CN108938502A - A kind of edible crystal mask and preparation method thereof - Google Patents
A kind of edible crystal mask and preparation method thereof Download PDFInfo
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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- A61K8/345—Alcohols containing more than one hydroxy group
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61Q19/08—Anti-ageing preparations
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Abstract
The invention belongs to cosmetic technical fields, it is poor in order to solve current facial mask toughness, it is easily broken can not vertically lift, the problems such as molding effect is poor, provide a kind of edible crystal mask and preparation method thereof and be prepared by a certain percentage by low-ester pectin, glycerol, sodium alginate, calcium lactate, raspberry extract, water.Edible crystal mask prepared by the present invention is powder face pack, and without adding chemical preservative, use is safe.The facial mask has the remarkable result of moisturizing oil-control, and transparency is high, soft docile.Anti-oxidant, anti-inflammatory, whitening, moisten and other effects.Production method is simple, and conducive to using in the harsh conditions such as family, travelling, aircraft, easy to use, application conditions are milder, and random raising.In addition weight can effectively be controlled by showing through zoopery, be had potential application in reducing formula face.
Description
Technical field
The invention belongs to cosmetic technical fields, and in particular to a kind of edible crystal mask and preparation method thereof.
Background technique
In the modern life, people are very universal to the use of mask product；But common mask carriers on the market
There are various problems, such as multi-layer packaging and carrier itself to use rear nondegradable environmental issue, Essence and preservative can
Can cause skin allergy safety problem and the bad experience problem of docile degree and existing crystal mask toughness it is inadequate, it is easily broken
It can not vertically lift, and the problems such as molding effect is bad.
It is entitled " edible beauty mask of high safety and preparation method thereof " application No. is 201310134133 .3,
Which disclose edible beauty mask of a kind of high safety and preparation method thereof, the component containing following mass percent:
Albumen 1-10%, polysaccharide 0.75%-1.5%, Sodium Hyaluronate 0.1%-0.25%, glycerine 20%-25%, deionized water surplus are supplied
100%.In the preparation method of edible face pack described in the patent, polysaccharide needs heated by microwave or at least 90 DEG C with up
It could sufficiently be dissolved in ionized water, obtain polysaccharide solution；Again in 65-75 DEG C of water bath, by protein solution, Sodium Hyaluronate
Solution and glycerine are added in polysaccharide solution, it is necessary to be mixed slowly so that protein molecule mixes well to be formed with polysaccharide molecule
Stable network structure, while preventing into and participating in excessive bubble in film liquid；Pad pasting carefully takes film off after being cooled and shaped completely,
It is soaked in vacuolar membrane liquid；It will be soaked in the ultraviolet light of the facial mask in vacuolar membrane liquid in super-clean environment and irradiate 25-35min.Obviously should
Microwave heating is not only related in patent production method, water bath mixes slowly, and ultraviolet disinfection is further related to, so that the invention
Not only be not suitable for home environment, self-control is completed, the use being less suitable in the environment such as journey, aircraft.
Summary of the invention
The present invention provides a kind of edible crystal mask and its preparation to solve the problems, such as that current common facial mask exists
Method, prepared edible crystal mask can not only improve skin quality, and moisten comfortable, safety and environmental protection.
The present invention is realized by following technical solution: a kind of edible crystal mask, is prepared by the raw material of following parts by weight
It forms: 0.36-0.9 parts of low-ester pectin；0.1-3.6 parts of glycerol；0.15-0.6 parts of sodium alginate；1-1.5 parts of calcium lactate；Raspberry mentions
Take 0.01-0.1 parts of object；110-140 parts of water, in which: 60-70 parts of 50 DEG C -60 DEG C of warm water；50-70 parts of cold water.
The edible crystal mask optimum ratio are as follows: 0.36 part of low-ester pectin；1.63 parts of glycerol；0.3 part of sodium alginate；
1 part of calcium lactate；0.05 part of raspberry extract；110 parts of water, in which: 60 parts of 50 DEG C -60 DEG C of warm water；50 parts of cold water.
The esterification degree of the low-ester pectin is lower than 60%.The glycerol, sodium alginate, low-ester pectin and calcium lactate are food
Grade raw material.The calcium lactate may be replaced by calcium chloride or calcium gluconate.
