CN105859138A - High-strength high-fire-resistance ceramic glaze and preparation method thereof - Google Patents
High-strength high-fire-resistance ceramic glaze and preparation method thereof Download PDFInfo
- Publication number
- CN105859138A CN105859138A CN201610208751.1A CN201610208751A CN105859138A CN 105859138 A CN105859138 A CN 105859138A CN 201610208751 A CN201610208751 A CN 201610208751A CN 105859138 A CN105859138 A CN 105859138A
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- glaze
- ceramic
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- ceramic glaze
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Structural Engineering (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Compositions Of Oxide Ceramics (AREA)
- Glass Compositions (AREA)
Abstract
The invention discloses a high-strength high-fire-resistance ceramic glaze and a preparation method thereof, relating to the technical field of ceramic production. The high-strength high-fire-resistance ceramic glaze is mainly prepared from meerschaum, sodium borate, kaolin, bone china powder, waste glass powder, tin oxide, silica-gel powder, zirconium silicate micropowder, limonite, dimethylaniline, nano zinc oxide, barium carbonate, cobaltic oxide, fruit tree ash and dimethylbenzene. The ceramic glaze has the advantages of high strength, high heat stability, no toxicity and no pollution; the interactions of the tin oxide, zirconium silicate micropowder and other components enhance the adhesion property of the internal structure of the ceramic glaze, thereby enhancing the strength and heat stability of the ceramic glaze; and the nano zinc oxide has certain mold resistance, and thus, is environment-friendly and healthy.
Description
Technical field
The present invention relates to technical field of ceramic production, ceramic glaze that a kind of intensity height fire resistance is good and
Its preparation method.
Background technology
Pottery is to prepare through pulverizing mixing, molding and calcining with natural clay and various natural minerals for primary raw material
The various goods of material.People were referred to as pottery the article of high-temperature firing in special kiln being fabricated to potter's clay in the past
Porcelain, pottery is the general name of pottery and porcelain.The traditional concept of pottery refers to all with Inorganic nonmetal mineral such as clays as raw material
Artificial industrial products.It include by clay or containing the mixture of clay through mixing, shape, calcining and the various systems made
Product.Broadly fall into its scope to the finest fine pottery and porcelain by the most coarse earthenware.Primary raw material for it is to take from
The silicate mineral (such as clay, quartz etc.) of nature, therefore with industry such as glass, cement, enamel, refractory materials, belongs to
The category of " silicate industry ".
Glaze used in ceramic product is the raw material that can not lack during ceramic product produces, along with sending out of ceramic industry
Exhibition, the kind of glaze is more and more rich and varied, and the glaze product that most domestic ceramicses use, classification is numerous with range of use
Many, high temperature glaze and low-temperature glaze can be divided into according to firing temperature, high temperature glaze has its uniqueness in the development of glaze
Place, is an important research direction of ceramic industry all the time to the research of high temperature glaze.
Summary of the invention
The invention aims to provide ceramic glaze that a kind of intensity height fire resistance is good and preparation method thereof.
It is an object of the invention to be achieved through the following technical solutions:
The ceramic glaze that a kind of intensity height fire resistance is good, is made up of following raw material: meerschaum 20-30, Borax 6-8, height
Ridge soil 8-10, china powder 3-5, waste glass powder 6-8, stannum oxide 2-4, silica white 2-4, zirconium silicate 3-5, limonite 4-6,
Dimethylaniline 1-3, nano zine oxide 2-4, brium carbonate 3-5, cobalt sesquioxide 1-3, fruit tree ash 3-5, dimethylbenzene 8-12.
The preparation method of the ceramic glaze that a kind of intensity height fire resistance is good, comprises the following steps:
(1) each raw material is weighed by weight；
(2) meerschaum after weighing, Borax, Kaolin, china powder, waste glass powder, stannum oxide, silica white, Zirconium orthosilicate. are ultra-fine
Powder, limonite, dimethylaniline, nano zine oxide, brium carbonate, cobalt sesquioxide, fruit tree ash, dimethylbenzene are sufficiently mixed and stir
Uniformly；
(3) mixed raw material in step (2) is calcined 2-4 time under the high temperature of 1120-1210 DEG C；
(4) raw material after calcining takes out and puts in ball milling and is ground, and is ground to the glaze that fineness is 325-500 mesh
Slurry, the concentration of its glaze slip is 40 degree；
(5) glaze slip is uniformly imposed on ceramic body, enter kiln oxidizing flame or reducing flame is fired, can at temperature 1250-1350 DEG C
Low fire ceramic finished product.
