CN105907475A - Tobacco flavor capable of reducing hazardous substance in smoke and bobbin paper containing same - Google Patents
Tobacco flavor capable of reducing hazardous substance in smoke and bobbin paper containing same Download PDFInfo
- Publication number
- CN105907475A CN105907475A CN201610410827.9A CN201610410827A CN105907475A CN 105907475 A CN105907475 A CN 105907475A CN 201610410827 A CN201610410827 A CN 201610410827A CN 105907475 A CN105907475 A CN 105907475A
- Authority
- CN
- China
- Prior art keywords
- tobacco
- obbbin
- flavouring essence
- celery seed
- vitexin
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H19/00—Coated paper; Coating material
- D21H19/10—Coatings without pigments
- D21H19/14—Coatings without pigments applied in a form other than the aqueous solution defined in group D21H19/12
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
- D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention provides tobacco flavor capable of reducing hazardous substance in smoke and a preparation method thereof. The invention further provides application of tobacco flavor in bobbin paper. Adopted celery seeds have pleasant strong fragrance and acrid and bitter taste, and can cover up the woodiness and scorch smell in bobbin paper made in China and improve smoking flavor of cigarettes after being combined with vitexin, umbelliferone and maltol; meanwhile, by adopting the specific production technology, the content of nitrosamine in smoke can be reduced, and therefore harm of smoke to the human body is reduced. Compared with the prior art, after bobbin paper is sprayed with the tobacco flavor, the woodiness and scorch smell in bobbin paper made in China are covered, simulation of the bobbin paper made in China is reduced, and the smoking flavor of the cigarettes is good. The content of the harmful ingredient nitrosamine in smoke can be reduced, and harm of smoke to the human body is reduced.
Description
Technical field
The invention belongs to cigarette additive technical field, particularly relate to one and can reduce in flue gas and have
The flavouring essence for tobacco of pest matter and the obbbin containing this essence.
Background technology
At present, it is considered that the main harmful substance in flue gas has: in flue gas gaseous substance
Carbonoxide, nitrogen oxide, acrylic aldehyde, volatile aromatics, hydrocyanic acid, volatility nitrous
Condensed-nuclei aromatics, phenols, nicotine, nitrosamine and some jeterocyclic chemistries in the Smoke Particulate matter such as amine
Compound and the radioelement etc. of trace, and gas phase and grain mutually in the free radical that all exists.Sub-
Nitramine is a kind of extremely strong carcinogen.Nicotiana tabacum L. during the fermentation and can produce when lighting
One nitrosamine growing tobacco special (TSNA).
In recent years, domestic cigarette bobbin paper processing enterprise achieves technological innovation, the cigarette paper of production
Reach higher level.But in the course of processing, it is limited to the defect of raw material, technique,
Domestic cigarette paper can produce some irritating abnormal smells from the patients, the especially stimulation to throat when burning
Very big, there is obvious peppery larynx to feel, reduce the physiology gratification of medicated cigarette smoker.
Summary of the invention
An object of the present invention is to provide a kind of cigarette perfume reducing harmful substances from flue gases
Essence.
The two of the purpose of the present invention are to provide the preparation method of described flavouring essence for tobacco.
The three of the purpose of the present invention are to provide the application on obbbin of the described flavouring essence for tobacco.
The present invention is achieved through the following technical solutions:
The present invention relates to a kind of flavouring essence for tobacco reducing harmful substances from flue gases, its feature exists
In: include the raw material of following weight proportion:
Celery seed 800-900 part, vitexin 0.5-1.2 part, umbelliferone 4-9 part, Fructus Hordei Germinatus
Phenol 50-86 part；
Its preparation method is:
1) the celery seed sodium chloride solution of 4000-5000 weight portion soaks 12-15h, filters, dries in the air
Dry, obtain pretreated celery seed, add the ethanol solution that volume fraction is 23-30%
Reflux, extract, 3 times, each 2h, merge 3 extracting solution, filter, concentrating under reduced pressure, fling to
Solvent, obtains Apium graveolens Linnaeus extract；
2) Apium graveolens Linnaeus extract is mixed at 80-90 DEG C with vitexin, maltol, be down to room temperature
After add umbelliferone, mix homogeneously, obtain flavouring essence for tobacco of the present invention.
