CN105801225B - It is exclusively used in the agricultural composite fertilizer containing Chinese medicine dreg of soybean - Google Patents
It is exclusively used in the agricultural composite fertilizer containing Chinese medicine dreg of soybean Download PDFInfo
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- CN105801225B CN105801225B CN201610114208.5A CN201610114208A CN105801225B CN 105801225 B CN105801225 B CN 105801225B CN 201610114208 A CN201610114208 A CN 201610114208A CN 105801225 B CN105801225 B CN 105801225B
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- 239000003814 drug Substances 0.000 title claims abstract description 57
- 235000010469 Glycine max Nutrition 0.000 title claims abstract description 33
- 244000068988 Glycine max Species 0.000 title claims abstract description 33
- 239000003337 fertilizer Substances 0.000 title claims abstract description 32
- 239000002131 composite material Substances 0.000 title claims abstract description 23
- 239000005696 Diammonium phosphate Substances 0.000 claims abstract description 24
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 claims abstract description 24
- MNNHAPBLZZVQHP-UHFFFAOYSA-N diammonium hydrogen phosphate Chemical compound [NH4+].[NH4+].OP([O-])([O-])=O MNNHAPBLZZVQHP-UHFFFAOYSA-N 0.000 claims abstract description 24
- 229910000388 diammonium phosphate Inorganic materials 0.000 claims abstract description 24
- 235000019838 diammonium phosphate Nutrition 0.000 claims abstract description 24
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 claims abstract description 24
- 239000007788 liquid Substances 0.000 claims abstract description 18
- 238000002360 preparation method Methods 0.000 claims abstract description 13
- QJZYHAIUNVAGQP-UHFFFAOYSA-N 3-nitrobicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid Chemical compound C1C2C=CC1C(C(=O)O)C2(C(O)=O)[N+]([O-])=O QJZYHAIUNVAGQP-UHFFFAOYSA-N 0.000 claims abstract description 12
- 229910021538 borax Inorganic materials 0.000 claims abstract description 12
- 239000004021 humic acid Substances 0.000 claims abstract description 12
- 235000011164 potassium chloride Nutrition 0.000 claims abstract description 12
- 239000001103 potassium chloride Substances 0.000 claims abstract description 12
- 235000010333 potassium nitrate Nutrition 0.000 claims abstract description 12
- 239000004323 potassium nitrate Substances 0.000 claims abstract description 12
- 235000010339 sodium tetraborate Nutrition 0.000 claims abstract description 12
- 239000004328 sodium tetraborate Substances 0.000 claims abstract description 12
- 238000003756 stirring Methods 0.000 claims abstract description 11
- 238000000034 method Methods 0.000 claims abstract description 8
- 239000002994 raw material Substances 0.000 claims abstract description 8
- 239000012467 final product Substances 0.000 claims abstract description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 23
- 239000000284 extract Substances 0.000 claims description 17
- 235000019441 ethanol Nutrition 0.000 claims description 11
- 238000000605 extraction Methods 0.000 claims description 9
- 241000205407 Polygonum Species 0.000 claims description 5
- 241001135312 Sinorhizobium Species 0.000 claims description 5
- 235000007516 Chrysanthemum Nutrition 0.000 claims description 4
- 244000247747 Coptis groenlandica Species 0.000 claims description 4
- 235000002991 Coptis groenlandica Nutrition 0.000 claims description 4
- 244000025361 Ficus carica Species 0.000 claims description 4
- 235000008730 Ficus carica Nutrition 0.000 claims description 4
- 240000004064 Poterium sanguisorba Species 0.000 claims description 4
- 235000008291 Poterium sanguisorba Nutrition 0.000 claims description 4
- 235000008282 Sanguisorba officinalis Nutrition 0.000 claims description 4
- 229940079593 drug Drugs 0.000 claims description 4
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 4
- 240000004980 Rheum officinale Species 0.000 claims description 3
- 235000008081 Rheum officinale Nutrition 0.000 claims description 3
- 229930006000 Sucrose Natural products 0.000 claims description 3
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims description 3
- 229940041514 candida albicans extract Drugs 0.000 claims description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 3
- 239000002054 inoculum Substances 0.000 claims description 3
- 239000005720 sucrose Substances 0.000 claims description 3
- 239000012138 yeast extract Substances 0.000 claims description 3
- 244000189548 Chrysanthemum x morifolium Species 0.000 claims 1
- 241000589180 Rhizobium Species 0.000 abstract description 6
