CN105918351A - Nano anion function material and preparing method thereof - Google Patents
Nano anion function material and preparing method thereof Download PDFInfo
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- CN105918351A CN105918351A CN201610312080.3A CN201610312080A CN105918351A CN 105918351 A CN105918351 A CN 105918351A CN 201610312080 A CN201610312080 A CN 201610312080A CN 105918351 A CN105918351 A CN 105918351A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N61/00—Biocides, pest repellants or attractants, or plant growth regulators containing substances of unknown or undetermined composition, e.g. substances characterised only by the mode of action
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/06—Aluminium; Calcium; Magnesium; Compounds thereof
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- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K3/00—Materials not provided for elsewhere
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Abstract
The invention discloses a nano anion function material and a preparing method thereof. The material is prepared from, by weight, 20-30 parts of tourmaline, 20-30 parts of germanite, 15-25 parts of opal shale, 10-20 parts of six-ring stone, 20-30 parts of Xiuyan jade, 5-15 parts of sienna stone, 25-35 parts of seabed placer, 10-20 parts of lvshou stone, 15-25 parts of muyu stone and 30-40 parts of changdao ballstone. The nano anion function material prepared from opal shale, six-ring stone, Xiuyan jade, sienna stone, seabed placer, lvshou stone, muyu stone and the like has a lasting anion generating function, a good far infrared emission function and excellent antibacterial and sterilization functions, has a wide application range, and is suitable for environment protection, cigarettes, paint, leather, plates, photocatalyst, ceramics, wallpaper, textile, cosmetics, water purification, air purification, electromagnetic radiation prevention, healthcare products and other fields.
Description
Technical field
The present invention relates to a kind of anion function material and preparation method thereof.
Background technology
Along with the further investigation that air ionization is theoretical, principle and application that negative aeroion is occurred by people cause
Interest greatly.It is known that the admixture of gas that air is made up of multiple gases, in some energy field
Under effect, in gas molecule, the outer-shell electron of some atom can leave track, becomes free electron, and free
Free electron can combine with the molecule of other neutrality so as to get the gas molecule of excess electron is negative electrode again
Property, it is referred to as " negative aeroion ".The anion Producing reason of nature, mainly cosmic ray, ore deposit
Thing lonizing radiation, corona discharge, current waterfall and the photosynthesis of forest plants.It is to say, anion produces
Exciting of energy is produced in the internal potential energy of Cucumber and the Nature meteorological activity.
Anion material, is the principle of human use's nature generation anion, synthetic or the one of proportioning
Plant complex mineral, because it has pyroelectricity and piezoelectricity, therefore in the case of having temperature and pressure change (i.e.
Make small change) electric potential difference between composition crystal can be caused, this electrostatic is up to 1,000,000 electron-volts,
So that air ionizes, that is hit is electronically attached to neighbouring water and oxygen molecule and makes it be converted into sky
Gas anion, i.e. negative oxygen ion.Negative oxygen ion has following functions: 1. can accelerate moisture movement, make general
Water flowing becomes activated water, so that the penetration of water, extension, dissolving power, metabolism power strengthen, and produces water
Protecting film.2. for blood circulation, expansion blood capillary can be played, strengthen blood circulation, promote new old generation
Thank, strengthen the effect of lymph circulation；For cell tissue, cell activation can be made, make the excretion of old dead cell or compose
Giving regeneration capacity, can strengthen cellular energy, function and the vigor etc. that strengthen cell act on, and improve asthma etc. and breathe
Systemic disease, improves anxious state of mind, depressed mood, confirmed fatigue, alleviates psychentonia situation etc., to people
Health, emotion, energy of great advantage, 3. chalk dust removing, except floating hair, eliminate the unusual smell, smoke abatement, sterilization, purify
Air, eliminates foreign flavor indoors and various harmful gas.