The method for preparing the edible crystal mask, steps are as follows:
(1) calcium lactate is soluble in water, obtains solution 1；
(2) glycerol is added in low-ester pectin, sodium alginate and raspberry extract, stirs evenly, obtains mixed material 1；
Mixed material 1 is added in (3) 50 DEG C -60 DEG C of warm water, stirs to being completely dissolved, obtains mixed material 2；
(4) mixed material 2 uniformly pours into facial mask mold, stands 3 minutes, and solution 1 sprays the mixed material 2 in facial mask mold
Completely up to covering, 10 minutes are stood.
Natural function cosmetic additive agent is added in step (3) warm water.
Raspberry extract employed in the present invention is according to document " raspberry dry fruit general flavone before purification after expression activitiy " (poplar
Wait quietly, food research and development, in December, 2015, the 23rd phase of volume 36) disclosed in method be prepared；Document " raspberry leaf
Middle main antioxidant substance optimal extraction technology research " (Han Hongjuan etc., Yunnan University's journal, in March, 2018, volume 40 the 2nd
Phase) in clearly propose that raspberry extract of the present invention itself has anti-oxidant and bacteriostasis.
Edible crystal mask prepared by the present invention, used low-ester pectin, esterification degree are lower than 60%, solidification
Temperature is lower than 35 DEG C, therefore good water solubility, and 50 DEG C or more of warm water can be compared with good dissolving, i.e. solidifiable after natural cooling；And it is high
It is water-soluble that ester pectin (esterification degree > 60%) relies on 90 DEG C or more high temperature, and gelation rate increases with esterification degree and increased, and lactic acid is added
Rapid hardening after calcium aqueous solution forms a film too fast, causes film forming uneven, and transparency is low, and therefore, it is difficult to make transparency height, uniform face
Film.Low-ester pectin prevents ultraviolet radiation to protection skin, treats wound, and beautifying face and moistering lotion all has certain effect.
Sodium alginate good water solubility, does not depend on water temperature, can be to avoid mixing temperature sensitive drug and protein isoreactivity
The inactivation of substance.When there is Ca2+、Sr2+Na in the presence of cation, on G unit+It is anti-that ion exchange occurs with bivalent cation
It answers, G unit is accumulated to form cross-linked network structure, when being condensed into membranoid substance rapidly, but being used cooperatively with proper proportion pectin, can use
It is long to mend short, formation gel.Sodium alginate has the effect of controlling dark sore, moisturizing is nourished.Glycerol has moisturizing and dissolution assistant effect.Tree
Certain kind of berries extract has anti-oxidant, anti-inflammatory, whitening, moist effect.Calcium lactate aqueous solution can provide the calcium ion of high concentration, make
For outstanding crosslinking agent, it can be replaced, cannot be replaced with calcium carbonate with calcium chloride, calcium gluconate.The experimental result table of embodiment
Bright, edible crystal mask provided by the invention is powder face pack defined in QB/T 2872-2017 " facial mask ", without addition
Chemical preservative, use are safe.
Food-grade low-ester pectin, sodium alginate, glycerol, calcium lactate and warm water by a certain percentage and order by merging, make
Pro-skin oil-control moisturizing, the crystal mask that toughness is good, pollution is small, is aided with a certain amount of raspberry extract, wherein being rich in SOD, cyanine
Element, ellagic acid and flavones isoreactivity ingredient have anti-oxidant, anti-inflammatory, whitening, moisten and other effects.
Edible face pack filming performance prepared by the present invention is good, it is not easy to prolong raw fracture, pulling force and hardness are high
In commercially available facial mask, while it is relatively low to prepare film-forming temperature, warm water, therefore further improves the application range of facial mask,
Conducive to household, self-control, safety, it is not necessarily to high temperature, and can be used in the case where such as aircraft etc. is difficult to the ambient conditions for obtaining high-temperature water, is made
With convenient, application conditions are more mild, and randomness improves.Edible crystal mask prepared by the present invention is QB/T
Powder face pack defined in 2872-2017 " facial mask ", without adding chemical preservative, use is safe, and production method is simple, is conducive to
It is used in the harsh conditions such as family, travelling, aircraft, has widened the environmental condition used.
Edible crystal mask prepared by the present invention, including low-ester pectin, sodium alginate and several masters of raspberry extract
Ingredient is wanted, showing through zoopery has control mouse weight, the good result of the locomitivity of mouse is improved, in reducing formula
Face has potential application.
