CN105962412A - Tobacco leaf particles suitable for preparing buccal cigarettes and application of tobacco leaf particles - Google Patents
Tobacco leaf particles suitable for preparing buccal cigarettes and application of tobacco leaf particles Download PDFInfo
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- CN105962412A CN105962412A CN201610323522.4A CN201610323522A CN105962412A CN 105962412 A CN105962412 A CN 105962412A CN 201610323522 A CN201610323522 A CN 201610323522A CN 105962412 A CN105962412 A CN 105962412A
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- buccal cigarette
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B13/00—Tobacco for pipes, for cigars, e.g. cigar inserts, or for cigarettes; Chewing tobacco; Snuff
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Abstract
The invention discloses tobacco leaf particles suitable for preparing buccal cigarettes and application of the tobacco leaf particles. According to the tobacco leaf particles, tobacco leaves are shredded, carbon dioxide expansion treatment is carried out, then fermentation treatment is carried out, screening is carried out after micro smashing, and the permeable part is taken. The bitterness and spicy taste of the tobacco leaves are removed through pertinent scientific treatment, the fragrance is rich and mellow, the tobacco leaf particles and auxiliary materials are scientifically matched, reasonable and safe seasoning treatment is carried out, and a new buccall cigarette material is obtained. The taste is richer, the flavor is coordinative and high in quality, the buccal cigarettes can be gradually molten in the mouth in the eating process, no particle feeling or rough feeling is generated in the oral cavity, and the buccal cigarettes do not need to be abandoned after being eaten.
Description
Technical field
The present invention relates to tobacco leaf production technical field, prepare buccal cigarette more particularly, to a kind of being applicable to
Tobacco leaf granule and application thereof.
Background technology
Smoke-free tobacco product refers to without combustion process, and is directly sucked the cigarette of consumption by oral cavity or nasal cavity
Straw-made articles.
World Health Organization's Framework Convention on Tobacco Control (WHO FCTC) proposes about forbidding tobacco smoke
Restriction and the ban such as diffusion in public places, the development to conventional tobacco products Medicated cigarette causes powerful impact.?
Under this background, countries in the world tobacco business is the research and development of smoke-free tobacco product with introduce work to the market
For solving the important means of tobacco business future development, in Europe, South and North America, India and Africa, smokelessly
Type tobacco product various in style, consumption figure in various countries all in the trend increased year by year.As a example by the U.S., 2006
In year, consumption figure is more than 4,000,000,000 dollars.
Buccal cigarette is a kind of smokeless tobacco containing nicotine, it is common that salt adding of being clayed into power by Nicotiana tabacum L. again and water
Mix, the most also can add spice, seem oleum bergamottae, Oleum Rosae Rugosae or Radix Glycyrrhizae.Buccal cigarette the earliest
It is in bulk, is kneaded into a little group with finger time to be sucked, then fills in upper lip rear.From the beginning of 1973, mouth
It is installed in the pouch as little tea bag containing cigarette.
The sense organ impact strength of buccal cigarette is mainly affected by the organoleptic attribute of tobacco material, and external product is in order to protect
Demonstrate,prove the fire-cured tobacco having significant proportion in the tobacco material formula that its distinctive organoleptic feature is conventional.Due to naked light
Flue-cured tobacco is external distinctive tobacco material, and it is smokeless that this largely limits the exploitation of domestic Foreign Experience
The raw material space of gas tobacco product.And at present the smoke-free tobacco product technique of domestic-developed is mostly and directly makes
With tobacco material grinding, seasoning, pack, have that zest is excessive, bitter taste is dense, acid is strong,
It is not directed to the fermentation process technique of tobacco material.
On the other hand, existing buccal cigarette all uses tobacco leaf (tobacco shred) as raw material, does not finds cabo
Use as buccal cigarette raw material.This is owing to cabo is very big with the nature difference of blade, compared with tobacco leaf,
Cabo contains lower volatile material (flavor component) and higher proportion of cell-wall biopolymers, as
Cellulose, lignin and colloid etc., its rigid structure is more, and fiber is thick, it is difficult to edible.But, cabo
Account for more than the 20% of total tobacco leaf quality, if cabo application problem in buccal cigarette can be solved, will
Tobacco material utilization rate preparation buccal cigarette in terms of is greatly improved.
Summary of the invention
The technical problem to be solved in the present invention is the technical deficiency overcoming existing buccal cigarette to prepare raw material, it is provided that one
Planting the tobacco leaf granule being applicable to prepare buccal cigarette, described tobacco leaf raw material prepares through Nicotiana tabacum L., goes
Except bitter taste and acid, enrich fragrance matter.
