CN105796374B - A kind of lipstick and preparation method thereof - Google Patents
A kind of lipstick and preparation method thereof Download PDFInfo
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- CN105796374B CN105796374B CN201610147711.0A CN201610147711A CN105796374B CN 105796374 B CN105796374 B CN 105796374B CN 201610147711 A CN201610147711 A CN 201610147711A CN 105796374 B CN105796374 B CN 105796374B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0216—Solid or semisolid forms
- A61K8/0233—Distinct layers, e.g. core/shell sticks
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0241—Containing particulates characterized by their shape and/or structure
- A61K8/025—Explicitly spheroidal or spherical shape
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/20—Halogens; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
- A61K8/675—Vitamin B3 or vitamin B3 active, e.g. nicotinamide, nicotinic acid, nicotinyl aldehyde
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/676—Ascorbic acid, i.e. vitamin C
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/68—Sphingolipids, e.g. ceramides, cerebrosides, gangliosides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/927—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of insects, e.g. shellac
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/001—Preparations for care of the lips
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/41—Particular ingredients further characterized by their size
- A61K2800/412—Microsized, i.e. having sizes between 0.1 and 100 microns
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Abstract
The present invention relates to a kind of lipstick, the lipstick includes internal layer, the outer layer for wrapping inner layer；The internal layer includes following component in parts by weight: 1-20wt% emulsifier, 5%-20% water phase components, the oil phase component of 20%-80%, auxiliary material 0.1%-10wt% and active constituent 0.1%-10wt%；The outer layer according to the following component of percent by weight by being made: the grease and wax of auxiliary material 0.1%-10wt%, active constituent 0.1%-10wt% and surplus.The present invention also provides the preparation methods of the lipstick.Lipstick of the invention, water content with higher have good water conservation, water supplement function, and quality is stable, can store for a long time, and preparation process is easy to operate, is convenient for industrial production application.
Description
Technical field
The present invention relates to cosmetic fields, and in particular to a kind of lipstick and preparation method thereof.
Background technique
Mostly based on cerul or oil-base gel, grease and wax are good due to possessing for common lip care product on the market at present
Good closure, the performance with long-acting water lock, can slow down lip itself water loss.But simple water lock is unable to satisfy moisturizing
To the double requirements of moisturizing and water lock, especially for cuticle thickness than relatively thin lip, need while lip care for lip
Skin moisturizing.Meanwhile some water-soluble active constituents, such as vitamin C, vitamin B3, Gotu Kola P.E, carnosine etc.,
Also it can not be widely used in lip care product.Therefore, there is the profit lip technology of some high-moistures or product.
Has there is the lip gloss product with certain water content in existing market, but its water content is generally still below 5%, limitation
The use of lip moisturizing efficiency and high level of water soluble active matter.Continue to improve water content, it will influence lipstick and store up for a long time
The quality problems deposited, such as be precipitated, sweat, crack, it also will affect the tall and straight and persistence of lotion itself.
Summary of the invention
That the purpose of the present invention is to provide a kind of water content is high, can the stable lipstick of long term storage, quality, the present invention is also
The preparation method of the lipstick is provided.
To solve the above problems, the technical solution adopted in the present invention is as follows:
A kind of lipstick, the lipstick include internal layer, the outer layer for wrapping inner layer；The internal layer includes in parts by weight
Following component: 1-20wt% emulsifier, 5%-20% water phase components, the oil phase component of 20%-80%, auxiliary material 0.1%-
10wt% and active constituent 0.1%-10wt%；The outer layer according to the following component of percent by weight by being made: auxiliary material
The grease and wax of 0.1%-10wt%, active constituent 0.1%-10wt% and surplus.
In the present invention, preferred scheme is that the internal layer includes foreign minister and Nei phase；The foreign minister is the non-liquid of cerul；Institute
Stating interior phase includes emulsifier and hydrogel microsphere, and the partial size of the hydrogel microsphere is 1-100 μm.
In the present invention, preferred scheme is the hydrogel microsphere by Sodium Hyaluronate, xanthan gum, tremella polysaccharides, fiber
At least one of element, trehalose, pulullan polysaccharide, maltose and sucrose are made.
In the present invention, preferred scheme is that the eutectic temperature of the internal layer is T1, and the eutectic temperature of the outer layer is T2,
Middle T1≤T2≤T1+10 DEG C；The eutectic temperature T1 of the internal layer is 45-50 DEG C.
