CN105820692A - Sand wall like coating containing water-based dyeing colored sand and preparation method of sand wall like coating - Google Patents
Sand wall like coating containing water-based dyeing colored sand and preparation method of sand wall like coating Download PDFInfo
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- CN105820692A CN105820692A CN201610365107.5A CN201610365107A CN105820692A CN 105820692 A CN105820692 A CN 105820692A CN 201610365107 A CN201610365107 A CN 201610365107A CN 105820692 A CN105820692 A CN 105820692A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D143/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and containing boron, silicon, phosphorus, selenium, tellurium, or a metal; Coating compositions based on derivatives of such polymers
- C09D143/04—Homopolymers or copolymers of monomers containing silicon
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/28—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes for wrinkle, crackle, orange-peel, or similar decorative effects
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
- C09D7/62—Additives non-macromolecular inorganic modified by treatment with other compounds
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
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- Engineering & Computer Science (AREA)
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Abstract
The invention discloses sand wall like coating containing water-based dyeing colored sand and a preparation method of the sand wall like coating .At present, a method for obtaining water-based dyeing colored sand by dyeing quartz sand with a dyeing agent prepared by compounding water glass and resin emulsion is provided; because the method is too complex and not controllable in operation when curing is conducted through condensed phosphoric acid, the final product is not stable enough and neither environmentally friendly .The sand wall like coating is prepared from, by mass, 260-320 parts of base slurry and 680-740 parts of water-based dyeing colored sand .The water-based dyeing colored sand is prepared from, by mass, 1000 parts of broken stone material and 120 parts of water-based composite dyeing agent, wherein the broken stone material is quartz sand .By means of the water-based dyeing colored sand, the production time of the sand wall like coating is shortened, production efficiency is improved, and production cost is reduced.
Description
Technical field
The present invention relates to building coating field, a kind of sand textured coating comprising water dyeing coloured silk sand and
Preparation method.
Background technology
Sand textured building coating is mainly made up of natural colour sand and acrylic emulsion, is that a kind of decorative effect exactly likes Dali
Stone, the coating of granite, be applied to the imitative stone effect of external wall, also referred to as stone similar paint.Building after fitting up with it, has
Natural real natural colour, gives elegance, harmony, serious aesthetic feeling, is suitable for the indoor and outdoor decoration of all kinds of building.Special
It not to decorate on curved-surface building thing, vivid, there is the effect of a kind of back to nature.Sand textured building coating have fire prevention,
Waterproof, acid and alkali-resistance, anti-pollution, nontoxic, tasteless, bonding force is strong, the feature such as will never fade, can effectively stop extraneous adverse circumstances
Building is corroded, extends the life-span of building, so commercially must be in substantial amounts of promotion and application.Sand textured building coating
Main performance depend on performance and the stability of color sand of acrylic emulsion, the performance of color sand determines the property of sand textured coating
Can, stablizing of color sand color determines the time that sand textured coating production is mixed colours, and affects the production efficiency of sand textured coating.
Color sand is owing to there being the advantage such as chromatic colour, stable performance to be largely used in stone similar paint.The color of color sand is steady
Whether determine to determine the production efficiency of sand textured coating.Color sand, as stone similar paint main material, is generally divided into natural colour sand and people
Two kinds of work coloured silk sand.From over 2000, along with the rise of sand textured building coating, the resource of natural colour sand is the most exhausted, color sand
Color is uneven, brings the biggest difficulty to production toning, and the toning time is long, and effect is low.And 2012 start, as natural
The northern areas such as the Hebei, the main place of production of color sand are affected by haze, and state compulsion closes the exploitation of most of color sand resource,
Cause coating industry coloured silk sand inadequate supply.The biggest obstacle that stone similar paint is developed by the scarcity of color sand resource beyond doubt.So, state
Interior sand textured coating manufacturer turns one's attention to artificial color sand.
Artificial color sand uses the nature resource raw material such as quartz sand, calcite widely, by different technological means,
Sand surface coloring film forming, makes transparent quartz sand possess different colors, thus makes colour stable, coloury sand wall
Shape coating.