Another technical problem that the invention solves the problems that is to provide the application of described tobacco leaf granule, is applied to system
Standby a kind of buccal cigarette tobacco material containing described tobacco leaf granule, arranges in pairs or groups with adjuvant science, or and cabo
Granule and adjuvant are comprehensively arranged in pairs or groups, and, can be eaten without granular sensation, harsh feeling in oral cavity by gradually containing changing when edible
Abandon without spuing with end.
The purpose of the present invention is achieved by the following technical programs:
A kind of tobacco leaf granule being applicable to prepare buccal cigarette is provided, is prepared by following steps:
S21. tobacco leaf use water is rinsed, remove surface dust, remove excessive moisture, shredding；
S22. the tobacco shred of step S21 shredding gained being carried out carbon dioxide expanding treatment, described carbon dioxide is expanded
The process conditions processed are: dip time 1～5min, expansion temperature 300～400 DEG C；
S23. step S22 expanding treatment gained tobacco shred is carried out fermentation process；By the tobacco shred Crushing of Ultrafine after fermentation,
Sieve, take permeation parts.
Fermentation described in step S23 is preparation inoculation liquid, is 1～15g inoculation liquid/100g tobacco shred according to inoculum concentration
Inoculation after fermentation；Fermentation temperature is 35～45 DEG C, and the time is 7～30 days.After fermentation process, effectively remove
Go bitter taste, acid, and obtain ferment local-flavor.
Described inoculation liquid consist of high fructose syrup: protein peptide: strain: the mass ratio of water=(50～200) g:
(0.1～10) g:(0.01～1) g:(100～500) g；It is further preferred that high fructose syrup: albumen
Peptide: strain: the mass ratio of water=(50～100) g:(1～10) g:(0.1～0.8) g:(200～500)
g。
Described water preferably employs distilled water.
Described protein peptide is soybean protein peptide, wheat protein peptide, rice protein peptide, casein peptide, milk surum egg
One or more of white peptide.
Described strain be monascus (Monascuspurpureus Went.), aspergillus oryzae (Aspergillus oryzae),
Zygosaccharomyces rouxii (Mucor roxianus) or rhizopus (Rhizopus), yeast (Saccharomyces) or lactic acid bacteria
(Lactobacillus) one or more.
Preferably, sieving described in step S23 was 160 mesh sieves, took permeation parts.
Present invention simultaneously provides the application of described tobacco leaf granule, be specifically applied to prepare a kind of buccal cigarette
Material, matches it with adjuvant, prepares buccal cigarette material.Preferably, described buccal cigarette material is
It is made up of according to mass percent following raw material: tobacco leaf granule 40～60%；Filler 30～50%；
Correctives 0.5～5%；Binding agent 1～10%；Essence 0.1～1%；Lubricant 0.5～3%.
Or it is arranged in pairs or groups with cabo particle science, then is equipped with adjuvant, prepare buccal cigarette material, wherein
The mass ratio of described tobacco leaf granule and cabo particle is 60～80%:40～20%.
Described adjuvant includes filler, correctives, binding agent, essence and lubricant.
Preferably, described buccal cigarette material is made up of according to percentage by weight following raw material: tobacco-containing material 40～
60%；Filler 30～50%；Correctives 0.5～5%；Binding agent 1～10%；Essence 0.1～1%；Profit
Lubrication prescription 0.5～3%；Described tobacco-containing material is made up of tobacco leaf granule and cabo particle of the present invention, its
The ratio of middle tobacco leaf granule and cabo particle is 60～80%:40～20%；
Described filler be starch, maltodextrin, cyclodextrin, microcrystalline Cellulose, white sugar, mannitol or
One or more in xylitol.
Described correctives is: one or more of Sal, sodium carbonate or sodium benzoate etc..
Described binding agent is: sodium carboxymethyl cellulose, hydroxypropyl cellulose, methylcellulose, ethyl cellulose
One or more in element, gelatin or white sugar.
Described essence is: naturally occurring or synthetic perfume monomer such as menthol, menthyl acetate, Borneolum Syntheticum etc., it is possible to
To be fruit, such as the extract of Fructus Mali pumilae, Fructus Citri junoris, Fructus Persicae, Fructus Citri Limoniae, Fructus Armeniacae Mume etc., it is also possible to be Folium Camelliae sinensis, chrysanthemum
The extract of flower, coffee bean, cacao bean etc..The corresponding essence of the existing use of tobacco enterprise can be used, as
Fruit is extracted, and extracting method is with reference to existing routine.
Described lubricant is magnesium stearate, Pulvis Talci, sodium lauryl sulphate or Polyethylene Glycol.
Described cabo particle preferably employs following methods and prepares:
S11. cabo is carried out wind and washes to remove surface dust, then shredding after microwave bulking；
S12. stem step S11 cut carries out fermentation process；
S13. stem step S12 fermented carries out Crushing of Ultrafine, sieves and obtains described cabo particle；
Preferably, the process conditions of microwave bulking described in step S11 are: cabo moisture content 14～18%, swollen
The swollen time 45～75s, expand power 600～900W.
