CN105902433A - Method for extracting agaric extract from agaric and application thereof - Google Patents
Method for extracting agaric extract from agaric and application thereof Download PDFInfo
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- CN105902433A CN105902433A CN201610345673.XA CN201610345673A CN105902433A CN 105902433 A CN105902433 A CN 105902433A CN 201610345673 A CN201610345673 A CN 201610345673A CN 105902433 A CN105902433 A CN 105902433A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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Abstract
The invention relates to the field of plant application research and particularly relates to a method for extracting agaric extract from agaric and application thereof. The dired agaric is subjected to the processes of crushing, soaking, vacuum extraction, filtering separation, secondary extraction, secondary separation, extracting solution concentration and the like so as to prepare the agaric extract. The agaric extract can serve as an ingredient to be added into a cosmetic so as to be particularly prepared into products, such as masks, facial cleansers, lotions, moisturizers, whitening cream and essence. The method provided by the invention has the beneficial effects that the flow is simple, and the operation is easy; the extraction is carried out twice, so that the extraction rate is higher; the vacuum extraction technology is adopted, and cell walls are broken under the internal pressure in the vacuum environment, so that the extraction rate is high; water is used as an extraction solvent, so that the concentration is convenient; and the agaric extract contains antioxidant ingredients and multiple nutritional ingredients, and the agaric extract is applied to the cosmetics, so that the range of application is enlarged.
Description
Technical field
The present invention relates to plant application research field, a kind of side extracting Auricularia extract from Auricularia
Method and application thereof.
Background technology
Auricularia extract high-quality Auricularia is raw material, forms through technique fermented extracted.Auricularia extract rich in
Abundant Auricularia polysaccharide, by L-fucose, L-arabinose, D-xylose, D-MANNOSE, D-Glucose and
The monosaccharide compositions such as glucuronic acid, the Auricularia melanin being separated to from Auricularia sporophore, is a kind of colour generation
Peptidoglycan, is made up of glucose, mannose, galactose, fucose and a short peptide chain, and these compositions dissociate
For not colour generation during monosaccharide body, water can be dissolved in, have the physiologically active of enhancing human body immunity function, Auricularia property is sweet,
Flat, nontoxic.Can fill blood, cooling blood for hemostasis, lung moistening stomach reinforcing, dryness moistening and intestine benefiting, relaxing muscles and tendons and activating QI and blood in the collateral, strong will of making light of one's life by commiting suicide.
The diseases such as treatment deficiency of both QI and blood, cough due to deficiency of the lung, puerperal asthenia.Auricularia contains the necessary eight kinds of aminoacid of human body
And vitamin, there is higher nutritive value and certain medical value.
Chinese patent storehouse discloses the application in Medicated cigarette of a kind of Auricularia extract
(CN201310091173.4), adding Auricularia extract in tobacco shred, tobacco shred processing characteristics significantly improves,
Miscellaneous QI and zest reduce, and sense of promoting the production of body fluid increases, and overall sucking quality is improved, and described extract is by following
Prepared by method: dried Auricularia → remove impurity pulverizes → soaks → multigelation → enzymatic hydrolysis → heating extraction →
Filter and separate clear liquid and filtering residue → filtering residue and to obtain clear liquid → clear liquid through acid hydrolysis → filter again and merge concentration → Auricularia
Extract.The invention have the characteristics that: use multigelation method wall breaking technology to improve Auricularia effective ingredient
Dissolution rate；Enzyme process is used to remove the protein affecting cigarette odor-absorbing；To poor the dividing greatly of dissolubility in Auricularia
Sub-glucide is further hydrolyzed, and improves the utilization rate of Auricularia effective ingredient.The present invention establishes letter
List is effective, be prone to the Auricularia extraction process by water of amplification, and its extract is applied to Medicated cigarette, does not change Medicated cigarette
Original performance and processing technique, therefore have more meaning and the value of actual production.
