CN105859138B - A kind of ceramic glaze and preparation method thereof that the high fire resistance of intensity is good - Google Patents
A kind of ceramic glaze and preparation method thereof that the high fire resistance of intensity is good Download PDFInfo
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- CN105859138B CN105859138B CN201610208751.1A CN201610208751A CN105859138B CN 105859138 B CN105859138 B CN 105859138B CN 201610208751 A CN201610208751 A CN 201610208751A CN 105859138 B CN105859138 B CN 105859138B
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- glaze
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Classifications
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
Abstract
The invention discloses a kind of good ceramic glazes and preparation method thereof of the high fire resistance of intensity, it is related to technical field of ceramic production, is mainly made of sepiolite, borax, kaolin, china powder, waste glass powder, tin oxide, silica white, zirconium silicate, limonite, dimethylaniline, nano zine oxide, barium carbonate, cobalt sesquioxide, fruit tree ash, dimethylbenzene.The ceramic glaze intensity of the present invention is high, and thermal stability is good, nontoxic and pollution-free, the ingredients such as tin oxide, zirconium silicate interact, and enhance the adhesiveness of ceramic glaze internal structure, and then enhance the intensity and thermal stability of ceramic glaze, nano zine oxide also has certain anti-microbial property, environment protection health.
Description
Technical field
The present invention relates to technical field of ceramic production, the good ceramic glaze of more specifically a kind of high fire resistance of intensity and
Preparation method.
Background technology
Ceramics are made as primary raw material by crushing to be kneaded, be molded and calcine using natural clay and various natural minerals
Material various products.People were referred to as the article fired in special kiln high temperature being fabricated to clay and made pottery in the past
Porcelain, ceramics are the general names of pottery and porcelain.The traditional concept of ceramics refers to all using Inorganic nonmetal minerals such as clays as raw material
Artificial industrial products.It includes the mixture by clay or containing clay through being kneaded, forming, calcining and manufactured various systems
Product.By most coarse earthenware its range is belonged to most fine fine pottery and porcelain.Primary raw material for it is to take from
The silicate mineral (such as clay, quartz) of nature, thus it is industrial with glass, cement, enamel, refractory material etc., it belongs to
The scope of " silicate industry ".
Glaze used in ceramic product is indispensable raw material in ceramic product production, with the hair of ceramic industry
Exhibition, the type of glaze is more and more abundant various, the glaze product that majority domestic ceramics uses at present, and classification is numerous with range of use
It is more, high temperature glaze and low-temperature glaze can be divided into according to firing temperature, high temperature glaze has its uniqueness in the development of glaze
Place, the research to high temperature glaze is an important research direction of ceramic industry always.
Invention content
The purpose of the invention is to provide a kind of ceramic glaze and preparation method thereof that the high fire resistance of intensity is good.
The purpose of the present invention is what is be achieved through the following technical solutions：
A kind of ceramic glaze that the high fire resistance of intensity is good, is made of following raw material：Sepiolite 20-30, borax 6-
8, kaolin 8-10, china powder 3-5, waste glass powder 6-8, tin oxide 2-4, silica white 2-4, zirconium silicate 3-5, limonite
4-6, dimethylaniline 1-3, nano zine oxide 2-4, barium carbonate 3-5, cobalt sesquioxide 1-3, fruit tree ash 3-5, dimethylbenzene 8-12.
A kind of preparation method of the good ceramic glaze of high fire resistance of intensity, includes the following steps：
（1）Each raw material is weighed by weight；
（2）By the sepiolite after weighing, borax, kaolin, china powder, waste glass powder, tin oxide, silica white, zirconium silicate
Superfine powder, limonite, dimethylaniline, nano zine oxide, barium carbonate, cobalt sesquioxide, fruit tree ash, dimethylbenzene are sufficiently mixed simultaneously
It stirs evenly；
（3）By step（2）In mixed raw material be calcined 2-4 times at a high temperature of 1120-1210 DEG C；
（4）Raw material after calcining is taken out and put into ball milling and is ground, the glaze that fineness is 325-500 mesh is ground to
Slurry, a concentration of 40 degree of glaze slip；
（5）Glaze slip is uniformly imposed on ceramic body, enters kiln oxidizing flame or reducing flame and fires, in 1250-1350 DEG C of temperature
Under can Low fire ceramic finished product.