Along with the function of anion material is constantly recognized by people, the research to anion product is subject to the most day by day
To paying attention to, and anion product is had important effect, become the focus of the market competition in recent years, before application
Scape is considerable.But, the most domestic research for anion function material is less, and exploitation anion is just produced by this
Product bring certain difficulty.Therefore, develop a kind of anion function material and there is important value and meaning.
Summary of the invention
Present invention aims to the deficiencies in the prior art, it is provided that a kind of nano-negative ion functional material and
Preparation method.The nano-negative ion functional material that the present invention prepares has permanent negative ion generating function, stronger
Far-infrared transmitting function and excellent antibiotic and sterilizing function.
For achieving the above object, the present invention adopts the following technical scheme that:
A kind of nano-negative ion functional material, is made up of the raw material of following weight portion: tourmaline 20-30, germanite
20-30, opal shale 15-25, hexacyclic ring stone 10-20, Xiuyan jade 20-30, loess stone 5-15, seabed
Placer 25-35, green longevity stone 10-20, Muyu-Stone 15-25, Long Island ballstone 30-40.
The preparation method of a kind of nano-negative ion functional material, comprises the following steps:
(1) by tourmaline, germanite, opal shale, hexacyclic ring stone, Xiuyan jade, loess stone, seabed sand
Ore deposit, green longevity stone, Muyu-Stone, the mixing of Long Island ballstone, calcine 2-5h at 480-560 DEG C, be cooled to room temperature,
It is ground into the granule that particle diameter is 35-45 μm, adds appropriate water stirring and make the suspension that concentration is 45-55%,
Then by the sodium hydroxide solution regulation pH of suspension that concentration is 15% to 8-9, microwave treatment 1-3h, microwave
Power is 300-500W, and magnetic force vibration 0.5-1.5h, frequency of oscillation is 400-600Hz, then is 20% by concentration
Hydrochloric acid solution regulation pH of suspension to 5-6, microwave treatment 1-2h, microwave power is 500-700W, ultrasonic
Vibration 0.5-1h, frequency of oscillation is 40-60KHz, is finally that 15% sodium carbonate liquor is neutralized to neutrality by concentration,
Under the rotating speed of 6000-8000r/min, centrifugal 5-10min, stands 10-15h, filters, and is dried and removes moisture removal
To moisture content≤2%；
(2) raw mineral materials that step (1) prepares being carried out secondary clacining, calcining heat is 540-620 DEG C,
Calcination time is 1-3h, is cooled to room temperature, is then milled to granule under the rotating speed of 8000-10000r/min
Particle diameter is 10-15 μm；
(3) raw mineral materials that step (2) prepares is milled under the rotating speed of 10000-15000r/min
Grain particle diameter is 50-100nm, gets product.
Beneficial effects of the present invention:
The present invention with opal shale, hexacyclic ring stone, Xiuyan jade, loess stone, seabed placer, green longevity stone 10-20,
The nano-negative ion functional material that the raw materials such as Muyu-Stone prepare has permanent negative ion generating function, stronger remote
Infrared emission function and excellent antibiotic and sterilizing function, applied range, it is adaptable to environmental protection, Medicated cigarette, coating,
Leather, sheet material, photocatalyst, pottery, wallpaper, weaving, cosmetics, purify water, purify air, anti-electric
The field such as magnetic radiation, health product.
Detailed description of the invention
Embodiment 1
A kind of nano-negative ion functional material, is made up of the raw material of following weight (kg): tourmaline 20, germanium
Stone 20, opal shale 15, hexacyclic ring stone 10, Xiuyan jade 20, loess stone 5, seabed placer 25, green longevity
Stone 10, Muyu-Stone 15, Long Island ballstone 30.