The mass fraction of described sodium chloride solution is 1.1-1.7%.
A kind of cigarette obbbin, it is characterised in that: it is coated with above-mentioned cigarette on described cigarette obbbin
Use essence.
A kind of cigarette obbbin, it is characterised in that: described flavouring essence for tobacco is pressed 0.1-0.15g/
The consumption of hectogram obbbin adds to obbbin.
A kind of cigarette obbbin, it is characterised in that: preparation method is: by above-mentioned flavouring essence for tobacco
The tow sides of obbbin are sprayed to the ethanol solution that volume fraction is 95%, so after dissolving
After make solvent volatilize and be dried under cryogenic.
Celery seed has pleasant enhanced aroma, and taste is micro-pungent and bitter, with vitexin, umbrella shape flower
The xylon gas in domestic obbbin and shrivelled breath can be covered after lactone, maltol compatibility, improve cigarette
Suction taste, use the specific production technology of the present invention can reduce containing of nitrosamine in flue gas simultaneously
Amount, thus reduce the flue gas injury to human body.
Relative to prior art, present invention have the advantage that
1., after spraying flavouring essence for tobacco of the present invention in obbbin, mask in domestic obbbin
Xylon gas and shrivelled breath, decrease the zest of domestic obbbin, make cigarette entirety inhale taste relatively
Good.
2. can reduce the content of harmful substances in flue gas nitrosamine, decrease flue gas to human body
Injury.
Specific embodiment
Embodiment 1: a kind of flavouring essence for tobacco reducing harmful substances from flue gases, it is characterised in that:
Raw material including following weight proportion:
Celery seed 850 parts, vitexin 0.8 part, umbelliferone 6 parts, maltol 65 parts；
Its preparation method is:
1) the celery seed sodium chloride solution of 4500 weight portions soaks 14h, filters, dries, obtain
Pretreated celery seed, adds the ethanol solution reflux, extract, 3 that volume fraction is 27%
Secondary, each 2h, merge 3 extracting solution, filter, concentrating under reduced pressure, fling to solvent, obtain
Apium graveolens Linnaeus extract；
2) Apium graveolens Linnaeus extract is mixed at 85 DEG C, after being down to room temperature with vitexin, maltol
Add umbelliferone, mix homogeneously, obtain flavouring essence for tobacco of the present invention.
The mass fraction of described sodium chloride solution is 1.4%.
A kind of cigarette obbbin, it is characterised in that: it is coated with above-mentioned cigarette on described cigarette obbbin
Use essence.
A kind of cigarette obbbin, it is characterised in that: described flavouring essence for tobacco is pressed 0.12g/ hundred
The consumption of gram obbbin adds to obbbin.
A kind of cigarette obbbin, it is characterised in that: preparation method is: by above-mentioned flavouring essence for tobacco
The tow sides of obbbin are sprayed to the ethanol solution that volume fraction is 95%, so after dissolving
After make solvent volatilize and be dried under cryogenic.
Embodiment 2: a kind of flavouring essence for tobacco reducing harmful substances from flue gases, it is characterised in that:
Raw material including following weight proportion:
Celery seed 800 parts, vitexin 0.5 part, umbelliferone 4 parts, maltol 50 parts；
Its preparation method is:
1) the celery seed sodium chloride solution of 4000 weight portions soaks 12h, filters, dries, obtain
Pretreated celery seed, adds the ethanol solution reflux, extract, 3 that volume fraction is 23%
Secondary, each 2h, merge 3 extracting solution, filter, concentrating under reduced pressure, fling to solvent, obtain
Apium graveolens Linnaeus extract；
2) Apium graveolens Linnaeus extract is mixed at 80 DEG C, after being down to room temperature with vitexin, maltol
Add umbelliferone, mix homogeneously, obtain flavouring essence for tobacco of the present invention.
The mass fraction of described sodium chloride solution is 1.1%.