Shredding described in step S11 is that cabo is cut to 0.5～5.0cm length, 0.3～0.9mm wide uniform stem.
Preferably, the fermentation processing method described in step S12 is:
Preparation inoculation liquid, is the inoculation after fermentation of 20～30g inoculation liquid/100g stem according to inoculum concentration, described in connect
That plants liquid consists of high fructose syrup: protein peptide: strain: the mass ratio of water=(50～200) g:(0.1～10)
G:(0.01～1) g:(100～500) g.After fermentation process, effectively removes bitter taste, acid,
And obtain ferment local-flavor.
The preferred distilled water of described water.
Described strain be monascus (Monascuspurpureus Went.), aspergillus oryzae (Aspergillus oryzae),
Zygosaccharomyces rouxii (Mucor roxianus) or rhizopus (Rhizopus), yeast (Saccharomyces) or lactic acid bacteria
(Lactobacillus) one or more.
Described in step S12 fermentation during, remain control temperature at 35～45 DEG C, fermentation time is
10～30 days.
Described Crushing of Ultrafine is with reference to existing conventional techniques.
Preferably, sieving described in step S13 was 160 mesh sieves, took permeation parts.
The present invention provides the preparation method of described buccal cigarette as follows:
S1. by after correctives, tobacco-containing material, filler, binding agent mix homogeneously, gather with dissolved with 10～15%
60～80% ethanol solution pelletize of vinylpyrrolidone, is dried 2～4h at 40～45 DEG C.
S2. by essence with after appropriate anhydrous alcohol solution, uniformly it is sprayed on above-mentioned granule, adds lubricant
Mixing, compression molding.
Beneficial effects of the present invention is as follows:
The invention provides a kind of new tobacco leaf granule, use the fermentation process technique of science, it is thus achieved that be suitable
For preparing the tobacco leaf granule of buccal cigarette, its nitrogen substance is reduced conversion, improves the mouth of raw material
Sense comfortableness, successfully eliminates blue foreign smell and the zest of raw material, without granular sensation, harsh feeling in oral cavity time edible.
Further, the invention provides a kind of new buccal cigarette material, material therefor is based on tobacco material.
All tobacco materials, all by fermentation process, eliminate the bitter taste of tobacco material, acid, and fragrance matter is rich
Rich mellow.And the seasoning combining reasonable benefit/risk processes, use correctives and sweeting agent etc. and the cigarette of rational proportion
Silk granule is compatible, it is thus achieved that more enrich mouthfeel, flavor coordination, high-quality buccal cigarette.
The all of tobacco-containing material of the present invention, after specific aim micronizing, does not have during disintegrate in the oral cavity
Grain sense, taste lubrication, for containing sheet form, can be the most edible, edible end abandons without spuing, will not be right
Environment.
Detailed description of the invention
The present invention is further described below in conjunction with specific embodiment.Unless stated otherwise, the present invention uses
Reagent, equipment be the art conventional reagent and equipment；Design philosophy of the present invention is based on long-term a large amount of real
Testing summary to obtain, following embodiment is merely to illustrate the present invention, but the most therefore limits the present invention.Following reality
Execute the raw material (protein peptide, strain, filler, correctives, binding agent, essence, lubricant etc.) that example uses,
Unless stated otherwise, it is conventional commercial raw material.
Embodiment 1
The present embodiment provides a kind of cabo particle being applicable to buccal cigarette, is prepared by following steps:
S11. cabo is carried out wind and washes to remove surface dust, then shredding after microwave bulking；
S12. stem step S11 cut carries out fermentation process, removes bitter taste, acid, and acquisition is sent out
Ferment local flavor；
S13. stem step S12 fermented carries out micronizing, crosses 160 mesh sieves, takes permeation parts and obtain
Described cabo particle；
The process conditions of microwave bulking described in step S11 are: cabo moisture content 14%, and Bulking Time 45s is swollen
Swollen power 750W.
Shredding described in step S11 is that cabo is cut to 1.0～3.0cm length, 0.3～0.5mm wide uniform stem.
Fermentation processing method described in step S12 is:
Preparation inoculation liquid, is 20g inoculation liquid/100g stem inoculation after fermentation according to inoculum concentration, described inoculation liquid
Consist of high fructose syrup: protein peptide: strain: the mass ratio=60g:0.5g:0.2g:200g of distilled water；
Controlling temperature 35 DEG C, fermentation time is 10 days.
Described strain is monascus (Monascuspurpureus Went.).Described protein peptide is soybean protein peptide.