Current artificially colored color sand mainly has: one, dyeing sand, number of patent application CN2015102155641 discloses use
Acroleic acid polyurethane, as film-forming binder, adds mill base coloring, wraps up quartz sand, finally dries and obtain.This mode compares
Simply, speed is fast, but the combination property such as water-fast, chemical-resistance and adhesive force is poor.Simultaneously as film former is at quartz sand
Surface parcel coloring, it is impossible to penetrate into sand nexine, is in use easy to when stirring decolour because of phase mutual friction.And
And, due to coloring agent is oleoresin, and the compatibility in aqueous sand textured coating exists the biggest risk hidden danger.Two,
Burning colorful sand, number of patent application CN2014104129789 discloses a kind of with quartz sand as raw material, adds high temperature resistant inorganic pigment
With low-temp ceramics glaze as binding agent, obtain through the high temperature sintering of 500-1100 DEG C, by stirring, preheat, calcine and cooling down
Four-stage forms, gained coloured silk sand stable performance, but power consumption is higher, and coloring agent used is inorganic ceramic binding agent, parcel
Thin and crisp film is formed on quartz sand top layer.Color is affected relatively big by calcining problem, less stable.Three, water dyeing is color
Sand, number of patent application CN2015103950049 discloses a kind of stain compound with waterglass and resin emulsion, by this dyeing
Agent contaminates quartz sand and the method for the color sand that must dye, but owing to the method is the most complicated, when solidifying with condensation of aluminum phosphate, operation is not
Controlled, thus bring final products to be not sufficiently stable, the most not environmentally.
Summary of the invention
The technical problem to be solved is the deficiency overcoming prior art to exist, it is provided that a kind of anti-wear performance is good,
Hydrophilic is strong and the water-base resin compatibility is good, color even is stable, good weatherability, can need, according to color, the sand that carries out producing
Textured coating, the water dyeing coloured silk sand that it uses solves and wears no resistance, good, only with the film former compatibility in sand textured coating
After needing room temperature, cold drying just can meet performance requirement.More hydrophilic with its sand textured coating prepared, with this artificial color sand
Having the higher compatibility, higher imitative stone effect and higher weatherability stain resistance, the color sand color of dyeing simultaneously is more steady
Fixed, the production toning time can be shortened, improve effect.
For solving above-mentioned technical problem, the technical solution used in the present invention is as follows: a kind of sand comprising water dyeing coloured silk sand
Textured coating, it includes the raw material components of following mass fraction:
Base paste 260-320 part,
Water dyeing coloured silk sand 680-740 part；
Described water dyeing coloured silk sand includes the raw material components of following mass fraction:
Rubble building stones 1000 parts,
Aqueous complex staining agent 120 parts；
Wherein, described rubble building stones are quartz sand, and aqueous complex staining agent includes the raw material components of following mass fraction:
The water dyeing coloured silk sand anti-wear performance that the present invention uses is good, and hydrophilic is strong, and good with the water-base resin compatibility, color is equal
Even stable, good weatherability, can need to produce according to color.This water dyeing coloured silk sand solves the problem worn no resistance, with
The film former compatibility in sand textured coating is good, it is only necessary to room temperature or cold drying just can meet performance requirement, the sand prepared with it
Textured coating is more hydrophilic, and the color sand color of dyeing simultaneously is more stable, can shorten the production toning time, improves effect.
Further, described Ludox is preferably modulus 3.0, SiO2Content is at the neutral Ludox of 25-30%, pH regulator
Agent is preferably AMP95, and silane coupler is preferably KH550.
Further, described base paste includes the raw material components of following mass fraction:
The preparation method of base paste is: added by the soft water of formula ratio in reactor, the speed of 700-900 rev/min
Put into cellulose under degree, disperse 10-15 minute；
Biocide mildewcide, propylene glycol, coalescents, pH adjusting agent it is sequentially added under the speed of 700-900 rev/min,
Disperseing 10-15 minute, add silicone acrylic emulsion under 400-500 rev/min, stir prepared base paste.
Further, described cellulose is preferably hydroxyethyl cellulose.
Further, described coalescents be preferably the one in Lauryl Alcohol ester, butyl glycol ether, propandiol butyl ether or
Several.
Further, described pH adjusting agent is preferably AMP95.
