CN105796406A - Rose composition and clay mask for removing wrinkles and preparation method thereof - Google Patents
Rose composition and clay mask for removing wrinkles and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a rose composition and a clay mask for removing wrinkles and a preparation method thereof, and belongs to the field of household chemicals.The rose composition for removing wrinkles is mainly prepared from rose extract, aloe extract and astragalus extract.The clay mask for removing wrinkles is mainly prepared from rose residue, bentonite, rose essential oil, aloe extract, highland barley powder, astragalus extract, pearl powder, an antiseptic and antibiotic agent and purified water.The rose composition and the clay mask can effectively remove wrinkles and moisten skin, and meanwhile give natural nutrition to skin; the rose residue is used as the main ingredient of the clay mask for removing wrinkles to be utilized, and resource waste is avoided; in addition, the clay mask is the pure natural skin care product and has the effects of removing wrinkles, whitening skin, protecting and improving skin and the like.The preparation technology of the mask is easy to implement and low in cost, avoids resource waste and improves economic benefits.
Description
Technical field
The present invention relates to the Flos Rosae Rugosae compositions of a kind of wrinkle reduction, facial film mud and preparation method thereof.Belong to household chemicals field.
Background technology
Human body skin is the initial barrier of human defensive system, protects internal various organ from temperature, and the extraneous factor such as humidity and radiation changes the damage brought.But, skin can be aging gradually along with the change of internal hormone level, and the defensive enginery of skin also can fail therewith.Additionally, the destruction of ozone layer causes physics and the stimulation of chemistry, accelerate skin aging.In order to protect and maintain skin health, a lot of at present resisting age of skin researchs all adopt the biological active substances from animals and plants or microorganism as object of study.
Flos Rosae Rugosae is long at China's cultivation history, and Flos Rosae Rugosae is except having ornamental value, or a kind of flowers with significantly high edibility and medical value, the bud of Flos Rosae Rugosae, leaf, stem, and root and fruit have the use history that this is long.Particularly being extracted, by Flos Rosae Rugosae, the Flos Rosae Rugosae quintessence oil that obtains, be widely used in the aspects such as beauty treatment, food, have antibacterial, calm, endocrine regulation, enhancing metabolism to wait acts on, and is referred to as " liquid golden ".But in the process producing Flos Rosae Rugosae quintessence oil, by-product rose slag does fuel except a part through natural air drying, and all the other substantial amounts of rose slags are only as waste disposal.Fermentation, stinking smell assaulting one's nostrils for the colored slag after going mouldy, both wasted resource, again severe contamination environment.Research confirms, contains many nutrients relevant with health such as substantial amounts of sugar, vitamin c, vitamin e, beta-carotene in rose slag, even taller than the content of some fruit.Possibly together with comprehensive amino acid composition, anthocyan composition and flavone compound in rose slag, it is the very abundant natural material of a kind of nutrition, there is important value of exploiting and utilizing.
Along with growth in the living standard, people are for skin care item, and especially the demand of the skin-protection product of natural component raises day by day.Wrinkle removal skin care item in the market generally have that chemical composition is too much and the shortcoming such as effect is undesirable.Nutrient substance abundant in rose slag has good oxidation resistance and free radical knows ability, and provided by the invention be main component with rose slag rose facial mask mud belong to pure natural skin-protection product, there is wrinkle removal whitening, the functions such as skin-moisturizing, skin, help people's protection and improve corresponding skin problem.Preparation is simple for facial film mud, less costly, it is to avoid the wasting of resources, improves economic benefit.
The Flos Rosae Rugosae compositions of a kind of wrinkle reduction disclosed by the invention has effect of the scavenging hydroxyl of significant scavenging free radicals sum, and oxidation resistance highlights, it is possible to be used to anti-skin oxidative, anti-aging, is particularly suited for wrinkle reduction.
Summary of the invention
The technical problem to be solved is to provide a kind of Appropriate application and extracts remaining rose slag after quintessence oil, thus reducing the wasting of resources, improves the rose facial mask mud of Flos Rosae Rugosae industrial economy benefit.Have wrinkle resistant, smoothing wrinkle, the effect releived.For solving the problems referred to above, rose facial mask mud of the present invention is based on rose slag；Described Flos Rosae Rugosae residue is the remaining solid residue fraction after Flos Rosae Rugosae extracts quintessence oil.
