CN105794802A - Pesticide composition containing fluazinam and emamectin benzoate - Google Patents
Pesticide composition containing fluazinam and emamectin benzoate Download PDFInfo
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- CN105794802A CN105794802A CN201610240015.4A CN201610240015A CN105794802A CN 105794802 A CN105794802 A CN 105794802A CN 201610240015 A CN201610240015 A CN 201610240015A CN 105794802 A CN105794802 A CN 105794802A
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- fluazinam
- benzoate
- emamectin
- nematicide
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
- A01N43/40—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom six-membered rings
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- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
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- General Health & Medical Sciences (AREA)
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Abstract
The invention discloses a pesticide composition containing fluazinam and emamectin benzoate. The pesticide composition comprises the active ingredients including the fluazinam and the emamectin benzoate and common auxiliary ingredients, wherein the weight ratio of the fluazinam to the emamectin benzoate is (15:1)-(1:1). A large number of indoor and outdoor experiments show that the pesticide composition has the advantages that the significant synergistic effect on multiple diseases, especially, the root rot and the nematode disease which damage agricultural production is achieved, the pesticide using amount is decreased, the residual pesticide amount on crops is decreased, pollution to the environment is reduced, generation of the pesticide resistance of the diseases is delayed, and the service life of the pesticide is prolonged.
Description
Technical field
The present invention relates to composition pesticide and application thereof, specifically a kind of with fluazinam and Affirm (Merck Co.) for the composite binary complex of active component, the preventing and treating that is mainly used on crops disease.
Background technology
Fluazinam (Fluazinam) is new substituted phenyl amines, wide-spectrum bactericide, and the mechanism of action is for suppressing the respiratory Mitochondria uncoupling agents of pathogenic bacteria.Pathogen specially good effect to the disease such as banded sclerotial blight and rice blast, wheat sharp eyespot, wheat scab, wheat powdery mildew, fruits and vegetables powdery mildew, downy mildew, gray mold, canker, dry rot, anthrax, ring spot and spot defoliation, anthrachose of grape and skin fester disease causing sclerotinia rot of colza, Oryza sativa L..With the existing antibacterial no interactions resistance in the market such as benzimidazole, dicarboximide class, succinate dehydrogenase inhibitors, electron transport chain Complex II I inhibitor and triazole type.The germ diseases such as interlink spore genus, Phytophthora, Plasmopara, Sclerotinia and Venturia also there is good activity.
Affirm (Merck Co.) (Emamectinbenzoate), it it is a kind of new and effective semisynthetic antibiotics insecticide, there is the feature of ultra high efficiency, low toxicity, low-residual, the biological pesticide such as nuisanceless, neurotic such as the effect of glutamic acid and γ-aminobutyric acid (GABA) by strengthening, a large amount of chloride ion is made to enter insect neurocyte, upset its nerve conduction, make larva that irreversible paralysis to occur, and it is dead to cause it.Affirm (Merck Co.) often exists with the form of benzoate in Pesticidal products.
The individually long-time use continuously of pesticide easily produces resistance risk and consumption increases risk, and then increase cost and carrying capacity of environment, and the compositions with notable synergistic function is filtered out by agriculture chemical compounding, Pesticide use amount can not only be reduced, reduce use cost, reduce resistance risk, moreover it is possible to reduce potential environmental risk.
Summary of the invention
It is desirable to provide a kind of composition pesticide containing fluazinam and Affirm (Merck Co.), said composition has significant synergistic function, can be used for multiple diseases on crops, especially the preventing and treating of root rot and nematicide.
Technical scheme: for achieving the above object, the present invention provides a kind of composition pesticide containing fluazinam and emamectin-benzoate, its weight ratio containing active component fluazinam and emamectin-benzoate, fluazinam and emamectin-benzoate is 15:1～1:1；Active component fluazinam and emamectin-benzoate gross weight percentage composition in the composition is 0.5%～80%, and all the other are allow in pesticide to use and acceptable auxiliary element.
Described auxiliary element is solvent, emulsifying agent, wetting agent, dispersant, stabilizer, antifreezing agent, thickening agent, binding agent, disintegrating agent, defoamer, penetrating agent, macromolecule cyst material, synergist, preservative and filler etc., it it is all conventional in pesticidal preparations or permission use composition, being not particularly limited, concrete composition and consumption are determined by test according to recipe requirements.
