CN105780181A - Method for manufacturing high-wet-permeability heat-preservation fiber - Google Patents
Method for manufacturing high-wet-permeability heat-preservation fiber Download PDFInfo
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- CN105780181A CN105780181A CN201610208909.5A CN201610208909A CN105780181A CN 105780181 A CN105780181 A CN 105780181A CN 201610208909 A CN201610208909 A CN 201610208909A CN 105780181 A CN105780181 A CN 105780181A
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- wet
- bamboo charcoal
- charcoal powder
- permeability
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
- D01F6/88—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds
- D01F6/92—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds of polyesters
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
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- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Textile Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention relates to a method for manufacturing high-wet-permeability heat-preservation fiber. The method comprises the following steps: I, pre-carbonizing bamboo charcoal powder; II, activating the bamboo charcoal powder; III, preparing so as to obtain nano bamboo charcoal powder; IV, uniformly mixing polyester chips, a silane coupling agent, zinc stearate as a surfactant and liquid wax so as to obtain molten polyester; V, uniformly mixing the bamboo charcoal powder, a hydrophilic wet-permeation finishing agent and the molten polyester according to a ratio so as to obtain a mixture; VI, pelletizing the mixture by using a pelletizer so as to obtain master batch; VII, uniformly mixing the master batch with the polyester chips, and performing melt spinning so as to obtain high-wet-permeability heat-preservation fiber yarns; and VIII, drafting and coiling the high-wet-permeability heat-preservation fiber yarns obtained in the step VII, thereby obtaining long high-wet-permeability heat-preservation fiber yarns. The method for manufacturing high-wet-permeability heat-preservation fiber, provided by the invention, has the advantage that functional fiber which is soft and comfortable in body feeling, good in air permeability and free of body sticking feeling, good in heat preservation, good in wet permeability and automatic in temperature and humidity adjustment can be manufactured.
Description
Technical field
The present invention relates to a kind of functional fibre fabric, be specially a kind of high manufacture method leading wet thermal fiber.
Background technology
Along with the raising of people's living standard, the fabric being used for making underwear is had higher requirement, does not require nothing more than durable, and require to have higher warmth retention property, skin-friendly and comfort level, also need to have stronger suction, wet transmitting performance, good springiness simultaneously.
At present, commercially available underwear fabric, although disclosure satisfy that the requirement of people in some aspects, but, also need to further raising generally.
Summary of the invention
For the deficiencies in the prior art, the technical problem that the present invention intends to solve is to provide a kind of high manufacture method leading wet thermal fiber, will possess body-sensing soft comfortable, ventilative without viscous body sense, warming, lead the wet functional fibre being automatically adjusted humiture.
To achieve these goals, the present invention adopts the following technical scheme that a kind of high manufacture method leading wet thermal fiber, comprises the steps:
Step one, the mixing of bamboo charcoal powder, dispersant and softening water is made bamboo carbon powder serum is kept 20min at the temperature of 400～450 DEG C by grinding so that bamboo charcoal powder obtains pre-carbonization；
Step 2, the bamboo charcoal powder after pre-carbonization is carried out at the temperature of about 1800 DEG C activation processing, after carrying out activation processing, make bamboo charcoal powder form cellular loose structure；
Step 3, step 2 is prepared bamboo charcoal powder nanorize it is processed into the bamboo-carbon powder of 50～100 nanometers；
Step 4, preparing and hydrophilic lead dressing agent, this is hydrophilic leads dressing agent and includes the component of following parts by weight:
Polyox-yethylene-polyoxypropylene block copolymer 4-10 part
Organic silicon modified polyurethane resin 10-15 part
Ethylene bis stearamide 15-20 part
Diboron trioxide 3-6 part
Fatty alcohol-polyoxyethylene ether 2-8 part
Firming agent 10-12 part
Microfine diatomaceous 1-4 part
Nano silicon 7-15 part
Nano magnesia 3-6 part
Aluminium chloride hexahydrate 8-10 part
Vitamin E2-3 parts
Solvent 50-100 part；
Step 5, polyester slice, silane coupler, zinc stearate and liquid wax as surfactant are at high temperature uniformly mixed to form the polyester thing of molten according to 100: 2～5: 4～6: 9～10 mass ratios；
Step 6, described bamboo-carbon powder, the hydrophilic polyester thing leading dressing agent and molten are uniformly mixed to form mixture according to 1: 1: 8-12 mass ratio；
Step 7, by described mixture through comminutor weaving formed master batch；
Step 8, by described master batch again with polyester slice according to after 1: 20～45 mass ratio Homogeneous phase mixing and form height through melt spinning and lead wet thermal fiber silk；
Step 9, by step 8 obtain described height lead wet thermal fiber silk through drawing-off winding formed height lead wet thermal fiber long filament.