Detailed description of the invention
Fig. 1 is the plan view in kind of edible crystal mask prepared by embodiment 1；Fig. 2 is the edible of the preparation of embodiment 1
The vertical view in kind of crystal mask；Fig. 3 is the sense organ evaluation and test figure that embodiment 1 and embodiment 2 prepare facial mask；Fig. 4 is this hair
Crystal mask prepared by bright embodiment 1 and existing commercially available crystal mask are prepared under 55 DEG C of water temperatures forms comparison diagram, in figure:
A is crystal mask material object plan view prepared by the embodiment of the present invention 1；B is that crystal mask material object prepared by the embodiment of the present invention 1 hangs down
Straight figure, C are existing commercially available crystal mask material object plan view.
Specific embodiment
In the present invention, used raspberry extract is according to document " raspberry dry fruit general flavone before purification after expression activitiy "
Method disclosed in (poplar is waited quietly, food research and development, in December, 2015, the 23rd phase of volume 36) is prepared；Document " raspberry
Main antioxidant substance optimal extraction technology is studied in leaf " (Han Hongjuan etc., Yunnan University's journal, in March, 2018, volume 40 the 2nd
Phase) in clearly propose that raspberry extract of the present invention itself has anti-oxidant and bacteriostasis.
Embodiment 1: a kind of edible crystal mask is prepared: low-ester pectin 0.36g by the raw material of following weight；It is sweet
Oily 1.63g；Sodium alginate 0.3g；Calcium lactate 1g；Raspberry extract 0.05g；Water 110ml, in which: 55 DEG C of warm water 60ml；It is cool
Water 50ml.
The esterification degree of the low-ester pectin is lower than 60%.The glycerol, sodium alginate, low-ester pectin and calcium lactate are food
Grade raw material.Flavones content >=25% in the raspberry extract.
The method of the preparation edible crystal mask, steps are as follows:
(1) calcium lactate is soluble in water, obtains solution 1；
(2) glycerol is added in low-ester pectin, sodium alginate and raspberry extract, stirs evenly, obtains mixed material 1；
Mixed material 1 is added in (3) 55 DEG C of warm water, stirs to being completely dissolved, obtains mixed material 2；
(4) mixed material 2 uniformly pours into facial mask mold, stands 3 minutes, and solution 1 sprays the mixed material 2 in facial mask mold
Completely up to covering, 10 minutes are stood.
Embodiment 2: a kind of edible crystal mask is prepared: low-ester pectin 0.9g by the raw material of following weight；Glycerol
3.6g；Sodium alginate 0.6g；Calcium lactate 1.5g；Raspberry extract 0.1g；Water 140ml, in which: 50 DEG C of warm water 70ml；Cold water
70ml.The esterification degree of the low-ester pectin is lower than 60%.The glycerol, sodium alginate, low-ester pectin and calcium lactate are food-grade
Raw material.Flavones content >=25% in the raspberry extract.Preparation method is the same as 1 the method for embodiment.
Embodiment 3: a kind of edible crystal mask is prepared: low-ester pectin 0.6g by the raw material of following weight；Glycerol
0.1g；Sodium alginate 0.15g；Calcium gluconate 1g；Raspberry extract 0.01g；Water 130ml, in which: 60 DEG C of warm water 65ml；
Cold water 65ml.The esterification degree of the low-ester pectin is lower than 60%.The glycerol, sodium alginate, low-ester pectin and calcium gluconate are equal
For food grade materials.Flavones content >=25% in the raspberry extract.Preparation method is the same as 1 the method for embodiment.
Embodiment 4: a kind of edible crystal mask is prepared: low-ester pectin 0.7g by the raw material of following weight；Glycerol
2.5g；Sodium alginate 0.5g；Calcium chloride 1.2g；Raspberry extract 0.08g；Water 120ml, in which: 50 DEG C of warm water 65ml；Cold water
55ml.The esterification degree of the low-ester pectin is lower than 60%.The glycerol, sodium alginate, low-ester pectin and calcium chloride are food-grade
Raw material.Flavones content >=25% in the raspberry extract.The addition of natural function cosmetics is added in preparation method step (3)
Agent, such as white-skinned face function raw material, light spot Effect raw material, crease-resistant Effect raw material, antiallergy Effect raw material, oil-control Effect raw material or anti-acne
Effect raw material, milk or honey etc..Preparation method is the same as 1 the method for embodiment.