In the present invention, preferred scheme is that the auxiliary material is selected from moisturizer, antifreeze, preservative, essence and pigment；It is described
Active constituent be with moisturizing, anti-oxidant, rich lip and repair lip at least one of function active constituent.
In the present invention, preferred scheme is that the grease is selected from vegetable fat, animal fat, mineral oil, silicone oil and synthesis
Grease；The wax is selected from vegetable wax, animal wax, petroleum refining wax and silicon wax.
In the present invention, preferred scheme is that the emulsifier is selected from the water-in-oil emulsifier of HLB value 2-8, HLB value 6-20
One of assistant for emulsifying agent and montmorillonite are to three kinds.
In the present invention, preferred scheme are as follows:
The internal layer includes the following component according to percent by weight: candelila wax 1-5%, beeswax 8-20%, synthesis
Saualane 10-30%.Shea butter 8-20% wins the emulsifier 1-10% of the model ABIL WE09 of wound industrial group production,
The production of Jia Fa lion companyThe emulsifier 1-10% of brand, deionized water 5-10%, glycerol 1-10%, fourth
Glycol 1-10%, xanthan gum 0.1-1%, active constituent 0.1%-10wt%, auxiliary material 0.1-10%, surplus are olive oil；
The outer layer includes the following component according to percent by weight: candelila wax 1-5%, beeswax 8-20%, synthesis
Saualane 10-40%, shea butter 10-20%, active constituent 0.1%-10wt%, auxiliary material 0.1-10% surplus are olive oil.
In the present invention, preferred scheme are as follows:
The internal layer includes the following component according to percent by weight: candelila wax 2%, and beeswax 12% synthesizes spiny dogfish
Alkane 25%.Shea butter 14%, wins the emulsifier 4% of the model ABIL WE09 of wound industrial group production, and Jia Fa lion company is raw
It producesThe emulsifier 5% of brand, deionized water 8.1%, glycerol 2%, butanediol 3%, xanthan gum 0.1%,
Salt 0.8%, Victoria C ethylether 0.5%, niacinamide 0.5%, olive oil 23%；
The outer layer includes the following component according to percent by weight: candelila wax 3%, and beeswax 17% synthesizes spiny dogfish
Alkane 35%, shea butter 14.5%, vitamin E 0.5%, ceramide 0.5%, surplus are olive oil 29.5%.
The present invention also provides the preparation methods of the lipstick, include the following steps:
A. prepared by internal layer substance: by the olive oil of formula ratio, candelila wax, beeswax, shea butter and partially synthetic angle
Shark alkane is heated to 90 DEG C and melts uniformly, is cooled to 80 DEG C, obtains mixture A；By the type of the win wound industrial group production of formula ratio
Number be ABIL WE09 emulsifier, Jia Fa lion company productionThe emulsifier of brand, with remaining synthesis
Saualane is uniformly mixed, and obtains mixture B, the remaining synthesis saualane is 2% by weight percentage；By xanthan gum plus
Enter in glycerol and be uniformly dispersed, obtains mixture C；The deionized water of formula ratio, butanediol, salt are uniformly mixed, are heated to
75 DEG C, Victoria C ethylether, niacinamide and mixture C is then added, is dispersed with stirring uniformly, obtains mixture D；Mixture D is slow
It is added in mixture B, stirs evenly, obtain mixture E；Mixture E is added in mixture A, is heated to 85 DEG C, mixing is equal
It is even to get；
B. prepared by outer substance: the olive oil of formula ratio, candelila wax, beeswax, synthesis saualane, shea butter are heated
To 90 DEG C melt uniformly, be cooled to 80 DEG C it is spare；Then the vitamin E and Cer NP of formula ratio is added, is dispersed with stirring
It is even to get；
C. prepared by product: take lipstick mould, by b step obtain in 70 DEG C of at a temperature of injection molding, put after being cooled to room temperature
In the environment of entering -25 DEG C after cooling 15min, demoulding forms the outer layer with hollow cavity；The internal layer object that a step is obtained
Matter 70 DEG C at a temperature of pour into molded outer hollow chamber and carry out injection molding, be cooled to and be put into -25 DEG C of environment after room temperature
After lower cooling 15min, demoulding；To obtain the final product.