The advantage of the invention is that：
The ceramic glaze intensity of the present invention is high, and thermal stability is good, nontoxic and pollution-free, the ingredients such as tin oxide, zirconium silicate
Interaction, enhances the adhesiveness of ceramic glaze internal structure, and then enhance the intensity and thermal stability of ceramic glaze, nano oxygen
Changing zinc also has certain anti-microbial property, environment protection health.
Specific implementation mode
Embodiment 1, a kind of ceramic glaze that the high fire resistance of intensity is good, by following weight（kg）Raw material is made：Sepiolite 20,
Borax 6, kaolin 8, china powder 3, waste glass powder 6, tin oxide 2, silica white 2, zirconium silicate 3, limonite 4, dimethyl
Aniline 1, nano zine oxide 2, barium carbonate 3, cobalt sesquioxide 1, fruit tree ash 3, dimethylbenzene 8.
A kind of preparation method of the good ceramic glaze of high fire resistance of intensity, includes the following steps：
（1）Each raw material is weighed by weight；
（2）By the sepiolite after weighing, borax, kaolin, china powder, waste glass powder, tin oxide, silica white, zirconium silicate
Superfine powder, limonite, dimethylaniline, nano zine oxide, barium carbonate, cobalt sesquioxide, fruit tree ash, dimethylbenzene are sufficiently mixed simultaneously
It stirs evenly；
（3）By step（2）In mixed raw material be calcined 2 times at a high temperature of 1120 DEG C；
（4）Raw material after calcining is taken out and put into ball milling and is ground, the glaze that fineness is 325 mesh is ground to
Slurry, a concentration of 40 degree of glaze slip；
（5）Glaze slip is uniformly imposed on ceramic body, enters kiln oxidizing flame or reducing flame and fires, can be burnt at 1250 DEG C of temperature
At ceramic product.
Embodiment 2, a kind of ceramic glaze that the high fire resistance of intensity is good, by following weight（kg）Raw material is made：Sepiolite 25,
Borax 7, kaolin 9, china powder 4, waste glass powder 7, tin oxide 3, silica white 3, zirconium silicate 4, limonite 5, dimethyl
Aniline 2, nano zine oxide 3, barium carbonate 4, cobalt sesquioxide 2, fruit tree ash 4, dimethylbenzene 10.
A kind of preparation method of the good ceramic glaze of high fire resistance of intensity, includes the following steps：
（1）Each raw material is weighed by weight；
（2）By the sepiolite after weighing, borax, kaolin, china powder, waste glass powder, tin oxide, silica white, zirconium silicate
Superfine powder, limonite, dimethylaniline, nano zine oxide, barium carbonate, cobalt sesquioxide, fruit tree ash, dimethylbenzene are sufficiently mixed simultaneously
It stirs evenly；
（3）By step（2）In mixed raw material be calcined 3 times at a high temperature of 1170 DEG C；
（4）Raw material after calcining is taken out and put into ball milling and is ground, the glaze that fineness is 400 mesh is ground to
Slurry, a concentration of 40 degree of glaze slip；
（5）Glaze slip is uniformly imposed on ceramic body, enters kiln oxidizing flame or reducing flame and fires, can be burnt at 1300 DEG C of temperature
At ceramic product.
Embodiment 3, a kind of ceramic glaze that the high fire resistance of intensity is good, by following parts by weight（kg）Raw material is made：Sepiolite
30, borax 8, kaolin 10, china powder 5, waste glass powder 8, tin oxide 4, silica white 4, zirconium silicate 5, limonite 6, two
Methylaniline 3, nano zine oxide 4, barium carbonate 5, cobalt sesquioxide 3, fruit tree ash 5, dimethylbenzene 12.
A kind of preparation method of the good ceramic glaze of high fire resistance of intensity, includes the following steps：
（1）Each raw material is weighed by weight；
（2）By the sepiolite after weighing, borax, kaolin, china powder, waste glass powder, tin oxide, silica white, zirconium silicate
Superfine powder, limonite, dimethylaniline, nano zine oxide, barium carbonate, cobalt sesquioxide, fruit tree ash, dimethylbenzene are sufficiently mixed simultaneously
It stirs evenly；
（3）By step（2）In mixed raw material be calcined 4 times at a high temperature of 1210 DEG C；
（4）Raw material after calcining is taken out and put into ball milling and is ground, the glaze that fineness is 500 mesh is ground to
Slurry, a concentration of 40 degree of glaze slip；
（5）Glaze slip is uniformly imposed on ceramic body, enters kiln oxidizing flame or reducing flame and fires, can be burnt at 1350 DEG C of temperature
At ceramic product.
