CN107043573A - A kind of water resistance prepared Chinese ink and preparation method thereof - Google Patents
A kind of water resistance prepared Chinese ink and preparation method thereof Download PDFInfo
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- CN107043573A CN107043573A CN201710161007.5A CN201710161007A CN107043573A CN 107043573 A CN107043573 A CN 107043573A CN 201710161007 A CN201710161007 A CN 201710161007A CN 107043573 A CN107043573 A CN 107043573A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/16—Writing inks
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- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The present invention provides a kind of water resistance prepared Chinese ink and preparation method thereof, and the water resistance prepared Chinese ink is made up of the raw material of following parts by weight：18 22 parts of colouring agent, 68 parts of animal glue, 46 parts of borax, 12 parts of castor oil polyoxyethylene ether, 0.1 0.5 parts of OIT, 13 parts of carboxymethyl cellulose, 0.05 0.2 parts of brightener, 0.05 0.2 parts of aromatic, 13 parts of polyvinyl alcohol, 30 40 parts of water.Water resistance ink formulation prepared by the present invention is scientific and reasonable, and performance is stable, can preserve for a long time, glossiness is good, and water-tolerant after ink marks drying, not by air impact, and book paints the impermeable ink marks of calligraphy and painting immersion, can preserve for a long time, with good application value.
Description
Technical field
The present invention relates to prepared Chinese ink technical field, and in particular to a kind of water resistance prepared Chinese ink and preparation method thereof.
Background technology
Ink is one of writing brush, ink stick, ink slab and paper, is indispensable element in Chinese Painting and Calligraphy works, and its traditional material has china ink stick and ink
Juice.China ink stick needs to be ground when in use, time-consuming, laborious very inconvenient.Clear and Bright thanks to Song beams brother's initiative ground second during the time ruled by Emperor Guang Xu
For painting and calligraphy creation material-prepared Chinese ink, due to that need not grind and easy to use, popularized quickly in painting and calligraphy creation.Traditional ink
Juice typically uses carbon black for primary raw material, and chemical property is stable under normal conditions for carbon, colour-fast long, just because of this feature
Ancient times, some books can be preserved so far.But the water resistance of traditional prepared Chinese ink is often very poor, such as during calligraphy creation or calligraphy
Prepared Chinese ink diffusion of the water loading on paper is met after the completion of works and occurs dizzy dye, the effect of calligraphy is influenceed, especially meets rainwater
Infiltration, the writing difficulty that will thicken distinguishes, due to there is this shortcoming, many precious document ancient books ruin once.
The content of the invention
In view of the shortcomings of the prior art, the invention provides a kind of water resistance prepared Chinese ink and preparation method thereof.
To realize object above, the present invention is achieved by the following technical programs：
A kind of water resistance prepared Chinese ink, is made up of the raw material of following parts by weight：18-22 parts of colouring agent, 6-8 parts of animal glue, borax
4-6 parts, 1-2 parts of castor oil polyoxyethylene ether, 0.1-0.5 parts of OIT, 1-3 parts of carboxymethyl cellulose, brightener 0.05-
0.2 part, 0.05-0.2 parts of aromatic, 1-3 parts of polyvinyl alcohol, 30-40 parts of water.
Preferably, it is made up of the raw material of following parts by weight：20 parts of colouring agent, 7 parts of animal glue, 5 parts of borax, castor oil polyoxy
1.5 parts of vinethene, 0.2 part of OIT, 2 parts of carboxymethyl cellulose, 0.1 part of brightener, 0.1 part of aromatic, polyvinyl alcohol
1.5 parts, 35 parts of water.
Preferably, the colouring agent is carbon black or lamp coal dust.
Preferably, the animal glue is selected from gelatine or shellac.
Preferably, one or more of mixtures of the aromatic in borneol, camphorated oil, Moschus, cloves.
The preparation method of water resistance prepared Chinese ink, comprises the following steps：
1) it is borax is soluble in water, 30-40 DEG C is heated to, animal glue is added thereto, 80-90 DEG C is heated to, stirring makes
It dissolves, and continuation adds castor oil polyoxyethylene ether thereto, stirs, obtains mixture I；
2) colouring agent is dissolved in suitable quantity of water, is heated to 60-70 DEG C, stirring is dispersed in water it, is cooled to normal temperature, turns
Move on in grinder and grind, obtain mixture II；
3) mixture II is added in mixture I, stirred, continuously add OIT, carboxymethyl cellulose,
Brightener, aromatic, polyvinyl alcohol, stir, with molecular sieve filtration 1-2 times.
