CN105832637A - Nanometer anion functional material for cosmetics and preparing method of nanometer anion functional material - Google Patents

Nanometer anion functional material for cosmetics and preparing method of nanometer anion functional material Download PDF

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Publication number
CN105832637A
CN105832637A CN201610312409.6A CN201610312409A CN105832637A CN 105832637 A CN105832637 A CN 105832637A CN 201610312409 A CN201610312409 A CN 201610312409A CN 105832637 A CN105832637 A CN 105832637A
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parts
functional material
stone
skin
nanometer anion
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沈平
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/26Aluminium; Compounds thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/987Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/10General cosmetic use

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical & Material Sciences (AREA)
  • Dermatology (AREA)
  • Zoology (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses a nanometer anion functional material for cosmetics and a preparing method of the nanometer anion functional material. The nanometer anion functional material is prepared from, by weight, 23-31 parts of natural crystal salt ore, 18-27 parts of Xiuyan jade, 12-19 parts of hectorite, 14-22 parts of sericite, 4-6 parts of polyaluminum chloride, 16-24 parts of natural ocean stone, 20-30 parts of germanite, 17-26 parts of actinolite, 13-21 parts of Tianying stone and 15-25 parts of pearl powder. The raw materials such as natural crystal salt ore, Xiuyan jade, natural ocean stone and germanite are added, and thus the nanometer anion functional material can release anions and emit far infrared rays, and can have the effects of promoting the metabolism of the skin, eliminating skin toxins, resisting radiation, repairing skin damaged cells and enhancing the cell activity when acting on the skin; the raw materials such as hectorite, Tianying stone and jade powder are added, and thus the nanometer anion functional material has a good adsorption effect, can adsorb harmful bacteria on the skin surface and inhibit growth of bacteria, is suitable for cosmetic skin-care products of emulsion, facial cleansers, night cream, shower gel, toning lotion, facial masks and pressed powder, and has the effects of eliminating acne, killing bacteria, removing freckles, whitening and moistening the skin, achieving rehabilitation and the like.