Further, described silicone acrylic emulsion is preferably 996AD, and described biocide mildewcide is preferably WL-3.
Further, one during the particle diameter of described rubble building stones is 10-20 mesh, 20-40 mesh, 40-80 mesh, 80-120 mesh or
Multiple.
The preparation method of above-mentioned sand textured coating, its step is as follows: is added by base paste in reactor, starts stirring,
Under the mixing speed of 100-200 rev/min, put into water dyeing coloured silk sand, control to put into speed, finished at 10-30 minute, anti-
Only dyeing color sand caking, continues stirring and obtains sand textured coating in 20-30 minute after adding；
The preparation method of described water dyeing coloured silk sand is:
A. the quartz sand of 10-20 mesh, 20-40 mesh, 40-80 mesh and 80-120 mesh is put into stirring in the ratio of 1:1:1:1
In device, under the rotating speed of 80-120 rev/min, spray into aqueous complex staining agent, stirring 5-10 minute after having sprayed；
B. the compound that step A obtains is poured into rotary drying machine, controls temperature 50-100 DEG C of drying；
C. drying material step B obtained obtains different by 10-20 mesh, 20-40 mesh, 40-80 mesh, the 80 above sieve classifications of mesh
The water dyeing coloured silk sand of particle diameter.
Further, the preparation method of aqueous complex staining agent is:
1) VAE emulsion procedure of pH adjustment: VAE emulsion is added in soft water, under the speed conditions of 400-500 rev/min
Stir 5-10 minute；Under 400-500 rev/min of stirring condition, it is slowly added dropwise pH adjusting agent the most again, surveys with wide pH value reagent paper
When examination mixed liquor pH value is 8.5-9.5 only；
2) Ludox step is added: to step 1 under 500-600 rev/min of stirring condition) solution that obtains slowly adds
Enter Ludox, aqueous color paste and titanium dioxide slurry to stir 10-15 minute；
3) silane coupler step is added: to step 2 under 800-1000 rev/min of stirring condition) in the solution that obtains
It is slowly added to silane coupler, stirs 15-20 minute, prepare aqueous complex staining agent.
The device have the advantages that as follows: water dyeing coloured silk sand, solve natural colour sand scarcity of resources and color not
Stable problem, thus enrich the color of sand textured coating, shorten the production time of sand textured coating simultaneously, improve life
Produce efficiency, reduce production cost；Sand textured coating, has good hydrophilic, and stain resistance is excellent, resistance to water, weatherability
Excellent.
Detailed description of the invention
The present invention is described in further detail by example below.
Embodiment 1
A kind of water dyeing coloured silk sand, composition of raw materials aqueous complex staining agent: quartz sand is 120:1000 (mass ratio).
The preparation process of described water dyeing coloured silk sand is:
A. by 10-20 mesh, 20-40 mesh, 40-80 mesh, the quartz sand of 80-120 mesh puts into agitator in the ratio of 1:1:1:1
In, under the rotating speed of 100 revs/min, spray into the aqueous complex staining agent of formula ratio, stirring 10 minutes after having sprayed.
B. the above-mentioned compound stirred is poured into rotary drying machine, controls temperature and dry 20 minutes at 80 DEG C.
C. drying material being pressed 10-20 mesh, 20-40 mesh, 40-80 mesh, the 80 above sieve classifications of mesh obtain the aqueous of different-grain diameter
The color sand of dyeing.
The composition of raw materials of aqueous complex staining agent is (mass fraction):
The preparation process of complex staining agent is:
1) VAE emulsion procedure of pH adjustment, adds in (252KG) water by the VAE emulsion (230KG) of metering, at 400 revs/min
Stir 5 minutes under the speed conditions of clock；Under 400 revs/min of stirring conditions, it is slowly added dropwise pH adjusting agent (1KG), uses wide pH value
Reagent paper test mixing liquid pH value is 9.0；
2) add Ludox step, under 500-rev/min of stirring condition, in above-mentioned solution, be slowly added to (500KG) silicon
Colloidal sol, mill base (50KG) and titanium dioxide slurry (5KG) stir 15 minutes；
3) add coupling agent step, under 800 revs/min of stirring conditions, be slowly added to (12KG) silane coupler, stirring
15 minutes, prepare aqueous complex staining agent.