Preferably, the aperture of the molecular sieve is 200-300 mesh.
Beneficial effect of the present invention：Preparation method of the present invention is simple, and the water resistance ink formulation of preparation is scientific and reasonable, and performance is steady
It is fixed, it can preserve for a long time, glossiness is good, and water-tolerant after ink marks drying, not by air impact, it is impermeable that book paints calligraphy and painting immersion
Ink marks, can be preserved for a long time, with good application value, available for writing billboard, distich and other.
Embodiment
To make the purpose, technical scheme and advantage of the embodiment of the present invention clearer, below in conjunction with the embodiment of the present invention,
Technical scheme in the embodiment of the present invention is clearly and completely described, it is clear that described embodiment is the present invention one
Divide embodiment, rather than whole embodiments.Based on the embodiment in the present invention, those of ordinary skill in the art are not making
The every other embodiment obtained under the premise of creative work, belongs to the scope of protection of the invention.
Embodiment 1：
A kind of water resistance prepared Chinese ink, is made up of the raw material of following parts by weight：20 parts of carbon black, 7 parts of shellac, 5 parts of borax, castor oil
1.5 parts of APEO, 0.2 part of OIT, 2 parts of carboxymethyl cellulose, 0.1 part of brightener, 0.1 part of camphorated oil, poly- second
1.5 parts of enol, 35 parts of water.
The preparation method of water resistance prepared Chinese ink, comprises the following steps：
1) it is borax is soluble in water, 35 DEG C are heated to, shellac is added thereto, 85 DEG C are heated to, stirring dissolves it, after
It is continuous to add castor oil polyoxyethylene ether thereto, stir, obtain mixture I；
2) carbon black is dissolved in suitable quantity of water, is heated to 65 DEG C, stirring is dispersed in water it, is cooled to normal temperature, is transferred to
Ground in grinder, obtain mixture II；
3) mixture II is added in mixture I, stirred, continuously add OIT, carboxymethyl cellulose,
Brightener, camphorated oil, polyvinyl alcohol, stir, with 250 mesh molecular sieve filtration 2 times.
Embodiment 2：
A kind of water resistance prepared Chinese ink, is made up of the raw material of following parts by weight：19 parts of lamp coal dust, 6.5 parts of gelatine, 5 parts of borax, castor
1.2 parts of sesame oil APEO, 0.3 part of OIT, carboxymethyl cellulose 1.5,0.15 part of brightener, 0.15 part of borneol,
2 parts of polyvinyl alcohol, 32 parts of water.
The preparation method of water resistance prepared Chinese ink, comprises the following steps：
1) it is borax is soluble in water, 30 DEG C are heated to, gelatine is added thereto, 80 DEG C are heated to, stirring dissolves it, after
It is continuous to add castor oil polyoxyethylene ether thereto, stir, obtain mixture I；
2) lamp coal ash is dissolved in suitable quantity of water, is heated to 60 DEG C, stirring is dispersed in water it, is cooled to normal temperature, shifts
Ground into grinder, obtain mixture II；
3) mixture II is added in mixture I, stirred, continuously add OIT, carboxymethyl cellulose,
Brightener, borneol, polyvinyl alcohol, stir, with 200 mesh molecular sieve filtration 2 times.
Embodiment 3：
A kind of water resistance prepared Chinese ink, is made up of the raw material of following parts by weight：20 parts of carbon black, 6 parts of gelatine, 6 parts of borax, castor oil
2 parts of APEO, 0.1 part of OIT, 3 parts of carboxymethyl cellulose, 0.1 part of brightener, 0.05 part of cloves, polyvinyl alcohol
1 part, 38 parts of water.