- 150000001875 compounds Chemical class 0.000 abstract description 5
- 239000000126 substance Substances 0.000 abstract description 4
- 238000002156 mixing Methods 0.000 abstract description 3
- 238000011065 in-situ storage Methods 0.000 abstract 1
- 239000003550 marker Substances 0.000 abstract 1
- 241000196324 Embryophyta Species 0.000 description 9
- 235000008216 herbs Nutrition 0.000 description 6
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- 241000723353 Chrysanthemum Species 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 238000000874 microwave-assisted extraction Methods 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- 206010028980 Neoplasm Diseases 0.000 description 2
- 244000046052 Phaseolus vulgaris Species 0.000 description 2
- 235000010627 Phaseolus vulgaris Nutrition 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 241000124033 Salix Species 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 238000004178 biological nitrogen fixation Methods 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 239000003480 eluent Substances 0.000 description 1
- 238000010828 elution Methods 0.000 description 1
- 210000003608 fece Anatomy 0.000 description 1
- 244000144972 livestock Species 0.000 description 1
- 239000010871 livestock manure Substances 0.000 description 1
- 230000000116 mitigating effect Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000013370 mutualism Effects 0.000 description 1
- 230000024121 nodulation Effects 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 230000024241 parasitism Effects 0.000 description 1
- 239000008188 pellet Substances 0.000 description 1
- 230000000243 photosynthetic effect Effects 0.000 description 1
- 244000144977 poultry Species 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000002893 slag Substances 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000009331 sowing Methods 0.000 description 1
- 235000013555 soy sauce Nutrition 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01C—PLANTING; SOWING; FERTILISING
- A01C21/00—Methods of fertilising, sowing or planting
- A01C21/005—Following a specific plan, e.g. pattern
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Soil Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Environmental Sciences (AREA)
- Fertilizers (AREA)
Abstract
The present invention relates to a kind of agricultural composite fertilizers containing Chinese medicine dreg for being exclusively used in soybean, are made of following raw material according to parts by weight: 1-2 parts of Diammonium phosphate (DAP), 0.5-1 parts of potassium nitrate, 1-3 parts of potassium chloride, 0.5-1 parts of borax, 1-5 parts of humic acid, 1-5 parts of Chinese medicine residue, 0.5-1 parts of root nodule fermented liquid.Preparation after Chinese medicine residue is pulverized with humic acid the method comprise the steps that be uniformly mixed, and then addition root nodule fermented liquid is added Diammonium phosphate (DAP), potassium nitrate, potassium chloride, borax, continues to stir after mixing evenly while stirring, after uniform, air-dries to obtain the final product.The present invention improves the dross vigor and marker technique in situ of rhizobium, can effectively reduce the use of chemical fertilizer, belong to environmentally friendly compound fertilizer, and substantially increase the content of albumen in soybean yields and soybean.
Description
Technical field
The present invention relates to a kind of agricultural composite fertilizers containing Chinese medicine dreg for being exclusively used in soybean, belong to agricultural fertilizer field.
Background technique
With the development of herbal pharmaceutical, solid waste-dregs of a decoction discharge amount is consequently increased, in the prior art to medicine
The processing of slag is mostly to stack, bury or burn, these processing modes not only waste resource, and easily cause the dirt of environment
Dye.
Soybean is a kind of crop that its seed contains abundant phytoprotein.Soybean is most commonly used for various bean product, squeezing
Soya-bean oil is taken, make soy sauce and extracts protein.Bean dregs or the soybean for wearing into coarse powder are also commonly used for poultry and livestock feed.Rihizobium japonicum
With leguminous plant mutualism, leguminous plant passes through the photosynthetic organic matter for renting manufacture, a part supply rhizobium；Rhizobium are logical
Cross the nitrogen supply leguminous plant of biological nitrogen fixation manufacture.Currently, the dross vigor urgently to be resolved for improving rihizobium japonicum and competition knot
Tumor ability.