The present invention is achieved by the following technical solutions:
The invention discloses the Flos Rosae Rugosae compositions of a kind of wrinkle reduction, the Flos Rosae Rugosae compositions of this wrinkle reduction mainly comprises following components, Flos Rosae Rugosae quintessence oil；Aloe extract；Radix Astragali extract.
The invention discloses the Flos Rosae Rugosae compositions of a kind of wrinkle reduction, the Flos Rosae Rugosae compositions of this wrinkle reduction mainly comprises following components, Flos Rosae Rugosae quintessence oil 0.5-1 part；Aloe extract 20-25 part；15-25 part in Radix Astragali extract.
The invention discloses the Flos Rosae Rugosae compositions of a kind of wrinkle reduction, the Flos Rosae Rugosae compositions of this wrinkle reduction mainly comprises following components: Flos Rosae Rugosae quintessence oil 0.5 part；Aloe extract 20 parts；Radix Astragali extract 20 parts.
The invention discloses the Flos Rosae Rugosae compositions of a kind of wrinkle reduction, the Flos Rosae Rugosae compositions of this wrinkle reduction mainly comprises following components: Flos Rosae Rugosae quintessence oil 0.5 part；Aloe extract 20 parts；Radix Astragali extract 15 parts..
The invention discloses the Flos Rosae Rugosae compositions of a kind of wrinkle reduction, the Flos Rosae Rugosae compositions of this wrinkle reduction mainly comprises following components: Flos Rosae Rugosae quintessence oil 1 part；Aloe extract 20 parts；Radix Astragali extract 15 parts.
The invention discloses the Flos Rosae Rugosae compositions of a kind of wrinkle reduction, the Flos Rosae Rugosae compositions of this wrinkle reduction mainly comprises following components: Flos Rosae Rugosae quintessence oil 1 part；Aloe extract 25 parts；Radix Astragali extract 25 parts.
The preparation method that the invention discloses the Flos Rosae Rugosae compositions of a kind of wrinkle reduction, comprises the steps of
(1) taking fresh aloe leaf, clean up, pulverize about 30s and obtain Aloe slurry, quickly boil to obtain Folium Aloe juice on pulverizer, it is Aloe original juice that the centrifugal 10min of 10000rpm obtains supernatant, and water-bath concentrates to obtain concentrated solution, obtains Aloe extract；
(2) the Radix Astragali powder 50g pulverized accurately is weighed in round-bottomed flask, add water 500ml, boiling and condensing reflux 2h, filter to get filtrate, add water 400ml in residue, boil and condensing reflux 1.5h, filter to get filtrate, merging filtrate, concentrate to obtain extractum, repeat the extractum of 3 preparation 3 times amount, obtain Radix Astragali extract；
(3) the commercially available Flos Rosae Rugosae quintessence oil of 0.5-1 part is taken, 20-25 part Aloe extract in step (1), 15-25 part Radix Astragali extract in step (2), stirring mixing, 90 degrees Celsius of sterilizings in 30 minutes, are cooled to subpackage after room temperature, seal and namely obtain Flos Rosae Rugosae compositions.
The invention discloses the rose facial mask mud of a kind of wrinkle reduction, the rose facial mask mud of this wrinkle reduction mainly comprises following components, rose slag, bentonite, Flos Rosae Rugosae quintessence oil, Aloe extract, Semen avenae nudae powder, Radix Astragali extract, Margarita powder, antiseptic and antibiotic agent, to methylparaben and pure water.
The invention discloses the rose facial mask mud of a kind of wrinkle reduction, the rose facial mask mud of this wrinkle reduction mainly comprises following components, 10-20 part in rose slag 20-30 part, 5-15 part, Flos Rosae Rugosae quintessence oil 0.5-1 part, Aloe extract 20-25 part, Semen avenae nudae powder 5-10 part, Radix Astragali extract, Margarita powder 1-5 part, to methylparaben 0.5-1 part, anticorrosion and bactericidal agent 0.5-1 part, remaining supplied by pure water.
This patent discloses the rose facial mask mud of a kind of wrinkle reduction, the rose facial mask mud of this wrinkle reduction is rose slag 25 parts, Flos Rosae Rugosae quintessence oil 0.5 part, bentonite 15 parts, Semen avenae nudae powder 5 parts, Aloe extract 20 parts, Radix Astragali extract 15 parts, Margarita powder 5 parts, anticorrosion and bactericidal agent 0.5 part by weight, to methylparaben 0.5 part, remainder is supplied by pure water.
