CN105920227A - Preparation method of saffron decoction piece - Google Patents
Preparation method of saffron decoction piece Download PDFInfo
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- CN105920227A CN105920227A CN201610457967.1A CN201610457967A CN105920227A CN 105920227 A CN105920227 A CN 105920227A CN 201610457967 A CN201610457967 A CN 201610457967A CN 105920227 A CN105920227 A CN 105920227A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/17—Preparation or pretreatment of starting material involving drying, e.g. sun-drying or wilting
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Abstract
The invention discloses a preparation method of a saffron decoction piece. The preparation method comprises the following steps of drying: saffron raw materials are flatly paved in a metal container, the metal container is heated by water vapor generated by water bath for drying, and uninterrupted turning is performed to obtain a semi-finished product 1, wherein the temperature of the water bath is 60 to 80 DEG C; humidification: the semi-finished product 1 is flatly paved in a containing tool with holes in the bottom, and the water vapor generated by the water bath humidifies the semi-finished product 1 through the holes, so that a semi-finished product 2 is obtained, wherein the water bath temperature is 85 to 88 DEG C; secondary drying: the semi-finished product 2 is flatly paved in the metal container, the metal container is heated by the water vapor generated by the water bath for drying, and uninterrupted turning is performed, wherein the water bath temperature is 60 to 80 DEG C. The contents of effective ingredients of crocin I and crocin II in the prepared saffron decoction piece are high; the appearance of the obtained saffron decoction piece is attractive; the consumption requirements on the saffron decoction piece in the market are met.
Description
Technical field
The present invention relates to Chinese medicine processing technique field, particularly relate to the preparation method of a kind of west safflower medicine materical crude slice.
Background technology
The cultigen of west safflower Shu Ying tail section crocus, Classification system Crocus Sativus L., have another name called safron,
Safflower, remove that fragrance is blue, pool husband is blue, for herbaceos perennial.
West safflower is used as medicine with gynoecium top column cap, and the sweet property of taste is put down, and has promoting blood circulation and removing blood stasis, removing pattogenic heat from the blood and toxic material from the body, resolving stagnation for tranquilization drug effect.West
The style of safflower and column cap contain several safron glycosides and bayer acid dimethyl ester, safron hardship glycosides etc., the another 0.4-Han volatile oil
1.3%, it is mainly composed of safranal, additionally contains rhamnetin, Kaempferol etc..
It is known that prepared slices of Chinese crude drugs clinical therapeutic efficacy is good and bad directly closely related with its active constituent content height,
West safflower curative effect is no exception.But, the common oven drying method of prior art not only reduces west safflower active constituent content, but also
Destroy medicine materical crude slice mode of appearance.Although west safflower active constituent content is increased by patent document CN201310003571.6, but
Or medicine materical crude slice mode of appearance cannot be improved.This seriously restricts clinical efficacy and the market acceptance level to product of medicine materical crude slice, especially
It is that west safflower does not more meet target market to its active constituent content and the high standard of outward appearance as health products gift sales.
Summary of the invention
The technical problem to be solved is the active ingredient overcoming west safflower medicine materical crude slice processing prior art to exist
Content is low, the defect of medicine materical crude slice cosmetic look difference, it is provided that the preparation method of a kind of west safflower medicine materical crude slice.The west that this preparation method prepares
Active ingredient crocin I in safflower medicine materical crude slice, crocin II content are higher, reach more than 24%, are above prior art, and add
Construction equipment is with low cost, simple to operate；And the medicine materical crude slice flower-shape appearance looks elegant obtained, relatively prior art meets target further
The market consumption demand to west safflower medicine materical crude slice.
The present invention solves above-mentioned technical problem by following technical proposals:
The invention provides the preparation method of a kind of west safflower medicine materical crude slice, it comprises the steps:
(1) it is dried: west safflower raw material is laid in canister, the steam heating metal container produced by water-bath
It is dried, and interval is stirred, and obtains semi-finished product 1；The temperature of described water-bath is 60～80 DEG C；
(2) humidification: be laid in by semi-finished product 1 in the container that bottom is porose, the steam that water-bath produces is through hole humidification half
Finished product 1, thus obtain semi-finished product 2；The temperature of described water-bath is 85～88 DEG C；
(3) redrying: be laid in again in canister by semi-finished product 2, the steam produced by water-bath adds thermometal
Drying containers, and be spaced stir,；The temperature of described water-bath is 60～80 DEG C.
Wherein, the west safflower raw material in the present invention is general commercially.
In step (1), described canister is preferably rustless steel container；The thickness of described tiling is preferably
0.3～0.8cm, it is more preferably 0.3～0.5cm.