Chinese patent storehouse discloses a kind of Auricularia polytricha (Mout) Sacc. extract and preparation method and application
(CN201310345474.5), this has the Auricularia polytricha (Mout) Sacc. extract of hypolipemic function, walks as follows according to including
Prepared by rapid method: precipitate Auricularia polytricha (Mout) Sacc. 3 work song entity Aqueous extracts with dehydrated alcohol, collects precipitation, is had
There is the Auricularia polytricha (Mout) Sacc. extract of hypolipemic function；Described Auricularia polytricha (Mout) Sacc. 3 work song entity Aqueous extracts is from Auricularia polytricha (Mout) Sacc. with water
The water-soluble substances extracted in the sporophore of No. 3.The Auricularia polytricha (Mout) Sacc. 3 with hypolipemic function of the present invention
Number extract not only has obvious reduction effect to TC and LDL-C, to the reduction degree of TG the 14th
Also define the degree (P < 0.05) of significant difference with high fat matched group on it and later test point thereof, right
The reduction degree of TC, TG and LDL-C substantially remains in same level on each test point, and effect is relative
Steadily.
The method of plant extract has a lot, and plant extract is applied primarily to the necks such as food, chemical industry, cosmetics
Territory, but extracting method and plant extract species have the biggest limitation, the most simply, safely, effectively
Extract plant, select which kind of plant, and being applied to its safety in cosmetics, protect sensitive skin, be
Problem demanding prompt solution.
Summary of the invention
For the problems referred to above, it is an object of the invention to provide a kind of method extracting Auricularia extract from Auricularia
And application, by dried Auricularia through pulverizing, soak, vacuum extraction, filter separate, secondary extraction, secondary
The techniques such as separation, extracting solution concentration make Auricularia extract, and Auricularia extract can add cosmetic to as dispensing
In product, specifically can be made into the products such as facial film, cleansing milk, surfactant, emollient cream, skin whitener, essence.
To achieve these goals, the present invention uses below scheme
According to the first aspect of the invention, a kind of method extracting Auricularia extract from Auricularia, it include with
Lower step:
(1) pulverizing, use pulverizer to be pulverized by dried Auricularia, make Auricularia microgranule, particle diameter is 20-50
Sieve mesh；
(2) soak, Auricularia microgranule is placed in container, add pure water and soak, water and Auricularia microgranule
Mass ratio is 1.5-3:1, and soak time is 2-6h, and temperature is 16-30 DEG C；
(3) vacuum extraction, is placed in obtaining steep raising Auricularia microgranule in step (2) in sealing container, adds
Pure water, water is 10-15:1 with the mass ratio of Auricularia microgranule, uses vacuum pump will seal container vacuum-pumping,
Vacuum is-75--50KPa, and the time is 3-6h, and temperature is 60-75 DEG C；
(4) filter separation, step (3) is obtained mixture and filters, obtain clear liquid and Auricularia residue；
(5) secondary extraction, is placed in Auricularia residue in sealing container, adds pure water, and water is micro-with Auricularia
The mass ratio of grain is 5-8:1, uses vacuum pump will seal container vacuum-pumping, and vacuum is-75--50KPa,
Time is 3-6h, and temperature is 60-75 DEG C；
(6) secondary separation, obtains mixture by step (3) and filters, and obtains clear liquid and Auricularia residue；
(7) extracting solution concentrates, and clear liquid step (4) and step (6) obtained concentrates, and obtains Auricularia
Extract, the water content of Auricularia extract is 30%-40%；
(8) decolorising agent or toner is selected to make required color according to the final color of Auricularia extract.
Preferably, Auricularia microgranule in step (1), particle diameter is 35-40 sieve mesh.
Preferably, in step (2), water is 2:1 with the mass ratio of Auricularia microgranule, and soak time is 4-5h,
Temperature is 20-26 DEG C.
