenzoate 0.2 part, deionized water 70 parts.

Embodiment 2

Moisturizing defying age class cosmetics containing Auricularia extract, by weight, including following components: Auricularia Extract 10 parts, vitamin 1.5 parts, tocopherol 1 part, tea-seed oil 1.2 parts, polysaccharide/hydrolytic collagen 1.5 Part, beta glucan 2.6 parts, Semen Vitis viniferae extracting solution 0.8 part, red wine polyphenols 2.2 parts, o-aminobenzoa 0.8 part, cinnamate derivative 1.2 parts, camphor derivative 1.1 parts, glycyrrhizic acid dipotassium 0.4 part, tea tree ethereal oil 0.8 part, licoflavone 1.3 parts, phloretin 1.8 parts, Semen Citri grandis extract 0.8 part, Folium Mori extract 1.2 parts, Glycerol 5.5 parts, Semen Maydis propylene glycol 3.2 parts, reed fragrant plant oil 2.4 parts, oligofructose 0.05 part, potassium hydroxide 0.15 Part, Acer Truncatum Buge seed oil 0.8 part, chelating agen 0.45 part, thickening agent 0.15 part, glyceryl stearate/PEG-100 Stearate 1.5 parts, cetearyl alcohol olive oil acid esters/Pyrusussuriensis smooth olive oil acid esters 1.6 parts, methyl Sesquistearate 1.8 parts, acrylic acid (ester) class/C10-30 alcohol acrylate crosspolymers potassium salt 0.8 part, Sodium benzoate 0.3 part, propyl hydroxybenzoate 0.2 part, deionized water 60 parts.

Embodiment 3

Moisturizing defying age class cosmetics containing Auricularia extract, by weight, including following components: Auricularia Extract 15 parts, vitamin 1.2 parts, tocopherol 1.2 parts, tea-seed oil 1 part, polysaccharide/hydrolytic collagen 1.8 Part, beta glucan 2.5 parts, Semen Vitis viniferae extracting solution 1.2 parts, red wine polyphenols 1.6 parts, o-aminobenzoa 1.2 parts, cinnamate derivative 1.1 parts, camphor derivative 0.8 part, glycyrrhizic acid dipotassium 0.4 part, tea tree ethereal oil 0.6 part, licoflavone 1.5 parts, phloretin 2 parts, Semen Citri grandis extract 0.8 part, Folium Mori extract 0.8 part, Glycerol 6 parts, Semen Maydis propylene glycol 4 parts, reed fragrant plant oil 2 parts, oligofructose 0.05 part, potassium hydroxide 0.13 part, Acer Truncatum Buge seed oil 0.7 part, chelating agen 0.5 part, thickening agent 0.15 part, glyceryl stearate/PEG-100 are stearic Acid esters 1.5 parts, cetearyl alcohol olive oil acid esters/Pyrusussuriensis smooth olive oil acid esters 1.6 parts, methyl sesquialter Stearate 2 parts, acrylic acid (ester) class/C10-30 alcohol acrylate crosspolymers potassium salt 0.8 part, benzene first Acid 0.3 part of sodium, propyl hydroxybenzoate 0.2 part, deionized water 50 parts.

The preparation method of above-described embodiment 1-3 is as follows:

(1) by smooth to glyceryl stearate/PEG-100 stearate, cetearyl alcohol olive oil acid esters/Pyrusussuriensis Olive oil acid esters, methyl sesquistearate, acrylic acid (ester) class/C10-30 alcohol are acrylate cross linked Polymer potassium salt, tocopherol, tea-seed oil, Acer Truncatum Buge seed oil put in oil phase pot successively, are heated to 70-85 DEG C, wait all components to be incubated after melting, prepare A phase；

(2) by vitamin, polysaccharide/hydrolytic collagen, beta glucan, Semen Vitis viniferae extracting solution, red wine polyphenols, O-aminobenzoa, cinnamate derivative, camphor derivative, glycyrrhizic acid dipotassium, tea tree ethereal oil, Radix Glycyrrhizae Flavone, phloretin, Semen Citri grandis extract, Folium Mori extract, glycerol, Semen Maydis propylene glycol, reed fragrant plant are oily, oligomeric Fructose, thickening agent, chelating agen and deionized water put in emulsifying pot successively, are heated to 70-85 DEG C, insulation 15-30m makes it fully dissolve, and prepares B phase；

(5) it is sequentially added into Auricularia extracting solution, propyl hydroxybenzoate, propyl hydroxybenzoate, stirs, obtain moisturizing Defying age class cosmetic composition.