In step (1), the temperature of described water-bath is preferably 65～70 DEG C, is more preferably 70 DEG C.
In step (1), the described time being dried is preferably 10～20 minutes.
In step (1), the time interval that described interval is stirred is preferably 3～5 minutes.
In step (2), the mesh number in described hole is preferably 4～18 mesh.
In step (2), the time of described humidification is preferably 3～5 minutes.
In step (3), described canister is preferably rustless steel container；The thickness of described tiling is preferably
0.3～0.8cm, it is more preferably 0.3～0.5cm.
In step (3), the temperature of described water-bath is preferably 65～70 DEG C, is more preferably 70 DEG C.
In step (3), the described time being dried is preferably 10～20 minutes.
In step (3), the time interval that described interval is stirred is preferably 3～5 minutes.
On the basis of meeting common sense in the field, above-mentioned each optimum condition, can be combined, obtain each preferable reality of the present invention
Example.
Agents useful for same of the present invention and raw material are the most commercially.
The most progressive effect of the present invention is:
(1) active ingredient crocin I, crocin II content in the west safflower medicine materical crude slice that the preparation method of the present invention prepares
Higher, reach more than 24%, be above prior art.
(2) fragranced specific to the west safflower medicine materical crude slice that the present invention prepares is denseer, the content of safranal reach 0.6% with
On.
(3) the medicine materical crude slice flower-shape appearance looks elegant that the present invention obtains, does not crimps, and relatively prior art meets target further
Market to west safflower medicine materical crude slice as the consumption demand of gift.
(4) tooling cost of the present invention is cheap, simple to operate.
Accompanying drawing explanation
Fig. 1 is the outward appearance photo of the west safflower medicine materical crude slice that the present invention prepares.
Fig. 2 is the outward appearance photo of the west safflower medicine materical crude slice that comparative example 1,2 prepares
Detailed description of the invention
Further illustrate the present invention below by the mode of embodiment, but the most therefore limit the present invention to described reality
Execute among example scope.The experimental technique of unreceipted actual conditions in the following example, conventionally and condition, or according to business
Product specification selects.
Percentage in following embodiment is mass percent.
Embodiment 1
(1) laid for west safflower metal (stainless steel) container is interior, paving flower thickness is 0.5cm, and canister is produced by water-bath
Raw steam heating, the temperature of water-bath is 70 DEG C, and in heating process, interval is stirred once in 5 minutes, 20 minutes heat times.
(2) humidification: the semi-finished product that step (1) obtains are laid in the container that bottom is porose (the mesh number in hole is 10 mesh),
The steam that water-bath produces humidifies 3 minutes through hole；The temperature of described water-bath is 88 DEG C；
(3) redrying: repeat the above steps (1),.
The colored good looking appearance of the west safflower medicine materical crude slice that the present embodiment prepares, is dried column cap without curling in thin-line-shaped, and top is wider
Greatly, the most tapered in shape of tail, rufous.Dry west safflower is loaded plastic film bag, every bag of 50mg.
Finished product is put the shady and cool place of being dried and is stored.Separately sampled in 0,12,24 months, by 2015 editions Chinese Pharmacopoeias (one) west safflower
Specifying detection under Xiang, result crocin I and crocin II total amount are respectively 26%, 20%, 18%.
The west safflower medicine materical crude slice prepared has denseer special fragranced, shows that safranal content is more, by ultraviolet-can
See that in spectrometer detection medicine materical crude slice, the content of safranal is 0.62%.
Fig. 1 is shown in by the outward appearance photo of the west safflower medicine materical crude slice that this embodiment prepares.
Embodiment 2
(1) laid for west safflower metal (stainless steel) container is interior, paving flower thickness is 0.5cm, and canister is produced by water-bath
Raw steam heating, the temperature of water-bath is 75 DEG C, and in heating process, interval is stirred once in 3 minutes, 15 minutes heat times.
(2) humidification: the semi-finished product that step (1) obtains are laid in the container that bottom is porose (the mesh number in hole is 18 mesh),
The steam that water-bath produces humidifies 4 minutes through hole；The temperature of described water-bath is 86 DEG C；
(3) redrying: repeat the above steps (1),.
The colored good looking appearance of the west safflower medicine materical crude slice that the present embodiment prepares, is dried column cap without curling in thin-line-shaped, and top is wider
Greatly, the most tapered in shape of tail, rufous.Dry west safflower is loaded plastic film bag, every bag of 50mg.
Finished product is put the shady and cool place of being dried and is stored.Separately sampled in 0,12,24 months, by 2015 editions Chinese Pharmacopoeias (one) west safflower
Specifying detection under Xiang, result crocin I and crocin II total amount are respectively 24%, 22%, 20%.
