CN105733697A - Environment-friendly graft chloroprene rubber and corn oil hybrid fuel oil and preparation method thereof - Google Patents
Environment-friendly graft chloroprene rubber and corn oil hybrid fuel oil and preparation method thereof Download PDFInfo
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- CN105733697A CN105733697A CN201610111618.4A CN201610111618A CN105733697A CN 105733697 A CN105733697 A CN 105733697A CN 201610111618 A CN201610111618 A CN 201610111618A CN 105733697 A CN105733697 A CN 105733697A
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/02—Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
- C10L1/14—Organic compounds
- C10L1/18—Organic compounds containing oxygen
- C10L1/192—Macromolecular compounds
- C10L1/195—Macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- C10L1/197—Macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds derived from monomers containing a carbon-to-carbon unsaturated bond and an acyloxy group of a saturated carboxylic or carbonic acid
- C10L1/1973—Macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds derived from monomers containing a carbon-to-carbon unsaturated bond and an acyloxy group of a saturated carboxylic or carbonic acid mono-carboxylic
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
- C10L1/14—Organic compounds
- C10L1/20—Organic compounds containing halogen
- C10L1/206—Organic compounds containing halogen macromolecular compounds
- C10L1/207—Organic compounds containing halogen macromolecular compounds containing halogen with or without hydrogen
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L2270/00—Specifically adapted fuels
- C10L2270/02—Specifically adapted fuels for internal combustion engines
- C10L2270/026—Specifically adapted fuels for internal combustion engines for diesel engines, e.g. automobiles, stationary, marine
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- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Treatments Of Macromolecular Shaped Articles (AREA)
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Abstract
The invention discloses environment-friendly graft chloroprene rubber and corn oil hybrid fuel oil and a preparation method thereof. The environment-friendly graft chloroprene rubber and corn oil hybrid fuel oil is prepared from 4-6 parts of potassium permanganate, 9-11 parts of methanol, 9-11 parts of glycol, 4-6 parts of pentaerythritol, 9-11 parts of sulfolane, 19-21 parts of zinc naphthenate, 200-220 parts of distilled water, 100-120 parts of a leather material; 5-7 parts of sepiida, 150-200 parts of corn oil, 12-14 parts of methylbenzene, 25-27 parts of methyl ethyl ketone, 10-12 parts of chloroprene rubber DCR-10, 10-25 parts of gasoline, 6-9 parts of phenolic resin, 1-2 parts of essence, 1-2 parts of a 40% caustic soda solution, 150-200 parts of soybeans, 20-30 parts of water, 10-15 parts of a modified amino and polyamide mixture, 20-25 parts of talcum powder, 0.5-1 part of fructus forsythia, 1-2 parts of isatis roots and 1-2 parts of folium isatidis. The fuel oil disclosed by the invention is simple and convenient in preparation process, high in quality, good in energy conservation property, free of impurity after combustion, free of black smoke in the combustion process, un-pungent, environmentally friendly and free of pollution, and meanwhile in the application process, the fuel oil can be combusted 20% longer than common plant oil, and is good in adhesion property.
Description
Technical field:
The present invention relates to industrial chemicals preparing technical field, be specifically related to a kind of environment-friendly type graft chloroprene rubber
With Semen Maydis oil blended fuel and preparation method thereof.
Background technology:
Plant fuel its indices of oil is all close with diesel oil, even taller than diesel combustion value.Plant
Fuel oil is made up of three parts: one is the vegetable oil of about 50%；Two is the ethanol of about 10%；Three is 40%
The adjuvant of left and right.According to a certain percentage, develop through strict technique, this product also with diesel oil one
Sample can be divided into-30# ,-20# ,-10#, 0#, and product has good sprayability, and it is excellent that calorific value high price is low etc.
Point, with the plant fuel oil of technical grade Oleum Glycines preparation, cost price is only 4000 yuan of left and right per ton, produces in the future
After product appear on the market, price will be less than 50 100 yuan per ton of diesel-fuel price on market.Vegetable oil is configured to fuel oil
Ratio be that 4000 tons of vegetable oil are than adjuvants such as 1 ton of additives；This production engine is used easily to start, power
Greatly, oil consumption is identical with oil product, life-time service not carbon deposit and colloid, and mechanical wear is little, and tail gas is harmful to
Thing discharge less than national standard, is a kind of for any Diesel engine and the fuel oil of diesel burning systems.
Summary of the invention:
The technical problem to be solved is to overcome the defect of prior art, it is provided that a kind of environment-friendly type
Graft chloroprene rubber and Semen Maydis oil blended fuel and preparation method thereof.
The technical problem to be solved realizes by the following technical solutions.