Composition pesticide of the present invention can be prepared as the multiple application forms being suitable for agriculturally using, and reasonable dosage form has microcapsule suspending agent, suspending agent, aqueous emulsion, microemulsion, granule, water dispersible granules and wettable powder.
The production technology of the various application forms of described composition pesticide all belongs to existing known technology, does not repeat them here.
Compared with prior art, it is an advantage of the current invention that:
1, fluazinam and emamectin-benzoate is composite has significant synergistic function, is used alone than single dose and significantly improves the prevention effect of disease on crops.
2, fluazinam and two kinds of active component of emamectin-benzoate are composite, decrease Pesticide use amount, reduce use cost, alleviate the pollution to environment.
3, fluazinam and two kinds of active component of emamectin-benzoate are composite, and the mechanism of action is different, and action site increases, and has delayed the generation of disease drug resistance, has added the service life of pesticide.
Detailed description of the invention
In order to be more fully understood that the essence of the present invention; below in conjunction with embodiment, present disclosure is described further; but limitation of the present invention can not be considered as; the following stated is only used for explaining the present invention; for not necessarily departing from amendment, replacement or the improvement that present invention spirit is made with principle, belong to the scope of protection of present invention.
Embodiment one:
Following material is all weight percentage: fluazinam 20%, emamectin-benzoate 4%, sodium carboxymethyl cellulose 3%, poly-hexylamine lactone 2%, tetrahydrofurfuryl alcohol 10%, fatty acid methyl ester 10%, terminal hydroxy group polyoxyethylene poly-oxygen propylene aether 5%, acrylate homopolymer sodium salt 3%, sodium hydroxide 2%, 1,2-benzisothiazole-3-ketone 1%, deionized water complements to 100%.By above-mentioned active component, macromolecule cyst material, solvent mixing, make to be dissolved into homogeneous oil phase, in a shear condition, oil phase is joined containing emulsifying agent, dispersant, pH adjusting agent, preservative aqueous phase solution in, surplus deionized water is supplied, bi-material reacts at oil-water interfaces, forms macromolecule cyst wall, can be prepared by 24% fluazinam emamectin benzoate microcapsule suspending agent.
This embodiment is used for preventing and treating Roots of Peanut maize ear rot and nematicide: 24% fluazinam emamectin benzoate microcapsule suspending agent is by 150ga.i./ha dilute root irrigation, and after medicine, 30d is to the preventive effect of Roots of Peanut maize ear rot and nematicide respectively 95.26%, 93.17%；200ga.i./ha dilute root irrigation pressed by the fluazinam suspending agent of 500g/L, and after medicine, 30d is to the preventive effect of Roots of Peanut maize ear rot and nematicide respectively 76.93%, 27.64%；2% emamectin benzoate suspending agent presses 40ga.i./ha dilute root irrigation, and after medicine, 30d is to the preventive effect of Roots of Peanut maize ear rot and nematicide respectively 13.54%, 72.19%.Visible, obvious synergy after fluazinam and emamectin-benzoate binary built, the lasting period is long, and the preventive effect of Roots of Peanut maize ear rot and nematicide is used alone significantly better than each single dose, meanwhile, in process of the test, do not find that Semen arachidis hypogaeae is produced poisoning by this binary built medicament.
Embodiment two:
Following material is all weight percentage: fluazinam 25%, emamectin-benzoate 5%, alkylphenol-polyethenoxy base ether formaldehyde condensation products sulfate 10%, triphen ethyl phenol polyoxyethylene ether phosphate 5%, acrylate homopolymer sodium salt 5%, propylene glycol 3%, carboxymethyl cellulose 1.5%, tributyl phosphate 0.2%, deionized water supplies 100%.By above-mentioned active component, wetting agent, dispersant, antifreezing agent, thickening agent and defoamer sand milling in high speed shear dispersion, sand mill, the high dispersive formed in water-medium, stable suspension system, can be prepared by 30% fluazinam emamectin benzoate suspending agent.