The rose facial mask mud of this wrinkle reduction can also be by weight rose slag 30 parts, bentonite 10 parts, Flos Rosae Rugosae quintessence oil 1 part, Aloe extract 20 parts, Radix Astragali extract 15 parts, Semen avenae nudae powder 10 parts, Margarita powder 5 parts, anticorrosion and bactericidal agent 0.5 part, to methylparaben 0.5 part, remaining supplied by pure water.
The rose facial mask mud of this wrinkle reduction can also be by weight Flos Rosae Rugosae residue 30 parts, bentonite 10 parts, Flos Rosae Rugosae quintessence oil 1 part, Aloe extract 25 parts, Radix Astragali extract 25 parts, Semen avenae nudae powder 5 parts, Margarita powder 2 parts, anticorrosion and bactericidal agent 1 part, to methylparaben 1 part, remaining supplied by pure water.
The rose facial mask mud of this wrinkle reduction can also be by weight rose slag 20 parts, bentonite 10 parts, Flos Rosae Rugosae quintessence oil 0.5 part, Aloe extract 20 parts, Radix Astragali extract 20 parts, Semen avenae nudae powder 10 parts, Margarita powder 1 part, to methylparaben 0.5 part, anticorrosion and bactericidal agent 0.5 part, remainder is supplied by pure water.
Preservative used is methyl parahydroxybenzoate or Nepal's gold ester, is conventional food, cosmetics, medicine sterilization antiseptic, and antibacterial ability is strong, and safety is high.
Another technical problem to be solved by this invention is to provide the preparation method producing rose facial mask mud.
In rose facial mask of the present invention, Flos Rosae Rugosae residue refers to after vapor distillation, extracts the remaining solid part after Flos Rosae Rugosae quintessence oil and MEIGUI CHUNLU.
For solving the problems referred to above, a kind of specific implementation of preparation method of the present invention comprises the following steps:
(1) collect solid rose slag, dry, dried colored slag is put in pulverizer and smash, cross 200 mesh sieves, obtain Flos Rosae Rugosae ground-slag；
(2) taking fresh aloe leaf, clean up, pulverize about 30s and obtain Aloe slurry, quickly boil to obtain Folium Aloe juice on pulverizer, it is Aloe original juice that the centrifugal 10min of 10000rpm obtains supernatant, and water-bath concentrates to obtain concentrated solution, obtains Aloe extract；
(3) the Radix Astragali powder 50g pulverized accurately is weighed in round-bottomed flask, add water 500ml, boiling and condensing reflux 2h, filter to get filtrate, add water 400ml in residue, boil and condensing reflux 1.5h, filter to get filtrate, merging filtrate, concentrate to obtain extractum, repeat the extractum of 3 preparation 3 times amount, obtain Radix Astragali extract；
(4) by 20-30 part Flos Rosae Rugosae ground-slag of preparation in step (1) and the commercially available Flos Rosae Rugosae quintessence oil of 0.5-1 part, 5-15 part bentonite, the commercially available Semen avenae nudae powder of 5-10 part, 20-25 part Aloe extract in step (2), 15-25 part Radix Astragali extract in step (3), 1-5 part Margarita powder, 0.5-1 part is to methylparaben, 0.5-1 part anticorrosion and bactericidal agent and pure water mix and blend by weight, 90 degrees Celsius preserve sterilizing in 30 minutes, it is cooled to subpackage after room temperature, seals and namely obtain rose facial mask mud.
The invention discloses the application in preparing antioxidation cosmetic product of the described rose facial mask mud.
The invention discloses the application in preparing wrinkle reduction cosmetics of the described rose facial mask mud.
The invention has the beneficial effects as follows:
1. the present invention is while effective wrinkle removal moisturizing skin, gives the nutrition that skin is natural.
2. rose slag is used by the present invention as the main component of wrinkle removal facial film, it is to avoid the wasting of resources.
3. the main component contained by the present invention is without zest and harmful substance, and in wrinkle removal moisturizing, cleaning moistens the respond well of aspect, is suitable for any skin quality, belongs to a kind of green safety, cost-effective facial-care product.
The Flos Rosae Rugosae compositions of a kind of wrinkle reduction disclosed by the invention has effect of the scavenging hydroxyl of significant scavenging free radicals sum, and oxidation resistance highlights, it is possible to be used to anti-skin oxidative, anti-aging, is particularly suited for wrinkle reduction.
