CN105918755A - Nano-selenium oyster polysaccharide solid drink - Google Patents
Nano-selenium oyster polysaccharide solid drink Download PDFInfo
- Publication number
- CN105918755A CN105918755A CN201610320410.3A CN201610320410A CN105918755A CN 105918755 A CN105918755 A CN 105918755A CN 201610320410 A CN201610320410 A CN 201610320410A CN 105918755 A CN105918755 A CN 105918755A
- Authority
- CN
- China
- Prior art keywords
- concha ostreae
- polysaccharide
- nanometer
- ostreae polysaccharide
- selenizing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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- 150000004676 glycans Chemical class 0.000 title claims abstract description 49
- 229920001282 polysaccharide Polymers 0.000 title claims abstract description 48
- 239000005017 polysaccharide Substances 0.000 title claims abstract description 48
- 239000007787 solid Substances 0.000 title claims abstract description 21
- 239000011669 selenium Substances 0.000 title abstract description 18
- 229910052711 selenium Inorganic materials 0.000 title abstract description 17
- 241000237502 Ostreidae Species 0.000 title abstract description 6
- 235000020636 oyster Nutrition 0.000 title abstract description 6
- 238000000502 dialysis Methods 0.000 claims abstract description 7
- 238000000605 extraction Methods 0.000 claims abstract description 7
- 238000004806 packaging method and process Methods 0.000 claims abstract description 3
- 235000013361 beverage Nutrition 0.000 claims description 14
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 4
- BVTBRVFYZUCAKH-UHFFFAOYSA-L disodium selenite Chemical compound [Na+].[Na+].[O-][Se]([O-])=O BVTBRVFYZUCAKH-UHFFFAOYSA-L 0.000 claims description 4
- 239000012153 distilled water Substances 0.000 claims description 4
- 229960001471 sodium selenite Drugs 0.000 claims description 4
- 239000011781 sodium selenite Substances 0.000 claims description 4
- 235000015921 sodium selenite Nutrition 0.000 claims description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 4
- 238000010009 beating Methods 0.000 claims description 2
- 238000004108 freeze drying Methods 0.000 claims description 2
- 239000007788 liquid Substances 0.000 claims description 2
- 239000000843 powder Substances 0.000 claims description 2
- 238000001556 precipitation Methods 0.000 claims description 2
- 238000001694 spray drying Methods 0.000 claims description 2
- 238000003756 stirring Methods 0.000 claims description 2
- 239000006228 supernatant Substances 0.000 claims description 2
- 229910021642 ultra pure water Inorganic materials 0.000 claims description 2
- 239000012498 ultrapure water Substances 0.000 claims description 2
- 238000009461 vacuum packaging Methods 0.000 claims description 2
- 238000003809 water extraction Methods 0.000 claims description 2
- 230000003078 antioxidant effect Effects 0.000 abstract description 2
- 239000000796 flavoring agent Substances 0.000 abstract description 2
- 235000019634 flavors Nutrition 0.000 abstract description 2
- 238000001035 drying Methods 0.000 abstract 1
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 description 14
- 229940091258 selenium supplement Drugs 0.000 description 14
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 2
- 230000004071 biological effect Effects 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- -1 hydroxyl radical free radical Chemical class 0.000 description 2
- 229910052500 inorganic mineral Inorganic materials 0.000 description 2
- 239000011707 mineral Substances 0.000 description 2
- 235000010755 mineral Nutrition 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 235000015170 shellfish Nutrition 0.000 description 2
- XOAAWQZATWQOTB-UHFFFAOYSA-N taurine Chemical compound NCCS(O)(=O)=O XOAAWQZATWQOTB-UHFFFAOYSA-N 0.000 description 2
- 235000013343 vitamin Nutrition 0.000 description 2
- 239000011782 vitamin Substances 0.000 description 2
- 229930003231 vitamin Natural products 0.000 description 2
- 229940088594 vitamin Drugs 0.000 description 2
- 239000011701 zinc Substances 0.000 description 2
- 229910052725 zinc Inorganic materials 0.000 description 2
- FPIPGXGPPPQFEQ-UHFFFAOYSA-N 13-cis retinol Natural products OCC=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-UHFFFAOYSA-N 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 208000024172 Cardiovascular disease Diseases 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- 229920002527 Glycogen Polymers 0.000 description 1
- 229920000869 Homopolysaccharide Polymers 0.000 description 1
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 1
- AHLPHDHHMVZTML-BYPYZUCNSA-N L-Ornithine Chemical compound NCCC[C@H](N)C(O)=O AHLPHDHHMVZTML-BYPYZUCNSA-N 0.000 description 1
- AHLPHDHHMVZTML-UHFFFAOYSA-N Orn-delta-NH2 Natural products NCCCC(N)C(O)=O AHLPHDHHMVZTML-UHFFFAOYSA-N 0.000 description 1