Compared with prior art, the present invention has the advantage that lipstick of the invention, by the combination of ectonexine, and
Ectonexine respectively selects the combination of combination, enables water phase is stable to be distributed and formed in internal layer under the action of emulsifier
Emulsification system will not discharge in production and storing process, only discharge nourishing skin due to disintegrating for emulsification system when in use
Skin；It will not be stored in there is a phenomenon where being precipitated, sweating, crack, so that lotion keeps tall and straight, lasting during storage；This
The outer lipstick water content is high, there is good water lock, water supplement function；The preparation method of the lipstick enables to lipstick water phase components
Stable is distributed in lipstick, and easy to operate, is convenient for industrial production application.
The present invention is described in detail With reference to embodiment.
Specific embodiment
A kind of lipstick, the lipstick include internal layer, the outer layer for wrapping inner layer；The internal layer includes in parts by weight
Following component: 1-20wt% emulsifier, 5%-20% water phase components, the oil phase component of 20%-80%, auxiliary material 0.1%-
10wt% and active constituent 0.1%-10wt%；The outer layer according to the following component of percent by weight by being made: auxiliary material
The grease and wax of 0.1%-10wt%, active constituent 0.1%-10wt% and surplus.In lipstick of the invention, outer layer is for protecting
Outer layer；Outer layer protection internal layer and after forming lotion, will not cause surface to be precipitated, sweat, open because the conditions such as temperature, humidity change
Phenomena such as splitting；Meanwhile the water-soluble active ingredient of high level can be applied in lipstick, make lipstick while having both stablize, mend
The effect of water, water lock, dual-nourishing.
In the present invention, preferred scheme is that the internal layer includes foreign minister and Nei phase；The foreign minister is the non-liquid of cerul；Institute
Stating interior phase includes emulsifier and hydrogel microsphere, and the partial size of the hydrogel microsphere is 1-100 μm.Hydrogel microsphere in interior phase
Water phase is enabled to form stable emulsification system with emulsifier, and system is more steady under the non-liquid foreign minister's protection of cerul
It is fixed；The partial size of hydrogel microsphere selects 1-100 μm, so that water phase components are more stable, will not release during production and storage
It puts, lipstick is enabled to include higher water；It may further be preferable that the partial size of hydrogel microsphere selects 10-50 μm.
In the present invention, the hydrogel microsphere can be selected from the water made of water-soluble poly polysaccharide and/or crystallinity polysaccharide
Gel micro-ball；The hydrogel microsphere by Sodium Hyaluronate, xanthan gum, tremella polysaccharides, cellulose, trehalose, pulullan polysaccharide,
At least one of maltose and sucrose are made.
In the present invention, preferred scheme is that the eutectic temperature of the internal layer is T1, and the eutectic temperature of the outer layer is T2,
Middle T1≤T2≤T1+10 DEG C；The eutectic temperature T1 of the internal layer is 45-50 DEG C.The setting of ectonexine fusing point gradient, so that in making
Layer foreign minister keeps the characteristic of cerul, while the characteristic of liquid is mutually kept in internal layer；Meanwhile the water phase of phase is coagulated in internal layer
Gelatinization reduces its permeability, forms the system of wax package hydrogel, so that product is more stable, lipstick can include higher water
Amount；It may further be preferable that T1+2 DEG C≤T2≤T1+7 DEG C.
In the present invention, the auxiliary material is the common auxiliary material of cosmetic field, can be selected from moisturizer, antifreeze, preservative, perfume (or spice)
Essence and pigment；The active constituent be with moisturizing, anti-oxidant, rich lip and repair lip at least one of function activity at
Point, such as Victoria C ethylether, niacinamide, vitamin E, ceramide etc..
In the present invention, the grease can be the grease of cosmetic field, can be selected from vegetable fat, animal fat, mine
Object oil, silicone oil and Synthetic Oil；The grease can be the grease of cosmetic field, can be selected from vegetable wax, animal wax, petroleum
Refine wax and silicon wax.
In the present invention, preferred scheme is that the emulsifier is selected from the water-in-oil emulsifier of HLB value 2-8, HLB value 6-20
One of assistant for emulsifying agent and montmorillonite are to three kinds.
