CN105862386B - A kind of preparation method of fluorescein polyester-cotton fabric - Google Patents
A kind of preparation method of fluorescein polyester-cotton fabric Download PDFInfo
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- CN105862386B CN105862386B CN201610260342.6A CN201610260342A CN105862386B CN 105862386 B CN105862386 B CN 105862386B CN 201610260342 A CN201610260342 A CN 201610260342A CN 105862386 B CN105862386 B CN 105862386B
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M10/00—Physical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. ultrasonic, corona discharge, irradiation, electric currents, or magnetic fields; Physical treatment combined with treatment with chemical compounds or elements
- D06M10/02—Physical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. ultrasonic, corona discharge, irradiation, electric currents, or magnetic fields; Physical treatment combined with treatment with chemical compounds or elements ultrasonic or sonic; Corona discharge
- D06M10/025—Corona discharge or low temperature plasma
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/16—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/38—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using reactive dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/94—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dyes dissolved in solvents which are in the supercritical state
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/004—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated using dispersed dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/008—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated using reactive dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/82—Textiles which contain different kinds of fibres
- D06P3/8204—Textiles which contain different kinds of fibres fibres of different chemical nature
- D06P3/8223—Textiles which contain different kinds of fibres fibres of different chemical nature mixtures of fibres containing hydroxyl and ester groups
- D06P3/8238—Textiles which contain different kinds of fibres fibres of different chemical nature mixtures of fibres containing hydroxyl and ester groups using different kinds of dye
- D06P3/8252—Textiles which contain different kinds of fibres fibres of different chemical nature mixtures of fibres containing hydroxyl and ester groups using different kinds of dye using dispersed and reactive dyes
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Physics & Mathematics (AREA)
- Plasma & Fusion (AREA)
- Coloring (AREA)
- Treatment Of Fiber Materials (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
Abstract
The object of the present invention is to provide a kind of preparation methods of fluorescein fabric, it carries out cold plasma processing first with 3 type corona treatment instrument of CGP to polyester-cotton fabric, then utilizes 10 20 parts of natural fatty alcohol polyoxyethylene ether, 12 30 parts of n-amyl alcohols, 0.05 0.25 parts of active fluoro yellow dye FL, 0.01 0.15 parts of scattered fluorescent yellow dyestuff 10GN, 40 60 parts of supercritical COs2It is put into high-pressure bottle with 0.01 6 parts of distilled water and prepares reverse micelle system, finally the polyester-cotton fabric through supercooling plasma treatment is put into high-pressure bottle and is dyed, obtains fluorescein polyester-cotton fabric.Fluorescein polyester-cotton fabric bright prepared by the present invention, color fastness is high, soft comfortable, and elasticity is big, and mechanical property is good.
Description
Technical field：
The present invention relates to textile technology fields, are specifically related to a kind of preparation method of fluorescein polyester-cotton fabric.
Background technology：
Fluorescent dye or fluorescent pigment are the dyestuffs that a kind of energy intense radiation in visible range goes out fluorescence, are widely used
In weaving, a variety of industries such as dyeing of plastics, printing pigment.With the raising of people's economic level, fluorescent fabric is because of its color and luster
Bright-coloured eye-catching, visual experience is unique novel, is widely current in recent years.Fluorescence class dyestuff not only has peace compared with conventional dyes
Entirely, the effect of warning, but also there are the apparent visuals such as beautiful, eye-catching.
Fire-fighting operation clothes are iridescent fabric mostly, and the fire-fighting operation of China's early development takes, the face in the majority with salmon pink
The warning operation that color rises in scene of fire can not show a candle to fluorescent yellow fabric.The fabric of previous fire-fighting operation clothes is mostly cotton fiber,
The moisture pick-up properties of cotton fiber is preferable, but the strength of fiber is poor.Polyester fiber has good stiffness and prominent intensity, institute
With, the wrinkle resistance of polyester fabric and tear that ultimate strength is preferable, but the wet guilding of fabric and electric conductivity are poor.Therefore, by cotton
After fiber and polyester fiber are according to the blended resultant yarn of different proportion, can weave moderate strength, good hygroscopicity various fabrics.Therefore,
Often application of the fluorescein polyester-cotton fabric in fire-fighting domain is greatly improved at present, but traditional colouring method irregular colour, easily
There are color spot, and poor color fastness.
Invention content：
The object of the present invention is to provide a kind of preparation method of fluorescein fabric, the fluorescein fabric prepared, dyeing is equal
Even, color fastness is high, polyester-cotton fabric soft comfortable obtained, and mechanical property is good.
