CN105985679A - Environment-friendly wearing-resistant ink and preparation method thereof - Google Patents
Environment-friendly wearing-resistant ink and preparation method thereof Download PDFInfo
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- CN105985679A CN105985679A CN201610541111.2A CN201610541111A CN105985679A CN 105985679 A CN105985679 A CN 105985679A CN 201610541111 A CN201610541111 A CN 201610541111A CN 105985679 A CN105985679 A CN 105985679A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/04—Printing inks based on proteins
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
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Abstract
The invention discloses environment-friendly wearing-resistant ink and a preparation method thereof. The environment-friendly wearing-resistant ink is prepared from the following components: soybean albumen glue, menthol, fatty alcohol-polyoxyethylene ether, isopropyl myristate, sodium silicate pentahydrate, ethylene bis stearamide, glyceryl monostearate, chitosan quaternary ammonium salt, methyl chloride isothiazolinone, white portland cement, bismuth powder, mica powder, pigment, lemon oil, jojoba seed oil, glycerinum and diacetone alcohol. The environment-friendly wearing-resistant ink disclosed by the invention is excellent in friction resistance, good in adhesion property, stable in property, good in use durability, free of toxin or VOC emission, green and environmentally friendly and safe to use, and development requirements of the ink industry can be well met.
Description
Technical field
The invention belongs to technical field of ink, be specifically related to a kind of Environment-friendlywear-resistant wear-resistant ink and preparation method thereof.
Background technology
Ink is one of important materials of printing industry, and it is by printing by pattern, literal table now on the substrate.Traditional ink is by the dispersed pulpous state colloid mixing of link stuff, pigment, filler, auxiliary agent and solvent.Existing printing-ink major part chemical stability is poor, light fugitive photograph, and adhesive force is more weak simultaneously, and wearability is poor, it is easy to come off or scratch, is difficult to persistently, leverage the quality of print product.In addition, in the manufacturing process of ink, often add the organic matter of substantial amounts of volatile organic solvent and difficult degradation, so not only bring serious health threat to the operating personnel in ink-making process and in printing process, also bring added burden to the depollution of environment simultaneously, other dried ink yet suffers from toxic component, it is unfavorable for using, therefore, it is necessary to design a kind of environmental protection, stable performance, wear-resisting scratch resistance, the ink of duration length, preferably develops to meet ink industry.
Content of the invention
To this end, the present invention provides a kind of Environment-friendlywear-resistant wear-resistant ink and preparation method thereof, solve in prior art not environmentally, wear no resistance, the technical problems such as duration is short.
For this, the present invention provides a kind of Environment-friendlywear-resistant wear-resistant ink, it is prepared from the following components, it is calculated as by weight: soybean protein glue 12-18 part, menthol 2-9 part, AEO 4-8 part, isopropyl myristate 10-17 part, metasilicate pentahydrate sodium 2-6 part, ethylene bis stearamide 3-9 part, glyceryl monostearate 8-16 part, chitosan quaternary ammonium salt 4-9 part, methylchloroisothiazandnone 3-9 part, white cement 0.5-4 part, bismuth meal 2-6 part, mica powder 3-8 part, pigment 0.5-3 part, lemon oil 0.2-2 part, SIMMONDSIA CHINENSIS SEED OIL 3-7 part, glycerine 15-23 part, diacetone alcohol 20-28 part.
According to an embodiment of the invention, wherein, described chitosan quaternary ammonium salt is the mixture of HACC that weight ratio is 1 ~ 3:2 ~ 5 and hydroxypropyl alkyl dimethyl ammonium chloride shitosan.
According to an embodiment of the invention, wherein, described pigment is iron oxide red, iron oxide yellow, iron oxide black, iron oxide green, iron oxide blue or aluminium powder.