Preferably, in step (3), water is 12:1 with the mass ratio of Auricularia microgranule, uses vacuum pump to seal
Container vacuum-pumping, vacuum is-75--50KPa, and the time is 4-5h, and temperature is 65 DEG C.
Preferably, step (7) uses vacuum and low temperature concentration technique.
Preferably, the water content of described Auricularia extract is 30%.
According to the second aspect of the invention, it is provided that the application of a kind of Auricularia extract, described Auricularia extract is made
Add in cosmetics for a kind of dispensing.
Preferably, Auricularia extract is applied in the cosmetics of skin moistening, moisturizing, defying age class.
Preferably, a kind of defying age class cosmetic combinations containing Auricularia extract, by weight, including with
Lower component: Auricularia extract 8-12 part, antioxidant 1-5 part, crease-resistant activating agent 3-8 part, anti-sensitizer 0.5-1.2
Part, whitening agent 1.5-3 part, potassium hydroxide 0.03-0.1 part, Acer Truncatum Buge seed oil 0.5-2 part, chelating agen 0.3-1.2
Part, thickening agent 0.1-0.3 part, emulsifying agent 1.5-4 part, preservative 0.2-0.6 part, deionized water 40-80 part.
The invention has the beneficial effects as follows: flow process is simple, easily operates；Secondary extracts, and extraction ratio is higher；Adopt
Using vacuum extraction technology, cell breaking cellular wall under internal pressure in vacuum environment, extraction ratio is high；Use water to do to extract
Taking solvent, it is convenient to concentrate；Containing antioxidant content and multiple nutritional components in Auricularia extract, Auricularia is carried
Take thing to be applied in cosmetics, expand range of application.
Detailed description of the invention
For the problems referred to above, it is an object of the invention to provide a kind of method extracting Auricularia extract from Auricularia
And application, by dried Auricularia through pulverizing, soak, vacuum extraction, filter separate, secondary extraction, secondary
The techniques such as separation, extracting solution concentration make Auricularia extract, and Auricularia extract can add cosmetic to as dispensing
In product, specifically can be made into the products such as facial film, cleansing milk, surfactant, emollient cream, skin whitener, essence.
To achieve these goals, the present invention uses below scheme
According to the first aspect of the invention, a kind of method extracting Auricularia extract from Auricularia, it include with
Lower step:
(1) pulverizing, use pulverizer to be pulverized by dried Auricularia, make Auricularia microgranule, particle diameter is 20-50
Sieve mesh；
(2) soak, Auricularia microgranule is placed in container, add pure water and soak, water and Auricularia microgranule
Mass ratio is 1.5-3:1, and soak time is 2-6h, and temperature is 16-30 DEG C；
(3) vacuum extraction, is placed in obtaining steep raising Auricularia microgranule in step (2) in sealing container, adds
Pure water, water is 10-15:1 with the mass ratio of Auricularia microgranule, uses vacuum pump will seal container vacuum-pumping,
Vacuum is-75--50KPa, and the time is 3-6h, and temperature is 60-75 DEG C；
(4) filter separation, step (3) is obtained mixture and filters, obtain clear liquid and Auricularia residue；
(5) secondary extraction, is placed in Auricularia residue in sealing container, adds pure water, and water is micro-with Auricularia
The mass ratio of grain is 5-8:1, uses vacuum pump will seal container vacuum-pumping, and vacuum is-75--50KPa,
Time is 3-6h, and temperature is 60-75 DEG C；
(6) secondary separation, obtains mixture by step (3) and filters, and obtains clear liquid and Auricularia residue；
(7) extracting solution concentrates, and clear liquid step (4) and step (6) obtained concentrates, and obtains Auricularia
Extract, the water content of Auricularia extract is 30%-40%；
(8) decolorising agent or toner is selected to make required color according to the final color of Auricularia extract.
Preferably, Auricularia microgranule in step (1), particle diameter is 35-40 sieve mesh.