To achieve the above object, the present invention uses following technical scheme：
A kind of preparation method of fluorescein polyester-cotton fabric, includes the following steps：
(1) by polyester-cotton fabric using CGP-3 type corona treatment instrument, using capacitive coupling glow discharge process 2-5h,
Supply frequency is 13.56MHz, and power 100W, discharge current 100mA, 5-50Pa vacuum discharge, Ar flow velocitys are 20ml/
min；
(2) by natural fatty alcohol polyoxyethylene ether, n-amyl alcohol, active fluoro yellow dye FL, scattered fluorescent yellow dyestuff 10GN,
Supercritical CO2Reverse micelle system is formed in high-pressure bottle of the distilled water under 10-30MPa pressure；
(3) polyester-cotton fabric Jing Guo glow discharge process is placed in high-pressure bottle, is warming up to 50-150 DEG C, dye 60-
150min；
(4) high-pressure bottle is decompressed to normal pressure, takes out polyester-cotton fabric, and recycle CO2And dyestuff, obtain fluorescein polyester-cotton blend face
Material.
As a preferred embodiment of the above technical solution, in step (1), the time of glow discharge process is 2h.
As a preferred embodiment of the above technical solution, in step (1), the pressure of the vacuum discharge is 15-30Pa.
As a preferred embodiment of the above technical solution, in step (2), the natural fatty alcohol polyoxyethylene ether, n-amyl alcohol, activity
Fluorescent yellow dye FL, scattered fluorescent yellow dyestuff 10GN, supercritical CO2Dosage with distilled water is in terms of parts by weight, respectively：
10-20 parts, 12-30 parts, 0.05-0.25 parts, 0.01-0.15 parts, 40-60 parts and 0.01-6 parts.
As a preferred embodiment of the above technical solution, in step (2), the natural fatty alcohol polyoxyethylene ether, n-amyl alcohol, activity
Fluorescent yellow dye FL, scattered fluorescent yellow dyestuff 10GN, supercritical CO2Dosage with distilled water is in terms of parts by weight, respectively：20
Part, 30 parts, 0.15 part, 0.09 part, 43.12 parts and 5.5 parts.
As a preferred embodiment of the above technical solution, in step (3), the temperature of the dyeing is 120 DEG C, the time of the dyeing
For 100min.
The invention has the advantages that：
The present invention dyes polyester-cotton fabric using supercritical fluid, supercritical CO2To scattered fluorescent yellow dyestuff 10GN
With good solubility property, so as to substantially increase the dyeability of dyestuff, and the present invention before dyeing to polyester-cotton fabric into
The processing of row cold plasma, and rationally control process condition so that the dyeing ability of polyester-cotton fabric is improved；
On the other hand in the reverse micelle system for preparing of the present invention, dyestuff it is dense, cotton fiber can be made salt-free
Under the conditions of dyed, largely avoided staining and speckiness of the dyestuff to fabric；
Fluorescein polyester-cotton fabric soft comfortable prepared by the present invention, bright, dye-uptake is high, and color fastness is big, preparation side
Method is simple, and production cost is low.
Specific embodiment：
In order to better understand the present invention, below by embodiment, the present invention is further described, and embodiment is served only for solving
The present invention is released, any restriction will not be formed to the present invention.
Embodiment 1
A kind of preparation method of fluorescein polyester-cotton fabric, includes the following steps：
(1) by polyester-cotton fabric using CGP-3 type corona treatment instrument, using capacitive coupling glow discharge process 2h, electricity
Source frequency is 13.56MHz, and power 100W, discharge current 100mA, 5Pa vacuum discharge, Ar flow velocitys are 20ml/min；
(2) by 10 parts of natural fatty alcohol polyoxyethylene ether, 12 parts of n-amyl alcohols, 0.05 part of active fluoro yellow dye FL, 0.01
Part 10GN, 40-60 parts of supercritical COs of scattered fluorescent yellow dyestuff2In high-pressure bottle of the 0.01 part of distilled water under 10MPa pressure
Form reverse micelle system；
(3) polyester-cotton fabric Jing Guo glow discharge process is placed in high-pressure bottle, is warming up to 50 DEG C, dye 60min；
(4) high-pressure bottle is decompressed to normal pressure, takes out polyester-cotton fabric, and recycle CO2And dyestuff, obtain fluorescein polyester-cotton blend face
Material.
Embodiment 2
A kind of preparation method of fluorescein polyester-cotton fabric, includes the following steps：
(1) by polyester-cotton fabric using CGP-3 type corona treatment instrument, using capacitive coupling glow discharge process 5h, electricity
Source frequency is 13.56MHz, and power 100W, discharge current 100mA, 50Pa vacuum discharge, Ar flow velocitys are 20ml/min；
(2) by 20 parts of natural fatty alcohol polyoxyethylene ether, 30 parts of n-amyl alcohols, 0.25 part of active fluoro yellow dye FL, 0.15
Part scattered fluorescent yellow dyestuff 10GN, 60 parts of supercritical COs2It is anti-with being formed in high-pressure bottle of 6 parts of distilled water under 30MPa pressure
Micelle volume；
(3) polyester-cotton fabric Jing Guo glow discharge process is placed in high-pressure bottle, is warming up to 150 DEG C, dye 150min；
(4) high-pressure bottle is decompressed to normal pressure, takes out polyester-cotton fabric, and recycle CO2And dyestuff, obtain fluorescein polyester-cotton blend face
Material.
