CN105838426A - Method for producing chlorinated paraffin through pressure photochlorination bubbling blast method - Google Patents

Method for producing chlorinated paraffin through pressure photochlorination bubbling blast method Download PDF

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Publication number
CN105838426A
CN105838426A CN201610234586.7A CN201610234586A CN105838426A CN 105838426 A CN105838426 A CN 105838426A CN 201610234586 A CN201610234586 A CN 201610234586A CN 105838426 A CN105838426 A CN 105838426A
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CN
China
Prior art keywords
chlorinated paraffin
pressure
photochlorination
chlorine
bubbling
Prior art date
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Pending
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CN201610234586.7A
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Chinese (zh)
Inventor
林群祥
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Individual
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Individual
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Publication date
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Priority to CN201610234586.7A priority Critical patent/CN105838426A/en
Publication of CN105838426A publication Critical patent/CN105838426A/en
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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G73/00—Recovery or refining of mineral waxes, e.g. montan wax
    • C10G73/38—Chemical modification of petroleum

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  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

The title of the invention is 'method for producing chlorinated paraffin through pressure photochlorination bubbling blast method', and belongs to the technical field of chlorinated paraffin. To improve the production speed of chlorinated paraffin, a faster production method is provided based on the improvement of the original patent having the application number of 87106851.6 and adopts the technical scheme of increasing the pressure in a kettle to 1 kilogram per square centimeter, arranging a light source in the kettle, and arranging a bubbler in the kettle in the patent having the application number of 87106851.6, wherein chlorine is directly put in the bubble.

Description

Pressurization Light chlorimation bubbling agitates method to produce chlorinated paraffin method
(1) technical field: the present invention relates to a kind of method producing chlorinated paraffin.
(2) background technology: " equipment for preparation of paraffin chloride by forced circulating blast method " (the former patent No.: 87106851.6) its technical scheme is: chlorine is sent into reactor space, the hydrogen chloride gas that chlorine and reaction generate is extracted out, through jet pump and hopper, it is only absorbed by the water, remaining chlorine drum is pressed into agitation device, fast reaction the most continuously.But it is the most preferable to be used for producing chlorinated paraffin speed, especially producing high chlorinated paraffin product, to the reaction later stage, speed eases up.
(3) summary of the invention: the task of the present invention is based on a kind of improvement to former 87106851.6 patents of invention, a kind of method that faster production chlorinated paraffin is provided, adopt the technical scheme that device improves pressure, light source is installed additional in still, separately add in its reactor and load onto bubbler, the chlorine supplied by chlorine source is passed directly into bubbler, and reactor material is carried out bubbling.Under forced circulation is agitated, so add bubbling improve reaction speed.
(4) detailed description of the invention: a set of " equipment for preparation of paraffin chloride by forced circulating blast method ", use 500 liters of reactors, in making device, pressure brings up to 1 kg/cm, installs 1000 watts of mercury lamps in its reactor additional, adds again and load onto existing current bubbler in its reactor.
Present invention operation is same with " equipment for preparation of paraffin chloride by forced circulating blast method ".

Claims (1)

1. pressurization Light chlorimation bubbling agitates method to produce a chlorinated paraffin method, including chlorine and chlorination Hydrogen is extracted out, and hydrogen chloride gas is only absorbed by the water at jet pump and hopper, and remaining chlorine drum is pressed into drum Dynamic device, the most continuously, is characterized in that: increasing reaction pressure, still is direct built with light source chlorination chlorine Put into still bubbler.
CN201610234586.7A 2016-04-09 2016-04-09 Method for producing chlorinated paraffin through pressure photochlorination bubbling blast method Pending CN105838426A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610234586.7A CN105838426A (en) 2016-04-09 2016-04-09 Method for producing chlorinated paraffin through pressure photochlorination bubbling blast method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610234586.7A CN105838426A (en) 2016-04-09 2016-04-09 Method for producing chlorinated paraffin through pressure photochlorination bubbling blast method

Publications (1)

Publication Number Publication Date
CN105838426A true CN105838426A (en) 2016-08-10

Family

ID=56588601

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610234586.7A Pending CN105838426A (en) 2016-04-09 2016-04-09 Method for producing chlorinated paraffin through pressure photochlorination bubbling blast method

Country Status (1)

Country Link
CN (1) CN105838426A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107723105A (en) * 2017-05-13 2018-02-23 林群祥 Pressurization Light chlorimation bubbling agitates method to produce chlorination gutter oil method

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN87106851A (en) * 1987-10-06 1988-07-27 林群祥 Equipment for preparation of paraffin chloride by forced circulating blast method
CN1599705A (en) * 2001-12-05 2005-03-23 巴斯福股份公司 Method for the production of 1,2-dichloroethane

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN87106851A (en) * 1987-10-06 1988-07-27 林群祥 Equipment for preparation of paraffin chloride by forced circulating blast method
CN1599705A (en) * 2001-12-05 2005-03-23 巴斯福股份公司 Method for the production of 1,2-dichloroethane

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
汪多仁: "氯化石蜡-70的开发与应用", 《聚合物与助剂》 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107723105A (en) * 2017-05-13 2018-02-23 林群祥 Pressurization Light chlorimation bubbling agitates method to produce chlorination gutter oil method

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WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20160810