CN105936804A - UV wood original paint and preparation method thereof - Google Patents
UV wood original paint and preparation method thereof Download PDFInfo
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- CN105936804A CN105936804A CN201610395600.1A CN201610395600A CN105936804A CN 105936804 A CN105936804 A CN 105936804A CN 201610395600 A CN201610395600 A CN 201610395600A CN 105936804 A CN105936804 A CN 105936804A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
- C09D175/14—Polyurethanes having carbon-to-carbon unsaturated bonds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/16—Antifouling paints; Underwater paints
- C09D5/1606—Antifouling paints; Underwater paints characterised by the anti-fouling agent
- C09D5/1612—Non-macromolecular compounds
- C09D5/1618—Non-macromolecular compounds inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Chemical And Physical Treatments For Wood And The Like (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses a UV wood original paint and a preparation method thereof. The UV wood original paint comprises the following components by weight: 10-15 parts of hexa-functional polyurethane acrylic resin, 20-25 parts of bifunctional polyurethane acrylic resin, 30-35 parts of a bifunctional modified UV monomer, 3-5 parts of a photosensitizer, 0.1-0.2 part of a leveling agent, 0.3-0.5 part of a defoaming agent, 0.3-0.5 part of a wetting agent, 15-20 parts of a nano silica dispersion liquid, and 10-15 parts of fused nano silica matte powder. The UV micro-coating paint can penetrate into wood fiber, and after UV irradiation, can undergo crosslinking reaction with wood fiber to form a very thin protective layer, thus reaching wear-resistant and waterproof effects, and also retaining the texture of wood. By adding the nano silica dispersion liquid, the ultraviolet aging resistance and stain resistance are improved, and the drying time is reduced. By adding the fused nano silica matte powder, the gloss is reduced.
Description
Technical field
The invention belongs to industrial coating field, be specifically related to a kind of UV wood crude oil paint and preparation method thereof, particularly to a kind of floor
With UV wood crude oil paint and preparation method thereof.
Background technology
Raising along with national consumption level and the raising to environmental requirement, people have had more selection when selectively slab products
With higher requirement, it is desirable to timber floor is closer to the essential color of timber and texture texture.At present, existing Traditional Wood floor
It is all by coating the thickest painting layer at wood surface, to reach protective effect and to realize aesthetic, but, this painting
Layer seems to cover one layer of overlay the thickest at wood surface, it is impossible to embody textural aesthetic and the sense of touch of timber essence.
Now, people are more likely to when choosing timber floor select wood surface to have thin layer protective layer, can retain the original stricture of vagina of timber
Reason and the timber floor of sense of touch.The most also the product after some improvement is occurred in that, such as dry vegetable oils such as wood wax oil, but due to
It is plant component, does not reaches the requirement of traditional paint on the wear-resisting and high temperature resistant soda acid of hardness.Therefore, increasing floor
Enterprise is highly desirable can have a kind of timber floor that can retain the original texture of timber and sense of touch to occur.
UV wood crude oil paint is a kind of liquid coating being made up of specific functionality organic polymer, and this coating may penetrate into lumber fibre
In, after ultraviolet light irradiates, it can rapidly and lumber fibre crosslinks reaction, reinforcing lumber fibre, and in wood surface shape
Become one layer of protective layer the thinnest, play wear-resisting, waterproof effect, the most do not change the texture texture of timber simultaneously.
Summary of the invention
It is an object of the invention to solve the problems referred to above, it is provided that a kind of UV wood crude oil paint and preparation method thereof, efficiently solve
Wood floor surface on the premise of the thickest painting, scumbling just can reach wear-resisting, drying time is short, pollution resistance is good and the waterproof effect such as good,
The most do not change the texture texture of timber simultaneously.
The technical solution used in the present invention is, a kind of UV wood crude oil paint, including the component of following weight portion:
The present invention with the addition of nano silicon dispersion liquid, and the anti-ultraviolet aging experimental performance of UV micro-coating paint can be by former
The 250h come brings up to more than 600h, and scrub resistance improves more than 10 times, and the drying time of coating is greatly lowered, anti-
Dirty performance is greatly improved, and has excellent self-cleaning property and adhesive force.If without nano silicon dispersion liquid, coating
Resistant and ultraviolet-resistant performance will reduce.