Embodiment 2
The present embodiment provides a kind of cabo particle being applicable to buccal cigarette, is prepared by following steps:
S11. cabo is carried out wind and washes to remove surface dust, then shredding after microwave bulking；
S12. stem step S11 cut carries out fermentation process, removes bitter taste, acid, and acquisition is sent out
Ferment local flavor；
S13. stem step S12 fermented carries out micronizing, crosses 160 mesh sieves, takes permeation parts and obtain
Described cabo particle；
The process conditions of microwave bulking described in step S11 are: cabo moisture content 16%, and Bulking Time 45s is swollen
Swollen power 750W.
Shredding described in step S11 is that cabo is cut to 0.5～1cm length, 0.3～0.5mm wide uniform stem.
Fermentation processing method described in step S12 is:
Preparation inoculation liquid, is 30g inoculation liquid/100g stem inoculation after fermentation according to inoculum concentration, described inoculation
Liquid consist of high fructose syrup: protein peptide: strain: the mass ratio=60g:0.3g:0.3g:100g of distilled water；
Controlling temperature 37 DEG C, fermentation time is 14 days.
Described strain is aspergillus oryzae (Aspergillus oryzae).Described protein peptide is wheat protein peptide.
Embodiment 3
The present embodiment provides a kind of cabo particle being applicable to buccal cigarette, is prepared by following steps:
S11. cabo is carried out wind and washes to remove surface dust, then shredding after microwave bulking；
S12. stem step S11 cut carries out fermentation process, removes bitter taste, acid, and acquisition is sent out
Ferment local flavor；
S13. stem step S12 fermented carries out micronizing, crosses 160 mesh sieves, takes permeation parts and obtain
Described cabo particle；
The process conditions of microwave bulking described in step S11 are: cabo moisture content 18%, and Bulking Time 60s is swollen
Swollen power 900W.
Shredding described in step S11 is that cabo is cut to 2～4cm length, 0.6～0.9mm wide uniform stem.
Fermentation processing method described in step S12 is:
Preparation inoculation liquid, is 20g inoculation liquid/100g stem inoculation after fermentation according to inoculum concentration, described inoculation liquid
Consist of high fructose syrup: protein peptide: strain: the mass ratio=100g:1g:0.5g:200g of distilled water；
Control temperature is at 40 DEG C, and fermentation time is 20 days.
Described strain is yeast (Saccharomyces).Described protein peptide is rice protein peptide.
Embodiment 4
The present embodiment provides a kind of cabo particle being applicable to buccal cigarette, is prepared by following steps:
S11. cabo is carried out wind and washes to remove surface dust, then shredding after microwave bulking；
S12. stem step S11 cut carries out fermentation process, removes bitter taste, acid, and acquisition is sent out
Ferment local flavor；
S13. stem step S12 fermented carries out micronizing, crosses 160 mesh sieves, takes permeation parts and obtain
Described cabo particle；
The process conditions of microwave bulking described in step S11 are: cabo moisture content 18%, and Bulking Time 70s is swollen
Swollen power 900W.
Shredding described in step S11 is that cabo is cut to 1.0～2.0cm length, 0.5～0.6mm wide uniform stalk
Silk.
Fermentation processing method described in step S12 is:
Preparation inoculation liquid, is 30g inoculation liquid/100g stem inoculation after fermentation according to inoculum concentration, described inoculation liquid
Consist of high fructose syrup: protein peptide: strain: the mass ratio=120g:3g:0.6g:200g of distilled water；
Controlling temperature 38 DEG C, fermentation time is 24 days.
Described strain is yeast (Saccharomyces) and the combined inoculation liquid of lactic acid bacteria (Lactobacillus),
The mixed proportion of the two does not do considered critical, preferably 1:4.Described protein peptide is whey protein peptide.
Embodiment 5
The present embodiment provides a kind of cabo particle being applicable to buccal cigarette, is prepared by following steps:
S11. cabo is carried out wind and washes to remove surface dust, then shredding after microwave bulking；
S12. stem step S11 cut carries out fermentation process, removes bitter taste, acid, and acquisition is sent out
Ferment local flavor；
S13. stem step S12 fermented carries out micronizing, crosses 160 mesh sieves, takes permeation parts and obtain
Described cabo particle；
The process conditions of microwave bulking described in step S11 are: cabo moisture content 18%, and Bulking Time 70s is swollen
Swollen power 900W.
Shredding described in step S11 is that cabo is cut to 2.0～3.0cm length, 0.4～0.6mm wide uniform stem.
Fermentation processing method described in step S12 is:
Preparation inoculation liquid, is 20g inoculation liquid/100g stem inoculation after fermentation according to inoculum concentration, described inoculation liquid
Consist of high fructose syrup: protein peptide: strain: the mass ratio=180g:8g:0.6g:300g of distilled water；
Controlling temperature 45 C, fermentation time is 20 days.