In the present invention, preferred scheme are as follows:
The internal layer includes the following component according to percent by weight: candelila wax 1-5%, beeswax 8-20%, synthesis
Saualane 10-30%.Shea butter 8-20% wins emulsifier (emulsification of the model ABIL WE09 of wound industrial group production
Agent includes following ingredient: PEG-4 isostearate, -10/ dimethyl siloxane of cetyl polyethylene/polypropylene glycol, lauric acid
Own ester) 1-10%, the production of Jia Fa lion company(emulsifier includes following ingredient to the emulsifier of brand: suddenly
Bar esters, Acacia decurrens floral wax, sunflower seed wax and polyglycereol -3 suddenly) 1-10%, deionized water 5-10%, glycerol 1-10%, fourth
Glycol 1-10%, xanthan gum 0.1-1%, active constituent 0.1%-10wt%, auxiliary material 0.1-10%, surplus are olive oil；
The outer layer includes the following component according to percent by weight: candelila wax 1-5%, beeswax 8-20%, synthesis
Saualane 10-40%, shea butter 10-20%, active constituent 0.1%-10wt%, auxiliary material 0.1-10% surplus are olive oil.
In the present invention, preferred scheme are as follows:
The internal layer includes the following component according to percent by weight: candelila wax 2%, and beeswax 12% synthesizes spiny dogfish
Alkane 25%.Shea butter 14%, wins the emulsifier 4% of the model ABIL WE09 of wound industrial group production, and Jia Fa lion company is raw
It producesThe emulsifier 5% of brand, deionized water 8.1%, glycerol 2%, butanediol 3%, xanthan gum
0.1%, salt 0.8%, Victoria C ethylether 0.5%, niacinamide 0.5%, olive oil 23%；The outer layer includes according to weight hundred
The following component of score meter: candelila wax 3%, beeswax 17% synthesize saualane 35%, shea butter 14.5%, vitamin
E0.5%, ceramide 0.5%, surplus are olive oil 29.5%.
In lipstick of the invention, oil phase component structure employed in inside and outside two layers is close, so that whole more stable.
The present invention also provides the preparation methods of the lipstick, include the following steps:
A. prepared by internal layer substance: by the olive oil of formula ratio, candelila wax, beeswax, shea butter and partially synthetic angle
Shark alkane is heated to 90 DEG C and melts uniformly, is cooled to 80 DEG C, obtains mixture A；By the type of the win wound industrial group production of formula ratio
Number be ABIL WE09 emulsifier, Jia Fa lion company productionThe emulsifier of brand, with remaining synthesis
Saualane is uniformly mixed, and obtains mixture B, the remaining synthesis saualane is 2% by weight percentage；By xanthan gum plus
Enter in glycerol and be uniformly dispersed, obtains mixture C；The deionized water of formula ratio, butanediol, salt are uniformly mixed, are heated to
75 DEG C, Victoria C ethylether, niacinamide and mixture C is then added, is dispersed with stirring uniformly, obtains mixture D；Mixture D is slow
It is added in mixture B, stirs evenly, obtain mixture E；Mixture E is added in mixture A, is heated to 85 DEG C, mixing is equal
It is even to get；
B. prepared by outer substance: the olive oil of formula ratio, candelila wax, beeswax, synthesis saualane, shea butter are heated
To 90 DEG C melt uniformly, be cooled to 80 DEG C it is spare；Then the vitamin E and Cer NP of formula ratio is added, is dispersed with stirring
It is even to get；
C. prepared by product: take lipstick mould, by b step obtain in 70 DEG C of at a temperature of injection molding, put after being cooled to room temperature
In the environment of entering -25 DEG C after cooling 15min, demoulding forms the outer layer with hollow cavity；The internal layer object that a step is obtained
Matter 70 DEG C at a temperature of pour into molded outer hollow chamber and carry out injection molding, be cooled to and be put into -25 DEG C of environment after room temperature
After lower cooling 15min, demoulding；To obtain the final product.
Embodiment 1
A kind of lipstick, including internal layer, for the outer layer of wrapping inner layer:
The internal layer includes the following component according to percent by weight: candelila wax 2%, and beeswax 13% synthesizes spiny dogfish
Alkane 25%.Shea butter 14%, wins the emulsifier 3% of the model ABIL WE09 of wound industrial group production, and Jia Fa lion company is raw
It producesThe emulsifier 4% of brand, deionized water 5%, glycerol 2%, butanediol 3%, xanthan gum 0.1%, food
Salt 0.8%, Victoria C ethylether 0.5%, niacinamide 0.5%, olive oil 27.1%；
The outer layer includes the following component according to percent by weight: candelila wax 3%, and beeswax 14% synthesizes spiny dogfish
Alkane 35%, shea butter 17.5%, vitamin E 0.5%, ceramide 0.5%, surplus are olive oil 29.5%.