This embodiment is used for preventing and treating Fusarium solani and nematicide: 30% fluazinam emamectin benzoate suspending agent is by 150ga.i./ha dilute root irrigation, and after medicine, 30d is to the preventive effect of Fusarium solani and nematicide respectively 91.34%, 94.56%；200ga.i./ha dilute root irrigation pressed by the fluazinam suspending agent of 500g/L, and after medicine, 30d is to the preventive effect of Fusarium solani and nematicide respectively 78.31%, 27.87%；2% emamectin benzoate suspending agent presses 40ga.i./ha dilute root irrigation, and after medicine, 30d is to the preventive effect of Fusarium solani and nematicide respectively 15.91%, 73.89%.Visible, obvious synergy after fluazinam and emamectin-benzoate binary built, the lasting period is long, and the preventive effect of Fusarium solani and nematicide is used alone significantly better than each single dose, meanwhile, in process of the test, do not find that Fructus Capsici is produced poisoning by this binary built medicament.
Embodiment three:
Following material is all weight percentage: fluazinam 35%, emamectin-benzoate 5%, trimethylbenzene 10%, tetrahydrofurfuryl alcohol 5%, polyol fatty acid ester and ethylene oxide adduct 10%, p-hydroxyphenyl lignin sulfonic acid sodium salt 3%, the formaldehyde condensation products 3% of methyl naphthalene sulfonic acid sodium, epoxychloropropane 1%, HPMC 2%, glycerol 1%, deionized water supplies 100%.Above-mentioned active component, solvent, emulsifying agent, dispersant, stabilizer and thickening agent are mixed to form oil phase, antifreezing agent dissolves formation aqueous phase in water, slowly oil phase is added in aqueous phase under cutter effect, and continue to shear about 30 minutes, prepare the fluazinam emamectin-benzoate aqueous emulsion of 40%.
This embodiment is used for preventing and treating Tobacco Root maize ear rot and nematicide: 40% fluazinam emamectin-benzoate aqueous emulsion is by 150ga.i./ha dilute root irrigation, and after medicine, 30d is to the preventive effect of Tobacco Root maize ear rot and nematicide respectively 94.61%, 97.25%；200ga.i./ha dilute root irrigation pressed by the fluazinam suspending agent of 500g/L, and after medicine, 30d is to the preventive effect of Tobacco Root maize ear rot and nematicide respectively 77.14%, 20.27%；2% emamectin benzoate suspending agent presses 40ga.i./ha dilute root irrigation, and after medicine, 30d is to the preventive effect of Tobacco Root maize ear rot and nematicide respectively 17.54%, 72.93%.Visible, obvious synergy after fluazinam and emamectin-benzoate binary built, the lasting period is long, and the preventive effect of Tobacco Root maize ear rot and nematicide is used alone significantly better than each single dose, meanwhile, in process of the test, do not find that Nicotiana tabacum L. is produced poisoning by this binary built medicament.
Embodiment four:
Following material is all weight percentage: fluazinam 37%, emamectin-benzoate 8%, trimethylbenzene 10%, tetrahydrofurfuryl alcohol 5%, triphen ethyl phenol polyoxyethylene groups ether phosphate 10%, triphenyl phosphite 1%, organosilicon 1%, propyl isome 2%, hydroxymethyl cellulose 2%, deionized water supplies 100%.Active component solvent is completely dissolved, then adds emulsifying agent, stabilizer, penetrating agent, synergist, thickening agent mix homogeneously, be eventually adding deionized water, after being sufficiently stirred for, can be prepared by the fluazinam emamectin benzoate microemulsion of 45%.
This embodiment is used for preventing and treating root rot and nematicide: 45% fluazinam emamectin benzoate microemulsion is by 150ga.i./ha dilute root irrigation, and after medicine, 30d is to the preventive effect of root rot and nematicide respectively 95.17%, 91.62%；200ga.i./ha dilute root irrigation pressed by the fluazinam suspending agent of 500g/L, and after medicine, 30d is to the preventive effect of root rot and nematicide respectively 79.02%, 27.15%；2% emamectin benzoate suspending agent presses 40ga.i./ha dilute root irrigation, and after medicine, 30d is to the preventive effect of root rot and nematicide respectively 16.87%, 76.91%.Visible, obvious synergy after fluazinam and emamectin-benzoate binary built, the lasting period is long, and the preventive effect of root rot and nematicide is used alone significantly better than each single dose, meanwhile, in process of the test, do not find that Semen sojae atricolor is produced poisoning by this binary built medicament.