The west safflower medicine materical crude slice prepared has denseer special fragranced, shows that safranal content is more, by ultraviolet-can
See that in spectrometer detection medicine materical crude slice, the content of safranal is 0.63%.
Fig. 1 is shown in by the outward appearance photo of the west safflower medicine materical crude slice that this embodiment prepares.
Embodiment 3
(1) laid for west safflower metal (stainless steel) container is interior, paving flower thickness is 0.5cm, and canister is produced by water-bath
Raw steam heating, the temperature of water-bath is 80 DEG C, and in heating process, interval is stirred once in 4 minutes, 17 minutes heat times.
(2) humidification: the semi-finished product that step (1) obtains are laid in the container that bottom is porose (the mesh number in hole is 4 mesh), water
The steam that bath produces humidifies 5 minutes through hole；The temperature of described water-bath is 85 DEG C；
(3) redrying: repeat the above steps (1),.
The colored good looking appearance of the west safflower medicine materical crude slice that the present embodiment prepares, is dried column cap without curling in thin-line-shaped, and top is wider
Greatly, the most tapered in shape of tail, rufous.Dry west safflower is loaded plastic film bag, every bag of 50mg.
Finished product is put the shady and cool place of being dried and is stored.Separately sampled in 0,12,24 months, by 2015 editions Chinese Pharmacopoeias (one) west safflower
Specifying detection under Xiang, result crocin I and crocin II total amount are respectively 25%, 22%, 20%.
The west safflower medicine materical crude slice prepared has denseer special fragranced, shows that safranal content is more, by ultraviolet-can
See that in spectrometer detection medicine materical crude slice, the content of safranal is 0.62%.
Fig. 1 is shown in by the outward appearance photo of the west safflower medicine materical crude slice that this embodiment prepares.
Embodiment 4
(1) laid for west safflower metal (stainless steel) container is interior, paving flower thickness is 0.4cm, and canister is produced by water-bath
Raw steam heating, the temperature of water-bath is 79 DEG C, and in heating process, interval is stirred once in 4 minutes, 10 minutes heat times.
(2) humidification: the semi-finished product that step (1) obtains are laid in the container that bottom is porose (the mesh number in hole is 15 mesh),
The steam that water-bath produces humidifies 4 minutes through hole；The temperature of described water-bath is 86 DEG C；
(3) redrying: repeat the above steps (1),.
The colored good looking appearance of the west safflower medicine materical crude slice that the present embodiment prepares, is dried column cap without curling in thin-line-shaped, and top is wider
Greatly, the most tapered in shape of tail, rufous.Dry west safflower is loaded plastic film bag, every bag of 50mg.
Finished product is put the shady and cool place of being dried and is stored.Separately sampled in 0,12,24 months, by 2015 editions Chinese Pharmacopoeias (one) west safflower
Specifying detection under Xiang, result crocin I and crocin II total amount are respectively 26%, 21%, 20%.
The west safflower medicine materical crude slice prepared has denseer special fragranced, shows that safranal content is more, by ultraviolet-can
See that in spectrometer detection medicine materical crude slice, the content of safranal is 0.63%.
Fig. 1 is shown in by the outward appearance photo of the west safflower medicine materical crude slice that this embodiment prepares.
Comparative example 1
Use commercially available micro-wave oven to be dried west safflower, paving flower thickness 0.4cm, temperature 90 DEG C, be spaced and stir once in 3 minutes, time
Between 15 minutes.
The product flower profile curling that this example prepares.Dry west safflower is loaded plastic film bag, every bag of 50mg.
Finished product is put the shady and cool place of being dried and is stored.Separately sampled in 0,12,24 months, by 2015 editions Chinese Pharmacopoeias (one) west safflower
Specifying detection under Xiang, result crocin I and crocin II total amount are respectively 20%, 18%, 18%.
The west safflower medicine materical crude slice prepared only has the lightest special fragranced, shows that safranal content is relatively low, by ultraviolet-can
See that in spectrometer detection medicine materical crude slice, the content of safranal is 0.32%.
Fig. 2 is shown in by the outward appearance photo of the west safflower medicine materical crude slice that this comparative example prepares.
Comparative example 2
Use commercially available micro-wave oven to be dried west safflower, paving flower thickness 0.4cm, temperature 60 C, be spaced and stir once in 3 minutes, time
Between 20 minutes.
The product flower profile curling that this example prepares.Dry west safflower is loaded plastic film bag, every bag of 50mg.