The preparation method of water resistance prepared Chinese ink, comprises the following steps：
1) it is borax is soluble in water, 40 DEG C are heated to, gelatine is added thereto, 90 DEG C are heated to, stirring dissolves it, after
It is continuous to add castor oil polyoxyethylene ether thereto, stir, obtain mixture I；
2) carbon black is dissolved in suitable quantity of water, is heated to 70 DEG C, stirring is dispersed in water it, is cooled to normal temperature, is transferred to
Ground in grinder, obtain mixture II；
3) mixture II is added in mixture I, stirred, continuously add OIT, carboxymethyl cellulose,
Brightener, cloves, polyvinyl alcohol, stir, with 200 mesh molecular sieve filtration 1 time.
Embodiment 4：
A kind of water resistance prepared Chinese ink, is made up of the raw material of following parts by weight：18 parts of lamp coal dust, 8 parts of shellac, 4 parts of borax, castor-oil plant
Oily 2 parts of APEO, 0.1 part of OIT, 3 parts of carboxymethyl cellulose, 0.05 part of brightener, 0.2 part of camphorated oil, poly- second
1 part of enol, 40 parts of water.
The preparation method of water resistance prepared Chinese ink, comprises the following steps：
1) it is borax is soluble in water, 35 DEG C are heated to, shellac is added thereto, 80 DEG C are heated to, stirring dissolves it, after
It is continuous to add castor oil polyoxyethylene ether thereto, stir, obtain mixture I；
2) lamp coal dust is dissolved in suitable quantity of water, is heated to 60 DEG C, stirring is dispersed in water it, is cooled to normal temperature, shifts
Ground into grinder, obtain mixture II；
3) mixture II is added in mixture I, stirred, continuously add OIT, carboxymethyl cellulose,
Brightener, camphorated oil, polyvinyl alcohol, stir, with 300 mesh molecular sieve filtration 1 time.
Embodiment 5：
A kind of water resistance prepared Chinese ink, is made up of the raw material of following parts by weight：22 parts of carbon black, 6 parts of shellac, 6 parts of borax, castor oil
1 part of APEO, 0.5 part of OIT, 1 part of carboxymethyl cellulose, 0.2 part of brightener, 0.05 part of cloves, polyvinyl alcohol
3 parts, 30 parts of water.
The preparation method of water resistance prepared Chinese ink, comprises the following steps：
1) it is borax is soluble in water, 40 DEG C are heated to, shellac is added thereto, 90 DEG C are heated to, stirring dissolves it, after
It is continuous to add castor oil polyoxyethylene ether thereto, stir, obtain mixture I；
2) carbon black is dissolved in suitable quantity of water, is heated to 70 DEG C, stirring is dispersed in water it, is cooled to normal temperature, is transferred to
Ground in grinder, obtain mixture II；
3) mixture II is added in mixture I, stirred, continuously add OIT, carboxymethyl cellulose,
Brightener, cloves, polyvinyl alcohol, stir, with 300 mesh molecular sieve filtration 2 times.
It should be noted that herein, such as first and second or the like relational terms are used merely to a reality
Body or operation make a distinction with another entity or operation, and not necessarily require or imply these entities or deposited between operating
In any this actual relation or order.Moreover, term " comprising ", "comprising" or its any other variant are intended to
Nonexcludability is included, so that process, method, article or equipment including a series of key elements not only will including those
Element, but also other key elements including being not expressly set out, or also include being this process, method, article or equipment
Intrinsic key element.In the absence of more restrictions, the key element limited by sentence "including a ...", it is not excluded that
Also there is other identical element in process, method, article or equipment including the key element.
The above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations；Although with reference to the foregoing embodiments
The present invention is described in detail, it will be understood by those within the art that：It still can be to foregoing each implementation
Technical scheme described in example is modified, or carries out equivalent substitution to which part technical characteristic；And these modification or
Replace, the essence of appropriate technical solution is departed from the spirit and scope of various embodiments of the present invention technical scheme.
Claims (7)
1. a kind of water resistance prepared Chinese ink, it is characterised in that be made up of the raw material of following parts by weight：18-22 parts of colouring agent, animal glue 6-
8 parts, 4-6 parts of borax, 1-2 parts of castor oil polyoxyethylene ether, 0.1-0.5 parts of OIT, 1-3 parts of carboxymethyl cellulose, increase
Bright dose 0.05-0.2 parts, 0.05-0.2 parts of aromatic, 1-3 parts of polyvinyl alcohol, 30-40 parts of water.
