CN105838422A - Method for producing chlorinated paraffin through catalysis pressure blast method - Google Patents

Method for producing chlorinated paraffin through catalysis pressure blast method Download PDF

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Publication number
CN105838422A
CN105838422A CN201610234504.9A CN201610234504A CN105838422A CN 105838422 A CN105838422 A CN 105838422A CN 201610234504 A CN201610234504 A CN 201610234504A CN 105838422 A CN105838422 A CN 105838422A
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CN
China
Prior art keywords
chlorinated paraffin
paraffin
pressure blast
catalysis
producing chlorinated
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Pending
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CN201610234504.9A
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Chinese (zh)
Inventor
林群祥
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Individual
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Individual
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Priority to CN201610234504.9A priority Critical patent/CN105838422A/en
Publication of CN105838422A publication Critical patent/CN105838422A/en
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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G73/00—Recovery or refining of mineral waxes, e.g. montan wax
    • C10G73/38—Chemical modification of petroleum

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  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

The title of the invention is 'method for producing chlorinated paraffin through catalysis pressure blast method', and belongs to the technical field of chlorinated paraffin. To improve the production speed of chlorinated paraffin, a faster production method is provided based on the improvement of the original patent having the application number of 87106851.6 and adopts the technical scheme of adding a ketones peroxide catalyst into paraffin and increasing the pressure in a kettle to 1 kilogram per square centimeter.

Description

Catalysis pressurization agitates method to produce chlorinated paraffin method
(1) technical field: the present invention relates to a kind of method producing chlorinated paraffin.
(2) background technology: " equipment for preparation of paraffin chloride by forced circulating blast method " (the former patent No.: 87106851.6) its technical scheme is: chlorine is sent into reactor space, the hydrogen chloride gas that chlorine and reaction generate is extracted out, through jet pump and hopper, it is only absorbed by the water, remaining chlorine drum is pressed into agitation device, fast reaction the most continuously.But it is the most preferable to be used for producing chlorinated paraffin speed, especially producing high chlorinated paraffin product, to the reaction later stage, speed eases up.
(3) summary of the invention: the task of the present invention is based on a kind of improvement to former 87106851.6 patents of invention, a kind of method that faster production chlorinated paraffin is provided, adopting the technical scheme that and add catalyst, device improves pressure, so agitates lower raising reaction speed in forced circulation.
(4) detailed description of the invention: a set of " equipment for preparation of paraffin chloride by forced circulating blast method ", uses 500 liters of reactors, adds ketone peroxide in advance in paraffin, and concentration is 0.01～6.00%, and in making device, pressure brings up to 1 kg/cm.
Present invention operation is same with " equipment for preparation of paraffin chloride by forced circulating blast method ".

Claims (1)

1. catalysis pressurization agitates method to produce a chlorinated paraffin method, including chlorine and hydrogen chloride gas Extracting out, hydrogen chloride gas is only absorbed by the water at jet pump and hopper, and remaining chlorine drum is pressed into agitation device, So continuously, it is characterized in that: adding concentration in paraffin is 0.01～6.00% ketone peroxide catalyzed, Increase reaction pressure.
CN201610234504.9A 2016-04-08 2016-04-08 Method for producing chlorinated paraffin through catalysis pressure blast method Pending CN105838422A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610234504.9A CN105838422A (en) 2016-04-08 2016-04-08 Method for producing chlorinated paraffin through catalysis pressure blast method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610234504.9A CN105838422A (en) 2016-04-08 2016-04-08 Method for producing chlorinated paraffin through catalysis pressure blast method

Publications (1)

Publication Number Publication Date
CN105838422A true CN105838422A (en) 2016-08-10

Family

ID=56588548

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610234504.9A Pending CN105838422A (en) 2016-04-08 2016-04-08 Method for producing chlorinated paraffin through catalysis pressure blast method

Country Status (1)

Country Link
CN (1) CN105838422A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106957684A (en) * 2017-04-04 2017-07-18 林群祥 Catalysis pressurization agitates method to produce Modified Chlorinated Paraffin method
CN107629882A (en) * 2017-05-13 2018-01-26 林群祥 Catalysis pressurization agitates method to produce chlorination gutter oil method

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2941013A (en) * 1958-11-06 1960-06-14 Diamond Alkali Co Paraffin wax chlorination process
CN87106851A (en) * 1987-10-06 1988-07-27 林群祥 Equipment for preparation of paraffin chloride by forced circulating blast method
CN1053081A (en) * 1989-12-30 1991-07-17 湖南大学 A kind of method of synthesizing paraffin chloride
CN101544911A (en) * 2009-05-06 2009-09-30 河南省化工研究所有限责任公司 Self circulation heat exchange method for materials in production of chlorinating paraffin-52 and chlorination reaction device therefor

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2941013A (en) * 1958-11-06 1960-06-14 Diamond Alkali Co Paraffin wax chlorination process
CN87106851A (en) * 1987-10-06 1988-07-27 林群祥 Equipment for preparation of paraffin chloride by forced circulating blast method
CN1053081A (en) * 1989-12-30 1991-07-17 湖南大学 A kind of method of synthesizing paraffin chloride
CN101544911A (en) * 2009-05-06 2009-09-30 河南省化工研究所有限责任公司 Self circulation heat exchange method for materials in production of chlorinating paraffin-52 and chlorination reaction device therefor

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106957684A (en) * 2017-04-04 2017-07-18 林群祥 Catalysis pressurization agitates method to produce Modified Chlorinated Paraffin method
CN107629882A (en) * 2017-05-13 2018-01-26 林群祥 Catalysis pressurization agitates method to produce chlorination gutter oil method

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Application publication date: 20160810