Comparative example 1

Vitamin 1.2 parts, tocopherol 0.6 part, tea-seed oil 1.5 parts, polysaccharide/hydrolytic collagen 1.8 parts, β- Glucosan 2.3 parts, Semen Vitis viniferae extracting solution 1.2 parts, red wine polyphenols 2 parts, o-aminobenzoa 0.8 part, meat Cinnamic acid esters 1.5 parts, camphor derivative 0.8 part, glycyrrhizic acid dipotassium 0.4 part, tea tree ethereal oil 0.6 part, sweet Straw colour ketone 1.5 parts, phloretin 2 parts, Semen Citri grandis extract 0.8 part, Folium Mori extract 1.2 parts, glycerol 5 parts, Semen Maydis propylene glycol 4 parts, reed fragrant plant oil 2.6 parts, oligofructose 0.05 part, potassium hydroxide 0.15 part, Acer Truncatum Buge seed Oil 0.7 part, chelating agen 0.5 part, thickening agent 0.15 part, glyceryl stearate/PEG-100 stearate 1.5 Part, cetearyl alcohol olive oil acid esters/Pyrusussuriensis smooth olive oil acid esters 1.6 parts, methyl sesquistearate 2 parts, acrylic acid (ester) class/C10-30 alcohol acrylate crosspolymers potassium salt 0.8 part, sodium benzoate 0.3 part, Propyl hydroxybenzoate 0.2 part, deionized water 70 parts.

Comparative example 2

Vitamin 1.5 parts, tocopherol 1 part, tea-seed oil 1.2 parts, polysaccharide/hydrolytic collagen 1.5 parts, β-Portugal Polysaccharide 2.6 parts, Semen Vitis viniferae extracting solution 0.8 part, red wine polyphenols 2.2 parts, o-aminobenzoa 0.8 part, meat Cinnamic acid esters 1.2 parts, camphor derivative 1.1 parts, glycyrrhizic acid dipotassium 0.4 part, tea tree ethereal oil 0.8 part, sweet Straw colour ketone 1.3 parts, phloretin 1.8 parts, Semen Citri grandis extract 0.8 part, Folium Mori extract 1.2 parts, glycerol 5.5 Part, Semen Maydis propylene glycol 3.2 parts, reed fragrant plant oil 2.4 parts, oligofructose 0.05 part, potassium hydroxide 0.15 part, unit Precious maple seed oil 0.8 part, chelating agen 0.45 part, thickening agent 0.15 part, glyceryl stearate/PEG-100 are stearic Acid esters 1.5 parts, cetearyl alcohol olive oil acid esters/Pyrusussuriensis smooth olive oil acid esters 1.6 parts, methyl sesquialter Stearate 1.8 parts, acrylic acid (ester) class/C10-30 alcohol acrylate crosspolymers potassium salt 0.8 part, benzene Sodium formate 0.3 part, propyl hydroxybenzoate 0.2 part, deionized water 60 parts.

Comparative example 3

Vitamin 1.2 parts, tocopherol 1.2 parts, tea-seed oil 1 part, polysaccharide/hydrolytic collagen 1.8 parts, β-Portugal Polysaccharide 2.5 parts, Semen Vitis viniferae extracting solution 1.2 parts, red wine polyphenols 1.6 parts, o-aminobenzoa 1.2 parts, meat Cinnamic acid esters 1.1 parts, camphor derivative 0.8 part, glycyrrhizic acid dipotassium 0.4 part, tea tree ethereal oil 0.6 part, sweet Straw colour ketone 1.5 parts, phloretin 2 parts, Semen Citri grandis extract 0.8 part, Folium Mori extract 0.8 part, glycerol 6 parts, Semen Maydis propylene glycol 4 parts, reed fragrant plant oil 2 parts, oligofructose 0.05 part, potassium hydroxide 0.13 part, Acer Truncatum Buge seed oil 0.7 part, chelating agen 0.5 part, thickening agent 0.15 part, glyceryl stearate/PEG-100 stearate 1.5 parts, Cetearyl alcohol olive oil acid esters/Pyrusussuriensis smooth olive oil acid esters 1.6 parts, methyl sesquistearate 2 parts, Acrylic acid (ester) class/C10-30 alcohol acrylate crosspolymers potassium salt 0.8 part, sodium benzoate 0.3 part, hydroxyl Phenylpropyl alcohol ester 0.2 part, deionized water 50 parts.

