CN105861052A - Method for producing chlorinated paraffin by catalysis and pressurization direct propelling - Google Patents

Method for producing chlorinated paraffin by catalysis and pressurization direct propelling Download PDF

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Publication number
CN105861052A
CN105861052A CN201610269304.7A CN201610269304A CN105861052A CN 105861052 A CN105861052 A CN 105861052A CN 201610269304 A CN201610269304 A CN 201610269304A CN 105861052 A CN105861052 A CN 105861052A
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CN
China
Prior art keywords
chlorinated paraffin
chlorine
paraffin
catalysis
producing chlorinated
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Pending
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CN201610269304.7A
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Chinese (zh)
Inventor
林群祥
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Individual
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Individual
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Priority to CN201610269304.7A priority Critical patent/CN105861052A/en
Publication of CN105861052A publication Critical patent/CN105861052A/en
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G73/00—Recovery or refining of mineral waxes, e.g. montan wax
    • C10G73/38—Chemical modification of petroleum

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  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

The invention discloses a method for producing chlorinated paraffin by catalysis and pressurization direct propelling, belonging to the technical field of chlorinated paraffin. Aiming at improving the productive speed of chlorinated paraffin and based on the patent 87106851.6, the adopted technical scheme is improved as that a catalyst ketone peroxide is added to paraffin and the pressure in a kettle is increased to 1 kilogram/square centimeter, the device of the patent 87106851.6 is improved to a propeller to which chlorine gas supplied by a chlorine source is directly introduced, and thus a quicker production method is provided.

Description

Catalysis pressurization directly agitates method to produce chlorinated paraffin method
(1) technical field: the present invention relates to a kind of method producing chlorinated paraffin.
(2) background technology: " equipment for preparation of paraffin chloride by forced circulating blast method " (the former patent No.: 87106851.6) its technical scheme is: chlorine is sent into reactor space, the hydrogen chloride gas that chlorine and reaction generate is extracted out, through ejector pump and hopper, it is only absorbed by the water, remaining chlorine drum is pressed into agitation device, fast reaction the most continuously.But it is the most preferable to be used for producing chlorinated paraffin speed, especially producing high chlorinated paraffin product, to the reaction later stage, speed eases up.
(3) summary of the invention: the task of the present invention is based on a kind of improvement to former 87106851.6 patents of invention, a kind of method that faster production chlorinated paraffin is provided, adopt the technical scheme that and add catalyst, device improves pressure, the chlorine supplied by chlorine source is passed directly into agitation device, agitates reactor material.So add under forced circulation is agitated and agitate raising response speed.
(4) detailed description of the invention: a set of " equipment for preparation of paraffin chloride by forced circulating blast method ", use 500 liters of reactors, ketone peroxide is added in advance in paraffin, concentration is 0.01～6.00%, in making device, pressure brings up to 1 kg/cm, the agitation device that its chlorine source supply reaction chlorine is passed directly in still.
Present invention operation is same with " equipment for preparation of paraffin chloride by forced circulating blast method ".

Claims (1)

1. catalysis pressurization directly agitates method to produce a chlorinated paraffin method, including chlorine and hydrogen chloride Gas is extracted out, and hydrogen chloride gas is only absorbed by the water in ejector pump and hopper, and remaining chlorine drum is pressed into agitates Device, the most continuously, is characterized in that: in paraffin add concentration be 0.01～6.00% ketone peroxide urge Changing, increase reaction pressure, chlorine source chlorine is directly placed into agitation device in still.
CN201610269304.7A 2016-04-16 2016-04-16 Method for producing chlorinated paraffin by catalysis and pressurization direct propelling Pending CN105861052A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610269304.7A CN105861052A (en) 2016-04-16 2016-04-16 Method for producing chlorinated paraffin by catalysis and pressurization direct propelling

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610269304.7A CN105861052A (en) 2016-04-16 2016-04-16 Method for producing chlorinated paraffin by catalysis and pressurization direct propelling

Publications (1)

Publication Number Publication Date
CN105861052A true CN105861052A (en) 2016-08-17

Family

ID=56629280

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610269304.7A Pending CN105861052A (en) 2016-04-16 2016-04-16 Method for producing chlorinated paraffin by catalysis and pressurization direct propelling

Country Status (1)

Country Link
CN (1) CN105861052A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107057761A (en) * 2017-04-04 2017-08-18 林群祥 Catalysis pressurization directly agitates method to produce Modified Chlorinated Paraffin method
CN107699365A (en) * 2017-05-13 2018-02-16 林群祥 Catalysis pressurization directly agitates method to produce chlorination gutter oil method

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN87106851A (en) * 1987-10-06 1988-07-27 林群祥 Equipment for preparation of paraffin chloride by forced circulating blast method

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN87106851A (en) * 1987-10-06 1988-07-27 林群祥 Equipment for preparation of paraffin chloride by forced circulating blast method

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
汪多仁: "氯化石蜡-70的开发与应用", 《聚合物与助剂》 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107057761A (en) * 2017-04-04 2017-08-18 林群祥 Catalysis pressurization directly agitates method to produce Modified Chlorinated Paraffin method
CN107699365A (en) * 2017-05-13 2018-02-16 林群祥 Catalysis pressurization directly agitates method to produce chlorination gutter oil method

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Application publication date: 20160817