Preferably, in step (2), water is 2:1 with the mass ratio of Auricularia microgranule, and soak time is 4-5h,
Temperature is 20-26 DEG C.
Preferably, in step (3), water is 12:1 with the mass ratio of Auricularia microgranule, uses vacuum pump to seal
Container vacuum-pumping, vacuum is-75--50KPa, and the time is 4-5h, and temperature is 65 DEG C.
Preferably, step (7) uses vacuum and low temperature concentration technique.
Preferably, the water content of described Auricularia extract is 30%.
According to the second aspect of the invention, it is provided that the application of a kind of Auricularia extract, described Auricularia extract is made
Add in cosmetics for a kind of dispensing.
Preferably, Auricularia extract is applied in the cosmetics of skin moistening, moisturizing, defying age class.
Preferably, a kind of defying age class cosmetic combinations containing Auricularia extract, by weight, including with
Lower component: Auricularia extract 8-12 part, antioxidant 1-5 part, crease-resistant activating agent 3-8 part, anti-sensitizer 0.5-1.2
Part, whitening agent 1.5-3 part, potassium hydroxide 0.03-0.1 part, Acer Truncatum Buge seed oil 0.5-2 part, chelating agen 0.3-1.2
Part, thickening agent 0.1-0.3 part, emulsifying agent 1.5-4 part, preservative 0.2-0.6 part, deionized water 40-80 part.
The ultimate principle of vacuum and low temperature extractive technique is to utilize water boiling point in the environment of vacuum to reduce, at 70 DEG C
Occur as soon as fluidized state, accelerate extract convection current, increase soluble substance and solvent strength in extraction raw material
Difference and extension energy, meanwhile, under vacuum environment, extract cell breaking cellular wall under internal pressure of raw material, useful
Composition is easier to extraction, and extraction yield is higher.
For the technical scheme making those skilled in the art be better understood from the application, below in conjunction with reality
Execute example technical scheme is clearly and completely described, it is clear that described embodiment is only
Being only a part of embodiment of the application, based on the embodiment in the application, those of ordinary skill in the art exist
Do not make the every other embodiment obtained under creative work premise, all should belong to the application protection
Scope.
Embodiment 1
A kind of method extracting Auricularia extract from Auricularia, it comprises the following steps:
Dried Auricularia weight: 10KG；
(1) pulverizing, use pulverizer to be pulverized by dried Auricularia, make Auricularia microgranule, particle diameter is 30 sieves
Mesh；
(2) soak, Auricularia microgranule is placed in container, add pure water and soak, water and Auricularia microgranule
Mass ratio is 2:1, and soak time is 4h, and temperature is 24 DEG C；
(3) vacuum extraction, is placed in obtaining steep raising Auricularia microgranule in step (2) in sealing container, adds
Pure water, water is 12:1 with the mass ratio of Auricularia microgranule, uses vacuum pump will seal container vacuum-pumping, very
Reciprocal of duty cycle is-75KPa, and the time is 4h, and temperature is 65 DEG C；
(4) filter separation, step (3) is obtained mixture and filters, obtain clear liquid and Auricularia residue；
(5) secondary extraction, is placed in Auricularia residue in sealing container, adds pure water, and water is micro-with Auricularia
The mass ratio of grain is 5-8:1, uses vacuum pump will seal container vacuum-pumping, and vacuum is-75KPa, time
Between be 4h, temperature is 65 DEG C；
(6) secondary separation, obtains mixture by step (3) and filters, and obtains clear liquid and Auricularia residue；
(7) extracting solution concentrates, and clear liquid step (4) and step (6) obtained concentrates, and obtains Auricularia
Extract, the water content of Auricularia extract is 30%；
(8) decolorising agent or toner is selected to make required color according to the final color of Auricularia extract.