Application No. is the preparation methods that treating piles with 9-medicinal herbs piece is described in 201410371512.9 application, are steeped by March
It is 400g, polygonum cuspidate 150g, garden burnet 200g, Liu Jisheng 100g, common fig leaf juice 100g, chrysanthemum 50g, hen egg-albumen 20g, coptis 150g, big
Yellow 50g is made as bulk pharmaceutical chemicals, which is characterized in that the preparation method is made of the following steps: taking bubble in March, polygonum cuspidate, willow
Parasitism is added to CO2In supercritical extract device, ethyl alcohol is as entrainer, the percent by volume of the total extractant of entrainer Zhan
4-6%, extracting pressure 15-30MPa, 30-50 DEG C of temperature, CO2Flow l-3ml/g crude drug min, extraction time 180-220min,
Supercritical extract is obtained, it is spare；Remaining Chinese medicine is taken, is crushed, 60% ethyl alcohol of 5L is added, is carried out in investment microwave extracting apparatus micro-
Wave extraction, extracts power 600-800W, extracts 2 times, 5-10 minutes each, combining extraction liquid, and concentration is added to Dl01 macroporous absorption
On resin column, 60% ethanol elution collects 5 times of amount column volume eluents, ethyl alcohol is recovered under reduced pressure, is concentrated and dried, obtains Microwave Extraction
Object, it is spare；Above-mentioned supercritical extract and Microwave Extraction object are mixed, starch is added, 70% ethyl alcohol makes pellet, dry, tabletting,
500 are made, every slice weight 0.3g.
Summary of the invention
In view of the above-mentioned problems, the present invention provides a kind of agricultural composite fertilizer containing Chinese medicine dreg for being exclusively used in soybean and its
Preparation method, the present invention can effectively reduce the use of chemical fertilizer, belong to environmentally friendly compound fertilizer, and substantially increase soybean
The content of albumen in yield and soybean is realized in addition, the present invention recycles the Chinese medicine residue for preparing treating piles with 9-medicinal herbs piece
The maximization of Chinese medicine value.Technical scheme is as follows:
A kind of agricultural composite fertilizer containing Chinese medicine dreg being exclusively used in soybean, by following raw material group according to parts by weight
At:
1-2 parts of Diammonium phosphate (DAP), 0.5-1 parts of potassium nitrate, 1-3 parts of potassium chloride, 0.5-1 parts of borax, 1-5 parts of humic acid, Chinese medicine
1-5 parts of residue, 0.5-1 parts of root nodule fermented liquid.
Preferably, it is made of following raw material according to parts by weight:
1.5 parts of Diammonium phosphate (DAP), 0.8 part of potassium nitrate, 1.8 parts of potassium chloride, 0.7 part of borax, 3 parts of humic acid, Chinese medicine residue 2.5
Part, 0.7 part of root nodule fermented liquid.
The root nodule fermented liquid the preparation method is as follows:
To take formula Sinorhizobium HN01(it is commercially available) sucrose mass concentration be 2.19%, yeast extract mass concentration be 0.9%,
Initial pH is 6.9, under conditions of temperature is 27.5 DEG C, cultivates 48h, inoculum concentration 10%(v/v) to get.
The mode that the Chinese medicine residue obtains is as follows:
Residue used in the present invention is that generated residue is prepared during inventor prepares treating piles with 9-medicinal herbs piece.
Chinese medicine residue of the present invention is made of Chinese medicine residue A and Chinese medicine residue B；
It takes steep 4 parts, 1.5 parts of polygonum cuspidate, 1 part of Liu Jisheng March, is added to CO2In supercritical extract device, ethyl alcohol is as entrainment
Agent, the percent by volume of the total extractant of entrainer Zhan are 4-6%, extracting pressure 15-30MPa, 30-50 DEG C of temperature, CO2Flow
It is l-3ml, extraction time 180-220min for 1 gram of crude drug flow per minute, after extracting critical extract, obtains Chinese medicine residue A；It takes
2 parts of garden burnet, 1 part of Liu Jisheng, 1 part of common fig leaf juice, 0.5 part of chrysanthemum, 0.2 part of hen egg-albumen, 1.5 parts of the coptis, 0.5 part of rheum officinale crush,
5 parts of 60% ethyl alcohol is added, puts into microwave extracting apparatus and carries out microwave abstracting, extraction power 600-800W, extraction 2 times, every time
5-10 minutes, after extracting extract liquor, obtain Chinese medicine residue B.
