CN105861049A - Method for producing chlorinated paraffin with catalytic bubbling excitation method - Google Patents

Method for producing chlorinated paraffin with catalytic bubbling excitation method Download PDF

Info

Publication number
CN105861049A
CN105861049A CN201610234544.3A CN201610234544A CN105861049A CN 105861049 A CN105861049 A CN 105861049A CN 201610234544 A CN201610234544 A CN 201610234544A CN 105861049 A CN105861049 A CN 105861049A
Authority
CN
China
Prior art keywords
chlorinated paraffin
paraffin
chlorine
bubbling
bubbler
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610234544.3A
Other languages
Chinese (zh)
Inventor
林群祥
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to CN201610234544.3A priority Critical patent/CN105861049A/en
Publication of CN105861049A publication Critical patent/CN105861049A/en
Pending legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G73/00—Recovery or refining of mineral waxes, e.g. montan wax
    • C10G73/38—Chemical modification of petroleum

Landscapes

  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

The invention discloses a method for producing chlorinated paraffin with a catalytic bubbling excitation method, and belongs to the technical field of chlorinated paraffin. To increase the chlorinated paraffin production speed, according to the technical scheme based on the improvement on the original patent 87106851.6, a ketone peroxide catalyst is added in paraffin, a bubbler is additionally arranged in a device kettle in the patent 87106851.6, and chlorine is directly introduced in the bubbler, so that the production method is higher in speed.

Description

Catalysis bubbling agitates method to produce chlorinated paraffin method
(1) technical field: the present invention relates to a kind of method producing chlorinated paraffin.
(2) background technology: " equipment for preparation of paraffin chloride by forced circulating blast method " (the former patent No.: 87106851.6) its technical scheme is: chlorine is sent into reactor space, the hydrogen chloride gas that chlorine and reaction generate is extracted out, through ejector pump and hopper, it is only absorbed by the water, remaining chlorine drum is pressed into agitation device, fast reaction the most continuously.But it is the most preferable to be used for producing chlorinated paraffin speed, especially producing high chlorinated paraffin product, to the reaction later stage, speed eases up.
(3) summary of the invention: the task of the present invention is based on a kind of improvement to former 87106851.6 patents of invention, a kind of method that faster production chlorinated paraffin is provided, adopt the technical scheme that and add catalyst, separately add in its reactor and load onto bubbler, the chlorine supplied by chlorine source is passed directly into bubbler, and reactor material is carried out bubbling.Under forced circulation is agitated, so add bubbling improve response speed.
(4) detailed description of the invention: a set of " equipment for preparation of paraffin chloride by forced circulating blast method ", use 500 liters of reactors, adding ketone peroxide in advance in paraffin, concentration is 0.01～6.00%, adds again and load onto existing current bubbler in its reactor.
Present invention operation is same with " equipment for preparation of paraffin chloride by forced circulating blast method ".

Claims (1)

1. catalysis bubbling agitates method to produce a chlorinated paraffin method, including chlorine and hydrogen chloride gas Extracting out, hydrogen chloride gas is only absorbed by the water in ejector pump and hopper, and remaining chlorine drum is pressed into agitation device, So continuously, it is characterized in that: adding concentration in paraffin is 0.01～6.00% ketone peroxide catalyzed, Chlorine is directly placed into bubbler in still.
CN201610234544.3A 2016-04-08 2016-04-08 Method for producing chlorinated paraffin with catalytic bubbling excitation method Pending CN105861049A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610234544.3A CN105861049A (en) 2016-04-08 2016-04-08 Method for producing chlorinated paraffin with catalytic bubbling excitation method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610234544.3A CN105861049A (en) 2016-04-08 2016-04-08 Method for producing chlorinated paraffin with catalytic bubbling excitation method

Publications (1)

Publication Number Publication Date
CN105861049A true CN105861049A (en) 2016-08-17

Family

ID=56637033

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610234544.3A Pending CN105861049A (en) 2016-04-08 2016-04-08 Method for producing chlorinated paraffin with catalytic bubbling excitation method