The main performance testing result of ceramic glaze made from above-described embodiment 1-3 is as follows：
The main performance testing result of ceramic glaze made from 1 embodiment 1-3 of table
| Serial number | Mohs' hardness | Water absorption rate | Glaze quality |
| Embodiment 1 | 7 | 1.96 | It is good |
| Embodiment 2 | 8 | 1.94 | It is good |
| Embodiment 3 | 7 | 1.97 | It is good |
Claims (2)
1. a kind of ceramic glaze that the high fire resistance of intensity is good, it is characterised in that：It is made of following raw material：Sepiolite 20-
30, borax 6-8, kaolin 8-10, china powder 3-5, waste glass powder 6-8, tin oxide 2-4, silica white 2-4, zirconium silicate
3-5, limonite 4-6, dimethylaniline 1-3, nano zine oxide 2-4, barium carbonate 3-5, cobalt sesquioxide 1-3, fruit tree ash 3-5,
Dimethylbenzene 8-12.
2. a kind of preparation method of the good ceramic glaze of the high fire resistance of intensity according to claim 1, it is characterised in that：Packet
Include following steps：
（1）Each raw material is weighed by weight；
（2）Sepiolite after weighing, borax, kaolin, china powder, waste glass powder, tin oxide, silica white, zirconium silicate is ultra-fine
Powder, limonite, dimethylaniline, nano zine oxide, barium carbonate, cobalt sesquioxide, fruit tree ash, dimethylbenzene are sufficiently mixed and stir
Uniformly；
（3）By step（2）In mixed raw material be calcined 2-4 times at a high temperature of 1120-1210 DEG C；
（4）Raw material after calcining is taken out and put into ball milling and is ground, the glaze that fineness is 325-500 mesh is ground to
Slurry, a concentration of 40 degree of glaze slip；
（5）Glaze slip is uniformly imposed on ceramic body, enters kiln oxidizing flame or reducing flame and fires, it can at 1250-1350 DEG C of temperature
Low fire ceramic finished product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610208751.1A CN105859138B (en) | 2016-04-06 | 2016-04-06 | A kind of ceramic glaze and preparation method thereof that the high fire resistance of intensity is good |
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|---|---|---|---|
| CN201610208751.1A CN105859138B (en) | 2016-04-06 | 2016-04-06 | A kind of ceramic glaze and preparation method thereof that the high fire resistance of intensity is good |
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| CN105859138A CN105859138A (en) | 2016-08-17 |
| CN105859138B true CN105859138B (en) | 2018-08-31 |
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| CN106316125B (en) * | 2016-08-23 | 2019-04-09 | 无锡太湖学院 | A kind of Environmental-friendceramic ceramic glaze and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103408328A (en) * | 2013-07-31 | 2013-11-27 | 蔡焕宜 | Ceramic glaze and preparation method thereof |
| CN103755389A (en) * | 2013-12-23 | 2014-04-30 | 宾阳县明翔新材料科技有限公司 | Glaze material with heat-insulation and heat-preservation functions and preparation method of glaze material |
| CN104140290A (en) * | 2014-07-29 | 2014-11-12 | 青岛乾祥环保技术有限公司 | Novel ceramic glaze |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS616145A (en) * | 1984-06-18 | 1986-01-11 | Matsushita Electric Ind Co Ltd | Glaze composition for porcelain enamel having low melting point |
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103408328A (en) * | 2013-07-31 | 2013-11-27 | 蔡焕宜 | Ceramic glaze and preparation method thereof |
| CN103755389A (en) * | 2013-12-23 | 2014-04-30 | 宾阳县明翔新材料科技有限公司 | Glaze material with heat-insulation and heat-preservation functions and preparation method of glaze material |
| CN104140290A (en) * | 2014-07-29 | 2014-11-12 | 青岛乾祥环保技术有限公司 | Novel ceramic glaze |
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| CN105859138A (en) | 2016-08-17 |
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| TA01 | Transfer of patent application right |
Effective date of registration: 20180713 Address after: 521000 F1 block, Ruyi Road Industrial Park, Fengxi District, Chaozhou, Guangdong Applicant after: Weiye Ceramics Co., Ltd. Address before: 325000 fourth, No. 86, Zhonghua Road, Zhongyuan new street, Longwan District, Wenzhou, Zhejiang. Applicant before: WENZHOU RENHE EDUCATION TECHNOLOGY CO., LTD. |
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