Embodiment five:
Following material is all weight percentage: fluazinam 0.9%, emamectin-benzoate 0.1%, Teepol 10%, terminal hydroxy group polyoxyethylene poly-oxygen propylene aether block copolymer 10%, triphen ethyl phenol polyoxyethylene ether phosphate 15%, carboxymethyl cellulose 5%, fine particle calcium carbonate 5%, Kaolin complements to 100%.Blended to above-mentioned active component, wetting agent, dispersant, binding agent and filler adding water is mediated; pinch-out granulator is used to pinch out and shape; afterwards by granule fluid bed drying, screening, can be prepared by 1% fluazinam emamectin-benzoate granule.
This embodiment is used for preventing and treating bird watching root rot and nematicide: 1% fluazinam emamectin-benzoate granule spreads fertilizer over the fields process by 150ga.i./ha, and after medicine, 30d is to the preventive effect of bird watching root rot and nematicide respectively 92.48%, 90.79%；200ga.i./ha dilute root irrigation pressed by the fluazinam suspending agent of 500g/L, and after medicine, 30d is to the preventive effect of bird watching root rot and nematicide respectively 74.13%, 22.95%；2% emamectin benzoate suspending agent presses 40ga.i./ha dilute root irrigation, and after medicine, 30d is to the preventive effect of bird watching root rot and nematicide respectively 21.17%, 78.54%.Visible, obvious synergy after fluazinam and emamectin-benzoate binary built, the lasting period is long, and the preventive effect of bird watching root rot and nematicide is used alone significantly better than each single dose, meanwhile, in process of the test, do not find that bird watching is produced poisoning by this binary built medicament.
Embodiment six:
Following material is all weight percentage: fluazinam 60%, emamectin-benzoate 10%, Teepol 5%, acrylate homopolymer sodium salt 5%, low-substituted hydroxypropyl cellulose 5%, white carbon 5%, Kaolin supplies 100%.By above-mentioned effective ingredient, wetting agent, dispersant, disintegrating agent and filler mix homogeneously, pulverize with micro jet, through mediating, it is subsequently adding in fluidized-bed granulation dryer and carries out pelletize, dry, screening, can be prepared by 70% fluazinam emamectin-benzoate water dispersible granules.
This embodiment is used for preventing and treating Radix Ginseng maize ear rot and nematicide: 70% fluazinam emamectin-benzoate water dispersible granules is by 150ga.i./ha dilute root irrigation, and after medicine, 30d is to the preventive effect of Radix Ginseng maize ear rot and nematicide respectively 97.32%, 94.56%；200ga.i./ha dilute root irrigation pressed by the fluazinam suspending agent of 500g/L, and after medicine, 30d is to the preventive effect of Radix Ginseng maize ear rot and nematicide respectively 71.15%, 20.24%；2% emamectin benzoate suspending agent presses 40ga.i./ha dilute root irrigation, and after medicine, 30d is to the preventive effect of Radix Ginseng maize ear rot and nematicide respectively 19.34%, 75.91%.Visible, obvious synergy after fluazinam and emamectin-benzoate binary built, the lasting period is long, and the preventive effect of Radix Ginseng maize ear rot and nematicide is used alone significantly better than each single dose, meanwhile, in process of the test, do not find that Radix Ginseng is produced poisoning by this binary built medicament.
Embodiment seven:
Following material is all weight percentage: fluazinam 65%, emamectin-benzoate 10%, Teepol 5%, alkyl phenol resin polyoxyethylene ether sulfate 5%, triphen ethyl phenol polyoxyethylene ether phosphate 5%, white carbon 5%, kieselguhr supplies 100%.By above-mentioned, effective ingredient, wetting agent, dispersant and filler are mixed, then through comminution by gas stream after mechanical activation comminution, mix homogeneously, can be prepared by 75% fluazinam emamectin-benzoate wettable powder.