A kind of cigarette obbbin, it is characterised in that: described flavouring essence for tobacco is pressed 0.1g/ hectogram
The consumption of obbbin adds to obbbin.
Remaining is with embodiment 1.
Embodiment 3: a kind of flavouring essence for tobacco reducing harmful substances from flue gases, it is characterised in that:
Raw material including following weight proportion:
Celery seed 900 parts, vitexin 1.2 parts, umbelliferone 9 parts, maltol 86 parts；
Its preparation method is:
1) the celery seed sodium chloride solution of 5000 weight portions soaks 15h, filters, dries, obtain
Pretreated celery seed, adds the ethanol solution reflux, extract, 3 that volume fraction is 30%
Secondary, each 2h, merge 3 extracting solution, filter, concentrating under reduced pressure, fling to solvent, obtain
Apium graveolens Linnaeus extract；
2) Apium graveolens Linnaeus extract is mixed at 90 DEG C, after being down to room temperature with vitexin, maltol
Add umbelliferone, mix homogeneously, obtain flavouring essence for tobacco of the present invention.
The mass fraction of described sodium chloride solution is 1.7%.
A kind of cigarette obbbin, it is characterised in that: described flavouring essence for tobacco is pressed 0.15g/ hundred
The consumption of gram obbbin adds to obbbin.
Remaining is with embodiment 1.
Embodiment 4: a kind of flavouring essence for tobacco reducing harmful substances from flue gases, its preparation method
For:
1) celery seed volume fraction is the ethanol solution reflux, extract, 3 times of 27%, and each 2h closes
And 3 extracting solution, filter, concentrating under reduced pressure, fling to solvent, obtain Apium graveolens Linnaeus extract；
2) Apium graveolens Linnaeus extract is mixed homogeneously with vitexin, maltol, umbelliferone, to obtain final product
Described flavouring essence for tobacco.
Remaining is with embodiment 1.
Embodiment 5: the Chinese patent of Application No. 201010501192.6 discloses a kind of energy
Remove flavouring essence for tobacco of miscellaneous QI caused by obbbin and preparation method thereof, interior described in embodiment 1
Rong Wei: weigh Fructus Dauci Sativae oil 5 parts, Semen Myristicae oil 10 parts, Oleum Anisi Stellati 2 parts, Oleum Caryophylli
1 part, eugenol 4 parts, laurel fat 0.5 part, cinnamic aldehyde 2 parts and ethanol 75.5 parts.?
Stirring 10min under room temperature condition makes raw material fully dissolve, and is configured to barrelling after uniform solution, puts
At lucifuge, cool place, deposit 24 hours and i.e. obtain required flavouring essence for tobacco.Described cigarette is fragrant
Essence application in Medicated cigarette.Particularly as follows: by described flavouring essence for tobacco, by 0.04-0.05g/ hundred
The consumption of gram obbbin adds to cigarette bobbin paper.
By embodiment 1-4 gained flavouring essence for tobacco, add to domestic dish by the explanation in each embodiment
In paper, the flavouring essence for tobacco that embodiment 5 prepares is pressed 0.05g/ hectogram obbbin and is added to domestic obbbin
In, by the obbbin containing embodiment 1-5 flavouring essence for tobacco and be not added with the obbbin of flavouring essence for tobacco by often
Rule method rolling cigarette sample, remaining adjuvant and additive all keep constant, and sample is smoked panel test
Test, then is measured the nitrosamine in cigarette smoke, the results are shown in Table 1 and table 2.
Table 1 is smoked panel test result of the test table
Table 2 content of nitrosamines compares
| Sample | Measured value (μ g/ props up) | Reduction rate (%) |
| Blank group | 13.02 | / |
| Embodiment 1 | 10.53 | 19.12 |
| Embodiment 2 | 10.96 | 15.82 |
| Embodiment 3 | 10.63 | 18.36 |
| Embodiment 4 | 13.01 | 0.08 |
| Embodiment 5 | 13.04 | / |
As shown in Table 1, the flavouring essence for tobacco that embodiment 1-4 prepares can after adding in domestic obbbin
Significantly improving the quality of cigarette, general effect is better than embodiment 5 and blank group.In table 2, add
After adding the flavouring essence for tobacco that embodiment 1-3 prepares, the content of nitrosamines in flue gas substantially reduces, real
Executing example 4 with embodiment 5 compared with blank group, content of nitrosamines change is little.