2. water resistance prepared Chinese ink as claimed in claim 1, it is characterised in that be made up of the raw material of following parts by weight：Colouring agent 20
Part, 7 parts of animal glue, 5 parts of borax, 1.5 parts of castor oil polyoxyethylene ether, 0.2 part of OIT, 2 parts of carboxymethyl cellulose, increasing
Bright dose 0.1 part, 0.1 part of aromatic, 1.5 parts of polyvinyl alcohol, 35 parts of water.
3. water resistance prepared Chinese ink as claimed in claim 2, it is characterised in that the colouring agent is carbon black or lamp coal dust.
4. water resistance prepared Chinese ink as claimed in claim 2, it is characterised in that the animal glue is selected from gelatine or shellac.
5. water resistance prepared Chinese ink as claimed in claim 2, it is characterised in that the aromatic be selected from borneol, camphorated oil, Moschus,
One or more of mixtures in cloves.
6. the preparation method of the water resistance prepared Chinese ink as described in claim 1-5 is any, it is characterised in that comprise the following steps：
1) it is borax is soluble in water, 30-40 DEG C is heated to, animal glue is added thereto, 80-90 DEG C is heated to, stirring makes its molten
Solution, continuation adds castor oil polyoxyethylene ether thereto, stirs, obtains mixture I；
2) colouring agent is dissolved in suitable quantity of water, is heated to 60-70 DEG C, stirring is dispersed in water it, is cooled to normal temperature, is transferred to
Ground in grinder, obtain mixture II；
3) mixture II is added in mixture I, stirred, continuously add OIT, carboxymethyl cellulose, blast
Agent, aromatic, polyvinyl alcohol, stir, with molecular sieve filtration 1-2 times.
7. the preparation method of water resistance prepared Chinese ink as claimed in claim 6, it is characterised in that the aperture of the molecular sieve is 200-
300 mesh.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710161007.5A CN107043573A (en) | 2017-03-17 | 2017-03-17 | A kind of water resistance prepared Chinese ink and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710161007.5A CN107043573A (en) | 2017-03-17 | 2017-03-17 | A kind of water resistance prepared Chinese ink and preparation method thereof |
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| Publication Number | Publication Date |
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| CN107043573A true CN107043573A (en) | 2017-08-15 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710161007.5A Pending CN107043573A (en) | 2017-03-17 | 2017-03-17 | A kind of water resistance prepared Chinese ink and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109796809A (en) * | 2019-02-18 | 2019-05-24 | 临沂晋墨坊文化用品有限公司 | A kind of writing charcoal liquid and preparation method thereof |
| CN114574034A (en) * | 2021-08-30 | 2022-06-03 | 廖双涛 | Antioxidant and corrosion-resistant ink after writing |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101798478A (en) * | 2010-03-11 | 2010-08-11 | 齐成森 | Leftover ink |
| CN102492332A (en) * | 2011-12-05 | 2012-06-13 | 天津市鸵鸟墨水有限公司 | Novel ink and production method thereof |
| CN103468060A (en) * | 2013-09-24 | 2013-12-25 | 昆明理工大学 | Humate-containing ink and preparation method thereof |
| CN105368154A (en) * | 2015-11-21 | 2016-03-02 | 兰州交通大学 | Novel waterproof prepared Chinese ink and preparation method thereof |
-
2017
- 2017-03-17 CN CN201710161007.5A patent/CN107043573A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101798478A (en) * | 2010-03-11 | 2010-08-11 | 齐成森 | Leftover ink |
| CN102492332A (en) * | 2011-12-05 | 2012-06-13 | 天津市鸵鸟墨水有限公司 | Novel ink and production method thereof |
| CN103468060A (en) * | 2013-09-24 | 2013-12-25 | 昆明理工大学 | Humate-containing ink and preparation method thereof |
| CN105368154A (en) * | 2015-11-21 | 2016-03-02 | 兰州交通大学 | Novel waterproof prepared Chinese ink and preparation method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109796809A (en) * | 2019-02-18 | 2019-05-24 | 临沂晋墨坊文化用品有限公司 | A kind of writing charcoal liquid and preparation method thereof |
| CN114574034A (en) * | 2021-08-30 | 2022-06-03 | 廖双涛 | Antioxidant and corrosion-resistant ink after writing |
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Application publication date: 20170815 |