According to an embodiment of the invention, wherein, it is prepared from the following components, is calculated as by weight: 14 parts of soybean protein glue, menthol 5 parts, AEO 6 parts, isopropyl myristate 16 parts, metasilicate pentahydrate sodium 3 parts, ethylene bis stearamide 5 parts, glyceryl monostearate 13 parts, chitosan quaternary ammonium salt 5 parts, methylchloroisothiazandnone 6 parts, white cement 2.4 parts, bismuth meal 3 parts, mica powder 7 parts, pigment 0.8 part, lemon oil 1.1 parts, SIMMONDSIA CHINENSIS SEED OIL 4.8 parts, glycerine 19 parts, diacetone alcohol 26 parts.
To this end, the present invention provides the preparation method of described Environment-friendlywear-resistant wear-resistant ink, including following preparation process:
Step (1) is weighed each raw material by above-mentioned weight portion；
Step (2) processes 30-80 minute at bismuth meal, mica powder and white cement are placed in 300-500 DEG C, is cooled to room temperature standby；
Step (3) is by lemon oil, SIMMONDSIA CHINENSIS SEED OIL, glycerine, diacetone alcohol mixing and stirring, it is then heated to 70-100 DEG C, add soybean protein glue, isopropyl myristate, glyceryl monostearate, stirring 30-80 minute for the first time, it is subsequently adding menthol, AEO, ethylene bis stearamide and chitosan quaternary ammonium salt, second time stirring 2-5 hour；
Step (4) treats that system temperature is down to 40-60 DEG C, adds bismuth meal, mica powder and the white cement processing in pigment and step (2), stirs 50-120 minute；
Step (5) is eventually adding metasilicate pentahydrate sodium and methylchloroisothiazandnone, sends into three-roller and be ground 3-5 time after stirring, and filtration is checked and qualified is finished product.
According to an embodiment of the invention, wherein, in step (2), it is placed at 430 DEG C process 55 minutes.
According to an embodiment of the invention, wherein, it is heated to 85 DEG C in step (3)；Stir 60 minutes for the first time in step (3)；Second time stirring 3 hours in step (3).
According to an embodiment of the invention, wherein, in step (4), treat that system temperature is down to 42 DEG C, stirring 80 minutes in step (4).
The invention have the benefit that
The ink that the present invention provides to have excellent rub resistance, adhesive force strong, stable performance, use persistence long, and this ink be nontoxic, Diamond Search discharge, environmental protection, use safety, can be good at meeting the growth requirement of ink industry.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described in further detail.Following example are used for illustrating the present invention, but are not limited to the scope of the present invention.
Embodiment 1
A kind of Environment-friendlywear-resistant wear-resistant ink, it is prepared from the following components, is calculated as by weight: 12 parts of soybean protein glue, menthol 2 parts, AEO 4 parts, isopropyl myristate 10 parts, metasilicate pentahydrate sodium 2 parts, ethylene bis stearamide 3 parts, glyceryl monostearate 8 parts, chitosan quaternary ammonium salt 4 parts, methylchloroisothiazandnone 3 parts, white cement 0.5 part, bismuth meal 2 parts, mica powder 3 parts, pigment 0.5 part, lemon oil 0.2 part, SIMMONDSIA CHINENSIS SEED OIL 3 parts, glycerine 15 parts, diacetone alcohol 20 parts.
Described chitosan quaternary ammonium salt is weight than the mixture for the HACC of 1:2 and hydroxypropyl alkyl dimethyl ammonium chloride shitosan.
Described pigment is iron oxide red, iron oxide yellow, iron oxide black, iron oxide green, iron oxide blue or aluminium powder.
The preparation method of described Environment-friendlywear-resistant wear-resistant ink, including following preparation process:
Step (1) is weighed each raw material by above-mentioned weight portion；
Bismuth meal, mica powder and white cement are placed at 300 DEG C process 30 minutes by step (2), are cooled to room temperature standby；
Step (3) is by lemon oil, SIMMONDSIA CHINENSIS SEED OIL, glycerine, diacetone alcohol mixing and stirring, it is then heated to 70 DEG C, add soybean protein glue, isopropyl myristate, glyceryl monostearate, stirring 30-minute for the first time, it is subsequently adding menthol, AEO, ethylene bis stearamide and chitosan quaternary ammonium salt, second time stirring 2 hours；
Step (4) treats that system temperature is down to 400 DEG C, adds bismuth meal, mica powder and the white cement processing in pigment and step (2), stirs 50 minutes；
Step (5) is eventually adding metasilicate pentahydrate sodium and methylchloroisothiazandnone, sends into three-roller and be ground 3-5 time after stirring, and filtration is checked and qualified is finished product.