Claims (8)
1. the flavouring essence for tobacco that can reduce harmful substances from flue gases, it is characterised in that: include as follows
Raw material: celery seed, vitexin, umbelliferone, maltol.
2. the flavouring essence for tobacco that can reduce harmful substances from flue gases, it is characterised in that: include as follows
The raw material of weight proportion: in celery seed 800-900 part, vitexin 0.5-1.2 part, umbrella shape are spent
Ester 4-9 part, maltol 50-86 part.
A kind of flavouring essence for tobacco reducing harmful substances from flue gases, it is special
Levy and be: include the raw material of following weight proportion: celery seed 850 parts, vitexin 0.8 part,
Umbelliferone 6 parts, maltol 65 parts.
A kind of flavouring essence for tobacco reducing harmful substances from flue gases, its
It is characterised by: preparation method is:
1) the celery seed sodium chloride solution of 4000-5000 weight portion soaks 12-15h, filters, dries in the air
Dry, obtain pretreated celery seed, add the ethanol solution that volume fraction is 23-30%
Reflux, extract, 3 times, each 2h, merge 3 extracting solution, filter, concentrating under reduced pressure, fling to
Solvent, obtains Apium graveolens Linnaeus extract；
2) Apium graveolens Linnaeus extract is mixed at 80-90 DEG C with vitexin, maltol, be down to room temperature
After add umbelliferone, mix homogeneously, to obtain final product；
The mass fraction of described sodium chloride solution is 1.1-1.7%.
A kind of flavouring essence for tobacco reducing harmful substances from flue gases, its
It is characterised by: preparation method is:
1) the celery seed sodium chloride solution of 4500 weight portions soaks 14h, filters, dries, obtain
Pretreated celery seed, adds the ethanol solution reflux, extract, 3 that volume fraction is 27%
Secondary, each 2h, merge 3 extracting solution, filter, concentrating under reduced pressure, fling to solvent, obtain
Apium graveolens Linnaeus extract；
2) Apium graveolens Linnaeus extract is mixed at 85 DEG C, after being down to room temperature with vitexin, maltol
Add umbelliferone, mix homogeneously, to obtain final product；
The mass fraction of described sodium chloride solution is 1.4%.
6. a cigarette obbbin, it is characterised in that: it is coated with right on described cigarette obbbin and wants
Seek 2,3,4,5 arbitrary described flavouring essence for tobaccos.
7. a kind of cigarette obbbin as claimed in claim 6, it is characterised in that: right is wanted
Ask 2,3,4,5 arbitrary described flavouring essence for tobaccos by the consumption of 0.1-0.15g/ hectogram obbbin
Add to obbbin.