The water dyeing coloured silk sand detection performance that the present invention prepares is as follows:
| Detection project | Technology requirement | Testing result |
| Resistance to water (168h) | Water is without muddiness, without variable color | Without muddy, without variable color |
| Boiling water resistance (20min) | Water is without the most muddy and variable color, and sand grains is without conglomeration | Unchanged, without conglomeration |
| Alkali resistance (24h) | Solution is without muddiness, without variable color | Pass through |
| Solvent resistance (24h) | Solution is without muddiness, without variable color | Pass through |
| Ultraviolet resistance is according to (168h) | Without efflorescence, without obvious variable color | Pass through |
| Mechanical stability | Without obvious variable color | Without variable color |
| Tarnish resistance | Rustless pitting | Rustless pitting |
Embodiment 2
The composition of raw materials of sand textured building coating is following (mass fraction):
The preparation process of described sand textured building coating is:
(260KG) base paste is added in reactor, starts stirring, put into each under the mixing speed of 100 revs/min
Water dyeing coloured silk sand (740KG), controls to put into speed, finished at 30 minutes, prevents the color sand caking that dyes, continues stirring after adding
Within 30 minutes, obtain sand textured coating.
Wherein base paste composition of raw materials:
The preparation process of base paste is:
A. 88.5KG soft water is added in reactor, under the speed of 700 revs/min, puts into cellulose HBR250 (2KG),
Disperse 15 minutes.
B. under the speed of 700 revs/min, it is sequentially added into biocide mildewcide (WL-3), propylene glycol, coalescents, pH regulator
Agent, disperses 10 minutes, adds silicone acrylic emulsion (996AD) and stir prepared base paste under 500 revs/min.
The sand textured building coating detection performance that the present invention prepares is as follows:
Embodiment 3
The formula material of sand textured building coating is following (mass fraction):
The preparation process of described sand textured building coating is as follows:
(320KG) base paste is added in reactor, starts stirring and put into each under the mixing speed of 100 revs/min
Water dyeing coloured silk sand (680KG), controls to put into speed, finished at 30 minutes, prevents the color sand caking that dyes.Stirring is continued after adding
Within 30 minutes, obtain sand textured coating.
Wherein base paste composition of raw materials:
The preparation process of base paste is:
A. 73KG soft water is added in reactor, under the speed of 700 revs/min, put into cellulose HBR250 (3KG), point
Dissipate 15 minutes.
B. under the speed of 700 revs/min, it is sequentially added into biocide mildewcide (WL-3), propylene glycol, coalescents, pH regulator
Agent, disperses 10 minutes, adds silicone acrylic emulsion (996AD) and stir prepared base paste under 500 revs/min.
The sand textured building coating detection performance that the present invention prepares is as follows:
Above-mentioned detailed description of the invention is used for illustrating the present invention rather than limiting the invention, the present invention's
In spirit and scope of the claims, any modifications and changes that the present invention is made, both fall within the protection model of the present invention
Enclose.
Claims (10)
1. comprising a sand textured coating for water dyeing coloured silk sand, it includes the raw material components of following mass fraction:
Base paste 260-320 part,
Water dyeing coloured silk sand 680-740 part；
Described water dyeing coloured silk sand includes the raw material components of following mass fraction:
Rubble building stones 1000 parts,
Aqueous complex staining agent 120 parts；
Wherein, described rubble building stones are quartz sand, and aqueous complex staining agent includes the raw material components of following mass fraction:
Sand textured coating the most according to claim 1, it is characterised in that described Ludox is modulus 3.0, SiO2Content
At the neutral Ludox of 25-30%, pH adjusting agent is AMP95, and silane coupler is KH550.
Sand textured coating the most according to claim 1 and 2, it is characterised in that described base paste includes following quality
The raw material components of number:
Sand textured coating the most according to claim 3, it is characterised in that described cellulose is hydroxyethyl cellulose.
Sand textured coating the most according to claim 3, it is characterised in that described coalescents is Lauryl Alcohol ester, second
One or more in glycol butyl ether, propandiol butyl ether.
Sand textured coating the most according to claim 3, it is characterised in that described pH adjusting agent is AMP95.