Accompanying drawing explanation
Fig. 1 is the different sample clearance rate to free radical in embodiment 4, and wherein QZ1 is the Flos Rosae Rugosae compositions of wrinkle reduction disclosed in formula 1 in embodiment 1；QZ2 is the Flos Rosae Rugosae compositions of wrinkle reduction disclosed in formula 2 in embodiment 1；QZ3 is the Flos Rosae Rugosae compositions that Flos Rosae Rugosae compositions QZ4 is wrinkle reduction disclosed in formula 4 in embodiment 1 of wrinkle reduction disclosed in formula 3 in embodiment 1；HQ is Radix Astragali extract；MG is rose extract；LH is Aloe extract.
Fig. 2 is the different sample clearance rate to hydroxy radical in embodiment 5, and wherein QZ1 is the Flos Rosae Rugosae compositions of wrinkle reduction disclosed in formula 1 in embodiment 1；QZ2 is the Flos Rosae Rugosae compositions of wrinkle reduction disclosed in formula 2 in embodiment 1；QZ3 is the Flos Rosae Rugosae compositions that Flos Rosae Rugosae compositions QZ4 is wrinkle reduction disclosed in formula 4 in embodiment 1 of wrinkle reduction disclosed in formula 3 in embodiment 1；HQ is Radix Astragali extract；MG is rose extract；LH is Aloe extract.
Fig. 3 is the ability that in embodiment 6, fibroblast growth facilitated by different samples, and wherein control is blank group；E1 is the Flos Rosae Rugosae compositions of wrinkle reduction disclosed in formula 1 in embodiment 1；E2 is the Flos Rosae Rugosae compositions of wrinkle reduction disclosed in formula 2 in embodiment 1；E3 is the Flos Rosae Rugosae compositions of wrinkle reduction disclosed in formula 3 in embodiment 1；E4 is the Flos Rosae Rugosae compositions of wrinkle reduction disclosed in formula 4 in embodiment 1；HQ is Radix Astragali extract；MG is rose extract；LH is Aloe extract.
Detailed description of the invention
Below in conjunction with specific embodiment, technical scheme is described in further detail, but protection scope of the present invention is not limited to described embodiment.
The constituent of the Flos Rosae Rugosae compositions of embodiment 1 wrinkle reduction and weight thereof
The invention discloses the Flos Rosae Rugosae compositions of a kind of wrinkle reduction, the Flos Rosae Rugosae compositions of this wrinkle reduction mainly comprises following components, Flos Rosae Rugosae quintessence oil；Aloe extract；Radix Astragali extract.
The invention discloses the Flos Rosae Rugosae compositions of a kind of wrinkle reduction, the Flos Rosae Rugosae compositions of this wrinkle reduction mainly comprises following components, Flos Rosae Rugosae quintessence oil 0.5-1 part；Aloe extract 10-20 part；10-20 part in Radix Astragali extract.
Formula 1: Flos Rosae Rugosae quintessence oil 0.025ml；Aloe extract 1g；Radix Astragali extract 1g.
Formula 2: Flos Rosae Rugosae quintessence oil 0.03ml；Aloe extract 1g；Radix Astragali extract 0.75g..
Formula 3: Flos Rosae Rugosae quintessence oil 0.05ml；Aloe extract 1g；Radix Astragali extract 0.75g.
Formula 4: Flos Rosae Rugosae quintessence oil 0.05ml；Aloe extract 1.25g；Radix Astragali extract 1.25g.
The constituent of the rose facial mask mud of embodiment 2 wrinkle reduction and weight thereof
The rose facial mask mud of wrinkle reduction disclosed by the invention mainly comprises following components, rose slag, bentonite, Flos Rosae Rugosae quintessence oil, Aloe extract, Semen avenae nudae powder, Radix Astragali extract, Margarita powder, antiseptic and antibiotic agent and pure water.
This patent discloses the rose facial mask mud of a kind of wrinkle reduction, the rose facial mask mud of this wrinkle reduction is rose slag 20g, rare quintessence oil 0.5ml, bentonite 10g, Semen avenae nudae powder 10g, Aloe extract 20g, Radix Astragali extract 20g, Margarita powder 1g, anticorrosion and bactericidal agent 0.5g, pure water 29.5ml.
A kind of rose facial mask mud of wrinkle reduction be rose slag 25g, bentonite 15g, Flos Rosae Rugosae quintessence oil 0.5ml, Aloe extract 20g, Radix Astragali extract 20g, Semen avenae nudae powder 5g, Margarita powder 5g, to methylparaben 0.5g, anticorrosion and bactericidal agent 0.5g, pure water 34.5ml.