Experimental example 1: the physical and chemical index of edible crystal mask prepared by embodiment 1 and embodiment 2 is measured, is tied
Fruit is shown in Table 1.
Table 1: embodiment 1 prepares the physical and chemical index of facial mask powder with embodiment 2
Experimental example 2: the edible crystal mask prepared to embodiment 1 and embodiment 2 carries out using effect measurement.Specifically such as
Under: as a control group with the non-woven fabrics (glycerol containing 1.5%) of wetting, 20 people are randomly selected, forms facial mask organoleptic detection group.
The moisture content value and the variation of oil content value of skin are carried out in 20 minutes front and backs of overlay film with digital skin water content detection pen test panelists,
Mean change amount is calculated, the results are shown in Table 2.The higher the better for the moisture content value of skin, in the variation of skin moisture value, embodiment 2
Moisturizing effect be better than embodiment 1, the moisturizing effect of embodiment 1 is better than control group；The lower the oil content value of skin the better, in skin
In the variation of oil content value, the oil-control effect of embodiment 2 is better than embodiment 1, and the oil-control effect of embodiment 1 is better than control group.
The moisturizing oil-control using effect of 2: three groups of facial masks of table
The online questionnaire investigation records people made of questionnaire star platform evaluate and test the sense organ of three kinds of facial masks.During the results are shown in attached figure 3,
Lines with diamond indicia represent control group facial mask, and the lines with square indicia represent 1 facial mask of embodiment, have triangle
The lines of shape label represent 2 facial mask of embodiment, which has a docile property, comfort, water moisture feeling, stick soapy feeling, absorbability, smell, outside
This 7 indexs are seen, fractional value is higher from the inside to surface, and the satisfaction for representing the index is better.It can be clearly from the radar map
Out, the level of each index of 2 facial mask of embodiment is very nearly the same, belongs to higher level；The each index of 1 facial mask of embodiment is omited
Height, and lines are recessed at smell index, represents that its smell is bad, and score is low；The lines of control group facial mask are unevenly distributed
It is even, hence it is evident that it is recessed at comfort, docile property, water moisture feeling index, represents its comfort and docile property effect is bad, water profit
Feel slightly worse.
Experimental example 3: to edible crystal mask prepared by embodiment 1 and commercially available crystal mask at 55 DEG C of identical water temperature
It prepares, observes its molding situation, as a result see Fig. 4, edible crystal mask prepared by the present invention and commercially available crystal are shown in Fig. 4
Facial mask is prepared at 55 DEG C of identical water temperature, and C is commercial membrane in Fig. 4, can not sprawl film forming in a mold at 55 DEG C, therefore can not
Lifting.Commercially available facial mask film-forming temperature needs to improve can form a film into 90-100 DEG C of boiling water, it is clear that commercially available crystal mask film forming
Temperature is too high, and high temperature is easily destroyed effective component in facial mask, causes the anti-oxidant, anti-inflammatory of facial mask, Bearberry Extract that will reduce
It even disappears, leads to not the effect of realizing facial mask.
By Fig. 4, it can be concluded that, crystal mask film-forming temperature prepared by the present invention is low, and the high temperature for reducing active principle becomes
Property, degradation the problems such as, and commercially available crystal mask is obviously that can not form a film in 50-70 DEG C of warm water, and filming performance is poor, easily broken
It splits.
Obviously edible face pack filming performance prepared by the present invention is good, it is not easy to prolong raw fracture, pulling force and hardness
It is above commercially available facial mask, while it is relatively low to prepare film-forming temperature, warm water, therefore further improve facial mask applies model
It encloses, is conducive to household, self-control, safety, be not necessarily to high temperature, and can make in the case where such as aircraft etc. is difficult to the ambient conditions for obtaining high-temperature water
With easy to use, application conditions have obtained more mildly, and random raising.
Comparing embodiment 1 and commercially available crystal mask pulling force uphold distance, the several index (see Table 3)s of consistency and elasticity.As a result
It has been shown that, the pulling force and hardness of embodiment 1 are higher than commercially available facial mask, there are significant difference (p < 0.05), illustrate the film of embodiment 1
With better lifting molding effect, it is not easy to fracture of extending.Commercially available crystal mask stretching distance and elasticity are higher than embodiment 1,
There are significant difference (p < 0.05), illustrate that commercially available crystal mask is not easy to lift, molding effect is bad.And it is greatly lowered
Water temperature when preparing has better safety and operability.