Described strain is monascus (Monascuspurpureus Went.) and yeast (Saccharomyces)
Combined inoculation liquid, the mixed proportion of the two is 1:1.Described protein peptide is casein peptide.
Embodiment 6
The present embodiment provides a kind of tobacco leaf granule, is prepared by following steps:
S21. tobacco leaf use water is rinsed, remove surface dust, remove excessive moisture, shredding；
S22. step S21 shredding gained tobacco shred is carried out carbon dioxide expanding treatment, the expanded place of described carbon dioxide
The process conditions of reason are: dip time 5min, expansion temperature 400 DEG C；
S23. step S22 expanding treatment gained tobacco shred is carried out fermentation process, removes bitter taste, acid, obtain
Must be fermented taste；Then by the tobacco shred Crushing of Ultrafine after fermentation, cross 160 mesh sieves, take permeation parts.
Fermentation described in step S23 is preparation inoculation liquid, is 10g inoculation liquid/100g tobacco shred inoculation according to inoculum concentration
After fermentation；Fermentation temperature is 35 DEG C, and the time is 10 days.
Described inoculation liquid consist of high fructose syrup: protein peptide: strain: the mass ratio=80g:0.05 of distilled water
G:0.2g:120g；Described protein peptide is soybean protein peptide and whey protein peptide mass ratio is 1:1.
Described strain is monascus (Monascuspurpureus Went.).
Embodiment 7
The present embodiment provides a kind of tobacco leaf granule, is prepared by following steps:
S21. tobacco leaf use water is rinsed, remove surface dust, remove excessive moisture, shredding；
S22. step S21 shredding gained tobacco shred is carried out carbon dioxide expanding treatment, the expanded place of described carbon dioxide
The process conditions of reason are: dip time 1min, expansion temperature 350 DEG C；
S23. step S22 expanding treatment gained tobacco shred is carried out fermentation process, removes bitter taste, acid,
Obtain fermentation taste；Then by the tobacco shred Crushing of Ultrafine after fermentation, cross 160 mesh sieves, take permeation parts.
Fermentation described in step S23 is preparation inoculation liquid, is 5g inoculation liquid/100g tobacco shred inoculation according to inoculum concentration
After fermentation；Fermentation temperature is 38 DEG C, and the time is 15 days.
Described inoculation liquid consist of high fructose syrup: protein peptide: strain: the mass ratio=60g:3g of distilled water:
0.5g:250g；Described strain is lactic acid bacteria (Lactobacillus).The protein peptide of described inoculation liquid is soybean protein
Peptide.
Embodiment 8
The present embodiment provides a kind of tobacco leaf granule, is prepared by following steps:
S21. tobacco leaf use water is rinsed, remove surface dust, remove excessive moisture, shredding；
S22. step S21 shredding gained tobacco shred is carried out carbon dioxide expanding treatment, the expanded place of described carbon dioxide
The process conditions of reason are: dip time 5min, expansion temperature 400 DEG C.
S23. step S22 expanding treatment gained tobacco shred is carried out fermentation process, removes bitter taste, acid,
Obtain fermentation taste；Then by the tobacco shred Crushing of Ultrafine after fermentation, cross 160 mesh sieves, take permeation parts.
Fermentation described in step S23 is preparation inoculation liquid, is 15g inoculation liquid/100g tobacco shred inoculation according to inoculum concentration
After fermentation；Fermentation temperature is 37 DEG C, and the time is 21 days.
Described inoculation liquid consist of high fructose syrup: protein peptide: strain: the mass ratio=50g:1g of distilled water:
0.08g:120g；Described protein peptide is whey protein peptide.Described strain is rhizopus (Rhizopus).
Embodiment 9
The present embodiment provides a kind of tobacco leaf granule, is prepared by following steps:
S21. tobacco leaf use water is rinsed, remove surface dust, remove excessive moisture, shredding；
S22. step S21 shredding gained tobacco shred is carried out carbon dioxide expanding treatment, the expanded place of described carbon dioxide
The process conditions of reason are: dip time 4min, expansion temperature 400 DEG C；
S23. step S22 expanding treatment gained tobacco shred is carried out fermentation process, removes bitter taste, acid,
Obtain fermentation taste；Then by the tobacco shred Crushing of Ultrafine after fermentation, cross 160 mesh sieves, take permeation parts.
Fermentation described in step S23 is preparation inoculation liquid, is 10g inoculation liquid/100g tobacco shred inoculation according to inoculum concentration
After fermentation；Fermentation temperature is 40 DEG C, and the time is 14 days.
Described inoculation liquid consist of high fructose syrup: protein peptide: strain: the mass ratio=80g:4g of distilled water:
0.3g:350g；Described protein peptide is rice protein peptide.Described strain is Zygosaccharomyces rouxii (Mucor roxianus).