It is an advantage of the current invention that:
The ceramic glaze intensity of the present invention is high, and Heat stability is good, nontoxic pollution-free, the composition such as stannum oxide, zirconium silicate is mutual
Effect, enhances the adhesiveness of ceramic glaze internal structure, and then enhances intensity and the heat stability of ceramic glaze, nano zine oxide
Also there is certain anti-microbial property, environment protection health.
Detailed description of the invention
Embodiment 1, the ceramic glaze that a kind of intensity height fire resistance is good, it is made up of following weight (kg) raw material: meerschaum 20,
Borax 6, Kaolin 8, china powder 3, waste glass powder 6, stannum oxide 2, silica white 2, zirconium silicate 3, limonite 4, dimethyl
Aniline 1, nano zine oxide 2, brium carbonate 3, cobalt sesquioxide 1, fruit tree ash 3, dimethylbenzene 8.
The preparation method of the ceramic glaze that a kind of intensity height fire resistance is good, comprises the following steps:
(1) each raw material is weighed by weight；
(2) meerschaum after weighing, Borax, Kaolin, china powder, waste glass powder, stannum oxide, silica white, Zirconium orthosilicate. are ultra-fine
Powder, limonite, dimethylaniline, nano zine oxide, brium carbonate, cobalt sesquioxide, fruit tree ash, dimethylbenzene are sufficiently mixed and stir
Uniformly；
(3) mixed raw material in step (2) is calcined 2 times under the high temperature of 1120 DEG C；
(4) raw material after calcining takes out and puts in ball milling and is ground, and is ground to the glaze slip that fineness is 325 mesh, its
The concentration of glaze slip is 40 degree；
(5) glaze slip is uniformly imposed on ceramic body, enter kiln oxidizing flame or reducing flame is fired, pottery can be burnt till at temperature 1250 DEG C
Porcelain finished product.
Embodiment 2, the ceramic glaze that a kind of intensity height fire resistance is good, it is made up of following weight (kg) raw material: meerschaum 25,
Borax 7, Kaolin 9, china powder 4, waste glass powder 7, stannum oxide 3, silica white 3, zirconium silicate 4, limonite 5, dimethyl
Aniline 2, nano zine oxide 3, brium carbonate 4, cobalt sesquioxide 2, fruit tree ash 4, dimethylbenzene 10.
The preparation method of the ceramic glaze that a kind of intensity height fire resistance is good, comprises the following steps:
(1) each raw material is weighed by weight；
(2) meerschaum after weighing, Borax, Kaolin, china powder, waste glass powder, stannum oxide, silica white, Zirconium orthosilicate. are ultra-fine
Powder, limonite, dimethylaniline, nano zine oxide, brium carbonate, cobalt sesquioxide, fruit tree ash, dimethylbenzene are sufficiently mixed and stir
Uniformly；
(3) mixed raw material in step (2) is calcined 3 times under the high temperature of 1170 DEG C；
(4) raw material after calcining takes out and puts in ball milling and is ground, and is ground to the glaze slip that fineness is 400 mesh, its
The concentration of glaze slip is 40 degree；
(5) glaze slip is uniformly imposed on ceramic body, enter kiln oxidizing flame or reducing flame is fired, pottery can be burnt till at temperature 1300 DEG C
Porcelain finished product.
Embodiment 3, the ceramic glaze that a kind of intensity height fire resistance is good, it is made up of following weight portion (kg) raw material: meerschaum
30, Borax 8, Kaolin 10, china powder 5, waste glass powder 8, stannum oxide 4, silica white 4, zirconium silicate 5, limonite 6, two
Monomethylaniline. 3, nano zine oxide 4, brium carbonate 5, cobalt sesquioxide 3, fruit tree ash 5, dimethylbenzene 12.
The preparation method of the ceramic glaze that a kind of intensity height fire resistance is good, comprises the following steps:
(1) each raw material is weighed by weight；
(2) meerschaum after weighing, Borax, Kaolin, china powder, waste glass powder, stannum oxide, silica white, Zirconium orthosilicate. are ultra-fine
Powder, limonite, dimethylaniline, nano zine oxide, brium carbonate, cobalt sesquioxide, fruit tree ash, dimethylbenzene are sufficiently mixed and stir
Uniformly；
(3) mixed raw material in step (2) is calcined 4 times under the high temperature of 1210 DEG C；
(4) raw material after calcining takes out and puts in ball milling and is ground, and is ground to the glaze slip that fineness is 500 mesh, its
The concentration of glaze slip is 40 degree；
(5) glaze slip is uniformly imposed on ceramic body, enter kiln oxidizing flame or reducing flame is fired, pottery can be burnt till at temperature 1350 DEG C
Porcelain finished product.