The present invention with the addition of gas phase nano silicon dioxide dumb light powder, can be substantially reduced the glossiness of coating, make coat side lustrous surface
Degree is below 5 degree.If using normal dull powder, do not reach surface gloss effect below 5 degree.
Preferably, described photosensitizer is cracking type photosensitizer.
Preferably, described levelling agent is fluorine richness carbonic ether acrylate.
Preferably, described defoamer is organosilicon defoamer.
Preferably, described wetting agent is polyether-modified poly-silicon dioxide siloxane copolymers class wetting agent.
The preparation method of a kind of UV wood crude oil paint, comprises the following steps:
1) in dispersion cylinder, six official's polyurethane acrylic resins, two official's polyurethane acrylic resins, double official are put into by weight successively
Modified UV monomer, photosensitizer, levelling agent, defoamer, wetting agent, stirring makes mix homogeneously, obtains component A of clear；
2) stirring component A, is added into nano silicon dispersion liquid, mix homogeneously, obtains component B；
3) stirring component B, is added into gas phase nano silicon dioxide dumb light powder, mix homogeneously, obtains described UV wood crude oil paint.
Preferably, in step 1) in, mixing speed is 2000RPM, and mixing time is 20 minutes.
Preferably, in step 2) in, mixing speed is 400RPM, and mixing time is 10 minutes.
Preferably, in step 3) in, mixing speed is 800RPM, and mixing time is 20 minutes.
The invention has the beneficial effects as follows, the UV wood crude oil paint of the present invention may penetrate in lumber fibre, after ultraviolet light irradiates,
Rapid and lumber fibre crosslinks reaction, reinforces lumber fibre, and forms one layer of protective layer the thinnest at wood surface, has
Wear-resisting, waterproof effect, remains again the texture texture of timber simultaneously；Add nano silicon dispersion liquid, improve this painting
The anti-ultraviolet aging performance of material and pollution resistance, be greatly lowered drying time；Add gas phase nano silicon dioxide dumb light powder, fall
The low glossiness of coating；This paint is without formaldehyde, benzene and heavy metal etc., and safety and environmental protection, VOC content are low.
Detailed description of the invention
For further appreciating that the present invention, below in conjunction with embodiment, the preferred embodiment of the invention is described, but it is to be understood that
These descriptions are intended merely to further illustrate the features and advantages of the present invention rather than limiting the scope of the invention.
Six official's polyurethane acrylic resins of the present invention can be selected for the 6145-100 of Changxing company；
Two official's polyurethane acrylic resins of the present invention can be selected for the EB-264 of Qing Te company；
Double official's UV monomers of the present invention can be selected for the EM222 in Changxing；
The photosensitizer of the present invention can use the cracking type photosensitizer 1173 that Hua Tai macromolecular material company produces；
The levelling agent of the present invention can be selected for the BYK-3510 of Bi Ke company；
The defoamer of the present invention can be selected for the BYK-055 of Bi Ke company；
The wetting agent agent of the present invention can be selected for the BYK-306 of Bi Ke company；
The nano silicon dispersion liquid of the present invention can be selected for the VK-S01A of Jing Rui company；
The gas phase nano silicon dioxide dumb light powder of the present invention can be selected for the R972 of goldschmidt chemical corporation.
Embodiment 1
A kind of UV wood crude oil paint, including the component of following weight portion:
UV wood crude oil paint preparation method: (1) put into successively in dispersion cylinder by weight 15 part of six official's polyurethane acrylic resin,
25 part of two official's polyurethane acrylic resin, 30 parts of double official's modification UV monomers, 4 parts of photosensitizer, 0.2 part of levelling agent, 0.3 part disappear
Infusion, 0.5 part of wetting agent, under blender rotating speed is 2000RPM, stirs 20 minutes, make mix homogeneously, obtains clarification thoroughly
Bright component A；(2) under blender rotating speed is 400RPM, stir component A, be added into 15 parts of nano silicons simultaneously and divide
Dissipate liquid, stir 10 minutes, mix homogeneously, obtain component B；(3) under blender rotating speed is transferred to 800PRM, component is stirred
B, is added into 10 parts of gas phase nano silicon dioxide dumb light powder simultaneously, stirs 20 minutes, mix homogeneously, i.e. obtain the present invention's
UV wood crude oil paint.