Embodiment 2
A kind of Environment-friendlywear-resistant wear-resistant ink, it is prepared from the following components, is calculated as by weight: 18 parts of soybean protein glue, menthol 9 parts, AEO 8 parts, isopropyl myristate 17 parts, metasilicate pentahydrate sodium 6 parts, ethylene bis stearamide 9 parts, glyceryl monostearate 16 parts, chitosan quaternary ammonium salt 9 parts, methylchloroisothiazandnone 9 parts, white cement 4 parts, bismuth meal 6 parts, mica powder 8 parts, pigment 3 parts, lemon oil 2 parts, SIMMONDSIA CHINENSIS SEED OIL 7 parts, glycerine 23 parts, diacetone alcohol 28 parts.
Described chitosan quaternary ammonium salt is weight than the mixture for the HACC of 3:5 and hydroxypropyl alkyl dimethyl ammonium chloride shitosan.
Described pigment is iron oxide red, iron oxide yellow, iron oxide black, iron oxide green, iron oxide blue or aluminium powder.
The preparation method of described Environment-friendlywear-resistant wear-resistant ink, including following preparation process:
Step (1) is weighed each raw material by above-mentioned weight portion；
Bismuth meal, mica powder and white cement are placed at 500 DEG C process 80 minutes by step (2), are cooled to room temperature standby；
Step (3) is by lemon oil, SIMMONDSIA CHINENSIS SEED OIL, glycerine, diacetone alcohol mixing and stirring, it is then heated to 100 DEG C, add soybean protein glue, isopropyl myristate, glyceryl monostearate, stirring 80 minutes for the first time, it is subsequently adding menthol, AEO, ethylene bis stearamide and chitosan quaternary ammonium salt, second time stirring 5 hours；
Step (4) treats that system temperature is down to 60 DEG C, adds bismuth meal, mica powder and the white cement processing in pigment and step (2), stirs 120 minutes；
Step (5) is eventually adding metasilicate pentahydrate sodium and methylchloroisothiazandnone, sends into three-roller and be ground 3-5 time after stirring, and filtration is checked and qualified is finished product.
Embodiment 3
A kind of Environment-friendlywear-resistant wear-resistant ink, it is prepared from the following components, is calculated as by weight: 15 parts of soybean protein glue, menthol 5 parts, AEO 6 parts, isopropyl myristate 13 parts, metasilicate pentahydrate sodium 2-6 part, ethylene bis stearamide 6 parts, glyceryl monostearate 12 parts, chitosan quaternary ammonium salt 6 parts, methylchloroisothiazandnone 6 parts, white cement 2.2 parts, bismuth meal 4 parts, mica powder 5 parts, pigment 1.8 parts, lemon oil 1.1 parts, SIMMONDSIA CHINENSIS SEED OIL 5 parts, glycerine 19 parts, diacetone alcohol 24 parts.
Described chitosan quaternary ammonium salt is weight than the mixture for the HACC of 2:3.5 and hydroxypropyl alkyl dimethyl ammonium chloride shitosan.
Described pigment is iron oxide red, iron oxide yellow, iron oxide black, iron oxide green, iron oxide blue or aluminium powder.
