CN105368154A - Novel waterproof prepared Chinese ink and preparation method thereof - Google Patents

Abstract

The invention relates to a novel waterproof prepared Chinese ink and a preparation method thereof. The novel waterproof prepared Chinese ink comprises the following components by weight part: 100 of a coloring agent, 200-230 of a dispersing agent, 3-5 of an emulsifier, 0.1-0.5 of a quick drying agent, 0.4-1.6 of a stabilizer, and 0.1-0.5 of a defoaming agent. The preparation method consists of: firstly placing an asphalt loaded container in constant temperature water bath to conduct preheating softening; then preparing the dispersing agent, the emulsifier, the quick drying agent and the stabilizer into soap liquid according to certain proportion, and adding the soap liquid into the softened asphalt, performing high speed stirring to mix the materials into a homogeneous system; and adding the defoaming agent, and after cooling, performing canning and storage. According to the invention, the waterproof prepared Chinese ink prepared with asphalt as the coloring agent has the characteristics of scientific and reasonable formula, low price of raw materials, stable properties, easy writing on paper or solid surface, strong adhesion, and excellent waterproof ability after drying, and is easy for long time preservation.

Description

A kind of new waterproof prepared Chinese ink and preparation method thereof

Technical field

The present invention relates to a kind of making method of new waterproof prepared Chinese ink.

Background technology

The rarity of Mo Shi state is indispensable element in Chinese Painting and Calligraphy works.Traditional prepared Chinese ink generally adopts carbon black to be main raw material.Because carbon is not easy and other material generation chemical reaction under normal conditions, therefore the stable chemical nature of ink, colour-fast for a long time, and just because of this feature, we can obtain knowledge from the sage of the past there of greatness.But traditional ink often water tolerance is very poor, especially meet the infiltration of rainwater, the writing difficulty that will thicken is distinguished, owing to there is this shortcoming, the document ancient books of many preciousnesses disappears thereupon.

In addition, the engineering of oil, geological prospecting and outdoor work often needs at wall, and rock point, rock core makes marks, and in order to ensure that gauge point is not subject to rain drop erosion, more the impact that dust storm corrodes, make to paint at present and carry out writing and spraying.Paint cost is high, and toxic volatile organic solvent pollution environment threat is brought to the health of constructor in paint.Along with people are to the pay attention to day by day of environmental problem, how effectively control the impact that organic volatile compound causes environment, develop that production technique is simple, cheap, the waterproof prepared Chinese ink of environmental protection, will wide market outlook be had.

Summary of the invention

The object of the present invention is to provide a kind of novel asphalt waterproof prepared Chinese ink, do not use in its manufacturing processed or a small amount of with an organic solvent, scribble rear ink marks dense, adhesive power is strong, cheap, be the environmentally friendly new waterproof prepared Chinese ink of large-scale application in a kind of applicable engineering.

In order to achieve the above object, the present invention is achieved by the following technical solutions:

A kind of waterproof prepared Chinese ink is made up of tinting material, dispersion agent, emulsifying agent, quick dry agent, stablizer, defoamer, and the parts by weight of each constitutive material are: tinting material 100, dispersion agent 200 ~ 230, emulsifying agent 3 ~ 5, quick dry agent 0.1 ~ 0.5, stablizer 0.4 ~ 1.6, defoamer 0.1 ~ 0.5.

Above-mentioned waterproof prepared Chinese ink preferred tinting material be the 90# pitch of softening temperature 45 DEG C ~ 55 DEG C.

The above-mentioned preferred dispersion agent of waterproof prepared Chinese ink institute is water.

Above-mentioned waterproof prepared Chinese ink preferred emulsifying agent be one or more in sodium lauryl sulphate, cetyl trimethylammonium bromide, OP-10.

Above-mentioned waterproof prepared Chinese ink preferred quick dry agent be one or both in manganous acetate or cobaltous acetate.

Above-mentioned waterproof prepared Chinese ink preferred stablizer be one or more in water glass, polyvinyl alcohol, polyacrylamide, Xylo-Mucine.

The above-mentioned preferred defoamer of waterproof prepared Chinese ink institute is dimethyl silicone oil.

The preparation method of described waterproof prepared Chinese ink, is characterized in that, comprise the following steps:

(a). pitch is placed in container, softening in water bath with thermostatic control;

(b). water, emulsifying agent, quick dry agent, stablizer are joined by a certain percentage abundant mixing in container and be made into soap lye;

(c). join in the soft pitch of step a by the soap lye described in step b, high-speed stirring makes pitch be uniformly dispersed in soap lye;

(d). in the emulsion of step c, add defoamer, slowly stir, until lather collapse;

(e). after the mixture cooling of steps d, tinning sealing is preserved, stand-by.

The preparation method of above-mentioned waterproof prepared Chinese ink, wherein, step 1 constant temperature water bath temperature is 80 ~ 90 DEG C.

The preparation method of above-mentioned waterproof prepared Chinese ink, wherein, the high-speed stirring time is 10 minutes.