Embodiment 3
A kind of preparation method of fluorescein polyester-cotton fabric, includes the following steps：
(1) by polyester-cotton fabric using CGP-3 type corona treatment instrument, using capacitive coupling glow discharge process 2h, electricity
Source frequency is 13.56MHz, and power 100W, discharge current 100mA, 30Pa vacuum discharge, Ar flow velocitys are 20ml/min；
(2) by 20 parts of natural fatty alcohol polyoxyethylene ether, 30 parts of n-amyl alcohols, 0.15 part of active fluoro yellow dye FL, 0.09
Part scattered fluorescent yellow dyestuff 10GN, 43.12 parts of supercritical COs2With high-pressure bottle of 5.5 parts of distilled water under 10-30MPa pressure
Middle formation reverse micelle system；
(3) polyester-cotton fabric Jing Guo glow discharge process is placed in high-pressure bottle, is warming up to 120 DEG C, dye 100min；
(4) high-pressure bottle is decompressed to normal pressure, takes out polyester-cotton fabric, and recycle CO2And dyestuff, obtain fluorescein polyester-cotton blend face
Material.
Embodiment 4
A kind of preparation method of fluorescein polyester-cotton fabric, includes the following steps：
(1) by polyester-cotton fabric using CGP-3 type corona treatment instrument, using capacitive coupling glow discharge process 3h, electricity
Source frequency is 13.56MHz, and power 100W, discharge current 100mA, 15Pa vacuum discharge, Ar flow velocitys are 20ml/min；
(2) by 12 parts of natural fatty alcohol polyoxyethylene ether, 15 parts of n-amyl alcohols, 0.1 part of active fluoro yellow dye FL, 0.05 part
Scattered fluorescent yellow dyestuff 10GN, 45 parts of supercritical COs2Anti- glue is formed in high-pressure bottle of the 1 part of distilled water under 15MPa pressure
Beam system；
(3) polyester-cotton fabric Jing Guo glow discharge process is placed in high-pressure bottle, is warming up to 70 DEG C, dye 80min；
(4) high-pressure bottle is decompressed to normal pressure, takes out polyester-cotton fabric, and recycle CO2And dyestuff, obtain fluorescein polyester-cotton blend face
Material.
Embodiment 5
A kind of preparation method of fluorescein polyester-cotton fabric, includes the following steps：
(1) by polyester-cotton fabric using CGP-3 type corona treatment instrument, using capacitive coupling glow discharge process 4h, electricity
Source frequency is 13.56MHz, and power 100W, discharge current 100mA, 25Pa vacuum discharge, Ar flow velocitys are 20ml/min；
(2) by 16 parts of natural fatty alcohol polyoxyethylene ether, 20 parts of n-amyl alcohols, 0.15 part of active fluoro yellow dye FL, 0.1 part
Scattered fluorescent yellow dyestuff 10GN, 50 parts of supercritical COs2Anti- glue is formed in high-pressure bottle of 2 parts of distilled water under 20MPa pressure
Beam system；
(3) polyester-cotton fabric Jing Guo glow discharge process is placed in high-pressure bottle, is warming up to 90 DEG C, dye 100min；
(4) high-pressure bottle is decompressed to normal pressure, takes out polyester-cotton fabric, and recycle CO2And dyestuff, obtain fluorescein polyester-cotton blend face
Material.
Embodiment 6
A kind of preparation method of fluorescein polyester-cotton fabric, includes the following steps：
(1) by polyester-cotton fabric using CGP-3 type corona treatment instrument, using capacitive coupling glow discharge process 4.5h,
Supply frequency is 13.56MHz, and power 100W, discharge current 100mA, 35Pa vacuum discharge, Ar flow velocitys are 20ml/min；
(2) by 18 parts of natural fatty alcohol polyoxyethylene ether, 25 parts of n-amyl alcohols, 0.2 part of active fluoro yellow dye FL, 0.13 part
Scattered fluorescent yellow dyestuff 10GN, 55 parts of supercritical COs2Anti- glue is formed in high-pressure bottle of 4 parts of distilled water under 25MPa pressure
Beam system；
(3) polyester-cotton fabric Jing Guo glow discharge process is placed in high-pressure bottle, is warming up to 110 DEG C, dye 120min；
(4) high-pressure bottle is decompressed to normal pressure, takes out polyester-cotton fabric, and recycle CO2And dyestuff, obtain fluorescein polyester-cotton blend face
Material.