The preparation method of described Environment-friendlywear-resistant wear-resistant ink, including following preparation process:
Step (1) is weighed each raw material by above-mentioned weight portion；
Bismuth meal, mica powder and white cement are placed at 4500 DEG C process 55 minutes by step (2), are cooled to room temperature standby；
Step (3) is by lemon oil, SIMMONDSIA CHINENSIS SEED OIL, glycerine, diacetone alcohol mixing and stirring, it is then heated to 85 DEG C, add soybean protein glue, isopropyl myristate, glyceryl monostearate, stirring 55 minutes for the first time, it is subsequently adding menthol, AEO, ethylene bis stearamide and chitosan quaternary ammonium salt, second time stirring 2-5 hour；
Step (4) treats that system temperature is down to 50 DEG C, adds bismuth meal, mica powder and the white cement processing in pigment and step (2), stirs 85 minutes；
Step (5) is eventually adding metasilicate pentahydrate sodium and methylchloroisothiazandnone, sends into three-roller and be ground 3-5 time after stirring, and filtration is checked and qualified is finished product.
Embodiment 4
A kind of Environment-friendlywear-resistant wear-resistant ink, it is prepared from the following components, is calculated as by weight: 14 parts of soybean protein glue, menthol 5 parts, AEO 6 parts, isopropyl myristate 16 parts, metasilicate pentahydrate sodium 3 parts, ethylene bis stearamide 5 parts, glyceryl monostearate 13 parts, chitosan quaternary ammonium salt 5 parts, methylchloroisothiazandnone 6 parts, white cement 2.4 parts, bismuth meal 3 parts, mica powder 7 parts, pigment 0.8 part, lemon oil 1.1 parts, SIMMONDSIA CHINENSIS SEED OIL 4.8 parts, glycerine 19 parts, diacetone alcohol 26 parts.
Described chitosan quaternary ammonium salt is weight than the mixture for the HACC of 1.8:3 and hydroxypropyl alkyl dimethyl ammonium chloride shitosan.
Described pigment is iron oxide red, iron oxide yellow, iron oxide black, iron oxide green, iron oxide blue or aluminium powder.
The preparation method of described Environment-friendlywear-resistant wear-resistant ink, including following preparation process:
Step (1) is weighed each raw material by above-mentioned weight portion；
Bismuth meal, mica powder and white cement are placed at 430 DEG C process 55 minutes by step (2), are cooled to room temperature standby；
Step (3) is by lemon oil, SIMMONDSIA CHINENSIS SEED OIL, glycerine, diacetone alcohol mixing and stirring, it is then heated to 85 DEG C, add soybean protein glue, isopropyl myristate, glyceryl monostearate, stirring 60 minutes for the first time, it is subsequently adding menthol, AEO, ethylene bis stearamide and chitosan quaternary ammonium salt, second time stirring 3 hours；
Step (4) treats that system temperature is down to 42 DEG C, adds bismuth meal, mica powder and the white cement processing in pigment and step (2), stirs 80 minutes；
Step (5) is eventually adding metasilicate pentahydrate sodium and methylchloroisothiazandnone, sends into three-roller and be ground 3-5 time after stirring, and filtration is checked and qualified is finished product.
Embodiment 5
A kind of Environment-friendlywear-resistant wear-resistant ink, it is prepared from the following components, is calculated as by weight: 17 parts of soybean protein glue, menthol 5 parts, AEO 7 parts, isopropyl myristate 12 parts, metasilicate pentahydrate sodium 4 parts, ethylene bis stearamide 8 parts, glyceryl monostearate 8-16 part, chitosan quaternary ammonium salt 4 parts, methylchloroisothiazandnone 4 parts, white cement 2 parts, bismuth meal 5 parts, mica powder 4 parts, pigment 1.2 parts, lemon oil 0.8 part, SIMMONDSIA CHINENSIS SEED OIL 6 parts, glycerine 16 parts, diacetone alcohol 24 parts.
Described chitosan quaternary ammonium salt is the mixture of HACC that weight ratio is 1 ~ 3:2 ~ 5 and hydroxypropyl alkyl dimethyl ammonium chloride shitosan.
Described pigment is iron oxide red, iron oxide yellow, iron oxide black, iron oxide green, iron oxide blue or aluminium powder.