Embodiment 10
Present invention simultaneously provides a kind of buccal cigarette material, this buccal cigarette is according to percentage by weight by following raw material
Composition: tobacco-containing material 60%；Filler 30%；Correctives 1%；Binding agent 7%；Essence 1%；Lubrication
Agent 1%；Described tobacco-containing material be by embodiment 6 to 9 arbitrary example gained tobacco leaf granule and embodiment 1 to
5 arbitrary example gained cabo particle compositions, wherein the mass ratio of tobacco leaf granule and cabo particle is
60%:40%.
Described filler is starch, and described correctives is Sal, and described binding agent is sodium carboxymethyl cellulose,
Described essence is menthol, and described lubricant is magnesium stearate.
The preparation method of described buccal cigarette is as follows:
S1. by after correctives, tobacco-containing material, filler, binding agent mix homogeneously, with dissolved with 10% polyethylene
60% ethanol solution pelletize of ketopyrrolidine, is dried 2h at 40～45 DEG C.
S2. by essence with after appropriate anhydrous alcohol solution, uniformly it is sprayed on above-mentioned granule, adds lubricant
Mixing, compression molding.Tablet forming technique is with reference to existing routine.
Embodiment 11
Present invention simultaneously provides a kind of buccal cigarette material, this buccal cigarette is according to percentage by weight by following raw material
Composition: tobacco-containing material 49%；Filler 35%；Correctives 2.5%；Binding agent 10%；Essence 0.5%；
Lubricant 3%；Described tobacco-containing material is by embodiment 6 to 9 arbitrary example gained tobacco leaf granule and embodiment
1 to 5 arbitrary example gained cabo particle composition, wherein the mass ratio of tobacco leaf granule and cabo particle is
80%:20%.
Described filler is maltodextrin, and described correctives is sodium carbonate, and described binding agent is ethyl cellulose,
Described essence is Folium Camelliae sinensis extract, and described lubricant is Pulvis Talci.
The preparation method of described buccal cigarette is with embodiment 10.
Embodiment 12
Present invention simultaneously provides a kind of buccal cigarette material, this buccal cigarette is according to percentage by weight by following raw material
Composition: tobacco-containing material 40%；Filler 50%；Correctives 0.5%；Binding agent 8.5%；Essence 0.5%；
Lubricant 0.5%；Described tobacco-containing material is by embodiment 6 to 9 arbitrary example gained tobacco leaf granule and enforcement
Example 1 to 5 arbitrary example gained cabo particle forms, wherein tobacco leaf granule and the mass ratio of cabo particle
For 70%:30%.
Described filler is cyclodextrin, and described correctives is sodium benzoate, and described binding agent is gelatin, described
Essence is Fructus Armeniacae Mume extract, and described lubricant is Polyethylene Glycol.
The preparation method of described buccal cigarette is with embodiment 10.
Embodiment 13
Present invention simultaneously provides a kind of buccal cigarette material, this buccal cigarette is according to percentage by weight by following raw material
Composition: tobacco-containing material 52%；Filler 40%；Correctives 5%；Binding agent 1%；Essence 1%；Lubrication
Agent 1%；Described tobacco-containing material be by embodiment 6 to 9 arbitrary example gained tobacco leaf granule and embodiment 1 to
5 arbitrary example gained cabo particle compositions, wherein the mass ratio of tobacco leaf granule and cabo particle is
65%:35%.
Described filler is starch and white sugar mixture (mixing quality ratio 1:1), and wherein white sugar is simultaneously
As binding agent, described correctives is Sal, and described essence is menthyl acetate, and described lubricant is 12
Alkyl sodium sulfate.
The preparation method of described buccal cigarette is with embodiment 10.
Embodiment 14
Present invention simultaneously provides a kind of buccal cigarette material, this buccal cigarette is according to percentage by weight by following raw material
Composition: tobacco-containing material 50%；Filler 45%；Correctives 0.5%；Binding agent 1%；Essence 0.5%；Profit
Lubrication prescription 3%；Described tobacco-containing material is by embodiment 6 to 9 arbitrary example gained tobacco leaf granule and embodiment 1
To 5 arbitrary example gained cabo particle compositions, wherein the mass ratio of tobacco leaf granule and cabo particle is
70%:30%.
Described filler is mannitol, and described correctives is Sal, and described binding agent is white sugar, described perfume (or spice)
Essence is Borneolum Syntheticum, and described lubricant is Polyethylene Glycol.
The preparation method of described buccal cigarette is with embodiment 10.
Embodiment 15
The present embodiment provides a kind of buccal cigarette material, and this buccal cigarette is according to percentage by weight group by following raw material
Become: tobacco leaf granule 40%；Filler 50%；Correctives 0.5%；Binding agent 8.5%；Essence 0.5%；
Lubricant 0.5%；Described tobacco leaf granule is by embodiment 6 to 9 arbitrary example gained tobacco leaf granule.