The preparation method of the lipstick, includes the following steps:
A. prepared by internal layer substance: by the olive oil of formula ratio, candelila wax, beeswax, shea butter and partially synthetic angle
Shark alkane is heated to 90 DEG C and melts uniformly, is cooled to 80 DEG C, obtains mixture A；By the type of the win wound industrial group production of formula ratio
Number be ABIL WE09 emulsifier, Jia Fa lion company productionThe emulsifier of brand, with remaining synthesis
Saualane is uniformly mixed, and obtains mixture B, the remaining synthesis saualane is 2% by weight percentage；By xanthan gum plus
Enter in glycerol and be uniformly dispersed, obtains mixture C；The deionized water of formula ratio, butanediol, salt are uniformly mixed, are heated to
75 DEG C, Victoria C ethylether, niacinamide and mixture C is then added, is dispersed with stirring uniformly, obtains mixture D；Mixture D is slow
It is added in mixture B, stirs evenly, obtain mixture E；Mixture E is added in mixture A, is heated to 85 DEG C, mixing is equal
It is even to get；
B. prepared by outer substance: the olive oil of formula ratio, candelila wax, beeswax, synthesis saualane, shea butter are heated
To 90 DEG C melt uniformly, be cooled to 80 DEG C it is spare；Then the vitamin E and Cer NP of formula ratio is added, is dispersed with stirring
It is even to get；
C. prepared by product: product preparation: taking lipstick mould, by b step obtain in 70 DEG C of at a temperature of injection molding, be cooled to
In the environment of being put into -25 DEG C after room temperature after cooling 15min, demoulding forms the outer layer with hollow cavity；A step is obtained
Internal layer substance 70 DEG C at a temperature of pour into molded outer hollow chamber and carry out injection molding, be put into -25 after being cooled to room temperature
In the environment of DEG C after cooling 15min, demoulding；To obtain the final product.
Embodiment 2
A kind of lipstick, including internal layer, for the outer layer of wrapping inner layer:
The internal layer includes the following component according to percent by weight: candelila wax 3%, and beeswax 12% synthesizes spiny dogfish
Alkane 25%.Shea butter 14%, wins the emulsifier 4% of the model ABIL WE09 of wound industrial group production, and Jia Fa lion company is raw
It producesThe emulsifier 5% of brand, deionized water 7%, glycerol 2%, butanediol 3%, xanthan gum 0.1%, food
Salt 0.8%, Victoria C ethylether 0.5%, niacinamide 0.5%, olive oil 23.1%；
The outer layer includes the following component according to percent by weight: candelila wax 3%, and beeswax 16% synthesizes spiny dogfish
Alkane 35%, shea butter 15.5%, vitamin E 0.5%, ceramide 0.5%, surplus are olive oil 29.5%.
The preparation method of the lipstick, includes the following steps:
A. prepared by internal layer substance: by the olive oil of formula ratio, candelila wax, beeswax, shea butter and partially synthetic angle
Shark alkane is heated to 90 DEG C and melts uniformly, is cooled to 80 DEG C, obtains mixture A；By the type of the win wound industrial group production of formula ratio
Number be ABIL WE09 emulsifier, Jia Fa lion company productionThe emulsifier of brand, with remaining synthesis
Saualane is uniformly mixed, and obtains mixture B, the remaining synthesis saualane is 2% by weight percentage；By xanthan gum plus
Enter in glycerol and be uniformly dispersed, obtains mixture C；The deionized water of formula ratio, butanediol, salt are uniformly mixed, are heated to
75 DEG C, Victoria C ethylether, niacinamide and mixture C is then added, is dispersed with stirring uniformly, obtains mixture D；Mixture D is slow
It is added in mixture B, stirs evenly, obtain mixture E；Mixture E is added in mixture A, is heated to 85 DEG C, mixing is equal
It is even to get；
B. prepared by outer substance: the olive oil of formula ratio, candelila wax, beeswax, synthesis saualane, shea butter are heated
To 90 DEG C melt uniformly, be cooled to 80 DEG C it is spare；Then the vitamin E and Cer NP of formula ratio is added, is dispersed with stirring
It is even to get；
C. prepared by product: product preparation: taking lipstick mould, by b step obtain in 70 DEG C of at a temperature of injection molding, be cooled to
In the environment of being put into -25 DEG C after room temperature after cooling 15min, demoulding forms the outer layer with hollow cavity；A step is obtained
Internal layer substance 70 DEG C at a temperature of pour into molded outer hollow chamber and carry out injection molding, be put into -25 after being cooled to room temperature
In the environment of DEG C after cooling 15min, demoulding；To obtain the final product.