The preparation method of described Environment-friendlywear-resistant wear-resistant ink, including following preparation process:
Step (1) is weighed each raw material by above-mentioned weight portion；
Bismuth meal, mica powder and white cement are placed at 380 DEG C process 40 minutes by step (2), are cooled to room temperature standby；
Step (3) is by lemon oil, SIMMONDSIA CHINENSIS SEED OIL, glycerine, diacetone alcohol mixing and stirring, it is then heated to 90 DEG C, add soybean protein glue, isopropyl myristate, glyceryl monostearate, stirring 60 minutes for the first time, it is subsequently adding menthol, AEO, ethylene bis stearamide and chitosan quaternary ammonium salt, second time stirring 2-5 hour；
Step (4) treats that system temperature is down to 45 DEG C, adds bismuth meal, mica powder and the white cement processing in pigment and step (2), stirs 75 minutes；
Step (5) is eventually adding metasilicate pentahydrate sodium and methylchloroisothiazandnone, sends into three-roller and be ground 3-5 time after stirring, and filtration is checked and qualified is finished product.
Comparative example 1
This comparative example is in place of the difference of embodiment 1: do not comprise chitosan quaternary ammonium salt, SIMMONDSIA CHINENSIS SEED OIL, bismuth meal.
Comparative example 2
This comparative example is in place of the difference of embodiment 1: without bismuth meal, white cement and isopropyl myristate.
Performance test
According to professional standard, the ink of above-described embodiment 1 to 5 and comparative example the 1st, 2 preparations is carried out correlated performance test, and its test result is:
Note: the grade of rub resistance test result is higher, crocking resistance is better.
As seen from the above table, the ink that the present invention provides to have excellent rub resistance, adhesive force strong, stable performance, use persistence long, and this ink be nontoxic, Diamond Search discharge, environmental protection, use safety, can be good at meeting the growth requirement of ink industry.
Claims (8)
1. an Environment-friendlywear-resistant wear-resistant ink, it is characterized in that, it is prepared from the following components, it is calculated as by weight: soybean protein glue 12-18 part, menthol 2-9 part, AEO 4-8 part, isopropyl myristate 10-17 part, metasilicate pentahydrate sodium 2-6 part, ethylene bis stearamide 3-9 part, glyceryl monostearate 8-16 part, chitosan quaternary ammonium salt 4-9 part, methylchloroisothiazandnone 3-9 part, white cement 0.5-4 part, bismuth meal 2-6 part, mica powder 3-8 part, pigment 0.5-3 part, lemon oil 0.2-2 part, SIMMONDSIA CHINENSIS SEED OIL 3-7 part, glycerine 15-23 part, diacetone alcohol 20-28 part.
2. Environment-friendlywear-resistant wear-resistant ink according to claim 1, it is characterised in that described chitosan quaternary ammonium salt is the mixture of HACC that weight ratio is 1 ~ 3:2 ~ 5 and hydroxypropyl alkyl dimethyl ammonium chloride shitosan.
3. Environment-friendlywear-resistant wear-resistant ink according to claim 1, it is characterised in that described pigment is iron oxide red, iron oxide yellow, iron oxide black, iron oxide green, iron oxide blue or aluminium powder.
4. Environment-friendlywear-resistant wear-resistant ink according to claim 1, it is characterized in that, it is prepared from the following components, is calculated as by weight: 14 parts of soybean protein glue, menthol 5 parts, AEO 6 parts, isopropyl myristate 16 parts, metasilicate pentahydrate sodium 3 parts, ethylene bis stearamide 5 parts, glyceryl monostearate 13 parts, chitosan quaternary ammonium salt 5 parts, methylchloroisothiazandnone 6 parts, white cement 2.4 parts, bismuth meal 3 parts, mica powder 7 parts, pigment 0.8 part, lemon oil 1.1 parts, SIMMONDSIA CHINENSIS SEED OIL 4.8 parts, glycerine 19 parts, diacetone alcohol 26 parts.