Preferably, described hydrophilic lead dressing agent and preferably include the component of following weight portion:
Polyox-yethylene-polyoxypropylene block copolymer 7 parts
Organic silicon modified polyurethane resin 12 parts
Ethylene bis stearamide 18 parts
Diboron trioxide 5 parts
Fatty alcohol-polyoxyethylene ether 5 parts
11 parts of firming agent
Microfine diatomaceous 2 parts
Nano silicon 12 parts
Nano magnesia 5 parts
Aluminium chloride hexahydrate 9 parts
Vitamin E2 .5 part
Solvent 75 parts.
Preferably, it is the 3 ~ 6% of total weight of fiber that described height leads bamboo charcoal content in wet thermal fiber, leads wet rate >=70%, breathability >=800mm/s.
This fiber above-mentioned, temperature value as required: in the hydrophilic various material mixture ratios leading dressing agent and fiber manufacture process, by constant for material, predetermined temperature, the structure and the performance that vary with temperature material have reversibility, when temperature raises or reduces, material can carry out self regulation along curve automatically, and reaches " intellectuality " hotness conduction temperature adjustment function.
Compared with the prior art, the superiority of technical solution of the present invention is:
1, the fiber of this structure, fastness is good, wash resistant, even if extexine fiber galls, function powder material is without running off easily, and hotness conduction memory function is lasting.
2, this fiber, extexine is very thin, soft comfortable is as good as with natural fiber.
3, this fiber, continues warmth sensation at low temperatures and conducts considerably beyond its synthetic fibers and the insulation of natural fiber, warming effect, be 3 times of its synthetic fibers, 8 times of natural fiber.
4, this fiber, takes out in ice cold water, and contact skin moment is warm.
Detailed description of the invention
By the examples below, technical scheme is described in further detail.
Embodiment one:
A kind of high manufacture method leading wet thermal fiber, it is characterised in that this manufacture method is undertaken by following technique:
Step one, the mixing of bamboo charcoal powder, dispersant and softening water is made bamboo carbon powder serum is kept 20min at the temperature of 400 DEG C by grinding so that bamboo charcoal powder obtains pre-carbonization；
Step 2, the bamboo charcoal powder after pre-carbonization is carried out at the temperature of about 1800 DEG C activation processing, after carrying out activation processing, make bamboo charcoal powder form cellular loose structure；
Step 3, step 2 is prepared bamboo charcoal powder nanorize it is processed into the bamboo-carbon powder of 50 nanometers；
Step 4, preparing and hydrophilic lead dressing agent, this is hydrophilic leads dressing agent and includes the component of following parts by weight:
Polyox-yethylene-polyoxypropylene block copolymer 4 parts
Organic silicon modified polyurethane resin 10 parts
Ethylene bis stearamide 15 parts
Diboron trioxide 3 parts
Fatty alcohol-polyoxyethylene ether 2 parts
10 parts of firming agent
Microfine diatomaceous 1 part
Nano silicon 7 parts
Nano magnesia 3 parts
Aluminium chloride hexahydrate 8 parts
Vitamin E2 part
Solvent 50 parts；
Step 5, polyester slice, silane coupler, zinc stearate and liquid wax as surfactant are at high temperature uniformly mixed to form the polyester thing of molten according to 100: 2: 4: 9 mass ratios；
Step 6, described bamboo-carbon powder, the hydrophilic polyester thing leading dressing agent and molten are uniformly mixed to form mixture according to 1: 1: 8 mass ratio；
Step 7, by described mixture through comminutor weaving formed master batch；
Step 8, by described master batch again with polyester slice according to after 1: 20 mass ratio Homogeneous phase mixing and form height through melt spinning and lead wet thermal fiber silk；
Step 9, by step 8 obtain described height lead wet thermal fiber silk through drawing-off winding formed height lead wet thermal fiber long filament.