Embodiment 3
A kind of lipstick, including internal layer, for the outer layer of wrapping inner layer:
The internal layer includes the following component according to percent by weight: candelila wax 4%, and beeswax 12% synthesizes spiny dogfish
Alkane 25%.Shea butter 14%, wins the emulsifier 6% of the model ABIL WE09 of wound industrial group production, and Jia Fa lion company is raw
It producesThe emulsifier 6% of brand, deionized water 9%, glycerol 2%, butanediol 3%, xanthan gum 0.1%, food
Salt 0.8%, Victoria C ethylether 0.5%, niacinamide 0.5%, olive oil 17.1%；
The outer layer includes the following component according to percent by weight: candelila wax 4%, and beeswax 18% synthesizes spiny dogfish
Alkane 35%, shea butter 12.5%, vitamin E 0.5%, ceramide 0.5%, surplus are olive oil 29.5%.
The preparation method of the lipstick, includes the following steps:
A. prepared by internal layer substance: by the olive oil of formula ratio, candelila wax, beeswax, shea butter and partially synthetic angle
Shark alkane is heated to 90 DEG C and melts uniformly, is cooled to 80 DEG C, obtains mixture A；By the type of the win wound industrial group production of formula ratio
Number be ABIL WE09 emulsifier, Jia Fa lion company productionThe emulsifier of brand, with remaining synthesis
Saualane is uniformly mixed, and obtains mixture B, the remaining synthesis saualane is 2% by weight percentage；By xanthan gum plus
Enter in glycerol and be uniformly dispersed, obtains mixture C；The deionized water of formula ratio, butanediol, salt are uniformly mixed, are heated to
75 DEG C, Victoria C ethylether, niacinamide and mixture C is then added, is dispersed with stirring uniformly, obtains mixture D；Mixture D is slow
It is added in mixture B, stirs evenly, obtain mixture E；Mixture E is added in mixture A, is heated to 85 DEG C, mixing is equal
It is even to get；
B. prepared by outer substance: the olive oil of formula ratio, candelila wax, beeswax, synthesis saualane, shea butter are heated
To 90 DEG C melt uniformly, be cooled to 80 DEG C it is spare；Then the vitamin E and Cer NP of formula ratio is added, is dispersed with stirring
It is even to get；
C. prepared by product: product preparation: taking lipstick mould, by b step obtain in 70 DEG C of at a temperature of injection molding, be cooled to
In the environment of being put into -25 DEG C after room temperature after cooling 15min, demoulding forms the outer layer with hollow cavity；A step is obtained
Internal layer substance 70 DEG C at a temperature of pour into molded outer hollow chamber and carry out injection molding, be put into -25 after being cooled to room temperature
In the environment of DEG C after cooling 15min, demoulding；To obtain the final product.
Experimental example
The lipstick of the lipstick of Example 01-03 and certain commercially available brand is coated in (will on the identical skin of skin quality respectively
Hope person's forearm position), then using skinanalysis apparatus test the instant moisture content of epidermis and 4 hours moisture contents, immediately it is transdermal
Percentage of water loss and 4 hours transdermal percentages of water loss, specific data see the table below 1 (10 people are averaged):
Table 1: lipstick water retaining function test data table
The result shows that, lipstick of the invention has greater advantage in terms of enhancing moisture content of skin in upper table；And it is preventing
Water loss, i.e., it is suitable with commercial product in terms of the transdermal percentage of water loss value of reduction skin.
Take the lipstick of 1-3 of the embodiment of the present invention, each 10, be individually positioned in -15 DEG C, -10 DEG C, -5 DEG C, 0 DEG C, 5 DEG C,
It is stored at a temperature of 10 DEG C, 20 DEG C, 30 DEG C, 40 DEG C, 45 DEG C 3 months, can completely keep its original rod-like morphology, and nothing goes out
The bad phenomenons such as sweat, cracking, stomata, blistering, surface detail and skew.