The method for preparing agricultural composite fertilizer of the present invention is as follows:
It is uniformly mixed after Chinese medicine residue is pulverized with humic acid, root nodule fermented liquid is then added while stirring, stirs
After mixing uniformly, Diammonium phosphate (DAP), potassium nitrate, potassium chloride, borax is added, continues to stir, after uniform, air-dry to obtain the final product.By the present invention
The compound fertilizer of method preparation, extends the time-to-live of rhizobium.
Apply 2-5 kilograms of dosage per acre in the agricultural composite fertilizer cave containing Chinese medicine dreg that the present invention is exclusively used in soybean.
Compared with the prior art, the present invention has the following advantages:
The present invention recycles the Chinese medicine residue for preparing treating piles with 9-medicinal herbs piece, realizes the maximization of Chinese medicine value, system
The Chinese medicine dreg of standby treating piles with 9-medicinal herbs piece is not only that soybean provides nutrient, and improves the dross vigor and competition knot of rhizobium
Tumor ability, the present invention can effectively reduce the use of chemical fertilizer, belong to environmentally friendly compound fertilizer, and substantially increase soybean production
The content of albumen in amount and soybean.
Specific embodiment
The invention will now be further described with reference to specific embodiments, the advantages and features of the present invention will be with description and
It is apparent.But examples are merely exemplary, and it is not intended to limit the scope of the present invention in any way.Those skilled in the art answer
It should be appreciated that without departing from the spirit and scope of the invention can details to technical solution of the present invention and form repair
Change or replace, but these modifications and replacement are fallen within the protection scope of the present invention.
A kind of embodiment 1 agricultural composite fertilizer containing Chinese medicine dreg for being exclusively used in soybean, by it is following according to parts by weight
Raw material composition:
1.5 parts of Diammonium phosphate (DAP), 0.8 part of potassium nitrate, 1.8 parts of potassium chloride, 0.7 part of borax, 3 parts of humic acid, Chinese medicine residue 2.5
Part, 0.7 part of root nodule fermented liquid.
The root nodule fermented liquid the preparation method is as follows:
To take formula Sinorhizobium HN01(it is commercially available) sucrose mass concentration be 2.19%, yeast extract mass concentration be 0.9%,
Initial pH is 6.9, under conditions of temperature is 27.5 DEG C, cultivates 48h, inoculum concentration 10%(v/v) to get.
The mode that the Chinese medicine residue obtains is as follows:
Residue used in the present invention is that generated residue is prepared during inventor prepares treating piles with 9-medicinal herbs piece.
Chinese medicine residue of the present invention is made of Chinese medicine residue A and Chinese medicine residue B；
It takes steep 4 parts, 1.5 parts of polygonum cuspidate, 1 part of Liu Jisheng March, is added to CO2In supercritical extract device, ethyl alcohol is as entrainment
Agent, the percent by volume of the total extractant of entrainer Zhan are 4-6%, extracting pressure 15-30MPa, 30-50 DEG C of temperature, CO2Flow
It is l-3ml, extraction time 180-220min for 1 gram of crude drug flow per minute, after extracting critical extract, obtains Chinese medicine residue A；It takes
2 parts of garden burnet, 1 part of Liu Jisheng, 1 part of common fig leaf juice, 0.5 part of chrysanthemum, 0.2 part of hen egg-albumen, 1.5 parts of the coptis, 0.5 part of rheum officinale crush,
5 parts of 60% ethyl alcohol is added, puts into microwave extracting apparatus and carries out microwave abstracting, extraction power 600-800W, extraction 2 times, every time
5-10 minutes, after extracting extract liquor, obtain Chinese medicine residue B.
The method for preparing agricultural composite fertilizer of the present invention is as follows:
It is uniformly mixed after Chinese medicine residue is pulverized with humic acid, root nodule fermented liquid is then added while stirring, stirs
After mixing uniformly, Diammonium phosphate (DAP), potassium nitrate, potassium chloride, borax is added, continues to stir, after uniform, air-dry to obtain the final product.By the present invention
The compound fertilizer of method preparation, extends the time-to-live of rhizobium.