The preparation method of a kind of nano-negative ion functional material, comprises the following steps:
(1) by tourmaline, germanite, opal shale, hexacyclic ring stone, Xiuyan jade, loess stone, seabed sand
Ore deposit, green longevity stone, Muyu-Stone, the mixing of Long Island ballstone, calcine 5h at 480 DEG C, be cooled to room temperature, be ground into
Particle diameter is the granule of 35 μm, adds appropriate water stirring and makes the suspension that concentration is 45%, then uses concentration
Be 15% sodium hydroxide solution regulation pH of suspension to 8, microwave treatment 1h, microwave power is 500W, magnetic
Forced oscillation 0.5h, frequency of oscillation is 600Hz, then by the hydrochloric acid solution regulation pH of suspension that concentration is 20% to 5,
Microwave treatment 1h, microwave power is 700W, sonic oscillation 0.5h, and frequency of oscillation is 60KHz, finally with dense
Degree is that 15% sodium carbonate liquor is neutralized to neutrality, and under the rotating speed of 6000r/min, centrifugal 10min, stands 10h,
Filter, be dried and go moisture removal to moisture content≤2%；
(2) raw mineral materials that step (1) prepares being carried out secondary clacining, calcining heat is 540 DEG C, calcining
Time is 3h, is cooled to room temperature, and being then milled to grain diameter under the rotating speed of 8000r/min is 10 μm；
(3) raw mineral materials that step (2) prepares is milled to grain diameter under the rotating speed of 10000r/min
For 50nm, get product.
Embodiment 2
A kind of nano-negative ion functional material, is made up of the raw material of following weight (kg): tourmaline 25, germanium
Stone 25, opal shale 20, hexacyclic ring stone 15, Xiuyan jade 25, loess stone 10, seabed placer 30, green
Longevity stone 15, Muyu-Stone 20, Long Island ballstone 35.
The preparation method of a kind of nano-negative ion functional material, comprises the following steps:
(1) by tourmaline, germanite, opal shale, hexacyclic ring stone, Xiuyan jade, loess stone, seabed sand
Ore deposit, green longevity stone, Muyu-Stone, the mixing of Long Island ballstone, calcine 3h at 530 DEG C, be cooled to room temperature, be ground into
Particle diameter is the granule of 40 μm, adds appropriate water stirring and makes the suspension that concentration is 50%, then uses concentration
Be 15% sodium hydroxide solution regulation pH of suspension to 8.5, microwave treatment 2h, microwave power is 400W,
Magnetic force vibration 1h, frequency of oscillation is 500Hz, then by the hydrochloric acid solution regulation pH of suspension that concentration is 20% extremely
5.5, microwave treatment 1.5h, microwave power is 600W, sonic oscillation 0.5h, and frequency of oscillation is 50KHz,
Being that 15% sodium carbonate liquor is neutralized to neutrality by concentration afterwards, under the rotating speed of 7000r/min, centrifugal 8min, stands
12h, filters, and is dried and goes moisture removal to moisture content≤2%；
(2) raw mineral materials that step (1) prepares being carried out secondary clacining, calcining heat is 580 DEG C, calcining
Time is 2h, is cooled to room temperature, and being then milled to grain diameter under the rotating speed of 9000r/min is 12 μm；
(3) raw mineral materials that step (2) prepares is milled to grain diameter under the rotating speed of 12000r/min
For 80nm, get product.
Embodiment 3
A kind of nano-negative ion functional material, is made up of the raw material of following weight (kg): tourmaline 30, germanium
Stone 30, opal shale 25, hexacyclic ring stone 20, Xiuyan jade 30, loess stone 15, seabed placer 35, green
Longevity stone 20, Muyu-Stone 25, Long Island ballstone 40.