The above embodiment is only the preferred embodiment of the present invention, and the scope of protection of the present invention is not limited thereto,
The variation and replacement for any unsubstantiality that those skilled in the art is done on the basis of the present invention belong to institute of the present invention
Claimed range.
Claims (8)
1. a kind of lipstick, it is characterised in that: the lipstick includes internal layer, the outer layer for wrapping inner layer；The internal layer includes pressing
According to the following component of percent by weight: candelila wax 1-5%, beeswax 8-20% synthesize saualane 10-30%, shea butter
8-20% wins emulsifier 1-10%, the Jia Fa lion company production of the model ABIL WE09 of wound industrial group productionThe emulsifier 1-10% of brand, deionized water 5-10%, glycerol 1-10%, butanediol 1-10%, xanthan gum
0.1-1%, active constituent 0.1%-10wt%, auxiliary material 0.1-10%, surplus are olive oil；The outer layer includes according to weight hundred
The following component of score meter: candelila wax 1-5%, beeswax 8-20% synthesize saualane 10-40%, shea butter 10-20%,
Active constituent 0.1%-10wt%, auxiliary material 0.1-10%, surplus are olive oil；The internal layer includes foreign minister and Nei phase；It is described outer
It is mutually the non-liquid of cerul；The interior phase includes emulsifier and hydrogel microsphere, and the partial size of the hydrogel microsphere is 1-100 μ
m。
2. lipstick according to claim 1, it is characterised in that: the hydrogel microsphere is by Sodium Hyaluronate, xanthan gum, silver
At least one of fungus polysaccharides, cellulose, trehalose, pulullan polysaccharide, maltose and sucrose are made.
3. lipstick according to claim 1, it is characterised in that: the eutectic temperature of the internal layer is T1, and the outer layer is total to
Melting temperatur is T2, wherein T1≤T2≤T1+10 DEG C；The eutectic temperature T1 of the internal layer is 45-50 DEG C.
4. lipstick according to claim 1, it is characterised in that: the auxiliary material is selected from moisturizer, antifreeze, preservative, perfume (or spice)
Essence and pigment；The active constituent be with moisturizing, anti-oxidant, rich lip and repair lip at least one of function activity at
Point.
5. lipstick according to claim 1, it is characterised in that: the Water-In-Oil that the emulsifier is selected from HLB value 2-8 emulsifies
One of agent, the assistant for emulsifying agent of HLB value 6-20 and montmorillonite are to three kinds.
6. lipstick according to claim 1, it is characterised in that:
The internal layer includes the following component according to percent by weight: candelila wax 2%, and beeswax 12% synthesizes saualane
25%, shea butter 14% wins the emulsifier 4% of the model ABIL WE09 of wound industrial group production, and Jia Fa lion company is raw
It producesThe emulsifier 5% of brand, deionized water 8.1%, glycerol 2%, butanediol 3%, xanthan gum 0.1%,
Salt 0.8%, Victoria C ethylether 0.5%, niacinamide 0.5%, olive oil 23%；
The outer layer includes the following component according to percent by weight: candelila wax 3%, and beeswax 17% synthesizes saualane
35%, shea butter 14.5%, vitamin E 0.5%, ceramide 0.5%, surplus is olive oil 29.5%.
7. the preparation method of lipstick according to claim 1, it is characterised in that include the following steps:
A. prepared by internal layer substance: the wax of formula ratio and amount of grease being heated to 90 DEG C and melted uniformly, 80 DEG C is cooled to, is mixed
Close object A；The emulsifier of formula ratio is uniformly mixed with remaining grease, obtains mixture B；By auxiliary material and active constituent in water phase
In be sufficiently dissolved as mixture C；Mixture C is slowly added in mixture B, is stirred evenly, mixture D is obtained；By mixture D
Be added mixture A in, be heated to 85 DEG C, be uniformly mixed to get；
B. outer substance prepare: by the wax of formula ratio and grease be heated to 90 DEG C melt uniformly, be cooled to 80 DEG C it is spare；Then plus
The auxiliary material and active constituent for entering formula ratio, be dispersed with stirring uniformly to get；
C. prepared by product: take lipstick mould, by b step obtain in 70 DEG C of at a temperature of injection molding, be put into -25 after being cooled to room temperature
In the environment of DEG C after cooling 15min, demoulding forms the outer layer with hollow cavity；The internal layer substance that a step is obtained is 70
It is poured at a temperature of DEG C in molded outer hollow chamber and carries out injection molding, be cooled to after room temperature cooling in the environment of being put into -25 DEG C
After 15min, demoulding；To obtain the final product.