Description

A kind of nano-negative ion functional material used for cosmetic and preparation method thereof
Technical field
The present invention relates to a kind of anion function material and preparation method thereof, be specifically related to a kind of nanometer used for cosmetic Anion function material and preparation method thereof.
Background technology
Along with the further investigation that air ionization is theoretical, principle and application that negative aeroion is occurred by people cause Interest greatly.It is known that the admixture of gas that air is made up of multiple gases, in some energy field Under effect, in gas molecule, the outer-shell electron of some atom can leave track, becomes free electron, and free Free electron can combine with the molecule of other neutrality so as to get the gas molecule of excess electron is negative electrode again Property, it is referred to as " negative aeroion ".The anion Producing reason of nature, mainly cosmic ray, ore deposit Thing lonizing radiation, corona discharge, current waterfall and the photosynthesis of forest plants.It is to say, anion produces Exciting of energy is produced in the internal potential energy of Cucumber and the Nature meteorological activity.
Anion material, is the principle of human use's nature generation anion, synthetic or the one of proportioning Plant complex mineral, because it has pyroelectricity and piezoelectricity, therefore in the case of having temperature and pressure change (i.e. Make small change) electric potential difference between composition crystal can be caused, this electrostatic is up to 1,000,000 electron-volts, So that air ionizes, that is hit is electronically attached to neighbouring water and oxygen molecule and makes it be converted into sky Gas anion, i.e. negative oxygen ion.Negative oxygen ion has following functions: 1. can accelerate moisture movement, make general Water flowing becomes activated water, so that the penetration of water, extension, dissolving power, metabolism power strengthen, and produces water Protecting film.2. for blood circulation, expansion blood capillary can be played, strengthen blood circulation, promote new old generation Thank, strengthen the effect of lymph circulation;For cell tissue, cell activation can be made, make the excretion of old dead cell or compose Giving regeneration capacity, can strengthen cellular energy, function and the vigor etc. that strengthen cell act on, and improve asthma etc. and breathe Systemic disease, improves anxious state of mind, depressed mood, confirmed fatigue, alleviates psychentonia situation etc., to people Health, emotion, energy of great advantage, 3. chalk dust removing, except floating hair, eliminate the unusual smell, smoke abatement, sterilization, purify Air, eliminates foreign flavor indoors and various harmful gas.
Along with the function of anion material is constantly recognized by people, the research to anion product is subject to the most day by day To paying attention to.Anion function material functional cosmetics high-grade for exploitation has important effect, becomes in recent years For the focus of the market competition, application prospect is considerable.But, the most domestic for anion function material used for cosmetic The research of material is less, and this just brings certain difficulty to exploitation negative ionization cosmetic.Therefore, exploitation oneization Cosmetic anion function material has important value and meaning.
Summary of the invention
Present invention aims to the deficiencies in the prior art, it is provided that a kind of nano-negative ion function used for cosmetic Material and preparation method thereof.
For achieving the above object, the present invention adopts the following technical scheme that:
A kind of nano-negative ion functional material used for cosmetic, is made up of the raw material of following weight portion: mineral crystal salt Ore 23-31, Xiuyan jade 18-27, hectorite 12-19, sericite 14-22, aluminium polychlorid 4-6, Stone 13-21, Margarita powder 15-25 are answered in natural marine stone 16-24, germanite 20-30, Actinolitum 17-26, sky.
The preparation method of a kind of nano-negative ion functional material used for cosmetic, comprises the following steps:
(1) by mineral crystal salt Ore, Xiuyan jade, hectorite, sericite, natural marine stone, germanite, Actinolitum, sky answer stone to mix, and calcine 2-4h, be cooled to room temperature at 440-490 DEG C, and being ground into particle diameter is The granule of 25-45 μm, adds appropriate water stirring and makes the suspension that concentration is 55-60%, then use concentration Be 15% sodium hydroxide solution regulation pH of suspension to 8-9, microwave treatment 2-3h, microwave power be 150-250W, magnetic force vibration 0.5-1h, frequency of oscillation is 400-500Hz, more molten with the hydrochloric acid that concentration is 20% Liquid regulation pH of suspension is 450-550W to 5-6, microwave treatment 1-2h, microwave power, sonic oscillation 1-2h, Frequency of oscillation is 40-50KHz, is finally that 15% sodium carbonate liquor is neutralized to neutrality by concentration, Under the rotating speed of 2000-4000r/min, centrifugal 10-20min, stands 10-15h, filters, and is dried and goes moisture removal extremely Moisture content≤2%;
(2) raw mineral materials that step (1) prepares being carried out secondary clacining, calcining heat is 590-660 DEG C, Calcination time is 1-3h, is cooled to room temperature, is then milled to granule under the rotating speed of 9000-11000r/min Particle diameter is 10-20 μm;
(3) raw mineral materials that step (2) prepares is mixed with the raw material such as aluminium polychlorid, Margarita powder, then Being milled to grain diameter under the rotating speed of 10000-12000r/min is 200-400nm, gets product.
Beneficial effects of the present invention:
The raw materials such as the mineral crystal salt Ore of present invention interpolation, Xiuyan jade, natural marine stone, germanite, permissible Anion releasing, emitting far-infrared, act on the metabolism that can promote skin on skin, get rid of skin poison Element, keeps out radiation, repairs skin damage cell and strengthens the effect of cell viability, the hectorite of interpolation, thin,tough silk cloud The raw material such as mother, sky Ying Shi, jade powder, has a good adsorption, adsorbable skin surface noxious bacteria, Bacteria growing inhibiting, it is adaptable to emulsion, cleansing milk, late frost, bath gel, astringent, facial film, muffin etc. are changed Adornment skin product, have the effects such as the pox that disappears, sterilization, speckle dispelling, whitening, skin moistening, rehabilitation.