- UTJLXEIPEHZYQJ-UHFFFAOYSA-N Ornithine Natural products OC(=O)C(C)CCCN UTJLXEIPEHZYQJ-UHFFFAOYSA-N 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- OUUQCZGPVNCOIJ-UHFFFAOYSA-M Superoxide Chemical compound [O-][O] OUUQCZGPVNCOIJ-UHFFFAOYSA-M 0.000 description 1
- FPIPGXGPPPQFEQ-BOOMUCAASA-N Vitamin A Natural products OC/C=C(/C)\C=C\C=C(\C)/C=C/C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-BOOMUCAASA-N 0.000 description 1
- 229930003270 Vitamin B Natural products 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- FPIPGXGPPPQFEQ-OVSJKPMPSA-N all-trans-retinol Chemical compound OC\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-OVSJKPMPSA-N 0.000 description 1
- 230000000259 anti-tumor effect Effects 0.000 description 1
- 230000010100 anticoagulation Effects 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000003653 coastal water Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000009509 drug development Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 235000013376 functional food Nutrition 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 229940096919 glycogen Drugs 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 235000013402 health food Nutrition 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 238000000338 in vitro Methods 0.000 description 1
- 150000002772 monosaccharides Chemical group 0.000 description 1
- 239000002105 nanoparticle Substances 0.000 description 1
- 239000002417 nutraceutical Substances 0.000 description 1
- 235000021436 nutraceutical agent Nutrition 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 230000000050 nutritive effect Effects 0.000 description 1
- 229960003104 ornithine Drugs 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 150000004804 polysaccharides Polymers 0.000 description 1
- 235000018102 proteins Nutrition 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000002000 scavenging effect Effects 0.000 description 1
- 210000003491 skin Anatomy 0.000 description 1
- 210000004927 skin cell Anatomy 0.000 description 1
- 230000001502 supplementing effect Effects 0.000 description 1
- 229960003080 taurine Drugs 0.000 description 1
- 235000019155 vitamin A Nutrition 0.000 description 1
- 239000011719 vitamin A Substances 0.000 description 1
- 235000019156 vitamin B Nutrition 0.000 description 1
- 239000011720 vitamin B Substances 0.000 description 1
- 229940045997 vitamin a Drugs 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/385—Concentrates of non-alcoholic beverages
- A23L2/39—Dry compositions
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
The invention relates to a nano-selenium oyster polysaccharide solid drink and belongs to the field of solid drinks. The solid drink with high solubility and good taste is prepared from oyster through polysaccharide extraction, dialysis, selenylation, drying and packaging. The polysaccharide content of the nano-selenium oyster polysaccharide solid drink is 7.67%, polysaccharide enrichment is realized, stability is high, organoleptic quality and flavor are good, and the solid drink has certain antioxidant activity and accords with relevant standards on solid drinks.
Description
Technical field
The invention belongs to solid beverage field, be specifically related to a kind of nanometer selenizing Concha Ostreae polysaccharide solid beverage product.
Background technology
Concha Ostreae has another name called oysters, oyster, is distributed in each ocean in temperate zone and the torrid zone stretch of coastal water, is the first big cultivated shellfish, one of big cultivated shellfish of Ye Shi China four in the world.Concha Ostreae is the marine food of a kind of comprehensive nutrition, internal containing nutrients such as abundant glycogen, protein, minerals and vitamins, has the non-nutritive element of different physiological roles possibly together with taurine, ornithine etc..Vitamin contained in Concha Ostreae and the kind of mineral are the most complete, including vitamin A, B, C, D, E, H etc. and calcium, selenium, phosphorus, ferrum, zinc etc., wherein vitamin B group, zinc, Se content are the abundantest, and this is that Concha Ostreae provides huge feasibility as nutraceutical, functional food, the raw material of drug development.
Concha Ostreae polysaccharide is by the homopolysaccharide of glucose polymerisation, and its structure is complicated, and relative molecular mass is between millions of to tens million of.Concha Ostreae polysaccharide has good biological activity, has obvious preventing and treating cardiovascular disease function, also has blood fat reducing, anticoagulation, the activity of raising body's immunity.Japanese Scientists also finds that Concha Ostreae polysaccharide can promote that Skin Cell regenerates, and alleviates the functions such as the damage that skin causes by ultraviolet.