A kind of environment-friendly type graft chloroprene rubber and Semen Maydis oil blended fuel, it is characterised in that: include following
The raw material composition of weight portion:
Potassium permanganate 4-6 part, methanol 9-11 part, ethylene glycol 9-11 part, tetramethylolmethane 4-6 part, sulfolane
9-11 part, zinc naphthenate 19-21 part, distilled water 200-220 part, skin material 100-120 part, spray 5-7 part,
Semen Maydis oil 150-200 part, toluene 12-14 part, butanone 25-27 part, neoprene DCR-10 10-12 part,
Gasoline 10-25 part, phenolic resin 6-9 part, essence 1-2 part, 40% caustic-soda aqueous solution 1-2 part；
Also include Semen sojae atricolor 150-200 part, water 20-30 part, essence 5-6 part, modified amine and polyamide mixture
10-15 part, Pulvis Talci 20-25 part, Fructus Forsythiae 0.5-1 part, Radix Isatidis 1-2 part, Folium Isatidis 1-2 part.
A kind of polyvinyl acetate-Semen sojae atricolor blended fuel, it is characterised in that: the preparation side of described fuel oil
Method, comprises the following steps:
1) skin material is put in distilled water, soak with vinegar, soak 1-2 days；
2) take spray to pulverize, be immersed in Semen Maydis oil, distill 3-4 hour, add essence, continue
Distill 3-4 hour, take out liquid；
3) take out step 2) in liquid mix with toluene, butanone, beat 3 hours；
4) take out step 1) in skin material, skin material is put in the liquid in step 3, heating, heating temperature
Degree is 100 DEG C, heats 10-12 hour；
5) by 40% aqueous solution of nitric acid mixing behind 2-3 hour of heating skin material, heat 10-12 hour, then
Take neoprene DCR-10, gasoline, phenolic resin stirring mixing；
6) hereafter taking glue once every 6 hours, take glue in three times, taking glue amount proportion for three times is 3:2:1；
7) from Semen sojae atricolor, separate albumen 8%-20%, carbamide 15%-17%, sodium polyphosphate 1%-10% simultaneously,
Carbamide is dispersed in water, is mixed and made into urea liquid, add albumen, at normal temperatures stirring 1-2 hour,
Add sodium polyphosphate, continue stirring 2-3 hour, finally essence is added, high-temperature stirring 20 minutes,
Temperature controls at 90-95 DEG C；
8) Pulvis Talci is added, stirring, cold preservation 1 hour, then modified amine is stirred with the addition of polyamide mixture
Mix, after having stirred, distill out liquid, take out impurity, obtain adjuvant；
9) take Fructus Forsythiae, Radix Isatidis, Folium Isatidis, wrap up with earth, dry, remove earth, clean, put
Enter baking 1 minute in steam box, add in alembic, distill 10 minutes, take out Fructus Forsythiae, Radix Isatidis, greatly
Folium Isatidis；
10) take step 6) in colloid, as in reactor, heating, then by the permanganic acid in raw material
Potassium, methanol, ethylene glycol, tetramethylolmethane, sulfolane, zinc naphthenate, all add in reactor, instead
Answer 1-2 hour, finally adjuvant is added, continue reaction 2-3 hour, go the removal of impurity, obtain fuel oil.
The invention has the beneficial effects as follows: the fuel oil of preparation in the present invention, it has preparation technology the most square
Just, the quality of fuel oil is high, good energy saving property, and free from admixture after combustion does not has black smoke in combustion process simultaneously,
It is not pungent, environment friendly and pollution-free, the most in the application, relative to common vegetable oil length burning time 20%,
Adhesive force is strong, and using effect is obvious.
Detailed description of the invention:
For the technological means making the present invention realize, creation characteristic, reach purpose and effect and be readily apparent from
Solve, below in conjunction with specific embodiment, the present invention is expanded on further.
Specific embodiment 1: a kind of environment-friendly type graft chloroprene rubber and Semen Maydis oil blended fuel, including with
The raw material composition of lower weight portion:
4 parts of potassium permanganate, methanol 9 parts, ethylene glycol 9 parts, tetramethylolmethane 4 parts, sulfolane 9 parts, aphthenic acids
19 parts of zinc, distilled water 200 parts, skin material 100 parts, spray 5 parts, Semen Maydis oil 150 parts, toluene 12 parts, first
Ethyl ketone 25 parts, neoprene DCR-10 10 parts, 10 parts of gasoline, 6 parts of phenolic resin, 1 part of essence, 40%
Caustic-soda aqueous solution 1 part；
Also include Semen sojae atricolor 150 parts, 20 parts of water, 5 parts of essence, modified amine and polyamide mixture 10 parts, slide
Stone powder 20 parts, Fructus Forsythiae 0.5 part, Radix Isatidis 1 part, Folium Isatidis 1 part.