5. the preparation method of the Environment-friendlywear-resistant wear-resistant ink according to Claims 1-4 any one, it is characterised in that include following preparation process:
Step (1) is weighed each raw material by above-mentioned weight portion；
Step (2) processes 30-80 minute at bismuth meal, mica powder and white cement are placed in 300-500 DEG C, is cooled to room temperature standby；
Step (3) is by lemon oil, SIMMONDSIA CHINENSIS SEED OIL, glycerine, diacetone alcohol mixing and stirring, it is then heated to 70-100 DEG C, add soybean protein glue, isopropyl myristate, glyceryl monostearate, stirring 30-80 minute for the first time, it is subsequently adding menthol, AEO, ethylene bis stearamide and chitosan quaternary ammonium salt, second time stirring 2-5 hour；
Step (4) treats that system temperature is down to 40-60 DEG C, adds bismuth meal, mica powder and the white cement processing in pigment and step (2), stirs 50-120 minute；
Step (5) is eventually adding metasilicate pentahydrate sodium and methylchloroisothiazandnone, sends into three-roller and be ground 3-5 time after stirring, and filtration is checked and qualified is finished product.
6. the preparation method of Environment-friendlywear-resistant wear-resistant ink according to claim 5, it is characterised in that be placed at 430 DEG C process 55 minutes in step (2).
7. the preparation method of Environment-friendlywear-resistant wear-resistant ink according to claim 5, it is characterised in that be heated to 85 DEG C in step (3)；Stir 60 minutes for the first time in step (3)；Second time stirring 3 hours in step (3).
8. the preparation method of Environment-friendlywear-resistant wear-resistant ink according to claim 5, it is characterised in that treat that system temperature is down to 42 DEG C in step (4), stirring 80 minutes in step (4).
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610541111.2A CN105985679A (en) | 2016-07-11 | 2016-07-11 | Environment-friendly wearing-resistant ink and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610541111.2A CN105985679A (en) | 2016-07-11 | 2016-07-11 | Environment-friendly wearing-resistant ink and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107443227A (en) * | 2017-07-31 | 2017-12-08 | 浦江县晶富农业科技有限公司 | A kind of low energy consumption steel wire rust removalling equipment |
| CN110964360A (en) * | 2019-11-08 | 2020-04-07 | 吴江山湖颜料有限公司 | High-strength pigment red and preparation method thereof |
| CN114193885A (en) * | 2022-01-04 | 2022-03-18 | 新乐华宝医疗器械有限公司 | Anti-skid water-absorbing floor mat and preparation method thereof |
| CN116356610A (en) * | 2023-05-23 | 2023-06-30 | 潍坊华港包装材料有限公司 | Transparent tipping paper product and preparation process thereof |
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|---|---|---|---|---|
| JP2005255888A (en) * | 2004-03-12 | 2005-09-22 | Toyo Ink Mfg Co Ltd | Aqueous printing ink composition and printed matter |
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2016
- 2016-07-11 CN CN201610541111.2A patent/CN105985679A/en active Pending
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2005255888A (en) * | 2004-03-12 | 2005-09-22 | Toyo Ink Mfg Co Ltd | Aqueous printing ink composition and printed matter |
Non-Patent Citations (1)
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| 凌云星等: "《油墨技术手册 上》", 31 May 2009, 印刷工业出版社 * |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107443227A (en) * | 2017-07-31 | 2017-12-08 | 浦江县晶富农业科技有限公司 | A kind of low energy consumption steel wire rust removalling equipment |
| CN110964360A (en) * | 2019-11-08 | 2020-04-07 | 吴江山湖颜料有限公司 | High-strength pigment red and preparation method thereof |
| CN114193885A (en) * | 2022-01-04 | 2022-03-18 | 新乐华宝医疗器械有限公司 | Anti-skid water-absorbing floor mat and preparation method thereof |
| CN114193885B (en) * | 2022-01-04 | 2023-09-08 | 新乐华宝医疗器械有限公司 | Anti-skid water-absorbing floor mat and preparation method thereof |
| CN116356610A (en) * | 2023-05-23 | 2023-06-30 | 潍坊华港包装材料有限公司 | Transparent tipping paper product and preparation process thereof |
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