The main performance testing result of the ceramic glaze that above-described embodiment 1-3 prepares is as follows:
The main performance testing result of the ceramic glaze that table 1 embodiment 1-3 prepares
| Sequence number | Mohs' hardness | Water absorption rate | Glaze quality |
| Embodiment 1 | 7 | 1.96 | Good |
| Embodiment 2 | 8 | 1.94 | Good |
| Embodiment 3 | 7 | 1.97 | Good |
Claims (2)
1. the ceramic glaze that an intensity height fire resistance is good, it is characterised in that: it is made up of following raw material: meerschaum 20-
30, Borax 6-8, Kaolin 8-10, china powder 3-5, waste glass powder 6-8, stannum oxide 2-4, silica white 2-4, zirconium silicate
3-5, limonite 4-6, dimethylaniline 1-3, nano zine oxide 2-4, brium carbonate 3-5, cobalt sesquioxide 1-3, fruit tree ash 3-5,
Dimethylbenzene 8-12.
The preparation method of the ceramic glaze that a kind of intensity height fire resistance the most according to claim 1 is good, it is characterised in that: bag
Include following steps:
(1) each raw material is weighed by weight；
(2) meerschaum after weighing, Borax, Kaolin, china powder, waste glass powder, stannum oxide, silica white, Zirconium orthosilicate. are ultra-fine
Powder, limonite, dimethylaniline, nano zine oxide, brium carbonate, cobalt sesquioxide, fruit tree ash, dimethylbenzene are sufficiently mixed and stir
Uniformly；
(3) mixed raw material in step (2) is calcined 2-4 time under the high temperature of 1120-1210 DEG C；
(4) raw material after calcining takes out and puts in ball milling and is ground, and is ground to the glaze that fineness is 325-500 mesh
Slurry, the concentration of its glaze slip is 40 degree；
(5) glaze slip is uniformly imposed on ceramic body, enter kiln oxidizing flame or reducing flame is fired, can at temperature 1250-1350 DEG C
Low fire ceramic finished product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610208751.1A CN105859138B (en) | 2016-04-06 | 2016-04-06 | A kind of ceramic glaze and preparation method thereof that the high fire resistance of intensity is good |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610208751.1A CN105859138B (en) | 2016-04-06 | 2016-04-06 | A kind of ceramic glaze and preparation method thereof that the high fire resistance of intensity is good |
Publications (2)
| Publication Number | Publication Date |
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| CN105859138A true CN105859138A (en) | 2016-08-17 |
| CN105859138B CN105859138B (en) | 2018-08-31 |
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| Application Number | Title | Priority Date | Filing Date |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106316125A (en) * | 2016-08-23 | 2017-01-11 | 宜兴市方卫明均陶艺术研究所 | Environment-friendly ceramic glaze material and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS616145A (en) * | 1984-06-18 | 1986-01-11 | Matsushita Electric Ind Co Ltd | Glaze composition for porcelain enamel having low melting point |
| CN103408328A (en) * | 2013-07-31 | 2013-11-27 | 蔡焕宜 | Ceramic glaze and preparation method thereof |
| CN103755389A (en) * | 2013-12-23 | 2014-04-30 | 宾阳县明翔新材料科技有限公司 | Glaze material with heat-insulation and heat-preservation functions and preparation method of glaze material |
| CN104140290A (en) * | 2014-07-29 | 2014-11-12 | 青岛乾祥环保技术有限公司 | Novel ceramic glaze |
-
2016
- 2016-04-06 CN CN201610208751.1A patent/CN105859138B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS616145A (en) * | 1984-06-18 | 1986-01-11 | Matsushita Electric Ind Co Ltd | Glaze composition for porcelain enamel having low melting point |
| CN103408328A (en) * | 2013-07-31 | 2013-11-27 | 蔡焕宜 | Ceramic glaze and preparation method thereof |
| CN103755389A (en) * | 2013-12-23 | 2014-04-30 | 宾阳县明翔新材料科技有限公司 | Glaze material with heat-insulation and heat-preservation functions and preparation method of glaze material |
| CN104140290A (en) * | 2014-07-29 | 2014-11-12 | 青岛乾祥环保技术有限公司 | Novel ceramic glaze |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106316125A (en) * | 2016-08-23 | 2017-01-11 | 宜兴市方卫明均陶艺术研究所 | Environment-friendly ceramic glaze material and preparation method thereof |
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| CN105859138B (en) | 2018-08-31 |
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Effective date of registration: 20180713 Address after: 521000 F1 block, Ruyi Road Industrial Park, Fengxi District, Chaozhou, Guangdong Applicant after: Weiye Ceramics Co., Ltd. Address before: 325000 fourth, No. 86, Zhonghua Road, Zhongyuan new street, Longwan District, Wenzhou, Zhejiang. Applicant before: WENZHOU RENHE EDUCATION TECHNOLOGY CO., LTD. |
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