This embodiment is used for preventing and treating notoginseng root rot and nematicide: 75% fluazinam emamectin-benzoate wettable powder is by 150ga.i./ha dilute root irrigation, and after medicine, 30d is to the preventive effect of notoginseng root rot and nematicide respectively 93.38%, 91.87%；200ga.i./ha dilute root irrigation pressed by the fluazinam suspending agent of 500g/L, and after medicine, 30d is to the preventive effect of notoginseng root rot and nematicide respectively 76.72%, 21.45%；2% emamectin benzoate suspending agent presses 40ga.i./ha dilute root irrigation, and after medicine, 30d is to the preventive effect of notoginseng root rot and nematicide respectively 11.85%, 73.69%.Visible, obvious synergy after fluazinam and emamectin-benzoate binary built, the lasting period is long, and the preventive effect of notoginseng root rot and nematicide is used alone significantly better than each single dose, meanwhile, in process of the test, do not find that Radix Notoginseng is produced poisoning by this binary built medicament.
Embodiment eight: fluazinam and the composite Toxicity Determination test that Semen arachidis hypogaeae is obstructed maize ear rot of emamectin-benzoate.
Test method, with reference to " antibacterial indoor bioassay test rule NY/T1156.2-2006 ", adopts mycelial growth rate method.Judging synergism by co-toxicity coefficient method, co-toxicity coefficient (CTC) >=120 shows as potentiation；Co-toxicity coefficient (CTC)≤80 shows as antagonism；80 < co-toxicity coefficient (CTC) < 120 show as summation action.
Semen arachidis hypogaeae is obstructed the indoor joint toxicity measuring result of maize ear rot by table 1, fluazinam and emamectin-benzoate
| Medicament title and proportioning (weight ratio) | EC50(mg/L) | ATI | TTI | CTC |
| Fluazinam | 1.13 | 100.00 | - | - |
| Emamectin-benzoate | 108.34 | 1.04 | - | - |
| Fluazinam: emamectin-benzoate (15:1) | 0.73 | 154.79 | 93.82 | 164.99 |
| Fluazinam: emamectin-benzoate (10:1) | 0.68 | 166.18 | 91.00 | 182.62 |
| Fluazinam: emamectin-benzoate (7:1) | 0.62 | 182.26 | 87.63 | 207.99 |
| Fluazinam: emamectin-benzoate (5:1) | 0.57 | 198.25 | 83.51 | 237.40 |
| Fluazinam: emamectin-benzoate (3:1) | 0.71 | 159.15 | 75.26 | 211.47 |
| Fluazinam: emamectin-benzoate (1:1) | 1.17 | 96.58 | 50.52 | 191.17 |
As can be seen from Table 1, when fluazinam and emamectin-benzoate are composite in the proportion of 15:1～1:1 (by weight), co-toxicity coefficient (CTC) is all higher than 120, Semen arachidis hypogaeae is obstructed maize ear rot and all shows synergistic function, especially fluazinam and emamectin-benzoate are composite with 5:1 (by weight), synergistic function is the most notable, and co-toxicity coefficient (CTC) is 237.40.Visible, fluazinam and emamectin-benzoate is composite has reasonability and feasibility.
Embodiment nine: fluazinam and the composite Toxicity Determination to Fructus Capsici nematicide of emamectin-benzoate are tested.
Test method: first take the Fructus Capsici root system producing a large amount of root knots, rinse well gently with tap water, followed by the milky egg capsule on dissecting needle gently picking old complaint, put into the little culture dish of diameter 6cm, add a small amount of sterilized water, 25 DEG C of calorstats are hatched 3～4d, collects 2 instar larvaes, and adding sterilized water, to be configured to the suspension of finite concentration (500/about ml) standby.
Set 5 Concentraton gradient to process, with sterilized water for blank.Take 96 porocyte culture plates, every hole adds medicament 150 microlitre of the variable concentrations prepared, add isopyknic nematicide suspension, under 25 DEG C of conditions, moisturizing is cultivated, the amount of survival of 48h microscopy nematicide and dead quantity after treatment, nematicide is stiff motionless for dead worm, and nematicide is the worm that lives in bending wriggling state.Calculate mortality rate and corrected mortality.