Described filler is cyclodextrin, and described correctives is sodium benzoate, and described binding agent is gelatin, described essence
For Fructus Armeniacae Mume extract, described lubricant is Polyethylene Glycol.
The preparation method of described buccal cigarette is with embodiment 10.
Embodiment 16
The present embodiment provides a kind of buccal cigarette material, and this buccal cigarette is according to percentage by weight group by following raw material
Become: tobacco leaf granule 49%；Filler 35%；Correctives 2.5%；Binding agent 10%；Essence 0.5%；
Lubricant 3%；Described tobacco leaf granule is by embodiment 6 to 9 arbitrary example gained tobacco leaf granule.Institute
Stating filler is maltodextrin, and described correctives is sodium carbonate, and described binding agent is ethyl cellulose, described
Essence is Folium Camelliae sinensis extract, and described lubricant is Polyethylene Glycol.
The preparation method of described buccal cigarette is with embodiment 10.
Embodiment 17
The present embodiment provides a kind of buccal cigarette material, and this buccal cigarette is according to percentage by weight group by following raw material
Become: tobacco leaf granule 60%；Filler 30%；Correctives 1%；Binding agent 7%；Essence 1%；Profit
Lubrication prescription 1%；Described tobacco leaf granule is by embodiment 6 to 9 arbitrary example gained tobacco leaf granule.Described
Filler is starch, and described correctives is Sal, and described binding agent is sodium carboxymethyl cellulose, described essence
For menthol, described lubricant is Polyethylene Glycol.
The preparation method of described buccal cigarette is as follows:
S1. by after correctives, tobacco-containing material, filler, binding agent mix homogeneously, with dissolved with 10% polyethylene
60% ethanol solution pelletize of ketopyrrolidine, is dried 2h at 40～45 DEG C.
S2. by essence with after appropriate anhydrous alcohol solution, uniformly it is sprayed on above-mentioned granule, adds lubricant
Mixing, compression molding.Tablet forming technique is with reference to existing routine.
Embodiment 18 detection and experiment of smokeing panel test
The product that Example 1 to embodiment 17 any embodiment prepares, is packaged as grain by the specification of 0.5g/
Shape form.
The mensuration of content of nitrite: the chromatography of ions (NY/T 1375-2007 plant product nitrite
Mensuration with nitrate)；The mensuration of protein content: Ke Daerfa (YCT 166-2003 Nicotiana tabacum L. and cigarette
The mensuration of straw-made articles total protein content)；The mensuration of content of cellulose: enzymolysis-flow analysis is (with reference to literary composition
To offer: Guo Song. China examines cigarette Nicotiana tabacum L. pectin, content of cellulose characteristic distributions and impact [D] Henan on reviewing prnciple:
Agricultural University Of He'nan, 2011,18～19)；The mensuration of pectin content: the chromatography of ions (YC/T 346-2010
The mensuration chromatography of ions of Nicotiana tabacum L. and tobacco product pectin)；The mensuration of content of cellulose: enzyme hydrolysis-ion color
Spectrometry (YC/T 283-2009 Nicotiana tabacum L. and tobacco product. the mensuration of starch. enzyme hydrolysis-chromatography of ions)；Wooden
The mensuration of cellulose content: sulfuric acid process (list of references: Tao Yongzhen, Guan Yingting. the chemical constitution of lignin and should
With [J]. Cellulose Science and technology, 2003,11 (1): 43-55).
Through inspection, the content of nitrite of embodiment 1 to 17 products obtained therefrom all between 1.25～1.30%,
Protein content all between 8.9～9.0%, content of cellulose all between 8.65～8.89%, pectin content
All between 12.3～12.5%.
Ask 10 experts that smoke panel test to carry out experiment of smokeing panel test the product that the embodiment of the present invention 1～17 prepares simultaneously.Comment
Absorbing method, for directly to insert between upper lip and upper row's tooth by product, puts into the tobacco shred granular mass of lip every time
For 0.2g, standard edible time is set to 10min.The entirety of embodiment 1 to 17 effect of smokeing panel test is bitter taste
All relatively lighter with acid, the most agreeable to the taste.
The smoking result of embodiment 1 to 17 products obtained therefrom is shown in Table 1.Scoring criterion is, the alkali of buccal cigarette
Rate of release, suck early stage and later stage strength, compliance (the below standard quasi-edible time of buccal cigarette edible time
Be considered as poor compliance by discharge), local flavor, fragrance, pleasant impression respectively account for 10 points, total score 70 points.Comparative example 1 is
The sample of 160 mesh sieves is crossed in unprocessed cabo shredding, and comparative example 2 crosses 160 mesh for unprocessed cabo shredding
The sample of sieve.
