CN105838429A - Method for producing chlorinated paraffin by catalytic pressurization, photochlorination, bubbling and propelling methods - Google Patents
Method for producing chlorinated paraffin by catalytic pressurization, photochlorination, bubbling and propelling methods Download PDFInfo
- Publication number
- CN105838429A CN105838429A CN201610241008.6A CN201610241008A CN105838429A CN 105838429 A CN105838429 A CN 105838429A CN 201610241008 A CN201610241008 A CN 201610241008A CN 105838429 A CN105838429 A CN 105838429A
- Authority
- CN
- China
- Prior art keywords
- chlorinated paraffin
- bubbling
- paraffin
- chlorine
- pressurization
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G73/00—Recovery or refining of mineral waxes, e.g. montan wax
- C10G73/38—Chemical modification of petroleum
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- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The invention provides a method for producing chlorinated paraffin by catalytic pressurization, photochlorination, bubbling and propelling methods, belonging to the technical field of chlorinated paraffin. In order to increase the chlorinated paraffin production speed, a technical scheme adopted based on improvement of the original 87106851.6 patent is that a catalyst ketone peroxide is added to paraffin to increase the pressure in a kettle to 1kg/lcm<2>, a light source is additionally installed in the kettle, a bubbler is additionally installed in the 87106851.6 device kettle, and chlorine is directly put in the bubbler. A faster production method is provided.
Description
(1) technical field: the present invention relates to a kind of method producing chlorinated paraffin.
(2) background technology: " equipment for preparation of paraffin chloride by forced circulating blast method " (the former patent No.: 87106851.6) its technical scheme is: chlorine is sent into reactor space, the hydrogen chloride gas that chlorine and reaction generate is extracted out, through ejector pump and hopper, it is only absorbed by the water, remaining chlorine drum is pressed into agitation device, fast reaction the most continuously.But it is the most preferable to be used for producing chlorinated paraffin speed, especially producing high chlorinated paraffin product, to the reaction later stage, speed eases up.
(3) summary of the invention: the task of the present invention is based on a kind of improvement to former 87106851.6 patents of invention, a kind of method that faster production chlorinated paraffin is provided, adopt the technical scheme that and add catalyst, device improves pressure, light source is installed additional in still, separately add in its reactor and load onto bubbler, chlorine source the chlorine supplied is passed directly into bubbler, and reactor material is carried out bubbling.Under forced circulation is agitated, so add bubbling improve response speed.
(4) detailed description of the invention: a set of " equipment for preparation of paraffin chloride by forced circulating blast method ", use 500 liters of reactors, ketone peroxide is added in advance in paraffin, concentration is 0.01～6.00%, in making device, pressure brings up to 1 kg/cm, install 1000 watts of mercury lamps in its reactor additional, add again in its reactor and load onto existing current bubbler.
Present invention operation is same with " equipment for preparation of paraffin chloride by forced circulating blast method ".
Claims (1)
1. catalysis pressurization Light chlorimation bubbling agitate method produce a chlorinated paraffin method, including chlorine with
Hydrogen chloride gas is extracted out, and hydrogen chloride gas is only absorbed by the water in ejector pump and hopper, remaining chlorine drum pressure
Enter agitation device, the most continuously, it is characterized in that: adding concentration in paraffin is 0.01～6.00% ketone peroxide
Compound is catalyzed, and increases reaction pressure, and still is directly placed into bubbler in still built with light source chlorination chlorine.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610241008.6A CN105838429A (en) | 2016-04-10 | 2016-04-10 | Method for producing chlorinated paraffin by catalytic pressurization, photochlorination, bubbling and propelling methods |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610241008.6A CN105838429A (en) | 2016-04-10 | 2016-04-10 | Method for producing chlorinated paraffin by catalytic pressurization, photochlorination, bubbling and propelling methods |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105838429A true CN105838429A (en) | 2016-08-10 |
Family
ID=56588448
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610241008.6A Pending CN105838429A (en) | 2016-04-10 | 2016-04-10 | Method for producing chlorinated paraffin by catalytic pressurization, photochlorination, bubbling and propelling methods |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105838429A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105838428A (en) * | 2016-04-13 | 2016-08-10 | 林群祥 | Method for producing chlorinated paraffin through catalysis photochlorination bubbling blast method |
| CN106929103A (en) * | 2017-04-04 | 2017-07-07 | 林群祥 | Catalysis pressurization Light chlorimation bubbling agitates method to produce Modified Chlorinated Paraffin method |
| CN106929106A (en) * | 2017-04-04 | 2017-07-07 | 林群祥 | Catalysis pressurization Light chlorimation bubbling agitates the hot method production method of Modified Chlorinated Paraffin 70 of air cooling |
| CN107699367A (en) * | 2017-05-13 | 2018-02-16 | 林群祥 | Catalysis pressurization Light chlorimation bubbling agitates method to produce chlorination gutter oil method |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN87106851A (en) * | 1987-10-06 | 1988-07-27 | 林群祥 | Equipment for preparation of paraffin chloride by forced circulating blast method |
| CN1053081A (en) * | 1989-12-30 | 1991-07-17 | 湖南大学 | A kind of method of synthesizing paraffin chloride |
-
2016
- 2016-04-10 CN CN201610241008.6A patent/CN105838429A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN87106851A (en) * | 1987-10-06 | 1988-07-27 | 林群祥 | Equipment for preparation of paraffin chloride by forced circulating blast method |
| CN1053081A (en) * | 1989-12-30 | 1991-07-17 | 湖南大学 | A kind of method of synthesizing paraffin chloride |
Non-Patent Citations (1)
| Title |
|---|
| 汪多仁: "氯化石蜡-70的开发与应用", 《聚合物与助剂》 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105838428A (en) * | 2016-04-13 | 2016-08-10 | 林群祥 | Method for producing chlorinated paraffin through catalysis photochlorination bubbling blast method |
| CN106929103A (en) * | 2017-04-04 | 2017-07-07 | 林群祥 | Catalysis pressurization Light chlorimation bubbling agitates method to produce Modified Chlorinated Paraffin method |
| CN106929106A (en) * | 2017-04-04 | 2017-07-07 | 林群祥 | Catalysis pressurization Light chlorimation bubbling agitates the hot method production method of Modified Chlorinated Paraffin 70 of air cooling |
| CN107699367A (en) * | 2017-05-13 | 2018-02-16 | 林群祥 | Catalysis pressurization Light chlorimation bubbling agitates method to produce chlorination gutter oil method |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20160810 |