Carry out statistical analysis with DPS statistical analysis software, calculate the EC of each medicament50, and judging synergism according to by co-toxicity coefficient method, co-toxicity coefficient (CTC) >=120 shows as potentiation；Co-toxicity coefficient (CTC)≤80 shows as antagonism；80 < co-toxicity coefficient (CTC) < 120 show as summation action.
Table 2, fluazinam and the emamectin-benzoate indoor joint toxicity measuring result to Fructus Capsici nematicide
| Medicament title and proportioning (weight ratio) | EC50(mg/L) | ATI | TTI | CTC |
| Fluazinam | 34.51 | 100.00 | - | - |
| Emamectin-benzoate | 7.85 | 439.62 | - | - |
| Fluazinam: emamectin-benzoate (15:1) | 16.12 | 214.08 | 121.23 | 176.59 |
| Fluazinam: emamectin-benzoate (10:1) | 13.31 | 259.28 | 130.87 | 198.12 |
| Fluazinam: emamectin-benzoate (7:1) | 10.97 | 314.59 | 142.45 | 220.84 |
| Fluazinam: emamectin-benzoate (5:1) | 8.69 | 397.12 | 156.60 | 253.59 |
| Fluazinam: emamectin-benzoate (3:1) | 8.24 | 418.81 | 184.91 | 226.49 |
| Fluazinam: emamectin-benzoate (1:1) | 7.03 | 490.90 | 269.81 | 181.94 |
As can be seen from Table 2, when fluazinam and emamectin-benzoate are composite in the proportion of 15:1～1:1 (by weight), co-toxicity coefficient (CTC) is all higher than 120, Fructus Capsici nematicide is all shown synergistic function, especially fluazinam and emamectin-benzoate are composite with 5:1 (by weight), synergistic function is the most notable, and co-toxicity coefficient (CTC) is 253.59.Visible, fluazinam and emamectin-benzoate is composite has reasonability and feasibility.
In sum, a kind of composition pesticide containing fluazinam and Affirm (Merck Co.) provided by the invention, obvious synergy, compared with existing unitary agent, to the multiple diseases on crops, especially the prevention effect of root rot and nematicide significantly improves, and to crop safety, is worth in agricultural production popularization and application.
Claims (4)
1. the composition pesticide containing fluazinam and Affirm (Merck Co.), it is characterised in that: the weight ratio including active component fluazinam and emamectin-benzoate, fluazinam and emamectin-benzoate is 15:1～1:1.
2. a kind of composition pesticide containing fluazinam and Affirm (Merck Co.) according to claim 1, it is characterized in that: fluazinam and emamectin-benzoate gross weight percentage composition in the composition is 0.5%～80%, all the other are allow in pesticide to use and receptible auxiliary element.
3. a kind of composition pesticide containing fluazinam and Affirm (Merck Co.) according to claim 1 and 2, it is characterised in that: the dosage form of described composition pesticide is the one in microcapsule suspending agent, suspending agent, aqueous emulsion, microemulsion, granule, water dispersible granules and wettable powder.
4. the application in root rot and nematicide on preventing and treating crops of a kind of composition pesticide containing fluazinam and Affirm (Merck Co.) described in claim 1.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110800741A (en) * | 2019-12-06 | 2020-02-18 | 李玉洁 | Efficient pesticide for preventing and treating field red spiders and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102802422A (en) * | 2009-06-17 | 2012-11-28 | 石原产业株式会社 | Control Agent For Soft Rot And Control Method For The Same |
| CN103202306A (en) * | 2013-04-28 | 2013-07-17 | 柳州市惠农化工有限公司 | Pesticide composition |
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102802422A (en) * | 2009-06-17 | 2012-11-28 | 石原产业株式会社 | Control Agent For Soft Rot And Control Method For The Same |
| CN103202306A (en) * | 2013-04-28 | 2013-07-17 | 柳州市惠农化工有限公司 | Pesticide composition |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110800741A (en) * | 2019-12-06 | 2020-02-18 | 李玉洁 | Efficient pesticide for preventing and treating field red spiders and preparation method thereof |
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Application publication date: 20160727 |