The preparation method of a kind of nano-negative ion functional material, comprises the following steps:
(1) by tourmaline, germanite, opal shale, hexacyclic ring stone, Xiuyan jade, loess stone, seabed sand
Ore deposit, green longevity stone, Muyu-Stone, the mixing of Long Island ballstone, calcine 2h at 560 DEG C, be cooled to room temperature, be ground into
Particle diameter is the granule of 45 μm, adds appropriate water stirring and makes the suspension that concentration is 55%, then uses concentration
Be 15% sodium hydroxide solution regulation pH of suspension to 9, microwave treatment 3h, microwave power is 300W, magnetic
Forced oscillation 1.5h, frequency of oscillation is 400Hz, then by the hydrochloric acid solution regulation pH of suspension that concentration is 20% to 6,
Microwave treatment 2h, microwave power is 700W, sonic oscillation 1h, and frequency of oscillation is 40KHz, finally uses concentration
Being that 15% sodium carbonate liquor is neutralized to neutrality, under the rotating speed of 8000r/min, centrifugal 5min, stands 15h, mistake
Filter, is dried and goes moisture removal to moisture content≤2%；
(2) raw mineral materials that step (1) prepares being carried out secondary clacining, calcining heat is 620 DEG C, calcining
Time is 1h, is cooled to room temperature, and being then milled to grain diameter under the rotating speed of 10000r/min is 15 μm；
(3) raw mineral materials that step (2) prepares is milled to grain diameter under the rotating speed of 15000r/min
For 100nm, get product.
Take the nano-negative ion functional material that the 500g present invention prepares to be placed in seal box, uniformly spread out, airtight
24h, with Japan day intrinsic safety sky generation air-anion concentration tester ITC-201A every detection in 1 hour once,
Taking 20 data, the meansigma methods trying to achieve each data is shown in Table 1 as final detection result, test result every time.
Table 1 negative ion concentration test tables of data
Claims (2)
1. a nano-negative ion functional material, it is characterised in that be made up of the raw material of following weight portion: tourmaline
20-30, germanite 20-30, opal shale 15-25, hexacyclic ring stone 10-20, Xiuyan jade 20-30, loess
Stone 5-15, seabed placer 25-35, green longevity stone 10-20, Muyu-Stone 15-25, Long Island ballstone 30-40.
2. the preparation method of a nano-negative ion functional material as claimed in claim 1, it is characterised in that bag
Include following steps:
(1) by tourmaline, germanite, opal shale, hexacyclic ring stone, Xiuyan jade, loess stone, seabed placer,
Green longevity stone, Muyu-Stone, Long Island ballstone mix, and calcine 2-5h, are cooled to room temperature, pulverize at 480-560 DEG C
The granule becoming particle diameter to be 35-45 μm, adds appropriate water stirring and makes the suspension that concentration is 45-55%, so
Afterwards by the sodium hydroxide solution regulation pH of suspension that concentration is 15% to 8-9, microwave treatment 1-3h, microwave merit
Rate is 300-500W, and magnetic force vibration 0.5-1.5h, frequency of oscillation is 400-600Hz, then is 20% by concentration
Hydrochloric acid solution regulation pH of suspension to 5-6, microwave treatment 1-2h, microwave power is 500-700W, ultrasonic
Vibration 0.5-1h, frequency of oscillation is 40-60KHz, is finally that 15% sodium carbonate liquor is neutralized to neutrality by concentration,
Under the rotating speed of 6000-8000r/min, centrifugal 5-10min, stands 10-15h, filters, and is dried and removes moisture removal
To moisture content≤2%；
(2) raw mineral materials that step (1) prepares being carried out secondary clacining, calcining heat is 540-620 DEG C, calcining
Time is 1-3h, is cooled to room temperature, is then milled to grain diameter under the rotating speed of 8000-10000r/min
For 10-15 μm；
(3) raw mineral materials that step (2) prepares is milled to particle under the rotating speed of 10000-15000r/min