Table 1 is smoked panel test result of the test
The invention provides a kind of new tobacco leaf granule, use the fermentation process technique of science, it is thus achieved that be suitable
For preparing the tobacco leaf granule of buccal cigarette, its nitrogen substance is reduced conversion, improves the mouth of raw material
Sense comfortableness, successfully eliminates blue foreign smell and the zest of raw material, without granular sensation, harsh feeling in oral cavity time edible.
Further, the invention provides a kind of new buccal cigarette material, material therefor is based on tobacco material.
All tobacco materials, all by fermentation process, eliminate the bitter taste of tobacco material, acid, and fragrance matter is rich
Rich mellow.And the seasoning combining reasonable benefit/risk processes, use correctives and sweeting agent etc. and the cigarette of rational proportion
Silk granule is compatible, it is thus achieved that more enrich mouthfeel, flavor coordination, high-quality buccal cigarette.
The all of tobacco-containing material of the present invention, after specific aim micronizing, does not have during disintegrate in the oral cavity
Grain sense, taste lubrication, for containing sheet form, can be the most edible, edible end abandons without spuing, will not be right
Environment.
Claims (10)
1. the tobacco leaf granule being applicable to prepare buccal cigarette, it is characterised in that through the following steps that prepare:
S21. tobacco leaf use water is rinsed, remove surface dust, remove excessive moisture, shredding；
S22. step S21 shredding gained tobacco shred is carried out carbon dioxide expanding treatment；
S23. step S22 expanding treatment gained tobacco shred is carried out fermentation process, then Crushing of Ultrafine, sieve, take permeation parts；
Wherein, fermentation described in step S23 is preparation inoculation liquid, is 1～15g inoculation liquid/100g tobacco shred inoculation after fermentation according to inoculum concentration；
Described inoculation liquid consist of high fructose syrup: protein peptide: strain: the mass ratio of water=(50～200) g:(0.1～10) g:(0.01～1) g:(100～500) g；
Described strain be monascus (Monascus purpureus
Went.), aspergillus oryzae (Aspergillus oryzae), Zygosaccharomyces rouxii (Mucor
roxianus) or rhizopus (Rhizopus), yeast (Saccharomyces) or lactic acid bacteria (Lactobacillus) one or more.
It is applicable to prepare the tobacco leaf granule of buccal cigarette the most according to claim 1, it is characterised in that described in step S22, the process conditions of carbon dioxide expanding treatment are: dip time 1～5min, expansion temperature 300～400 DEG C.
It is applicable to prepare the tobacco leaf granule of buccal cigarette the most according to claim 1, it is characterized in that, described inoculation liquid described in step S23 consist of high fructose syrup: protein peptide: strain: the mass ratio of water=(50～100) g:(1～10) g:(0.1～0.8) g:(200～500) g；Fermentation temperature described in step S23 is 35～45 DEG C, and the time is 7～30 days.
4. be applicable to according to Claims 2 or 3 prepare buccal cigarette tobacco leaf granule, it is characterised in that described protein peptide be soybean protein peptide, wheat protein peptide, rice protein peptide, casein peptide, whey protein peptide one or more.
It is applicable to prepare the tobacco leaf granule of buccal cigarette the most according to claim 1, it is characterised in that sieving described in step S23 was 160 mesh sieves, took permeation parts.
6. the application of tobacco leaf granule described in any one of claim 1 to 5, it is characterised in that described tobacco leaf granule is matched with adjuvant, prepares buccal cigarette material.
7. the application of tobacco leaf granule described in any one of claim 1 to 5, it is characterized in that, being matched with cabo particle and adjuvant by described tobacco leaf granule, prepare buccal cigarette material, the mass ratio of described tobacco leaf granule and cabo particle is 60～80%:40～20%.
8. according to the application described in claim 6 or 7, it is characterised in that described adjuvant is for including filler, correctives, binding agent, essence and lubricant.
Application the most according to claim 8, it is characterised in that according to buccal cigarette material 100% mass meter, mass ratio shared by filler is 30～50%；Mass ratio shared by correctives is 0.5～5%；Mass ratio shared by binding agent is 1～10%；Mass ratio shared by essence is 0.1～1%；Mass ratio shared by lubricant is 0.5～3%.
Application the most according to claim 9, it is characterised in that described filler is one or more in starch, maltodextrin, cyclodextrin, microcrystalline Cellulose, white sugar, mannitol or xylitol；Described correctives is one or more of Sal, sodium carbonate or sodium benzoate etc.；Described binding agent is one or more in sodium carboxymethyl cellulose, hydroxypropyl cellulose, methylcellulose, ethyl cellulose, gelatin or white sugar；Described essence is naturally occurring or synthetic perfume monomer, fruit extract or vegetable material extract；Described lubricant is magnesium stearate, Pulvis Talci, sodium lauryl sulphate or Polyethylene Glycol.
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