Measure of merit

Each embodiment and comparative example all select 100 people to try out.

Using method: the moisturizing anti-aging cream prepared by each embodiment and comparative example smears face and cervical region, often Day each 1 time sooner or later.

Efficacy assessment standard: user is moist, pale with rear face and the cervical region colour of skin, wrinkle reduces, Skin is glossy is effective.Result on trial: the user of embodiment 1～3 tries out effective percentage after 8 weeks continuously Reach 91%, the user of comparative example 1～3 try out continuously 8 weeks after effective percentage 45%.

Finally illustrate, above example only in order to technical scheme to be described and unrestricted, ability Other amendment or equivalents that technical scheme is made by territory those of ordinary skill, as long as not taking off From the spirit and scope of technical solution of the present invention, all should contain in the middle of scope of the presently claimed invention.

Claims

1. the moisturizing defying age class cosmetics containing Auricularia extract, it is characterised in that by weight, including Following components: Auricularia extract 5-15 part, vitamin 0.6-3.2 part, antioxidant 1-5 part, anti- Wrinkle activating agent 3-12 part, sunscreen 1-3 part, anti-sensitizer 0.5-2 part, whitening agent 2.5-6 part, Wetting agent 2-12 part, potassium hydroxide 0.03-0.2 part, Acer Truncatum Buge seed oil 0.5-2 part, chelating agen 0.3-1.2 part, thickening agent 0.1-0.3 part, emulsifying agent 1.5-5.8 part, preservative 0.2-1 part, Deionized water 40-80 part.

Moisturizing defying age class cosmetics containing Auricularia extract the most according to claim 1, its feature exists In, described antioxidant be weight part ratio be (1-3): the tocopherol of (2-5) and tea-seed oil Mixture.

Moisturizing defying age class cosmetics containing Auricularia extract the most according to claim 1, its feature exists In, described crease-resistant activating agent be weight part ratio be (1-3): (1-2.5): (0.6-1.8): (1-3.5) Polysaccharide/hydrolytic collagen, beta glucan, Semen Vitis viniferae extracting solution and the mixture of red wine polyphenols.

Moisturizing defying age class cosmetics containing Auricularia extract the most according to claim 1, its feature exists In, described sunscreen be weight part ratio be (1-3): (2-4): the o-amino benzoyl of (1.5-4) The mixture of acid esters, cinnamate derivative and camphor derivative.

Moisturizing defying age class cosmetics containing Auricularia extract the most according to claim 1, its feature exists In, described anti-sensitizer be weight part ratio be (1-2.5): the glycyrrhizic acid dipotassium of (1.5-4), Camellia sinensis The mixture of quintessence oil.

Moisturizing defying age class cosmetics containing Auricularia extract the most according to claim 1, its feature exists In, described whitening agent be weight part ratio be (1-2.5): (2-4): (0.3-1.2): (0.5-2.4) Licoflavone, phloretin, Semen Citri grandis extract and the mixture of Folium Mori extract.

Moisturizing defying age class cosmetics containing Auricularia extract the most according to claim 1, its feature exists In, described wetting agent be weight part ratio be (3-10): (2-8): (0.1-3): (0.1-0.6) Glycerol, Semen Maydis propylene glycol, reed fragrant plant oil and the mixture of oligofructose.

Moisturizing defying age class cosmetics containing Auricularia extract the most according to claim 1, its feature exists In, described emulsifying agent be weight part ratio be (1-3): (1-3): (0.5-3): the glycerol of (0.8-3) Stearate/PEG-100 stearate, cetearyl alcohol olive oil acid esters/Pyrusussuriensis smooth olive oil acid esters, first Base glucose sesquistearate and acrylic acid (ester) class/C 10-30 alcohol acrylate crosspolymers The mixture of potassium salt.

Moisturizing defying age class cosmetics containing Auricularia extract the most according to claim 1, its feature exists In, described preservative be weight part ratio be (3-5): the sodium benzoate of (2-4), propyl hydroxybenzoate are mixed Compound.

10. the preparation method of the moisturizing defying age class cosmetics containing Auricularia extract, it is characterised in that its bag Include following steps:

(2) by vitamin, crease-resistant activating agent, sunscreen, anti-sensitizer, whitening agent, wetting agent, Chelating agen, thickening agent and deionized water put in emulsifying pot successively, are heated to 70-85 DEG C, are incubated 15-30m Make it fully dissolve, prepare B phase；