Claims (5)
1. a kind of preparation method of fluorescein polyester-cotton fabric, which is characterized in that include the following steps：
(1) by polyester-cotton fabric using CGP-3 type corona treatment instrument, using capacitive coupling glow discharge process 2-5h, power supply
Frequency is 13.56MHz, and power 100W, discharge current 100mA, 5-50Pa vacuum discharge, Ar flow velocitys are 20ml/min；
(2) by natural fatty alcohol polyoxyethylene ether, n-amyl alcohol, active fluoro yellow dye FL, scattered fluorescent yellow dyestuff 10GN, super face
Boundary CO2Reverse micelle system is formed in high-pressure bottle of the distilled water under 10-30MPa pressure；
(3) polyester-cotton fabric Jing Guo glow discharge process is placed in high-pressure bottle, is warming up to 50-150 DEG C, dye 60-
150min；
(4) high-pressure bottle is decompressed to normal pressure, takes out polyester-cotton fabric, and recycle CO2And dyestuff, obtain fluorescein polyester-cotton fabric；
Wherein, natural fatty alcohol polyoxyethylene ether, n-amyl alcohol, active fluoro yellow dye FL, scattered fluorescent yellow dyestuff 10GN, super face
Boundary CO2Dosage with distilled water is in terms of parts by weight, respectively：10-20 parts, 12-30 parts, 0.05-0.25 parts, 0.01-0.15
Part, 40-60 parts and 0.01-6 parts.
2. a kind of preparation method of fluorescein polyester-cotton fabric as described in claim 1, which is characterized in that in step (1), aura
The time of discharge treatment is 2h.
3. a kind of preparation method of fluorescein polyester-cotton fabric as described in claim 1, which is characterized in that described in step (1)
The pressure of vacuum discharge is 15-30Pa.
4. a kind of preparation method of fluorescein polyester-cotton fabric as described in claim 1, which is characterized in that described in step (2)
Natural fatty alcohol polyoxyethylene ether, n-amyl alcohol, active fluoro yellow dye FL, scattered fluorescent yellow dyestuff 10GN, supercritical CO2And steaming
The dosage of distilled water is in terms of parts by weight, respectively：20 parts, 30 parts, 0.15 part, 0.09 part, 43.12 parts and 5.5 parts.
5. a kind of preparation method of fluorescein polyester-cotton fabric as described in claim 1, which is characterized in that described in step (3)
The temperature of dyeing is 120 DEG C, and the time of the dyeing is 100min.
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| CN201610260342.6A CN105862386B (en) | 2016-04-25 | 2016-04-25 | A kind of preparation method of fluorescein polyester-cotton fabric |
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| CN201610260342.6A CN105862386B (en) | 2016-04-25 | 2016-04-25 | A kind of preparation method of fluorescein polyester-cotton fabric |
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| CN105862386B true CN105862386B (en) | 2018-07-03 |
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| CN101117764A (en) * | 2007-07-06 | 2008-02-06 | 绍兴中纺院江南分院有限公司 | Atmospheric plasma processing method used for fabric topical finish |
| CN102409527A (en) * | 2011-10-20 | 2012-04-11 | 浙江理工大学 | Plasma finishing method for endowing fabric durable super-hydrophobic property |
| CN102926185B (en) * | 2012-11-05 | 2014-04-23 | 南通纺织职业技术学院 | Dyeing and finishing process for polyester-cotton blending woven fluorescent yellow fabrics |
| CN104018370B (en) * | 2014-05-28 | 2016-01-20 | 河南工程学院 | A kind of preparation method of polyester-cotton blend fluorescein fabric |
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Effective date of registration: 20180413 Address after: 318050 17A04 room, peninsula garden, Tengda Road, road, Taizhou Road, Luqiao District, Zhejiang, China Applicant after: Taizhou lace Agel Ecommerce Ltd Address before: 523000 Guangdong province Dongguan City Songshan Lake high tech Industrial Zone Building 406 industrial development productivity Applicant before: Dongguan Lianzhou Intellectual Property Operation Management Co.,Ltd. |
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Effective date of registration: 20180522 Address after: 521000 the 2-3 floor of B building, Dong GUI resin complex, West Lake industrial town, Xinyang Road, Chaozhou, Guangdong. Applicant after: Chaozhou City Press Fashion Co., Ltd. Address before: 318050 17A04 room 2, Peninsular garden, Tengda Road, Luqiao District, Taizhou, Zhejiang. Applicant before: Taizhou lace Agel Ecommerce Ltd |
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Inventor after: Huang Qingwen Inventor after: Zheng Jianbo Inventor after: Zheng Yangtao Inventor before: Wang Wenqing |
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