After tested, it is the 3% of total weight of fiber that described height leads bamboo charcoal content in wet thermal fiber, and leading wet rate is 82%, and breathability is 950mm/s.
Embodiment two:
A kind of high manufacture method leading wet thermal fiber, it is characterised in that this manufacture method is undertaken by following technique:
Step one, the mixing of bamboo charcoal powder, dispersant and softening water is made bamboo carbon powder serum is kept 20min at the temperature of 450 DEG C by grinding so that bamboo charcoal powder obtains pre-carbonization；
Step 2, the bamboo charcoal powder after pre-carbonization is carried out at the temperature of about 1800 DEG C activation processing, after carrying out activation processing, make bamboo charcoal powder form cellular loose structure；
Step 3, step 2 is prepared bamboo charcoal powder nanorize it is processed into the bamboo-carbon powder of 100 nanometers；
Step 4, preparing and hydrophilic lead dressing agent, this is hydrophilic leads dressing agent and includes the component of following parts by weight:
Polyox-yethylene-polyoxypropylene block copolymer 10 parts
Organic silicon modified polyurethane resin 15 parts
Ethylene bis stearamide 20 parts
Diboron trioxide 6 parts
Fatty alcohol-polyoxyethylene ether 8 parts
12 parts of firming agent
Microfine diatomaceous 4 parts
Nano silicon 15 parts
Nano magnesia 6 parts
Aluminium chloride hexahydrate 10 parts
Vitamin E 3 parts
Solvent 100 parts；
Step 5, polyester slice, silane coupler, zinc stearate and liquid wax as surfactant are at high temperature uniformly mixed to form the polyester thing of molten according to 100: 5: 6: 10 mass ratios；
Step 6, described bamboo-carbon powder, the hydrophilic polyester thing leading dressing agent and molten are uniformly mixed to form mixture according to 1: 1: 12 mass ratio；
Step 7, by described mixture through comminutor weaving formed master batch；
Step 8, by described master batch again with polyester slice according to after 1: 45 mass ratio Homogeneous phase mixing and form height through melt spinning and lead wet thermal fiber silk；
Step 9, by step 8 obtain described height lead wet thermal fiber silk through drawing-off winding formed height lead wet thermal fiber long filament.
After tested, it is the 5.8% of total weight of fiber that described height leads bamboo charcoal content in wet thermal fiber, and leading wet rate is 94%, and breathability is 1000mm/s.
The above; it is only the specific embodiment of the present invention; but protection scope of the present invention is not limited thereto; any those of ordinary skill in the art are in the technical scope that disclosed herein; the change can expected without creative work or replacement, all should be encompassed within protection scope of the present invention.Therefore, protection scope of the present invention should be as the criterion with claims protection defined.
Claims (3)
1. the one kind high manufacture method leading wet thermal fiber, it is characterised in that comprise the following steps:
Step one, the mixing of bamboo charcoal powder, dispersant and softening water is made bamboo carbon powder serum is kept about 20min at the temperature of 400～450 DEG C by grinding so that bamboo charcoal powder obtains pre-carbonization；
Step 2, the bamboo charcoal powder after pre-carbonization is carried out at the temperature of about 1800 DEG C activation processing, after carrying out activation processing, make bamboo charcoal powder form cellular loose structure；
Step 3, step 2 is prepared bamboo charcoal powder nanorize it is processed into the bamboo-carbon powder of 50～100 nanometers；
Step 4, preparing and hydrophilic lead dressing agent, this is hydrophilic leads dressing agent and includes the component of following parts by weight:
Polyox-yethylene-polyoxypropylene block copolymer 4-10 part
Organic silicon modified polyurethane resin 10-15 part
Ethylene bis stearamide 15-20 part
Diboron trioxide 3-6 part
Fatty alcohol-polyoxyethylene ether 2-8 part
Firming agent 10-12 part
Microfine diatomaceous 1-4 part
Nano silicon 7-15 part
Nano magnesia 3-6 part
Aluminium chloride hexahydrate 8-10 part
Vitamin E2-3 parts
Solvent 50-100 part；
Step 5, polyester slice, silane coupler, zinc stearate and liquid wax as surfactant are at high temperature uniformly mixed to form the polyester thing of molten according to 100: 2～5: 4～6: 9～10 mass ratios；
Step 6, described bamboo-carbon powder, the hydrophilic polyester thing leading dressing agent and molten are uniformly mixed to form mixture according to 1: 1: 8-12 mass ratio；
Step 7, by described mixture through comminutor weaving formed master batch；
Step 8, by described master batch again with polyester slice according to after 1: 20～45 mass ratio Homogeneous phase mixing and form height through melt spinning and lead wet thermal fiber silk；
Step 9, by step 8 obtain described height lead wet thermal fiber silk through drawing-off winding formed height lead wet thermal fiber long filament.