Advantage of the present invention and beneficial effect as follows:

By the waterproof prepared Chinese ink that present method is obtained, scientific formulation is reasonable, low in raw material price, and prepared Chinese ink stable in properties, easily writes on paper or solid surface, and adhesive power is strong, has excellent waterproof ability, be easy to long-time preservation after drying.

Embodiment

Specific embodiment of the invention scheme and effect will be illustrated by following examples, but not limit practical range of the present invention with this.

Example 1

Constituent mass number

90# pitch 100 parts

230 parts, water

Cetyl trimethylammonium bromide 4.5 parts

Manganous acetate 0.2 part

Dimethyl silicone oil 0.3 part

Preparation method: the water bath with thermostatic control the preheating first container filling pitch being placed in 90 DEG C; Again by 230 parts of water, join after 4.5 parts of cetyl trimethylammonium bromides and 0.2 part of manganous acetate are mixed into soap lye in 100 parts of softening pitches, under constant temperature, high-speed stirring becomes homogeneous system; Add 0.3 part of dimethyl silicone oil and stir, being cooled to room temperature, tinning sealing is preserved.

Example 2

Constituent mass number

90# road bitumen 100 parts

200 parts, water

Sodium lauryl sulphate 4.5 parts

OP-100.5 part

Manganous acetate 0.2 part

Water glass 1.6 parts

Dimethyl silicone oil 0.3 part

Preparation method: the water bath with thermostatic control the preheating first container filling pitch being placed in 85 DEG C; Again by 200 parts of water, 4.5 parts of sodium lauryl sulphate, 0.2 part of manganous acetate, join after 0.5 part of OP-10 and 1.60 part water glass is mixed into soap lye in 100 parts of softening pitches, under constant temperature, high-speed stirring becomes homogeneous system; Add 0.3 part of dimethyl silicone oil and stir, being cooled to room temperature, tinning sealing is preserved.

Example 3

Constituent mass number

90# road bitumen 100 parts

200 parts, water

Cetyl trimethylammonium bromide 4.0 parts

Manganous acetate 0.1 part

Carboxymethyl cellulose 0.4 part

Dimethyl silicone oil 0.3 part

Preparation method: the water bath with thermostatic control the preheating first container filling pitch being placed in 90 DEG C; Again by 200 parts of water, 4.0 parts of cetyl trimethylammonium bromides, join after 0.1 part of manganous acetate and 0.4 part of carboxymethyl cellulose are mixed into soap lye in 100 parts of softening pitches, under constant temperature, high-speed stirring becomes homogeneous system; Add 0.3 part of dimethyl silicone oil and stir, being cooled to room temperature, tinning sealing is preserved.

Claims (9)

1. new waterproof prepared Chinese ink and preparation method thereof: first the container filling pitch is placed in the pre-thermal softening of water bath with thermostatic control; Again by dispersion agent, emulsifying agent, quick dry agent, stablizer, by certain mass than joining after mixing in softening pitch, high-speed stirring becomes homogeneous system, adds defoamer, and tinning is after cooling preserved.

2. the preparation method of waterproof prepared Chinese ink according to claim 1, is characterized in that: tinting material is the 90# pitch of softening temperature 45 DEG C-55 DEG C.

3. the preparation method of waterproof prepared Chinese ink according to claim 1, is characterized in that: dispersion agent is water.

4. the preparation method of waterproof prepared Chinese ink according to claim 1, is characterized in that: emulsifying agent is one or more in sodium lauryl sulphate, cetyl trimethylammonium bromide, OP-10.

5. the preparation method of waterproof prepared Chinese ink according to claim 1, is characterized in that: quick dry agent is one or both in manganous acetate or zinc acetate.

6. the preparation method of waterproof prepared Chinese ink according to claim 1, is characterized in that: stablizer is one or more in water glass, polyacrylamide, carboxymethyl cellulose.

7. the preparation method of waterproof prepared Chinese ink according to claim 1, is characterized in that: defoamer is dimethyl silicone oil.

8. the preparation method of waterproof prepared Chinese ink according to claim 1, is characterized in that: the parts by weight of tinting material, dispersion agent, emulsifying agent, quick dry agent, stablizer, defoamer are: 100:200 ~ 230:3 ~ 5:0.1 ~ 0.5:0.4 ~ 1.6:0.1 ~ 0.5.

9. the preparation method of the new waterproof prepared Chinese ink described in claim 1 ~ 8, is characterized in that, comprise the following steps:

(a). pitch is placed in container, softening in water bath with thermostatic control;

(b). water, emulsifying agent, quick dry agent, stablizer are joined by a certain percentage abundant mixing in container and be made into soap lye;

(c). join in the soft pitch of step a by the soap lye described in step b, high-speed stirring makes pitch be uniformly dispersed in soap lye;

(d). in the emulsion of step c, add defoamer, slowly stir, until lather collapse;

(e). after the mixture cooling of steps d, tinning sealing is preserved, stand-by.