8. the preparation method of lipstick according to claim 7, it is characterised in that include the following steps:
A. prepared by internal layer substance: by the olive oil of formula ratio, candelila wax, beeswax, shea butter and partially synthetic saualane
It is heated to 90 DEG C to melt uniformly, is cooled to 80 DEG C, obtains mixture A；By the model of the win wound industrial group production of formula ratio
The emulsifier of ABIL WE09, the production of Jia Fa lion companyThe emulsifier of brand, with remaining synthesis spiny dogfish
Alkane is uniformly mixed, and obtains mixture B, the remaining synthesis saualane is 2% by weight percentage；Xanthan gum is added sweet
It in oil and is uniformly dispersed, obtains mixture C；The deionized water of formula ratio, butanediol, salt are uniformly mixed, are heated to 75 DEG C,
Then Victoria C ethylether, niacinamide and mixture C is added, is dispersed with stirring uniformly, obtains mixture D；Mixture D is slowly added to
It in mixture B, stirs evenly, obtains mixture E；Mixture E is added in mixture A, is heated to 85 DEG C, is uniformly mixed, i.e.,
?；
B. prepared by outer substance: the olive oil of formula ratio, candelila wax, beeswax, synthesis saualane, shea butter are heated to 90
DEG C melt uniformly, be cooled to 80 DEG C it is spare；Then the vitamin E and ceramide of formula ratio is added, is dispersed with stirring uniformly, i.e.,
?；
C. prepared by product: taking lipstick mould, the outer substance that b step is obtained is cooled to room temperature in 70 DEG C of at a temperature of injection molding
After be put into -25 DEG C in the environment of after cooling 15min, demoulding forms the outer layer with hollow cavity；In a step is obtained
Layer substance 70 DEG C at a temperature of pour into molded outer hollow chamber and carry out injection molding, be put into -25 DEG C after being cooled to room temperature
Under environment after cooling 15min, demoulding；To obtain the final product.
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| CN105796374B true CN105796374B (en) | 2019-04-16 |
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Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106726876A (en) * | 2016-11-25 | 2017-05-31 | 南通博泰美术图案设计有限公司 | One kind self-control lipstick |
| CN106726706B (en) * | 2017-01-22 | 2020-09-04 | 花安堂生物科技集团有限公司 | A full-oil lip balm containing water or water soluble components and its preparation method |
| CN109966631A (en) * | 2019-04-22 | 2019-07-05 | 张璐 | A kind of portable sensible lotion device |
| CN109966173A (en) * | 2019-04-25 | 2019-07-05 | 傅征澜 | A kind of production method of the lipstick with cuticula repair function |
| CN115887286A (en) * | 2022-11-23 | 2023-04-04 | 美尚(广州)化妆品股份有限公司 | Composition for thickening and cosmetic |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1109322A (en) * | 1993-07-18 | 1995-10-04 | 珠海东大集团东大化妆品厂 | Basic fiber cell growth factor sandwich lipstick |
| CN101606901A (en) * | 2008-06-20 | 2009-12-23 | 赢创德固赛(中国)投资有限公司 | Lipstick with high water content and preparation method thereof |
| CN102688162A (en) * | 2012-06-12 | 2012-09-26 | 澳宝化妆品（惠州）有限公司 | Pure natural component lip gloss |
| CN103655405A (en) * | 2013-11-20 | 2014-03-26 | 青岛晨讯通商贸有限公司 | Moisturizing lip pomade |
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2016
- 2016-03-15 CN CN201610147711.0A patent/CN105796374B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1109322A (en) * | 1993-07-18 | 1995-10-04 | 珠海东大集团东大化妆品厂 | Basic fiber cell growth factor sandwich lipstick |
| CN101606901A (en) * | 2008-06-20 | 2009-12-23 | 赢创德固赛(中国)投资有限公司 | Lipstick with high water content and preparation method thereof |
| CN102688162A (en) * | 2012-06-12 | 2012-09-26 | 澳宝化妆品（惠州）有限公司 | Pure natural component lip gloss |
| CN103655405A (en) * | 2013-11-20 | 2014-03-26 | 青岛晨讯通商贸有限公司 | Moisturizing lip pomade |
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