Detailed description of the invention
Embodiment 1
A kind of nano-negative ion functional material used for cosmetic, is made up of the raw material of following weight (kg): natural water Brilliant salt Ore 23, Xiuyan jade 18, hectorite 12, sericite 14, aluminium polychlorid 4, natural marine stone 16, stone 13, Margarita powder 15 are answered in germanite 20, Actinolitum 17, sky.
The preparation method of a kind of nano-negative ion functional material used for cosmetic, comprises the following steps:
(1) by mineral crystal salt Ore, Xiuyan jade, hectorite, sericite, natural marine stone, germanite, Actinolitum, sky answer stone to mix, and calcine 4h, be cooled to room temperature at 440 DEG C, and being ground into particle diameter is 25 μm Granule, add the stirring of appropriate water and make the suspension that concentration is 55%, be then the hydrogen-oxygen of 15% by concentration Change sodium solution regulation pH of suspension to 8, microwave treatment 2h, microwave power is 250W, magnetic force vibration 0.5h, Frequency of oscillation is 500Hz, then by the hydrochloric acid solution regulation pH of suspension that concentration is 20% to 5, microwave treatment 1h, Microwave power is 550W, sonic oscillation 1h, and frequency of oscillation is 50KHz, is finally that 15% sodium carbonate is molten by concentration Liquid is neutralized to neutrality, and under the rotating speed of 2000r/min, centrifugal 20min, stands 10h, filters, and is dried and removes Moisture is to moisture content≤2%;
(2) raw mineral materials that step (1) prepares being carried out secondary clacining, calcining heat is 590 DEG C, calcining Time is 3h, is cooled to room temperature, and being then milled to grain diameter under the rotating speed of 9000r/min is 10 μm;
(3) raw mineral materials that step (2) prepares is mixed with the raw material such as aluminium polychlorid, Margarita powder, then Being milled to grain diameter under the rotating speed of 10000r/min is 200nm, gets product.
Embodiment 2
A kind of nano-negative ion functional material used for cosmetic, is made up of the raw material of following weight (kg): natural water Brilliant salt Ore 27, Xiuyan jade 23, hectorite 16, sericite 18, aluminium polychlorid 5, natural marine stone 20, stone 17, Margarita powder 20 are answered in germanite 25, Actinolitum 21, sky.
The preparation method of a kind of nano-negative ion functional material used for cosmetic, comprises the following steps:
(1) by mineral crystal salt Ore, Xiuyan jade, hectorite, sericite, natural marine stone, germanite, Actinolitum, sky answer stone to mix, and calcine 3h, be cooled to room temperature at 460 DEG C, and being ground into particle diameter is 35 μm Granule, add the stirring of appropriate water and make the suspension that concentration is 56%, be then the hydrogen-oxygen of 15% by concentration Change sodium solution regulation pH of suspension to 8.5, microwave treatment 2.5h, microwave power is 200W, magnetic force vibration 0.5h, Frequency of oscillation is 450Hz, then by the hydrochloric acid solution regulation pH of suspension that concentration is 20% to 5.5, microwave treatment 1.5h, microwave power is 500W, sonic oscillation 1.5h, and frequency of oscillation is 45KHz, is finally 15% by concentration Sodium carbonate liquor is neutralized to neutrality, and under the rotating speed of 3000r/min, centrifugal 15min, stands 12h, filters, Being dried goes moisture removal to moisture content≤2%;
(2) raw mineral materials that step (1) prepares being carried out secondary clacining, calcining heat is 620 DEG C, calcining Time is 2h, is cooled to room temperature, and being then milled to grain diameter under the rotating speed of 10000r/min is 15 μm;
(3) raw mineral materials that step (2) prepares is mixed with the raw material such as aluminium polychlorid, Margarita powder, then Being milled to grain diameter under the rotating speed of 11000r/min is 300nm, gets product.
Embodiment 3
A kind of nano-negative ion functional material used for cosmetic, is made up of the raw material of following weight (kg): mineral crystal Salt Ore 31, Xiuyan jade 27, hectorite 19, sericite 22, aluminium polychlorid 6, natural marine stone 24, Stone 21, Margarita powder 25 are answered in germanite 30, Actinolitum 26, sky.
The preparation method of a kind of nano-negative ion functional material used for cosmetic, comprises the following steps:
(1) by mineral crystal salt Ore, Xiuyan jade, hectorite, sericite, natural marine stone, germanite, Actinolitum, sky answer stone to mix, and calcine 2h, be cooled to room temperature at 490 DEG C, and being ground into particle diameter is 45 μm Granule, add the stirring of appropriate water and make the suspension that concentration is 60%, be then the hydrogen-oxygen of 15% by concentration Change sodium solution regulation pH of suspension is to 9, and microwave treatment 3h, microwave power is 150W, magnetic force vibration 1h, shakes Swinging frequency is 400Hz, then by the hydrochloric acid solution regulation pH of suspension that concentration is 20% to 6, microwave treatment 2h, Microwave power is 450W, sonic oscillation 2h, and frequency of oscillation is 40KHz, is finally that 15% sodium carbonate is molten by concentration Liquid is neutralized to neutrality, and under the rotating speed of 4000r/min, centrifugal 10min, stands 15h, filters, and is dried and removes Moisture is to moisture content≤2%;
(2) raw mineral materials that step (1) prepares being carried out secondary clacining, calcining heat is 660 DEG C, calcining Time is 1h, is cooled to room temperature, and being then milled to grain diameter under the rotating speed of 11000r/min is 10 μm;
(3) raw mineral materials that step (2) prepares is mixed with the raw material such as aluminium polychlorid, Margarita powder, then Being milled to grain diameter under the rotating speed of 12000r/min is 400nm, gets product.
Take the nano-negative ion functional material that the 500g present invention prepares to be placed in seal box, uniformly spread out, airtight 24h, with Japan day intrinsic safety sky generation air-anion concentration tester ITC-201A every detection in 1 hour once, Taking 20 data, the meansigma methods trying to achieve each data is shown in Table 1 as final detection result, test result every time.
Table 1 negative ion concentration test tables of data