Sand textured coating the most according to claim 3, it is characterised in that described silicone acrylic emulsion is 996AD, described kills
Bacterium antifungus agent is WL-3.
Sand textured coating the most according to claim 1 and 2, it is characterised in that the particle diameter of described rubble building stones is 10-20
One or more in mesh, 20-40 mesh, 40-80 mesh, 80-120 mesh.
9. the preparation method of sand textured coating described in any one of claim 1-8, its step is as follows: base paste is added reaction
In still, start stirring, under the mixing speed of 100-200 rev/min, put into water dyeing coloured silk sand, control to put into speed, at 10-
Within 30 minutes, finish, prevent the color sand caking that dyes, continue stirring after adding and obtain sand textured coating in 20-30 minute；
The preparation method of described water dyeing coloured silk sand is:
A. the quartz sand of 10-20 mesh, 20-40 mesh, 40-80 mesh and 80-120 mesh is put in agitator in the ratio of 1:1:1:1,
Aqueous complex staining agent is sprayed into, stirring 5-10 minute after having sprayed under the rotating speed of 80-120 rev/min；
B. the compound that step A obtains is poured into rotary drying machine, controls temperature 50-100 DEG C of drying；
C. drying material step B obtained obtains different-grain diameter by 10-20 mesh, 20-40 mesh, 40-80 mesh, the 80 above sieve classifications of mesh
Water dyeing coloured silk sand.
Preparation method the most according to claim 9, it is characterised in that the preparation method of aqueous complex staining agent is:
1) VAE emulsion procedure of pH adjustment: VAE emulsion is added in soft water, stir under the speed conditions of 400-500 rev/min
5-10 minute；It is slowly added dropwise pH adjusting agent the most again under 400-500 rev/min of stirring condition, mixed with the test of wide pH value reagent paper
Close when liquid pH value is 8.5-9.5 and stop；
2) Ludox step is added: to step 1 under 500-600 rev/min of stirring condition) solution that obtains is slowly added to silicon
Colloidal sol, aqueous color paste and titanium dioxide slurry stir 10-15 minute；
3) add silane coupler step: to step 2 under 800-1000 rev/min of stirring condition) in the solution that obtains slowly
Add silane coupler, stir 15-20 minute, prepare aqueous complex staining agent.
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| CN201610365107.5A CN105820692B (en) | 2016-05-27 | 2016-05-27 | A kind of sand textured coating and preparation method thereof comprising water dyeing color sand |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106978081A (en) * | 2017-03-29 | 2017-07-25 | 湖北武大珞珈工程结构检测咨询有限公司 | A kind of sintered quartz sand sand textured coating |
| CN107353747A (en) * | 2017-06-22 | 2017-11-17 | 河北晨阳工贸集团有限公司 | A kind of imitation wood line texture sand textured coating and preparation method thereof |
| CN107721223A (en) * | 2017-11-14 | 2018-02-23 | 山西亮龙涂料有限公司 | A kind of aqueous, environmental protective coloured silk sand and its preparation technology |
| CN108298852A (en) * | 2016-09-30 | 2018-07-20 | 立邦涂料（中国）有限公司 | Aqueous color sand made from the aqueous dye sand method of one kind and use the method |
| CN108840604A (en) * | 2018-06-29 | 2018-11-20 | 河南颂源涂料有限公司 | A kind of artificial color sand and preparation method thereof |
| CN110104991A (en) * | 2019-04-30 | 2019-08-09 | 浙江志强涂料有限公司 | A kind of heat preservation sand textured coating and preparation method thereof |
| CN113004757A (en) * | 2021-04-06 | 2021-06-22 | 陈素平 | Dyed sand slurry, artificial colored sand and preparation method |
| CN113527923A (en) * | 2021-08-11 | 2021-10-22 | 广东美涂士建材股份有限公司 | Color stone paint for building external wall |
| CN115093728A (en) * | 2022-07-11 | 2022-09-23 | 浙江华德新材料有限公司 | Inorganic real stone paint and preparation method thereof |
| CN115895307A (en) * | 2022-12-12 | 2023-04-04 | 成都迪泰化工有限公司 | Sand-wall-shaped pure-color-texture natural stone coating and preparation method thereof |
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