A kind of rose facial mask mud of wrinkle reduction can also be by weight Flos Rosae Rugosae residue 30g, bentonite 10g, Flos Rosae Rugosae quintessence oil 1ml, Aloe extract 20g, Radix Astragali extract 15g, Semen avenae nudae powder 10g, Margarita powder 5g, to methylparaben 0.5g, anticorrosion and bactericidal agent 0.5g, pure water 24ml.
A kind of rose facial mask mud of wrinkle reduction be rose slag 30g, bentonite 5g, Flos Rosae Rugosae quintessence oil 1ml, Aloe extract 25g, Radix Astragali extract 25g, Semen avenae nudae powder 5g, Margarita powder 2g, to methylparaben 1g, anticorrosion and bactericidal agent 1g, pure water 14ml.
The preparation method of the rose facial mask mud of embodiment 3 wrinkle reduction
1. in rose facial mask of the present invention, Flos Rosae Rugosae residue refers to after vapor distillation, extracts the remaining solid part after Flos Rosae Rugosae quintessence oil and MEIGUI CHUNLU.
(1) collect solid rose slag, dry, dried colored slag is put in pulverizer and smash, cross 200 mesh sieves, obtain Flos Rosae Rugosae ground-slag；
(2) taking fresh aloe leaf, clean up, pulverize about 30s and obtain Aloe slurry, quickly boil to obtain Folium Aloe juice on pulverizer, it is Aloe original juice that the centrifugal 10min of 10000rpm obtains supernatant, and water-bath concentrates to obtain concentrated solution, obtains Aloe extract；
(3) the Radix Astragali powder 50g pulverized accurately is weighed in round-bottomed flask, add water 500ml, boiling and condensing reflux 2h, filter to get filtrate, add water 400ml in residue, boil and condensing reflux 1.5h, filter to get filtrate, merging filtrate, concentrate to obtain extractum, repeat the extractum of 3 preparation 3 times amount, obtain Radix Astragali extract；
(4) by 20-30 part Flos Rosae Rugosae ground-slag of preparation in step (1) and the commercially available Flos Rosae Rugosae quintessence oil of 0.5-1 part, 5-15 part bentonite, the commercially available Semen avenae nudae powder of 5-10 part, 20-25 part Aloe extract in step (2), 15-25 part Radix Astragali extract in step (3), 1-5 part Margarita powder, 0.5-1 part is to methylparaben, 0.5-1 part anticorrosion and bactericidal agent and pure water mix and blend by weight, 90 degrees Celsius preserve sterilizing in 30 minutes, it is cooled to subpackage after room temperature, seals and namely obtain rose facial mask mud.
Above-mentioned Flos Rosae Rugosae quintessence oil is commercially available；Semen avenae nudae powder is bought from delicacy from mountain shop, Gongga, Szechwan Ganzi.
2. in rose facial mask of the present invention, Flos Rosae Rugosae residue refers to after vapor distillation, extracts the remaining solid part after Flos Rosae Rugosae quintessence oil and MEIGUI CHUNLU.
(1) collect solid rose slag, dry, dried colored slag is put in pulverizer and smash, cross 200 mesh sieves, obtain Flos Rosae Rugosae ground-slag；
(2) taking fresh aloe leaf, clean up, pulverize about 30s and obtain Aloe slurry, quickly boil to obtain Folium Aloe juice on pulverizer, it is Aloe original juice that the centrifugal 10min of 10000rpm obtains supernatant, and water-bath concentrates to obtain concentrated solution, obtains Aloe extract；
(3) the Radix Astragali powder 50g pulverized accurately is weighed in round-bottomed flask, add water 500ml, boiling and condensing reflux 2h, filter to get filtrate, add water 400ml in residue, boil and condensing reflux 1.5h, filter to get filtrate, merging filtrate, concentrate to obtain extractum, repeat the extractum of 3 preparation 3 times amount, obtain Radix Astragali extract；
(4) by the 20 parts of Flos Rosae Rugosae ground-slags prepared in step (1) and 0.5 part of commercially available Flos Rosae Rugosae quintessence oil, 10 parts of bentonite, 10 parts of commercially available Semen avenae nudae powder, 20 parts of Aloe extracts in step (2), 20 parts of Radix Astragali extracts in step (3), 1 part of Margarita powder, 0.5 part to methylparaben, 0.5 part of anticorrosion and bactericidal agent and pure water mix and blend by weight, 90 degrees Celsius preserve sterilizing in 30 minutes, it is cooled to subpackage after room temperature, seals and namely obtain rose facial mask mud.