Specific embodiment 2: a kind of environment-friendly type graft chloroprene rubber and Semen Maydis oil blended fuel, including with
The raw material composition of lower weight portion:
6 parts of potassium permanganate, methanol 11 parts, ethylene glycol 11 parts, tetramethylolmethane 6 parts, sulfolane 11 parts, ring
21 parts of alkanoic acid zinc, distilled water 220 parts, skin material 120 parts, spray 7 parts, Semen Maydis oil 200 parts, toluene 14 parts,
Butanone 27 parts, neoprene DCR-1012 part, 25 parts of gasoline, 9 parts of phenolic resin, 2 parts of essence,
40% caustic-soda aqueous solution 2 parts；
Also include Semen sojae atricolor 200 parts, 30 parts of water, 6 parts of essence, modified amine and polyamide mixture 15 parts, slide
Stone powder 25 parts, Fructus Forsythiae 1 part, Radix Isatidis 2 parts, Folium Isatidis 2 parts.
A kind of polyvinyl acetate-Semen sojae atricolor blended fuel preparation method, comprises the following steps:
1) skin material is put in distilled water, soak with vinegar, soak 1-2 days；
2) take spray to pulverize, be immersed in Semen Maydis oil, distill 3-4 hour, add essence, continue
Distill 3-4 hour, take out liquid；
3) take out step 2) in liquid mix with toluene, butanone, beat 3 hours；
4) take out step 1) in skin material, skin material is put in the liquid in step 3, heating, heating temperature
Degree is 100 DEG C, heats 10-12 hour；
5) by 40% aqueous solution of nitric acid mixing behind 2-3 hour of heating skin material, heat 10-12 hour, then
Take neoprene DCR-10, gasoline, phenolic resin stirring mixing；
6) hereafter taking glue once every 6 hours, take glue in three times, taking glue amount proportion for three times is 3:2:1；
7) from Semen sojae atricolor, separate albumen 8%-20%, carbamide 15%-17%, sodium polyphosphate 1%-10% simultaneously,
Being dispersed in water by carbamide, be mixed and made into urea liquid, add albumen, stirring 1-2 is little at normal temperatures
Time, add sodium polyphosphate, continue stirring 2-3 hour, finally essence is added, high-temperature stirring
20 minutes, temperature controlled at 90-95 DEG C；
8) Pulvis Talci is added, stirring, cold preservation 1 hour, then modified amine is stirred with the addition of polyamide mixture
Mix, after having stirred, distill out liquid, take out impurity, obtain adjuvant；
9) take Fructus Forsythiae, Radix Isatidis, Folium Isatidis, wrap up with earth, dry, remove earth, clean, put
Enter baking 1 minute in steam box, add in alembic, distill 10 minutes, taking-up Fructus Forsythiae, Radix Isatidis,
Folium Isatidis；
10) take step 6) in colloid, as in reactor, heating, then by the potassium permanganate in raw material,
Methanol, ethylene glycol, tetramethylolmethane, sulfolane, zinc naphthenate, all add in reactor, instead
Answer 1-2 hour, finally adjuvant is added, continue reaction 2-3 hour, go the removal of impurity, obtain fuel
Oil.
The ultimate principle of the present invention, principal character and advantages of the present invention have more than been shown and described.One's own profession
Skilled person will appreciate that of industry, the present invention is not restricted to the described embodiments, above-described embodiment and explanation
The principle that the present invention is simply described described in book, without departing from the spirit and scope of the present invention,
The present invention also has various changes and modifications, and these changes and improvements both fall within claimed invention model
In enclosing.Claimed scope is defined by appending claims and equivalent thereof.
Claims (2)
1. an environment-friendly type graft chloroprene rubber and Semen Maydis oil blended fuel, it is characterised in that: include with
The raw material composition of lower weight portion:
Potassium permanganate 4-6 part, methanol 9-11 part, ethylene glycol 9-11 part, tetramethylolmethane 4-6 part, sulfolane
9-11 part, zinc naphthenate 19-21 part, distilled water 200-220 part, skin material 100-120 part, spray 5-7 part,
Semen Maydis oil 150-200 part, toluene 12-14 part, butanone 25-27 part, neoprene DCR-1010-12 part,
Gasoline 10-25 part, phenolic resin 6-9 part, essence 1-2 part, 40% caustic-soda aqueous solution 1-2 part；
Also include Semen sojae atricolor 150-200 part, water 20-30 part, essence 5-6 part, modified amine and polyamide mixture
10-15 part, Pulvis Talci 20-25 part, Fructus Forsythiae 0.5-1 part, Radix Isatidis 1-2 part, Folium Isatidis 1-2 part.