Embodiment 2
A kind of method extracting Auricularia extract from Auricularia, it comprises the following steps:
Dried Auricularia weight: 50KG；
(1) pulverizing, use pulverizer to be pulverized by dried Auricularia, make Auricularia microgranule, particle diameter is 40 sieves
Mesh；
(2) soak, Auricularia microgranule is placed in container, add pure water and soak, water and Auricularia microgranule
Mass ratio is 2.5:1, and soak time is 4.5h, and temperature is 26 DEG C；
(3) vacuum extraction, is placed in obtaining steep raising Auricularia microgranule in step (2) in sealing container, adds
Pure water, water is 12:1 with the mass ratio of Auricularia microgranule, uses vacuum pump will seal container vacuum-pumping, very
Reciprocal of duty cycle is-65KPa, and the time is 4.5h, and temperature is 70 DEG C；
(4) filter separation, step (3) is obtained mixture and filters, obtain clear liquid and Auricularia residue；
(5) secondary extraction, is placed in Auricularia residue in sealing container, adds pure water, and water is micro-with Auricularia
The mass ratio of grain is 7:1, uses vacuum pump will seal container vacuum-pumping, and vacuum is-75KPa, the time
For 4.5h, temperature is 70 DEG C；
(6) secondary separation, obtains mixture by step (3) and filters, and obtains clear liquid and Auricularia residue；
(7) extracting solution concentrates, and clear liquid step (4) and step (6) obtained concentrates, and obtains Auricularia
Extract, the water content of Auricularia extract is 35%；
(8) decolorising agent or toner is selected to make required color according to the final color of Auricularia extract.
Embodiment 3
A kind of method extracting Auricularia extract from Auricularia, it comprises the following steps:
Dried Auricularia weight: 100KG；
(1) pulverizing, use pulverizer to be pulverized by dried Auricularia, make Auricularia microgranule, particle diameter is 50 sieves
Mesh；
(2) soak, Auricularia microgranule is placed in container, add pure water and soak, water and Auricularia microgranule
Mass ratio is 3:1, and soak time is 5h, and temperature is 28 DEG C；
(3) vacuum extraction, is placed in obtaining steep raising Auricularia microgranule in step (2) in sealing container, adds
Pure water, water is 12:1 with the mass ratio of Auricularia microgranule, uses vacuum pump will seal container vacuum-pumping, very
Reciprocal of duty cycle is-75KPa, and the time is 4h, and temperature is 65 DEG C；
(4) filter separation, step (3) is obtained mixture and filters, obtain clear liquid and Auricularia residue；
(5) secondary extraction, is placed in Auricularia residue in sealing container, adds pure water, and water is micro-with Auricularia
The mass ratio of grain is 8:1, uses vacuum pump will seal container vacuum-pumping, and vacuum is-55KPa, the time
For 5h, temperature is 72 DEG C；
(6) secondary separation, obtains mixture by step (3) and filters, and obtains clear liquid and Auricularia residue；
(7) extracting solution concentrates, and clear liquid step (4) and step (6) obtained concentrates, and obtains Auricularia
Extract, the water content of Auricularia extract is 40%；
(8) decolorising agent or toner is selected to make required color according to the final color of Auricularia extract.
Finally illustrate, above example only in order to technical scheme to be described and unrestricted, ability
Other amendment or equivalents that technical scheme is made by territory those of ordinary skill, as long as not taking off
From the spirit and scope of technical solution of the present invention, all should contain in the middle of scope of the presently claimed invention.