Apply 2.5 kilograms of dosage per acre in the agricultural composite fertilizer cave containing Chinese medicine dreg for being exclusively used in soybean prepared by embodiment 1.
A kind of embodiment 2 agricultural composite fertilizer containing Chinese medicine dreg for being exclusively used in soybean, by it is following according to parts by weight
Raw material composition:
1 part of Diammonium phosphate (DAP), 0.5 part of potassium nitrate, 1.2 parts of potassium chloride, 1.7 parts of borax, 4 parts of humic acid, Chinese medicine residue 3.5
Part, 0.9 part of root nodule fermented liquid.
The preparation method is the same as that of Example 1 for the root nodule fermented liquid, Chinese medicine residue and agricultural composite fertilizer.
Apply 4.8 kilograms of dosage per acre in the agricultural composite fertilizer cave containing Chinese medicine dreg for being exclusively used in soybean prepared by embodiment 2.
A kind of embodiment 3 agricultural composite fertilizer containing Chinese medicine dreg for being exclusively used in soybean, by it is following according to parts by weight
Raw material composition:
2 parts of Diammonium phosphate (DAP), 0.8 part of potassium nitrate, 3 parts of potassium chloride, 0.5 part of borax, 1.5 parts of humic acid, 2 parts of Chinese medicine residue,
0.5 part of root nodule fermented liquid.
The preparation method is the same as that of Example 1 for the root nodule fermented liquid, Chinese medicine residue and agricultural composite fertilizer.
Apply 3 kilograms of dosage per acre in the agricultural composite fertilizer cave containing Chinese medicine dreg for being exclusively used in soybean prepared by embodiment 3.
The detection of 1 soybean nodulation situation of test example
Sample: embodiment 1, embodiment 2, embodiment 3；
Control 1: being free of Chinese medicine dreg, and the soil of the corresponding deal Soybean-planting of mitigation is supplied；
Control 2: take formula Sinorhizobium HN01 preparation (commercially available)；
Control 3: blank control.
Observation period: full-bloom stage
Conclusion: the average every plant of dross number of embodiment 1 is 65.3, and the average every plant of dross number of embodiment 2 is 59.9, embodiment 3
Average every plant of dross number is 62.8, and the average every plant of dross number of control 1 is 27.1, and the average every plant of dross number of control 2 is 39.8, control
3 average every plant of dross numbers are 26.5.By test it is found that the present invention can effectively improve the dross vigor of rihizobium japonicum, into
And promote fixed nitrogen.
Influence of 2 present invention of test example as base manure to spring sowing soybean yields
Sample: embodiment 1, embodiment 2, embodiment 3；
Control 1: take formula Sinorhizobium HN01 preparation (commercially available)；
Control 2: blank control.
Soybean varieties: Xindou No.1 is commercially available.
Place: Jinan, Shandong Province.
Conclusion: the average soybean yields per acre of embodiment 1 is 430.5 kilograms, and the average soybean yields per acre of embodiment 2 is
405.5 kilograms, the average soybean yields per acre of embodiment 3 is 412.8 kilograms, and the average soybean yields per acre of control 1 is 365 kilograms,
The average soybean yields per acre of control 2 is 309.8 kilograms.
Claims (4)
1. a kind of agricultural composite fertilizer containing Chinese medicine dreg for being exclusively used in soybean, which is characterized in that the agricultural composite fertilizer by with
Under according to parts by weight raw material composition:
1-2 parts of Diammonium phosphate (DAP), 0.5-1 parts of potassium nitrate, 1-3 parts of potassium chloride, 0.5-1 parts of borax, 1-5 parts of humic acid, Chinese medicine residue
1-5 parts, 0.5-1 parts of root nodule fermented liquid；
The root nodule fermented liquid the preparation method is as follows:
To take formula Sinorhizobium HN01 in sucrose mass concentration be 2.19%, yeast extract mass concentration is 0.9%, and initial pH is
6.9, temperature be 27.5 DEG C under conditions of, cultivate 48h, inoculum concentration be 10%v/v to get；
The Chinese medicine residue is made of Chinese medicine residue A and Chinese medicine residue B；Specific step is as follows:
It takes steep 4 parts, 1.5 parts of polygonum cuspidate, 1 part of Liu Jisheng March, is added to CO2In supercritical extract device, ethyl alcohol is as entrainer, folder
Percent by volume with the total extractant of agent Zhan be 4-6%, extracting pressure 15-30MPa, 30-50 DEG C of temperature, CO2Flow is every
Minute, 1 gram of crude drug flow was l-3ml, extraction time 180-220min, after extracting critical extract, obtained Chinese medicine residue A；Take garden burnet
2 parts, 1 part of Liu Jisheng, 1 part of common fig leaf juice, 0.5 part of chrysanthemum, 0.2 part of hen egg-albumen, 1.5 parts of the coptis, 0.5 part of rheum officinale are crushed, and are added
5 parts of 60% ethyl alcohol puts into microwave extracting apparatus and carries out microwave abstracting, extracts power 600-800W, extracts 2 times, each 5-
10 minutes, after extracting extract liquor, obtain Chinese medicine residue B.