Nanometer selenium is as a kind of existence form of selenium element, it is possible to directly remove interior free yl, and bio-toxicity is low, can be absorbed rapidly by organism.But, nanometer selenium is easily reunited so that it is non-oxidizability and anti-tumor activity are gradually lowered along with the increase of particle diameter, this greatly limits nanometer selenium in health food and the application of field of medicaments.
Summary of the invention
It is an object of the invention to provide a kind of nanometer selenizing Concha Ostreae polysaccharide solid beverage, thus provide a kind of good stability, preparation method simple nanometer selenium product, to make up the deficiency of existing nanometer selenium supplementing preparation.
A kind of nanometer selenizing Concha Ostreae polysaccharide solid beverage, it is characterised in that described solid beverage is to be prepared with following steps:
1) extraction of Concha Ostreae polysaccharide: take fresh Carnis ostreae and clean up, stir evenly with refiner making beating, then hot water extraction is carried out, by centrifugal for lixiviating solution except precipitation, cryoconcentration, then according to certain proportioning adds the ethanol of the 95% of appropriate volume in concentrated solution, it is centrifuged off supernatant and i.e. obtains Concha Ostreae polysaccharide；
2) dialysis treatment: the Concha Ostreae polysaccharide distilled water obtained in step 1) is dissolved again, putting into molecular weight interception is in 8000 daltonian bag filters, with the distilled water dialysis 24h of flowing, then dialyse 24h with ultra-pure water, then by the Concha Ostreae polysaccharide solution cryoconcentration after dialysis；
3) selenization: with step 2) in the Concha Ostreae polysaccharide that obtains as template, add a certain proportion of sodium selenite solution and Vc solution, water-bath 30min, carry out nanometer selenization；
4) it is dried: by the nanometer selenizing Concha Ostreae polysaccharide solution cryoconcentration in step 3), then carry out lyophilization or low temperature spray drying；
5) packaging: dried Concha Ostreae polysaccharide powder is carried out vacuum packaging and is nanometer selenizing Concha Ostreae polysaccharide solid beverage.
Preferably, it is 30mL/g-50ml/g that Concha Ostreae polysaccharide extraction conditions controls liquid ratio, Extracting temperature 50 DEG C-60 DEG C, extraction time 3h-6h.
Preferably, the condition of selenization is final concentration of 200 mg/L-400mg/L, the Vc of Concha Ostreae polysaccharide and the mol ratio of sodium selenite is 3:1.
The structure of Concha Ostreae polysaccharide is complicated, has abundant glycosidic bond, monosaccharide residue and link position, it is possible to form different space conformations, is a kind of preferably nanometer selenium size control agent.The present invention is combined with nanometer selenium and the respective feature of Concha Ostreae polysaccharide and advantage, carrys out constructing function nanometer selenium with Concha Ostreae polysaccharide for biological template adjusting control agent, alleviates the reuniting effect of nanoparticle, enhances the biological activity of nanometer selenium and Concha Ostreae polysaccharide.
Accompanying drawing explanation
Fig. 1: the scanning electron microscope (SEM) photograph of nanometer selenizing Concha Ostreae polysaccharide.
Fig. 2: the transmission electron microscope picture of nanometer selenizing Concha Ostreae polysaccharide.
Nanometer selenizing Concha Ostreae polysaccharide prepared by the present invention, nanometer selenium diameter is at about 50nm, and these nano granules of selenium are combined in (Fig. 1) on Concha Ostreae polysaccharide skeleton by physical absorption.Nanometer selenium surface is without covering, and size is consistent, and be evenly distributed (Fig. 2).The nanometer selenizing Concha Ostreae polysaccharide of the present invention has certain antioxidant activity in vitro.When the concentration of nanometer selenizing Concha Ostreae polysaccharide is 56mg/L, 32mg/L and 320mg/L, the Scavenging activity of hydroxyl radical free radical, DPPH free radical and superoxide radical is respectively 32.7%, 94.7% and 21.7%.The nanometer selenizing Concha Ostreae polysaccharide solid beverage that the present invention produces, polyoses content is 7.67%, has reached the purpose of polysaccharide enrichment, good stability, has good organoleptic quality and local flavor, meets solid beverage relevant criterion.