8. a kind of cigarette obbbin as claimed in claim 6, it is characterised in that: preparation method
For: it is 95% by arbitrary for claim 2,3,4,5 described flavouring essence for tobacco volume fraction
Ethanol solution dissolve after spray to the tow sides of obbbin, make the most under cryogenic
Solvent volatilizees and is dried.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610410827.9A CN105907475A (en) | 2016-06-13 | 2016-06-13 | Tobacco flavor capable of reducing hazardous substance in smoke and bobbin paper containing same |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610410827.9A CN105907475A (en) | 2016-06-13 | 2016-06-13 | Tobacco flavor capable of reducing hazardous substance in smoke and bobbin paper containing same |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105907475A true CN105907475A (en) | 2016-08-31 |
Family
ID=56750829
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610410827.9A Pending CN105907475A (en) | 2016-06-13 | 2016-06-13 | Tobacco flavor capable of reducing hazardous substance in smoke and bobbin paper containing same |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105907475A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106562467A (en) * | 2016-11-02 | 2017-04-19 | 浙江泽源植物科技有限公司 | Tobacco/non-tobacco slice composite coating processing method |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101613333A (en) * | 2008-06-25 | 2009-12-30 | 吉林省书祯经贸有限公司 | A kind of preparation method of apigenin and application |
| CN101974368A (en) * | 2010-10-09 | 2011-02-16 | 红云红河烟草(集团)有限责任公司 | Essence capable of lowering smoke stimulation for cigarette and preparation method and application thereof |
| CN104824836A (en) * | 2015-03-11 | 2015-08-12 | 广西中烟工业有限责任公司 | Tobacco humectant nano emulsion and method for preparing same |
| CN107034017A (en) * | 2017-04-27 | 2017-08-11 | 河南中烟工业有限责任公司 | A kind of cigarette quick-fried pearl savory essence of dried orange peel and its application in cigarette |
-
2016
- 2016-06-13 CN CN201610410827.9A patent/CN105907475A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101613333A (en) * | 2008-06-25 | 2009-12-30 | 吉林省书祯经贸有限公司 | A kind of preparation method of apigenin and application |
| CN101974368A (en) * | 2010-10-09 | 2011-02-16 | 红云红河烟草(集团)有限责任公司 | Essence capable of lowering smoke stimulation for cigarette and preparation method and application thereof |
| CN104824836A (en) * | 2015-03-11 | 2015-08-12 | 广西中烟工业有限责任公司 | Tobacco humectant nano emulsion and method for preparing same |
| CN107034017A (en) * | 2017-04-27 | 2017-08-11 | 河南中烟工业有限责任公司 | A kind of cigarette quick-fried pearl savory essence of dried orange peel and its application in cigarette |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106562467A (en) * | 2016-11-02 | 2017-04-19 | 浙江泽源植物科技有限公司 | Tobacco/non-tobacco slice composite coating processing method |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US10271573B2 (en) | Tobacco with an increased level of natural tar diluents | |
| US20160366928A1 (en) | Solvent for electronic cigarette liquid and an electronic cigarette liquid | |
| CN102002440B (en) | Essence for tonka bean odor type cigarettes | |
| CN105112161B (en) | A kind of flavoring essence of cigar cigarette paper | |
| TW201531239A (en) | Tobacco treatment | |
| CN104397871A (en) | Electronic cigarette liquid containing tea extracts and preparation method of electronic cigarette liquid containing tea extracts | |
| CN103005696A (en) | Agilawood cigar and preparation method thereof | |
| CN109091696A (en) | A kind of plant type air freshener and preparation method thereof | |
| CN110584185A (en) | Flavor composition and electronic cigarette liquid containing same | |
| CN110982625A (en) | Licorice-flavored dried beads for cigarette filter tips and preparation method thereof | |
| CN108175123A (en) | A kind of health suction product or the preparation method of cigarette | |
| CN104432494A (en) | Method for preparing tobacco shreds capable of improving smoking satisfaction and low tar cigarette | |
| CN102920008B (en) | Preparation method of burley tobacco shreds for cigarettes | |
| CN110833207A (en) | Air-cured tobacco style transformation method | |
| CN103300466B (en) | A kind of for the compensation method of low tar scent of fire cured tobacco | |
| CN105907475A (en) | Tobacco flavor capable of reducing hazardous substance in smoke and bobbin paper containing same | |
| CN102204717A (en) | Formula of mint fragrant tobacco additive essence | |
| CN103230089A (en) | Preparation method for ultralow tar oil flue-cured tobacco type cigarettes with quiet and beautiful aroma | |
| CN103099309A (en) | Application of japonica rice in cigarettes | |
| CN105029677B (en) | Tobacco gel and preparation method thereof | |
| CN105831799A (en) | Method for preparing cigarette tobacco suitable for snus and application of cigarette tobacco | |
| CN109259292A (en) | A kind of tobacco roasting odor type reconstituted tobacco and preparation method thereof | |
| CN113749278A (en) | Lily-flavored electronic atomized liquid and preparation method thereof | |
| CN113088391A (en) | Glutinous rice flavor type essence for cigarette and cigarette containing essence | |
| CN112553955A (en) | Perfuming and moisture-retaining groove paper and preparation method of groove filter tip |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20160831 |