Footpath is 50-100nm, gets product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201610312080.3A CN105918351A (en) | 2016-05-11 | 2016-05-11 | Nano anion function material and preparing method thereof |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106473917A (en) * | 2016-11-01 | 2017-03-08 | 淄博福万工贸有限公司 | Hot moxibustion particle of nano biological and preparation method thereof |
| CN107057140A (en) * | 2017-05-17 | 2017-08-18 | 黑龙江工业学院 | A kind of function protective gear material being used in sports field and preparation method thereof |
| CN108554065A (en) * | 2018-05-14 | 2018-09-21 | 合肥奇呗数字科技有限公司 | A kind of preparation method of high efficient air purifier |
| CN109536019A (en) * | 2018-11-21 | 2019-03-29 | 邓小武 | A kind of nano-negative ion function dry powder wall clothing and preparation method thereof |
| CN109736077A (en) * | 2018-11-26 | 2019-05-10 | 福建省绿城环保科技有限公司 | For spraying the liquor and preparation method that shine wall clothing anion function fibrous material |
| CN109879664A (en) * | 2019-01-02 | 2019-06-14 | 深圳市紫莹新材料科技有限公司 | A kind of preparation method of infrared porous ceramics powder and its application in tobacco |
| CN113248827A (en) * | 2021-05-14 | 2021-08-13 | 广州市纳能环保技术开发有限公司 | Sterilizing and fresh-keeping tablet and preparation method and application thereof |
| CN114455948A (en) * | 2020-11-10 | 2022-05-10 | 李昭林 | Calcined synthetic material and preparation method thereof, and negative oxygen ion ceramic and preparation method thereof |
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| CN103964826A (en) * | 2014-04-08 | 2014-08-06 | 安徽省亚欧陶瓷有限责任公司 | Ceramic tile containing radium stone powder and preparation method of ceramic tile |
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| US20100068299A1 (en) * | 2003-01-27 | 2010-03-18 | Van Der Krieken Wilhelmus Maria | Lignosulfonate compositions for control of plant pathogens |
| CN102268209A (en) * | 2010-06-04 | 2011-12-07 | 费解东 | Preparation of coating material releasing negative ions |
| CN103708482A (en) * | 2013-12-23 | 2014-04-09 | 杨立新 | Preparation method of medicinal attapulgite powder preparation |
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Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106473917A (en) * | 2016-11-01 | 2017-03-08 | 淄博福万工贸有限公司 | Hot moxibustion particle of nano biological and preparation method thereof |
| CN107057140A (en) * | 2017-05-17 | 2017-08-18 | 黑龙江工业学院 | A kind of function protective gear material being used in sports field and preparation method thereof |
| CN108554065A (en) * | 2018-05-14 | 2018-09-21 | 合肥奇呗数字科技有限公司 | A kind of preparation method of high efficient air purifier |
| CN109536019A (en) * | 2018-11-21 | 2019-03-29 | 邓小武 | A kind of nano-negative ion function dry powder wall clothing and preparation method thereof |
| CN109736077A (en) * | 2018-11-26 | 2019-05-10 | 福建省绿城环保科技有限公司 | For spraying the liquor and preparation method that shine wall clothing anion function fibrous material |
| CN109879664A (en) * | 2019-01-02 | 2019-06-14 | 深圳市紫莹新材料科技有限公司 | A kind of preparation method of infrared porous ceramics powder and its application in tobacco |
| CN109879664B (en) * | 2019-01-02 | 2021-07-27 | 深圳市紫莹新材料科技有限公司 | Preparation method of infrared porous ceramic powder and application of infrared porous ceramic powder in tobacco |
| CN114455948A (en) * | 2020-11-10 | 2022-05-10 | 李昭林 | Calcined synthetic material and preparation method thereof, and negative oxygen ion ceramic and preparation method thereof |
| CN114455948B (en) * | 2020-11-10 | 2024-02-02 | 李昭林 | Calcining synthetic material and preparation method thereof, negative oxygen ion ceramic and preparation method thereof |
| CN113248827A (en) * | 2021-05-14 | 2021-08-13 | 广州市纳能环保技术开发有限公司 | Sterilizing and fresh-keeping tablet and preparation method and application thereof |
| CN113248827B (en) * | 2021-05-14 | 2023-04-28 | 广州市纳能环保技术开发有限公司 | Sterilizing fresh-keeping tablet and preparation method and application thereof |
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