Finished product is put the shady and cool place of being dried and is stored.Separately sampled in 0,12,24 months, by 2015 editions Chinese Pharmacopoeias (one) west safflower
Specifying detection under Xiang, result crocin I and crocin II total amount are respectively 22%, 16%, 12%.
The west safflower medicine materical crude slice prepared only has the lightest special fragranced, shows that safranal content is relatively low, by ultraviolet-can
See that in spectrometer detection medicine materical crude slice, the content of safranal is 0.3%.
Fig. 2 is shown in by the outward appearance photo of the west safflower medicine materical crude slice that this comparative example prepares.
From the comparison of Fig. 1, Fig. 2, the west safflower medicine materical crude slice flower-shape appearance looks elegant that the present invention prepares, do not crimp；And
The west safflower medicine materical crude slice that comparative example 1～2 obtains after using microwave drying can crimp.
Comparative example 3
Use water proof to be evaporated technique and west safflower is dried process: laid for west safflower metal (stainless steel) container is interior,
Paving flower thickness is 0.5cm, directly uses heating water bath canister, and bath temperature is 90 DEG C, and in heating process, interval is stirred for 5 minutes
Once, heat time 15 minutes.
The product flower profile curling that this example prepares.Dry west safflower is loaded plastic film bag, every bag of 50mg.
Finished product is put the shady and cool place of being dried and is stored.Separately sampled in 0,12,24 months, by 2015 editions Chinese Pharmacopoeias (one) west safflower
Specifying detection under Xiang, result crocin I and crocin II total amount are respectively 21%, 19%, 18%.
The west safflower medicine materical crude slice prepared only has the lightest special fragranced, shows that safranal content is relatively low, by ultraviolet-can
See that in spectrometer detection medicine materical crude slice, the content of safranal is 0.1%.
Claims (10)
1. a preparation method for west safflower medicine materical crude slice, it comprises the steps:
(1) it is dried: being laid in canister by west safflower raw material, the steam heating metal container produced by water-bath is carried out
It is dried, and interval is stirred, and obtains semi-finished product 1；The temperature of described water-bath is 60～80 DEG C；
(2) humidification: being laid in by semi-finished product 1 in the container that bottom is porose, the steam that water-bath produces humidifies semi-finished product through hole
1, thus obtain semi-finished product 2；The temperature of described water-bath is 85～88 DEG C；
(3) redrying: semi-finished product 2 are laid in canister again, the steam heating metal container produced by water-bath
It is dried, and interval is stirred,；The temperature of described water-bath is 60～80 DEG C.
2. preparation method as claimed in claim 1, it is characterised in that in step (1), described canister is that stainless steel holds
Device；The thickness of described tiling is 0.3～0.8cm, preferably 0.3～0.5cm.
3. preparation method as claimed in claim 1, it is characterised in that in step (1), the temperature of described water-bath is 65～70
DEG C, preferably 70 DEG C.
4. preparation method as claimed in claim 1, it is characterised in that in step (1), the described time being dried is 10～20
Minute.
5. preparation method as claimed in claim 1, it is characterised in that in step (1), the time interval that described interval is stirred
It it is 3～5 minutes.
6. preparation method as claimed in claim 1, it is characterised in that in step (2), the mesh number in described hole is 4～18 mesh.
7. preparation method as claimed in claim 1, it is characterised in that in step (2), the time of described humidification is 3～5 points
Clock.
8. preparation method as claimed in claim 1, it is characterised in that in step (3), described canister is that stainless steel holds
Device；The thickness of described tiling is 0.3～0.8cm, preferably 0.3～0.5cm.
9. preparation method as claimed in claim 1, it is characterised in that in step (3), the temperature of described water-bath is 65～70
DEG C, preferably 70 DEG C.
10. preparation method as claimed in claim 1, it is characterised in that in step (3), the described time being dried be 10～
20 minutes；
In step (3), the time interval that described interval is stirred is 3～5 minutes.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110522826A (en) * | 2019-08-28 | 2019-12-03 | 广东元德中药饮片有限公司 | A kind of west safflower prepared slices of Chinese crude drugs and preparation method thereof |
| CN114431385A (en) * | 2022-02-18 | 2022-05-06 | 杭州康馨宏生物技术有限公司 | Saffron-containing solid beverage, preparation method and application |
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| CN110522826A (en) * | 2019-08-28 | 2019-12-03 | 广东元德中药饮片有限公司 | A kind of west safflower prepared slices of Chinese crude drugs and preparation method thereof |
| CN114431385A (en) * | 2022-02-18 | 2022-05-06 | 杭州康馨宏生物技术有限公司 | Saffron-containing solid beverage, preparation method and application |
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