2. a kind of high manufacture method leading wet thermal fiber according to claim 1, it is characterised in that: described hydrophilic lead dressing agent and preferably include the component of following weight portion:
Polyox-yethylene-polyoxypropylene block copolymer 7 parts
Organic silicon modified polyurethane resin 12 parts
Ethylene bis stearamide 18 parts
Diboron trioxide 5 parts
Fatty alcohol-polyoxyethylene ether 5 parts
11 parts of firming agent
Microfine diatomaceous 2 parts
Nano silicon 12 parts
Nano magnesia 5 parts
Aluminium chloride hexahydrate 9 parts
Vitamin E2 .5 part
Solvent about 75 parts.
3. a kind of high manufacture method leading wet thermal fiber according to claim 1 and 2, it is characterised in that: it is the 3 ~ 6% of total weight of fiber that described height leads bamboo charcoal content in wet thermal fiber, leads wet rate >=70%, breathability >=800mm/s.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610208909.5A CN105780181A (en) | 2016-04-06 | 2016-04-06 | Method for manufacturing high-wet-permeability heat-preservation fiber |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610208909.5A CN105780181A (en) | 2016-04-06 | 2016-04-06 | Method for manufacturing high-wet-permeability heat-preservation fiber |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105780181A true CN105780181A (en) | 2016-07-20 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610208909.5A Pending CN105780181A (en) | 2016-04-06 | 2016-04-06 | Method for manufacturing high-wet-permeability heat-preservation fiber |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108193315A (en) * | 2017-12-18 | 2018-06-22 | 杭州泰富纺织化纤有限公司 | A kind of preparation method of unstressed configuration diatomite anti-bacterial fibre |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101215729A (en) * | 2008-01-10 | 2008-07-09 | 孙嘉良 | Binchotan fibre |
| CN102154715A (en) * | 2010-02-11 | 2011-08-17 | 浙江三马锦纶科技股份有限公司 | Bamboo charcoal profiled fiber and preparation method thereof |
| CN103882551A (en) * | 2014-04-13 | 2014-06-25 | 临沂市裕成纺织有限公司 | Bamboo charcoal polyester fiber and preparation technology thereof |
| CN104389100A (en) * | 2014-11-29 | 2015-03-04 | 滁州惠智科技服务有限公司 | Fluorescent sunscreen fabric production method |
-
2016
- 2016-04-06 CN CN201610208909.5A patent/CN105780181A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101215729A (en) * | 2008-01-10 | 2008-07-09 | 孙嘉良 | Binchotan fibre |
| CN102154715A (en) * | 2010-02-11 | 2011-08-17 | 浙江三马锦纶科技股份有限公司 | Bamboo charcoal profiled fiber and preparation method thereof |
| CN103882551A (en) * | 2014-04-13 | 2014-06-25 | 临沂市裕成纺织有限公司 | Bamboo charcoal polyester fiber and preparation technology thereof |
| CN104389100A (en) * | 2014-11-29 | 2015-03-04 | 滁州惠智科技服务有限公司 | Fluorescent sunscreen fabric production method |
Non-Patent Citations (1)
| Title |
|---|
| 杨建忠: "《新型纺织材料及应用》", 31 October 2011, 东华大学出版社 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108193315A (en) * | 2017-12-18 | 2018-06-22 | 杭州泰富纺织化纤有限公司 | A kind of preparation method of unstressed configuration diatomite anti-bacterial fibre |
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Application publication date: 20160720 |