Claims (3)
1. a nanometer selenizing Concha Ostreae polysaccharide solid beverage, it is characterised in that described nanometer selenizing Concha Ostreae polysaccharide solid beverage is to be prepared with following steps:
1) extraction of Concha Ostreae polysaccharide: take fresh Carnis ostreae and clean up, stir evenly with refiner making beating, then hot water extraction is carried out, by centrifugal for lixiviating solution except precipitation, cryoconcentration, then according to certain proportioning adds the ethanol of the 95% of appropriate volume in concentrated solution, it is centrifuged off supernatant and i.e. obtains Concha Ostreae polysaccharide；
2) dialysis treatment: the Concha Ostreae polysaccharide distilled water obtained in step 1) is dissolved again, putting into molecular weight interception is in 8000 daltonian bag filters, with the distilled water dialysis 24h of flowing, then dialyse 24h with ultra-pure water, then by the Concha Ostreae polysaccharide solution cryoconcentration after dialysis；
3) selenization: with step 2) in the Concha Ostreae polysaccharide that obtains as template, add a certain proportion of sodium selenite solution and Vc solution, water-bath 30min, carry out nanometer selenization；
4) it is dried: by the nanometer selenizing Concha Ostreae polysaccharide solution cryoconcentration in step 3), then carry out lyophilization or low temperature spray drying；
5) packaging: dried Concha Ostreae polysaccharide powder is carried out vacuum packaging and is nanometer selenizing Concha Ostreae polysaccharide solid beverage.
2. nanometer selenizing Concha Ostreae polysaccharide solid beverage as claimed in claim 1, it is characterised in that it is 30mL/g-50ml/g that Concha Ostreae polysaccharide extraction conditions controls liquid ratio, Extracting temperature 50 DEG C-60 DEG C, extraction time 3h-6h.
3. nanometer selenizing Concha Ostreae polysaccharide solid beverage as claimed in claim 1, it is characterised in that the condition of selenization be final concentration of 200 mg/L-400mg/L, the Vc of Concha Ostreae polysaccharide be 3:1 with the mol ratio of sodium selenite.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610320410.3A CN105918755A (en) | 2016-05-16 | 2016-05-16 | Nano-selenium oyster polysaccharide solid drink |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610320410.3A CN105918755A (en) | 2016-05-16 | 2016-05-16 | Nano-selenium oyster polysaccharide solid drink |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105918755A true CN105918755A (en) | 2016-09-07 |
Family
ID=56835965
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610320410.3A Pending CN105918755A (en) | 2016-05-16 | 2016-05-16 | Nano-selenium oyster polysaccharide solid drink |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105918755A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110200287A (en) * | 2019-06-29 | 2019-09-06 | 华南理工大学 | A kind of oyster polypeptide-nano granules of selenium compound and the preparation method and application thereof with relieving alcoholism and protecting liver effect |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1594236A (en) * | 2004-07-06 | 2005-03-16 | 湖南大学 | Nano selenium nutrition conditioning agent for fruit and vegetable and its preparing process |
| CN102895258A (en) * | 2011-07-25 | 2013-01-30 | 香港理工大学 | Pleurotus tuber-regium polysaccharide functionalized nanometer selenium hydrosol having anti-tumor activity and preparation method thereof |
| CN105418789A (en) * | 2016-01-20 | 2016-03-23 | 济宁医学院 | Method for preparing low-molecular oyster polysaccharide with immune adjustment and anti-tumor activity |
-
2016
- 2016-05-16 CN CN201610320410.3A patent/CN105918755A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1594236A (en) * | 2004-07-06 | 2005-03-16 | 湖南大学 | Nano selenium nutrition conditioning agent for fruit and vegetable and its preparing process |
| CN102895258A (en) * | 2011-07-25 | 2013-01-30 | 香港理工大学 | Pleurotus tuber-regium polysaccharide functionalized nanometer selenium hydrosol having anti-tumor activity and preparation method thereof |
| CN105418789A (en) * | 2016-01-20 | 2016-03-23 | 济宁医学院 | Method for preparing low-molecular oyster polysaccharide with immune adjustment and anti-tumor activity |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110200287A (en) * | 2019-06-29 | 2019-09-06 | 华南理工大学 | A kind of oyster polypeptide-nano granules of selenium compound and the preparation method and application thereof with relieving alcoholism and protecting liver effect |
| CN110200287B (en) * | 2019-06-29 | 2023-06-09 | 华南理工大学 | Oyster polypeptide-nano selenium particle compound with effects of dispelling effects of alcohol and protecting liver as well as preparation method and application thereof |
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| PB01 | Publication | ||
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| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20160907 |
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