Above-mentioned Flos Rosae Rugosae quintessence oil is purchased from Dong Fangtianrun company；Semen avenae nudae powder is bought from delicacy from mountain shop, Gongga, Szechwan Ganzi.
The mensuration of the Flos Rosae Rugosae composition removing free radical ability of embodiment 4 wrinkle reduction
Adopt the Flos Rosae Rugosae compositions the measuring DPPH method assessment wrinkle reduction Scavenging activity to free radical, i.e. oxidation resistance.DPPH.free radical (DPPH) is a kind of very stable free radical centered by nitrogen.
Radix Astragali extract preparation method: accurately weighing the Radix Astragali powder 50g pulverized in round-bottomed flask, add water 500ml, boils and condensing reflux 2h, filtering to get filtrate, add water 400ml in residue, boils and condensing reflux 1.5h, filter to get filtrate, merging filtrate, concentrate to obtain extractum.Repeat the extractum of 3 preparation 3 times amount, obtain Radix Astragali extract.
Rose extract preparation method: 40g roseleaf is pulverized, add 10 times amount dehydrated alcohol reflux, extract, 2 hours, medicinal residues add 10 times of dehydrated alcohol reflux, extract, 1.5 hours, and extracting solution is machine filter mistake by centrifugation, and be evaporated at 65 DEG C measuring relative density is the thick paste of 1.31-1.35.
Aloe extract preparation method: take fresh aloe leaf, clean up, pulverizes about 30s on pulverizer and obtains Aloe slurry, quickly boil to obtain Folium Aloe juice, and it is Aloe original juice that the centrifugal 10min of 10000rpm obtains supernatant, and water-bath concentrates to obtain concentrated solution, prepares Aloe extract.
In the embodiment 1 accurately weigh each positive reference substance, preparing, each 0.1g of Flos Rosae Rugosae composition sample of formula 1,2,3,4, is dissolved in 1ml ethanol solution, fully mixes, centrifugal, abandons precipitation, and supernatant is used for testing.
Specific experiment step is as follows:
1, in 96 orifice plates, 160ul0.1777mmol/LDPPH solution is added.
2, add testing sample solution 80ul/ hole, fully mix.
3,520nm place absorbance is detected after 10 minutes.
4, often group sample replication 3 times, average.
5, the clearance rate to free radical is calculated.Clearance rate=1-A sample/A is blank
Experimental result: error bar is marked, due to absorbance measurement, between parallel, absorbance difference is less, and error is inconspicuous
Known in scavenging free radicals DPPH.free radical (DPPH) ability by the experimental result of Fig. 1, the Flos Rosae Rugosae composition effect of wrinkle reduction is better than Radix Astragali extract, rose extract and Aloe extract respectively.Each formula is removed the ability of DPPH and is followed successively by formula 3 > formula 2 > formula 4 > formula 1.
The mensuration of the Flos Rosae Rugosae composition removing hydroxyl radicals of embodiment 5 wrinkle reduction
Radix Astragali extract preparation method: accurately weighing the Radix Astragali powder 50g pulverized in round-bottomed flask, add water 500ml, boils and condensing reflux 2h, filtering to get filtrate, add water 400ml in residue, boils and condensing reflux 1.5h, filter to get filtrate, merging filtrate, concentrate to obtain extractum.Repeat the extractum of 3 preparation 3 times amount, obtain Radix Astragali extract.
Rose extract preparation method: 40g roseleaf is pulverized, add 10 times amount dehydrated alcohol reflux, extract, 2 hours, medicinal residues add 10 times of dehydrated alcohol reflux, extract, 1.5 hours, and extracting solution is machine filter mistake by centrifugation, and be evaporated at 65 DEG C measuring relative density is the thick paste of 1.31-1.35.
Aloe extract preparation method: take fresh aloe leaf, clean up, pulverizes about 30s on pulverizer and obtains Aloe slurry, quickly boil to obtain Folium Aloe juice, and it is Aloe original juice that the centrifugal 10min of 10000rpm obtains supernatant, and water-bath concentrates to obtain concentrated solution, prepares Aloe extract.
In the embodiment 1 accurately weigh each positive reference substance, preparing, each 0.1g of Flos Rosae Rugosae composition sample in formula 1,2,3,4, is dissolved in 1ml ethanol solution, fully mixes, centrifugal, abandons precipitation, and supernatant is used for testing.