Country Status (1)

Country Link
CN (1) CN105861049A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106929105A (en) * 2017-04-04 2017-07-07 林群祥 Catalysis agitates method to produce Modified Chlorinated Paraffin method
CN107099329A (en) * 2017-04-04 2017-08-29 林群祥 Catalysis bubbling agitates method to produce Modified Chlorinated Paraffin method
CN107629885A (en) * 2017-05-13 2018-01-26 林群祥 Catalysis bubbling agitates method to produce chlorination gutter oil method

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN87106851A (en) * 1987-10-06 1988-07-27 林群祥 Equipment for preparation of paraffin chloride by forced circulating blast method

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN87106851A (en) * 1987-10-06 1988-07-27 林群祥 Equipment for preparation of paraffin chloride by forced circulating blast method

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
汪多仁: "氯化石蜡-70的开发与应用", 《聚合物与助剂》 *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106929105A (en) * 2017-04-04 2017-07-07 林群祥 Catalysis agitates method to produce Modified Chlorinated Paraffin method
CN107099329A (en) * 2017-04-04 2017-08-29 林群祥 Catalysis bubbling agitates method to produce Modified Chlorinated Paraffin method
CN107629885A (en) * 2017-05-13 2018-01-26 林群祥 Catalysis bubbling agitates method to produce chlorination gutter oil method

Similar Documents

Publication Publication Date Title
CN105838429A (en) Method for producing chlorinated paraffin by catalytic pressurization, photochlorination, bubbling and propelling methods
CN105838428A (en) Method for producing chlorinated paraffin through catalysis photochlorination bubbling blast method
CN105861049A (en) Method for producing chlorinated paraffin with catalytic bubbling excitation method
CN109810150A (en) A method of fulvic acid in lignite is extracted using supersonic synergic catalysis oxidation
CN105838430A (en) Method for producing chlorinated paraffin by catalytic pressurization photo-chlorination direct agitation process
CN105838438A (en) Method for producing chlorinated paraffin-70 through catalytic pressurizing bubbling agitating gas heating and cooling method
CN105925308A (en) Catalytic pressurized bubbling method for producing chlorinated paraffin
CN106047407A (en) Method for producing chlorinated paraffin-70 by catalytic photo-chlorination bubbling agitation gas cooling-heating method
CN105838431A (en) Method for producing chlorcosane through catalysis direct propelling method
CN105838434A (en) Method for producing chlorinated paraffin-70 through catalytic pressurizing photo-chlorination bubbling agitating gas heating and cooling method
CN105925311A (en) Method for producing chlorinated paraffin-70 through catalyzing, pressurizing and direct gas agitating cold-hot method
CN105838424A (en) Method for producing chlorinated paraffin through bubbling blast method
CN105838432A (en) Method for producing chlorcosane through catalytic light chlorination direct propelling method
CN105838423A (en) Method for producing chlorinated paraffin through catalysis blast method
CN105861052A (en) Method for producing chlorinated paraffin by catalysis and pressurization direct propelling
CN105838425A (en) Method for producing chlorinated paraffin through pressure bubbling blast method
CN105838422A (en) Method for producing chlorinated paraffin through catalysis pressure blast method
CN105861051A (en) Method for producing chlorinated paraffin through direct agitating process by pressurization and photochlorination
CN105838421A (en) Method for producing chlorinated paraffin through photochlorination bubbling blast method
CN105838436A (en) Method for producing chlorinated paraffin-70 through catalytic bubbling agitating gas heating and cooling method
CN105861050A (en) Method for producing chlorinated paraffin by direct propelling
CN105838420A (en) Method for producing chlorinated paraffin through pressure blast method
CN106010643A (en) Method for producing chlorinated paraffin by photochlorination direct agitating method
CN105925309A (en) Method for producing chlorinated paraffin through pressurizing direct agitation technology
CN105861048A (en) Method for producing chlorinated paraffin through photochlorination propelling

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20160817

WD01 Invention patent application deemed withdrawn after publication