This UV wood crude oil paint is coated on wood product surface, comprises the steps: that (1) sanding surface processes, it is ensured that element plate table
Face Glabrous thorn；(2) prime treatment is dried with UV: the plain plate UV former paint of wood that will handle well, it is ensured that coating weight
For 5-8g/m2, then it being dried with UV drying machine, drying energy is 100-120mJ/cm2；(3) paint and be dried: will be dried
Plain plate Waterborne wood former paint coating colouring, it is ensured that coating weight is 10-15g/m2, make the former paint of Waterborne wood enter in fiber pore,
Then being dried by the levelling passage that element plate is placed in 10-20 rice long, drying condition is dried 1-2 minute at being 55-60 DEG C；(4) sand
Light, dedusting: dried element plate sanding in step (3) is carried out dust removal process to Waterborne wood former paint smooth surface impulse-free robustness；
(5) middle level processes one: repeat step (2), and to smooth surface impulse-free robustness, gained element plate sanding is carried out dust removal process；(6)
Middle level processes two: by the former paint of gained element plate UV wood in step (5), it is ensured that coating weight is 3-5g/m2, then use
UV drying machine is dried, and drying energy is 100-120mJ/cm2；Sanding carries out dust removal process to smooth surface impulse-free robustness again；(7)
Finish paint processes: repeats step (2), i.e. obtains being coated with the woodwork of UV wood crude oil paint.
Embodiment 2
A kind of UV wood crude oil paint, including the component of following weight portion:
Raw material uses above weight, uses the method for embodiment 1 to prepare UV wood crude oil paint, uses embodiment 1
The UV wood crude oil paint of preparation is coated on wood product surface by method.
Embodiment 3
A kind of UV wood crude oil paint, including the component of following weight portion:
Raw material uses above weight, uses the method for embodiment 1 to prepare UV wood crude oil paint, uses embodiment 1
The UV wood crude oil paint of preparation is coated on wood product surface by method.
Embodiment 4
A kind of UV wood crude oil paint, including the component of following weight portion:
Raw material uses above weight, uses the method for embodiment 1 to prepare UV wood crude oil paint, uses embodiment 1
The UV wood crude oil paint of preparation is coated on wood product surface by method.
UV wood crude oil paint prepared by the present invention, under the conditions of 30 DEG C, is the 15-20 second by salt pan cup tested viscosity.At timber floor element
Continuous roller coat three times on plate, each coating weight 5-8 gram every square, by curing under the energy of 80-120 MJ every square centimeter
Being dried, make paint film, result shows, wood surface is smooth, water-fast, acidproof, wear-resisting.
Comparative example 1
A kind of UV wood crude oil paint, including the component of following weight portion:
This UV wood crude oil paint preparation method: (1) puts into 25 part of six official polyurethane acroleic acid tree by weight in dispersion cylinder successively
Fat, 32 part of two official's polyurethane acrylic resin, 37 parts of double official's modification UV monomers, 5 parts of photosensitizer, 0.2 part of levelling agent, 0.4
Part defoamer, 0.4 part of wetting agent, under blender rotating speed is 2000RPM, stirs 20 minutes, make mix homogeneously, i.e. obtain
This UV wood crude oil paint.
The UV wood crude oil paint of preparation is coated on wood product surface by the method using embodiment 1.
UV wood crude oil paint prepared by embodiment 1-4, has good wear-resisting and waterproof effect, also has good uvioresistant
Line ageing properties and pollution resistance, drying time is short, does not also contain formaldehyde, benzene and heavy metal etc., and safety and environmental protection, VOC content are low；
Compared with common UV wood crude oil paint, its anti-ultraviolet aging experimental performance is 600 hours, common UV wood crude oil paint
Anti-ultraviolet aging experimental performance is only 250 hours, and scrub performance is more than 10 times of common UV wood crude oil paint.
And the UV wood crude oil paint of preparation in comparative example 1, rub resistance and stain resistance are relatively low, and anti-ultraviolet aging performance is also
Poor.
UV wood crude oil paint embodiment 1-4 and comparative example 1 prepared is coated on wood product surface, gained woodwork after coating
Performance test results as shown in table 1.