(1) in 5ml centrifuge tube, 0.5ml0.4mmol/L crystal violet, 1.4ml, 0.2mol/L, PBS, the 0.5ml1mmol/LFeSO of pH7.4 it are separately added into4, 0.1ml sample is divided into blank group (adding dehydrated alcohol 0.1ml, C), formula 1 (QZ1), formula 2 (QZ2), formula 3 (QZ3), formula 4 (QZ4), Radix Astragali extract group (HQ), rose extract group (MG), Aloe extract group (LH), sample is anhydrous alcohol solution, concentration 0.1g/ml, it is eventually adding 0.5ml6%H2O2。
(2) its absorbance A 0 under 584nm is measured after placing 1 hour.
(3) time with distilled water replacement sample, absorbance is designated as A1, replaces sample and H with distilled water2O2Time absorbance be designated as A2.
(4) interpretation of result.
Clearance rate (%)=(A0-A1)/(A0-A2)
Known in the ability of scavenging hydroxyl by the experimental result of Fig. 2, the effect of the Chinese medicine composition of the rose facial mask mud of wrinkle reduction is far superior to Radix Astragali extract and Aloe extract respectively, slightly below rose extract.The ability of each formula scavenging hydroxyl is followed successively by formula 2 > formula 4 > formula 3 > formula 1.
Embodiment 6 Fibroblasts in vitro competence for added value detects
Biomaterial: human skin fibroblast HFF-1；
Buyer: Chinese Academy of Sciences's stem cell bank；
Numbering: SCSP-109；
Radix Astragali extract preparation method: accurately weighing the Radix Astragali powder 50g pulverized in round-bottomed flask, add water 500ml, boils and condensing reflux 2h, filtering to get filtrate, add water 400ml in residue, boils and condensing reflux 1.5h, filter to get filtrate, merging filtrate, concentrate to obtain extractum.Repeat the extractum of 3 preparation 3 times amount, obtain Radix Astragali extract.
Rose extract preparation method: 40g roseleaf is pulverized, add 10 times amount dehydrated alcohol reflux, extract, 2 hours, medicinal residues add 10 times of dehydrated alcohol reflux, extract, 1.5 hours, and extracting solution is machine filter mistake by centrifugation, and be evaporated at 65 DEG C measuring relative density is the thick paste of 1.31-1.35.
Aloe extract preparation method: take fresh aloe leaf, clean up, pulverizes about 30s on pulverizer and obtains Aloe slurry, quickly boil to obtain Folium Aloe juice, and it is Aloe original juice that the centrifugal 10min of 10000rpm obtains supernatant, and water-bath concentrates to obtain concentrated solution, prepares Aloe extract.
In the embodiment 1 accurately weigh each positive reference substance, preparing, each 0.1g of Flos Rosae Rugosae composition sample of formula 1,2,3,4, is dissolved in 1ml ethanol solution, fully mixes, centrifugal, abandons precipitation, and supernatant is used for testing.
(1) human fibroblasts of cultivation digested and be diluted to 1x10 with Hanks liquid6Individual/ml, 10ml, is inoculated in culture plate altogether, and given the test agent group and matched group is added in culture medium with certain concentration.
(2) cellar culture cell, every day, often group took three parallel sample countings, continuous counter 3 days.
(3) cell growth curve is drawn.
Known in the ability facilitating fibroblast growth by the experimental result of Fig. 3, the effect of the Flos Rosae Rugosae compositions of wrinkle reduction is better than in first three sky or is equivalent to Radix Astragali extract and Aloe extract respectively, is better than rose extract and blank.
To sum up, the removing DPPH of the Flos Rosae Rugosae compositions of wrinkle reduction, the effect of hydroxy radical is substantially better than matched group, it may have certain ability facilitating fibrocyte proliferation.
The assessment of Scavenging ability, the mensuration of scavenging hydroxyl ability and facilitate the experimental result of ability of fibroblast growth to show, the Flos Rosae Rugosae compositions of a kind of wrinkle reduction disclosed by the invention has effect of the scavenging hydroxyl of significant scavenging free radicals sum, oxidation resistance highlights, can be used anti-skin oxidative, anti-aging, it is particularly suited for wrinkle reduction.
Claims (9)
1. the Flos Rosae Rugosae compositions of a wrinkle reduction, it is characterised in that the Flos Rosae Rugosae compositions of this wrinkle reduction mainly comprises following components, rose extract；Aloe extract；Radix Astragali extract.