3: two groups of facial mask performances of table compare
According to pairing t detection display: identical file, " * " expression significant difference (p < 0.05)。
Experimental example 4: calcium lactate crosslinking is not added to edible crystal mask prepared by embodiment 1 and embodiment 2 and (omits and walks
It is rapid 4), be only in jelly state, stomach-filling mouse.It is embodied as follows: 8 weeks 40 big ICR mouse is randomly divided into 4 groups,
Every group 10.Difference stomach-filling pure water (control group), embodiment 1, embodiment 2 and Leaves From Raspberry extract are (with embodiment 2 daily
Additive amount is identical) each 0.3ml/ of aqueous solution is only.The weight and anury height of measurement mouse after two weeks, calculating body index (BMI=
Weight (KG)/height2(m2)), mouse swimming time (mouse in water temperature be 30 ± 1 DEG C 40cm × 30cm barrel containers
In, weight bearing 0.5% own wt galvanized wire swimming, when mouse Head And Face sinks under the water 8 seconds completely, stopping timing, this is the power of mouse
Exhaust the time).It the results are shown in Table 4, the results show that weight, power exhaust the time to administration group compared with the control group and body refers to after two weeks
Number BMI between there are group difference (p < 0.05), the weight of administration group and BMI substantially reduce (p < 0.05), especially
In embodiment 2 weight compared with before medicine feed no significant difference (p > 0.05)；The power of administration group exhausts the time and extends one times
Above (p < 0.05), illustrate the main component in facial mask component: low-ester pectin, sodium alginate and Leaves From Raspberry extract to
Mouse exception is had no during medicine, and there is control mouse weight, improves the good result of the locomitivity of mouse.
Table 4: the changes of weight and power of mouse exhaust the time before and after medicine feed
Detected and shown according to single factor test Duncan ' s: identical row, same letter indicate group difference it is not significant (p >
0.05), different letters indicate group differences it is significant (p < 0.05)。
Claims (8)
1. a kind of edible crystal mask, it is characterised in that: be prepared by the raw material of following parts by weight: low-ester pectin 0.36-
0.9 part；0.1-3.6 parts of glycerol；0.15-0.6 parts of sodium alginate；1-1.5 parts of calcium lactate；0.01-0.1 parts of raspberry extract；Water
110-140 parts, in which: 60-70 parts of 50 DEG C -60 DEG C of warm water；50-70 parts of cold water.
2. a kind of edible crystal mask according to claim 1, it is characterised in that: prepared by the raw material of following parts by weight
It forms: 0.36 part of low-ester pectin；1.63 parts of glycerol；0.3 part of sodium alginate；1 part of calcium lactate；0.05 part of raspberry extract；Water 110
Part, in which: 60 parts of 50 DEG C -60 DEG C of warm water；50 parts of cold water.
3. a kind of edible crystal mask according to claim 1 or 2, it is characterised in that: the esterification of the low-ester pectin
Degree is lower than 60%.
4. a kind of edible crystal mask according to claim 1 or 2, it is characterised in that: the glycerol, sodium alginate,
Low-ester pectin and calcium lactate are food grade materials.
5. a kind of edible crystal mask according to claim 1 or 2, it is characterised in that: the calcium lactate replaces with chlorine
Change calcium or calcium gluconate.
6. a kind of edible crystal mask according to claim 1 or 2, it is characterised in that: yellow in the raspberry extract
Ketone content >=25%.
7. the method for preparing a kind of edible crystal mask of any of claims 1 or 2, it is characterised in that: steps are as follows:
(1) calcium lactate is soluble in water, obtains solution 1；
(2) glycerol is added in low-ester pectin, sodium alginate and raspberry extract, stirs evenly, obtains mixed material 1；
Mixed material 1 is added in (3) 50 DEG C -60 DEG C of warm water, stirs to being completely dissolved, obtains mixed material 2；
(4) mixed material 2 uniformly pours into facial mask mold, stands 3 minutes, and solution 1 sprays the mixed material 2 in facial mask mold
Completely up to covering, 10 minutes are stood.
8. the method according to claim 7 for preparing edible crystal mask, it is characterised in that: add in step (3) warm water
Enter natural function cosmetic additive agent.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111357991A (en) * | 2020-03-18 | 2020-07-03 | 华熙生物科技股份有限公司 | Edible water-soluble paper and preparation method thereof |
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