CN105861047A - Method for producing chlorinated paraffin with catalytic photochlorination excitation method - Google Patents

Method for producing chlorinated paraffin with catalytic photochlorination excitation method Download PDF

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Publication number
CN105861047A
CN105861047A CN201610234502.XA CN201610234502A CN105861047A CN 105861047 A CN105861047 A CN 105861047A CN 201610234502 A CN201610234502 A CN 201610234502A CN 105861047 A CN105861047 A CN 105861047A
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CN
China
Prior art keywords
chlorinated paraffin
catalytic
paraffin
photochlorination
producing chlorinated
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Pending
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CN201610234502.XA
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Chinese (zh)
Inventor
林群祥
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Individual
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Individual
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Priority to CN201610234502.XA priority Critical patent/CN105861047A/en
Publication of CN105861047A publication Critical patent/CN105861047A/en
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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G73/00—Recovery or refining of mineral waxes, e.g. montan wax
    • C10G73/38—Chemical modification of petroleum

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  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

The invention discloses a method for producing chlorinated paraffin with a catalytic photochlorination excitation method, and belongs to the technical field of chlorinated paraffin. To increase the chlorinated paraffin production speed, according to the technical scheme based on the improvement on the original patent 87106851.6, a ketone peroxide catalyst is added in paraffin, and a light source is additionally arranged in a kettle, so that the production method is higher in speed.

Description

Catalytic light chlorination agitates method to produce chlorinated paraffin method
(1) technical field: the present invention relates to a kind of method producing chlorinated paraffin.
(2) background technology: " equipment for preparation of paraffin chloride by forced circulating blast method " (the former patent No.: 87106851.6) its technical scheme is: chlorine is sent into reactor space, the hydrogen chloride gas that chlorine and reaction generate is extracted out, through ejector pump and hopper, it is only absorbed by the water, remaining chlorine drum is pressed into agitation device, fast reaction the most continuously.But it is the most preferable to be used for producing chlorinated paraffin speed, especially producing high chlorinated paraffin product, to the reaction later stage, speed eases up.
(3) summary of the invention: the task of the present invention is based on a kind of improvement to former 87106851.6 patents of invention, a kind of method that faster production chlorinated paraffin is provided, adopt the technical scheme that catalyst, install light source in still additional, so agitate lower raising response speed in forced circulation.
(4) detailed description of the invention: a set of " equipment for preparation of paraffin chloride by forced circulating blast method ", uses 500 liters of reactors, adds ketone peroxide in advance in paraffin, and concentration is 0.01～6.00%, installs 1000 watts of mercury lamps in its reactor additional.
Present invention operation is same with " equipment for preparation of paraffin chloride by forced circulating blast method ".

Claims (1)

1. Catalytic light chlorination agitates method to produce a chlorinated paraffin method, including chlorine and hydrogen chloride gas Body is extracted out, and hydrogen chloride gas is only absorbed by the water in ejector pump and hopper, and remaining chlorine drum is pressed into agitation device, So continuously, it is characterized in that: adding concentration in paraffin is 0.01～6.00% ketone peroxide catalyzed, Still is built with light source chlorination.
CN201610234502.XA 2016-04-08 2016-04-08 Method for producing chlorinated paraffin with catalytic photochlorination excitation method Pending CN105861047A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610234502.XA CN105861047A (en) 2016-04-08 2016-04-08 Method for producing chlorinated paraffin with catalytic photochlorination excitation method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610234502.XA CN105861047A (en) 2016-04-08 2016-04-08 Method for producing chlorinated paraffin with catalytic photochlorination excitation method

Publications (1)

Publication Number Publication Date
CN105861047A true CN105861047A (en) 2016-08-17

Family

ID=56637056

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610234502.XA Pending CN105861047A (en) 2016-04-08 2016-04-08 Method for producing chlorinated paraffin with catalytic photochlorination excitation method

Country Status (1)

Country Link
CN (1) CN105861047A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107699362A (en) * 2017-05-13 2018-02-16 林群祥 Catalytic light chlorination agitates method to produce chlorination gutter oil method

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN87106851A (en) * 1987-10-06 1988-07-27 林群祥 Equipment for preparation of paraffin chloride by forced circulating blast method
CN1027809C (en) * 1989-12-30 1995-03-08 湖南大学 Method for synthesizing paraffin chloride

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN87106851A (en) * 1987-10-06 1988-07-27 林群祥 Equipment for preparation of paraffin chloride by forced circulating blast method
CN1027809C (en) * 1989-12-30 1995-03-08 湖南大学 Method for synthesizing paraffin chloride

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
魏文德主编: "《有机化工原料大全》", 31 January 1999, 化学工业出版社 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107699362A (en) * 2017-05-13 2018-02-16 林群祥 Catalytic light chlorination agitates method to produce chlorination gutter oil method

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Application publication date: 20160817