2. the Flos Rosae Rugosae compositions of a kind of wrinkle reduction according to claim 1, it is characterised in that by weight:
Flos Rosae Rugosae quintessence oil 0.5-1 part；
Aloe extract 20-25 part；
15-25 part in Radix Astragali extract.
3. the preparation method of the Flos Rosae Rugosae compositions of a wrinkle reduction as claimed in claim 2, it is characterised in that comprise the steps of
(1) taking fresh aloe leaf, clean up, pulverize about 30s and obtain Aloe slurry, quickly boil to obtain Folium Aloe juice on pulverizer, it is Aloe original juice that the centrifugal 10min of 10000rpm obtains supernatant, and water-bath concentrates to obtain concentrated solution, obtains Aloe extract；
(2) the Radix Astragali powder 50g pulverized accurately is weighed in round-bottomed flask, add water 500ml, boiling and condensing reflux 2h, filter to get filtrate, add water 400ml in residue, boil and condensing reflux 1.5h, filter to get filtrate, merging filtrate, concentrate to obtain extractum, repeat the extractum of 3 preparation 3 times amount, obtain Radix Astragali extract；
(3) by weight, the commercially available Flos Rosae Rugosae quintessence oil of 0.5-1 part is taken, 20-25 part Aloe extract in step (1), 15-25 part Radix Astragali extract in step (2), stirring mixing, 90 degrees Celsius of sterilizings in 30 minutes, it is cooled to subpackage after room temperature, seals and namely obtain Flos Rosae Rugosae compositions.
4. the rose facial mask mud of a wrinkle reduction, it is characterised in that the rose facial mask mud of this wrinkle reduction mainly comprises following components, rose slag；Bentonite；Flos Rosae Rugosae quintessence oil；Aloe extract；Semen avenae nudae powder；Radix Astragali extract；Margarita powder；Anticorrosion and bactericidal agent；To methylparaben and pure water.
5. the rose facial mask mud of a kind of wrinkle reduction according to claim 4, it is characterised in that by weight:
Rose slag 20-30 part；
Bentonite 5-15 part；
Flos Rosae Rugosae quintessence oil 0.5-1 part；
Aloe extract 20-25 part；
Semen avenae nudae powder 5-10 part；
15-25 part in Radix Astragali extract；
Margarita powder 1-5 part；
To methylparaben 0.5-1 part；
Anticorrosion and bactericidal agent 0.5-1 part；
Remainder is supplied by pure water.
6. the preparation method of the rose facial mask mud of a wrinkle reduction as claimed in claim 5, it is characterised in that comprise the steps of
(1) collect solid rose slag, dry, dried colored slag is put in pulverizer and smash, cross 200 mesh sieves, obtain Flos Rosae Rugosae ground-slag；
(2) taking fresh aloe leaf, clean up, pulverize about 30s and obtain Aloe slurry, quickly boil to obtain Folium Aloe juice on pulverizer, it is Aloe original juice that the centrifugal 10min of 10000rpm obtains supernatant, and water-bath concentrates to obtain concentrated solution, obtains Aloe extract；
(3) the Radix Astragali powder 50g pulverized accurately is weighed in round-bottomed flask, add water 500ml, boiling and condensing reflux 2h, filter to get filtrate, add water 400ml in residue, boil and condensing reflux 1.5h, filter to get filtrate, merging filtrate, concentrate to obtain extractum, repeat the extractum of 3 preparation 3 times amount, obtain Radix Astragali extract；
(4) by 20-30 part Flos Rosae Rugosae ground-slag of preparation in step (1) and the commercially available Flos Rosae Rugosae quintessence oil of 0.5-1 part, 5-15 part bentonite, the commercially available Semen avenae nudae powder of 5-10 part, 20-25 part Aloe extract in step (2), 15-25 part Radix Astragali extract in step (3), 1-5 part Margarita powder, 0.5-1 part is to methylparaben, 0.5-1 part anticorrosion and bactericidal agent and pure water mix and blend by weight, 90 degrees Celsius preserve sterilizing in 30 minutes, it is cooled to subpackage after room temperature, seals and namely obtain rose facial mask mud.
7. the rose facial mask mud of a kind of wrinkle reduction according to any one of claim 4 to 6, it is characterised in that described anticorrosion and bactericidal agent is methyl hydroxybenzoate or Nepal's gold ester.
8. the application in preparing antioxidation cosmetic product of a kind of rose facial mask mud according to any one of claim 4 to 6.
9. the application in preparing wrinkle reduction cosmetics of a kind of rose facial mask mud according to any one of claim 4 to 6.
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