Claims (9)
1. the method extracting Auricularia extract from Auricularia, it is characterised in that it comprises the following steps:
(1) pulverizing, use pulverizer to be pulverized by dried Auricularia, make Auricularia microgranule, particle diameter is 20-50
Sieve mesh；
(2) soak, Auricularia microgranule is placed in container, add pure water and soak, water and Auricularia microgranule
Mass ratio is 1.5-3:1, and soak time is 2-6h, and temperature is 16-30 DEG C；
(3) vacuum extraction, is placed in obtaining steep raising Auricularia microgranule in step (2) in sealing container, adds
Pure water, water is 10-15:1 with the mass ratio of Auricularia microgranule, uses vacuum pump will seal container vacuum-pumping,
Vacuum is-75--50KPa, and the time is 3-6h, and temperature is 60-75 DEG C；
(4) filter separation, step (3) is obtained mixture and filters, obtain clear liquid and Auricularia residue；
(5) secondary extraction, is placed in Auricularia residue in sealing container, adds pure water, and water is micro-with Auricularia
The mass ratio of grain is 5-8:1, uses vacuum pump will seal container vacuum-pumping, and vacuum is-75--50KPa,
Time is 3-6h, and temperature is 60-75 DEG C；
(6) secondary separation, obtains mixture by step (3) and filters, and obtains clear liquid and Auricularia residue；
(7) extracting solution concentrates, and clear liquid step (4) and step (6) obtained concentrates, and obtains Auricularia
Extract, the water content of Auricularia extract is 30%-40%；
(8) decolorising agent or toner is selected to make institute according to the final color of Auricularia extract
Need color.
A kind of method extracting Auricularia extract from Auricularia the most according to claim 1, its feature exists
In, Auricularia microgranule in step (1), particle diameter is 35-40 sieve mesh.
A kind of method extracting Auricularia extract from Auricularia the most according to claim 1, its feature exists
In, in step (2), water is 2:1 with the mass ratio of Auricularia microgranule, and soak time is 4-5h, and temperature is 20-26 DEG C.
A kind of method extracting Auricularia extract from Auricularia the most according to claim 1, its feature exists
In, in step (3), water is 12:1 with the mass ratio of Auricularia microgranule, uses vacuum pump to be taken out very by sealing container
Sky, vacuum is-75--50KPa, and the time is 4-5h, and temperature is 65 DEG C.
A kind of method extracting Auricularia extract from Auricularia the most according to claim 1, its feature exists
In, step (7) uses vacuum and low temperature concentration technique.
A kind of method extracting Auricularia extract from Auricularia the most according to claim 1, its feature exists
In, the water content of described Auricularia extract is 30%.
7. the application of an Auricularia extract, it is characterised in that described Auricularia extract adds as a kind of dispensing
It is added in cosmetics.
A kind of method extracting Auricularia extract from Auricularia the most according to claim 7, its feature exists
In, Auricularia extract is applied in the cosmetics of skin moistening, moisturizing, defying age class.
9. according to a kind of method extracting Auricularia extract from Auricularia described in claim 7 or 8, its feature
It is, a kind of defying age class cosmetic combinations containing Auricularia extract, by weight, including following components:
Auricularia extract 8-12 part, antioxidant 1-5 part, crease-resistant activating agent 3-8 part, anti-sensitizer 0.5-1.2
Part, whitening agent 1.5-3 part, potassium hydroxide 0.03-0.1 part, Acer Truncatum Buge seed oil 0.5-2 part,
Chelating agen 0.3-1.2 part, thickening agent 0.1-0.3 part, emulsifying agent 1.5-4 part, preservative
0.2-0.6 part, deionized water 40-80 part.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201610345673.XA CN105902433A (en) | 2016-05-21 | 2016-05-21 | Method for extracting agaric extract from agaric and application thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610345673.XA CN105902433A (en) | 2016-05-21 | 2016-05-21 | Method for extracting agaric extract from agaric and application thereof |
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Cited By (1)
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| CN107663236A (en) * | 2017-11-09 | 2018-02-06 | 吉林农业科技学院 | The alkalinity extraction method and moisture retention water of black agaric collagen albumen are washed one's face film |
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| CN107663236A (en) * | 2017-11-09 | 2018-02-06 | 吉林农业科技学院 | The alkalinity extraction method and moisture retention water of black agaric collagen albumen are washed one's face film |
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