Claims (2)

1. a nano-negative ion functional material used for cosmetic, it is characterised in that be made up of the raw material of following weight portion: Mineral crystal salt Ore 23-31, Xiuyan jade 18-27, hectorite 12-19, sericite 14-22, polymerization chlorine Stone 13-21, Margarita are answered in change aluminum 4-6, natural marine stone 16-24, germanite 20-30, Actinolitum 17-26, sky Powder 15-25.
2. a preparation method for nano-negative ion functional material used for cosmetic as claimed in claim 1, its feature It is, comprises the following steps:
(1) by mineral crystal salt Ore, Xiuyan jade, hectorite, sericite, natural marine stone, germanite, sun Play stone, sky answers stone to mix, and calcines 2-4h, be cooled to room temperature at 440-490 DEG C, and being ground into particle diameter is 25-45 The granule of μm, adds the stirring of appropriate water and makes the suspension that concentration is 55-60%, is then 15% by concentration Sodium hydroxide solution regulation pH of suspension be 150-250W to 8-9, microwave treatment 2-3h, microwave power, Magnetic force vibration 0.5-1h, frequency of oscillation is 400-500Hz, then suspends with the hydrochloric acid solution regulation that concentration is 20% Liquid pH to 5-6, microwave treatment 1-2h, microwave power is 450-550W, sonic oscillation 1-2h, frequency of oscillation For 40-50KHz, it is finally that 15% sodium carbonate liquor is neutralized to neutrality, 2000-4000r/min's by concentration Under rotating speed, centrifugal 10-20min, stands 10-15h, filters, and is dried and goes moisture removal to moisture content≤2%;
(2) raw mineral materials that step (1) prepares being carried out secondary clacining, calcining heat is 590-660 DEG C, calcining Time is 1-3h, is cooled to room temperature, is then milled to grain diameter under the rotating speed of 9000-11000r/min For 10-20 μm;
(3) raw mineral materials that step (2) prepares is mixed with the raw material such as aluminium polychlorid, Margarita powder, then exist Being milled to grain diameter under the rotating speed of 10000-12000r/min is 200-400nm, gets product.
CN201610312409.6A 2016-05-11 2016-05-11 Nanometer anion functional material for cosmetics and preparing method of nanometer anion functional material Pending CN105832637A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106924061A (en) * 2017-03-31 2017-07-07 广东宝爵新材料实业有限公司 A kind of nano-negative ion face cleaning composition
CN109704646A (en) * 2018-11-26 2019-05-03 福建省绿城环保科技有限公司 A kind of nano-negative ion functional wall clothing dry powder and preparation method thereof
CN113521049A (en) * 2021-07-29 2021-10-22 姚雷利 Stretch mark demolding repair method

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106924061A (en) * 2017-03-31 2017-07-07 广东宝爵新材料实业有限公司 A kind of nano-negative ion face cleaning composition
CN109704646A (en) * 2018-11-26 2019-05-03 福建省绿城环保科技有限公司 A kind of nano-negative ion functional wall clothing dry powder and preparation method thereof
CN113521049A (en) * 2021-07-29 2021-10-22 姚雷利 Stretch mark demolding repair method

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