2. agricultural composite fertilizer according to claim 1, which is characterized in that the agricultural composite fertilizer by it is following in parts by weight
The raw material of meter forms:
1.5 parts of Diammonium phosphate (DAP), 0.8 part of potassium nitrate, 1.8 parts of potassium chloride, 0.7 part of borax, 3 parts of humic acid, 2.5 parts of Chinese medicine residue,
0.7 part of root nodule fermented liquid.
3. agricultural composite fertilizer according to claim 1 or 2, which is characterized in that apply 2-5 kilograms of dosage per acre in cave.
4. the method for preparing agricultural composite fertilizer as claimed in claim 1 or 2, which is characterized in that specific step is as follows:
It is uniformly mixed after Chinese medicine residue is pulverized with humic acid, root nodule fermented liquid is then added while stirring, stirring is equal
After even, Diammonium phosphate (DAP), potassium nitrate, potassium chloride, borax is added, continues to stir, after uniform, air-dry to obtain the final product.
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| CN107986824A (en) * | 2017-11-30 | 2018-05-04 | 广东佳泰药业股份有限公司 | A kind of slag fertilizer for planting Japanses beauty-berry and preparation method thereof |
| CN108675905A (en) * | 2018-08-15 | 2018-10-19 | 中国科学院地球环境研究所 | Chinese medicine slag mixed organic manure and production method suitable for loess plateau lean soil |
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| CN103274875A (en) * | 2013-06-17 | 2013-09-04 | 山东亿丰源生物科技股份有限公司 | Organic fertilizer containing medical dregs and biological germs and preparation method thereof |
| CN104130077A (en) * | 2014-08-19 | 2014-11-05 | 安徽莱姆佳肥业有限公司 | Special humic acid-urea coated rhizobium fertilizer for soybean and preparation method thereof |
| CN104311265A (en) * | 2014-09-30 | 2015-01-28 | 胡伟东 | Special chemical fertilizer for soybeans and preparation method thereof |
| CN104355800A (en) * | 2014-10-23 | 2015-02-18 | 安徽省颍上鑫泰化工有限责任公司 | Compound fertilizer for soybeans |
| CN104529665A (en) * | 2015-01-30 | 2015-04-22 | 李峰 | Special fertilizer for spring sowing soybeans in loess ariplain regions and application thereof |
| CN105036964A (en) * | 2015-08-06 | 2015-11-11 | 青岛点石文具用品有限公司 | Soybean compound fertilizer |
| CN105130681A (en) * | 2015-09-24 | 2015-12-09 | 山东省农作物种质资源中心 | Special fermentation medical fertilizer for soybeans and preparation method thereof |
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| CN105801225A (en) | 2016-07-27 |
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Effective date of registration: 20231201 Address after: Room 2102, block a, building 1, Jinan pharmaceutical Valley R & D platform area, No.1, north section of Gangxing Third Road, comprehensive bonded zone, Jinan high tech Zone, Shandong Province Patentee after: Jinan Xinglu Medical Technology Co.,Ltd. Address before: 250101, Building A, Building 1, Jinan Yaogu, North Section of Gangxing Third Road, Licheng District, Jinan City, Shandong Province, China 2105 Patentee before: JINAN ASIA PHARMA TECH Co.,Ltd. |