Described a kind of environment-friendly type graft chloroprene rubber the most according to claim 1 and Semen Maydis oil mixing
Fuel oil, it is characterised in that: the preparation method of described fuel oil, comprise the following steps:
1) skin material is put in distilled water, soak with vinegar, soak 1-2 days；
2) take spray to pulverize, be immersed in Semen Maydis oil, distill 3-4 hour, add essence, continue
Distill 3-4 hour, take out liquid；
3) take out step 2) in liquid mix with toluene, butanone, beat 3 hours；
4) take out step 1) in skin material, skin material is put in the liquid in step 3, heating, heating temperature
Degree is 100 DEG C, heats 10-12 hour；
5) by 40% aqueous solution of nitric acid mixing behind 2-3 hour of heating skin material, heat 10-12 hour, then
Take neoprene DCR-10, gasoline, phenolic resin stirring mixing；
6) hereafter taking glue once every 6 hours, take glue in three times, taking glue amount proportion for three times is 3:2:1；
7) from Semen sojae atricolor, separate albumen 8%-20%, carbamide 15%-17%, sodium polyphosphate 1%-10% simultaneously,
Carbamide is dispersed in water, is mixed and made into urea liquid, add albumen, at normal temperatures stirring 1-2 hour,
Add sodium polyphosphate, continue stirring 2-3 hour, finally essence is added, high-temperature stirring 20 minutes,
Temperature controls at 90-95 DEG C；
8) Pulvis Talci is added, stirring, cold preservation 1 hour, then modified amine is stirred with the addition of polyamide mixture
Mix, after having stirred, distill out liquid, take out impurity, obtain adjuvant；
9) take Fructus Forsythiae, Radix Isatidis, Folium Isatidis, wrap up with earth, dry, remove earth, clean, put
Enter baking 1 minute in steam box, add in alembic, distill 10 minutes, take out Fructus Forsythiae, Radix Isatidis, greatly
Folium Isatidis；
10) take step 6) in colloid, as in reactor, heating, then by the permanganic acid in raw material
Potassium, methanol, ethylene glycol, tetramethylolmethane, sulfolane, zinc naphthenate, all add in reactor, instead
Answer 1-2 hour, finally adjuvant is added, continue reaction 2-3 hour, go the removal of impurity, obtain fuel oil.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610111618.4A CN105733697A (en) | 2016-02-27 | 2016-02-27 | Environment-friendly graft chloroprene rubber and corn oil hybrid fuel oil and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610111618.4A CN105733697A (en) | 2016-02-27 | 2016-02-27 | Environment-friendly graft chloroprene rubber and corn oil hybrid fuel oil and preparation method thereof |
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| Publication Number | Publication Date |
|---|---|
| CN105733697A true CN105733697A (en) | 2016-07-06 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610111618.4A Pending CN105733697A (en) | 2016-02-27 | 2016-02-27 | Environment-friendly graft chloroprene rubber and corn oil hybrid fuel oil and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107474916A (en) * | 2017-07-29 | 2017-12-15 | 巢湖鹏远金属焊管有限公司 | A kind of metal tube conveyer engine lubricating agent oil and preparation method thereof |
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| WO2004024849A1 (en) * | 2002-09-13 | 2004-03-25 | Dometic Ag | Fuel composition |
| CN103396857A (en) * | 2013-06-25 | 2013-11-20 | 雷学军 | Device and method for planting and comprehensive utilization of fast-growing plants to replace fossil energy |
| CN104694178A (en) * | 2015-01-30 | 2015-06-10 | 安徽海德石油化工有限公司 | Method for preparing fuel oil |
| CN104711043A (en) * | 2015-01-30 | 2015-06-17 | 安徽海德石油化工有限公司 | Novel burner plant oil and preparation method thereof |
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2016
- 2016-02-27 CN CN201610111618.4A patent/CN105733697A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1319647A (en) * | 2001-03-20 | 2001-10-31 | 中油燃料油有限公司 | High sulfur heavy fuel desulfurating agent and use thereof |
| WO2004024849A1 (en) * | 2002-09-13 | 2004-03-25 | Dometic Ag | Fuel composition |
| CN103396857A (en) * | 2013-06-25 | 2013-11-20 | 雷学军 | Device and method for planting and comprehensive utilization of fast-growing plants to replace fossil energy |
| CN104694178A (en) * | 2015-01-30 | 2015-06-10 | 安徽海德石油化工有限公司 | Method for preparing fuel oil |
| CN104711043A (en) * | 2015-01-30 | 2015-06-17 | 安徽海德石油化工有限公司 | Novel burner plant oil and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107474916A (en) * | 2017-07-29 | 2017-12-15 | 巢湖鹏远金属焊管有限公司 | A kind of metal tube conveyer engine lubricating agent oil and preparation method thereof |
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Application publication date: 20160706 |