The performance test results of the woodwork of table 1 embodiment 1-4 and comparative example 1 coating
As shown in Table 1, UV wood crude oil paint prepared by the present invention is coated on wood product surface, and the woodwork of gained all meets every
Index, and the UV wood crude oil paint using comparative example 1 to prepare (does not contains nano silicon dispersion liquid and gas phase nanometer titanium dioxide
Silicon dumb light powder) it is coated on wood product surface, the woodwork rub resistance of gained and stain resistance are substantially reduced, and do not meet every finger
Target specifies.By coating UV wood crude oil paint on woodwork so that it is penetrate into lumber fibre, after ultraviolet light irradiates, fast
Speed and lumber fibre crosslink reaction, reinforce lumber fibre.On the other hand also obtain one at wood surface has relatively thin guarantor
Sheath, waterproof antiwear excellent performance, save again texture and the texture of timber essence simultaneously.
Claims (9)
1. a UV wood crude oil paint, it is characterised in that include the component of following weight portion:
UV wood crude oil paint the most according to claim 1, it is characterised in that described photosensitizer is cracking type photosensitizer.
UV wood crude oil paint the most according to claim 1, it is characterised in that described levelling agent is fluorine richness carbonic ether acrylic acid
Ester.
UV wood crude oil paint the most according to claim 1, it is characterised in that described defoamer is organosilicon defoamer.
UV wood crude oil paint the most according to claim 1, it is characterised in that described wetting agent is polyether-modified poly-silicon dioxide
Siloxane copolymers class wetting agent.
6. the preparation method according to the UV wood crude oil paint according to any one of claim 1-5, it is characterised in that include following
Step:
1) in dispersion cylinder, put into six official's polyurethane acrylic resins, two official's polyurethane acrylic resins, double official modification by weight successively
UV monomer, photosensitizer, levelling agent, defoamer, wetting agent, stirring makes mix homogeneously, obtains component A of clear；
2) stirring component A, is added into nano silicon dispersion liquid, mix homogeneously, obtains component B；
3) stirring component B, is added into gas phase nano silicon dioxide dumb light powder, mix homogeneously, obtains described UV wood crude oil paint.
The preparation method of UV wood crude oil paint the most according to claim 6, it is characterised in that in step 1) in mixing speed be
2000RPM, mixing time is 20 minutes.
The preparation method of UV wood crude oil paint the most according to claim 6, it is characterised in that in step 2) in mixing speed be
400RPM, mixing time is 10 minutes.
The preparation method of UV wood crude oil paint the most according to claim 6, it is characterised in that in step 3) in mixing speed be
800RPM, mixing time is 20 minutes.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610395600.1A CN105936804A (en) | 2016-06-03 | 2016-06-03 | UV wood original paint and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610395600.1A CN105936804A (en) | 2016-06-03 | 2016-06-03 | UV wood original paint and preparation method thereof |
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| CN105936804A true CN105936804A (en) | 2016-09-14 |
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| CN201610395600.1A Pending CN105936804A (en) | 2016-06-03 | 2016-06-03 | UV wood original paint and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114619533A (en) * | 2022-04-12 | 2022-06-14 | 久盛地板有限公司 | Low-luminosity floor production process |
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| CN103275612A (en) * | 2013-05-15 | 2013-09-04 | 江门市国美化工有限公司 | Environment-friendly coating agent and preparation method thereof |
| WO2015068682A1 (en) * | 2013-11-11 | 2015-05-14 | Dic株式会社 | Active energy ray-curable composition, cured product thereof, and article having cured coating film thereof |
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-
2016
- 2016-06-03 CN CN201610395600.1A patent/CN105936804A/en active Pending
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| CN103275612A (en) * | 2013-05-15 | 2013-09-04 | 江门市国美化工有限公司 | Environment-friendly coating agent and preparation method thereof |
| WO2015068682A1 (en) * | 2013-11-11 | 2015-05-14 | Dic株式会社 | Active energy ray-curable composition, cured product thereof, and article having cured coating film thereof |
| CN105273586A (en) * | 2015-10-20 | 2016-01-27 | 宁波大榭开发区综研化学有限公司 | Anti-fouling and anti-UV (ultraviolet) coating composition, hard coating film and preparation method |
| CN105505092A (en) * | 2015-12-25 | 2016-04-20 | 澳达树熊涂料(惠州)有限公司 | Odorless and wear-resisting smooth UV (ultraviolet) matt finish paint coating and preparation method thereof |
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Cited By (1)
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| CN114619533A (en) * | 2022-04-12 | 2022-06-14 | 久盛地板有限公司 | Low-luminosity floor production process |
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Application publication date: 20160914 |