CN105713681A - Low-temperature EVA hot melt adhesive-corn oil mixed fuel oil for paper and preparation method of mixed fuel oil - Google Patents
Low-temperature EVA hot melt adhesive-corn oil mixed fuel oil for paper and preparation method of mixed fuel oil Download PDFInfo
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- CN105713681A CN105713681A CN201610111566.0A CN201610111566A CN105713681A CN 105713681 A CN105713681 A CN 105713681A CN 201610111566 A CN201610111566 A CN 201610111566A CN 105713681 A CN105713681 A CN 105713681A
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/02—Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
- C10L1/12—Inorganic compounds
- C10L1/1233—Inorganic compounds oxygen containing compounds, e.g. oxides, hydroxides, acids and salts thereof
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
- C10L1/14—Organic compounds
- C10L1/16—Hydrocarbons
- C10L1/1625—Hydrocarbons macromolecular compounds
- C10L1/1633—Hydrocarbons macromolecular compounds homo- or copolymers obtained by reactions only involving carbon-to carbon unsaturated bonds
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
- C10L1/14—Organic compounds
- C10L1/18—Organic compounds containing oxygen
- C10L1/182—Organic compounds containing oxygen containing hydroxy groups; Salts thereof
- C10L1/1822—Organic compounds containing oxygen containing hydroxy groups; Salts thereof hydroxy group directly attached to (cyclo)aliphatic carbon atoms
- C10L1/1826—Organic compounds containing oxygen containing hydroxy groups; Salts thereof hydroxy group directly attached to (cyclo)aliphatic carbon atoms poly-hydroxy
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L2200/00—Components of fuel compositions
- C10L2200/04—Organic compounds
- C10L2200/0461—Fractions defined by their origin
- C10L2200/0469—Renewables or materials of biological origin
- C10L2200/0484—Vegetable or animal oils
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- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Solid Fuels And Fuel-Associated Substances (AREA)
Abstract
The invention discloses low-temperature EVA hot melt adhesive-corn oil mixed fuel oil for paper and a preparation method of the mixed fuel oil. The mixed fuel oil is prepared from 4-6 parts of potassium permanganate, 9-11 parts of methanol, 9-11 parts of ethanediol, 4-6 parts of pentaerythritol, 9-11 parts of sulfolane, 19-21 parts of zinc naphthenate, 200-220 parts of distilled water, 100-120 parts of leather materials, 5-7 parts of flowering branches, 150-200 parts of corn oil, 25-29 parts of EVA resin, 2-5 parts of low-molecular-weight polyethylene, 2-4 parts of calcium carbonate, 20-25 parts of thermoplastic phenolic resin, 10-13 parts of dibutyl phthalate, 1-2 parts of essence, 1-2 parts of a 40% aqueous caustic soda solution, 150-200 parts of soybeans, 20-30 parts of water, 5-6 parts of essence, 10-15 parts of a mixture of modified amine and polyamide, 20-25 parts of talcum powder, 0.5-1 part of fructus forsythiae, 1-2 parts of radix isatidis and 1-2 parts of folium isatidis. The fuel oil prepared through the method has the advantages that the preparation technology is simple and convenient, the quality is high, the energy saving property is good, and no impurity is generated after the fuel oil is burnt; meanwhile, no black smoke is generated in the burning process, no pungent smell is generated, environmental friendliness is achieved, and no pollution is generated; in addition, in application of the fuel oil, the burning time is 20% longer than that of common plant oil, and the adhesive force is high.
Description
Technical field:
The present invention relates to industrial chemicals preparing technical field, be specifically related to a kind of paper low temperature EVA hot-melt adhesive and Semen Maydis oil blended fuel and preparation method thereof.
Background technology:
Plant fuel its indices of oil is all close with diesel oil, even taller than diesel combustion value.Plant fuel oil is made up of three parts: one is the vegetable oil of about 50%；Two is the ethanol of about 10%；Three is the adjuvant of about 40%.According to a certain percentage, develop through strict technique, this product is also the same with diesel oil is divided into-30# ,-20# ,-10#, 0#, product has good sprayability, the advantages such as calorific value high price is low, with the plant fuel oil of technical grade Oleum Glycines preparation, cost price is only 4000 yuan of left and right per ton, after product appears on the market in the future, price will be less than 50 100 yuan per ton of diesel-fuel price on market.It is that 4000 tons of vegetable oil are than adjuvants such as 1 ton of additives that vegetable oil is configured to the ratio of fuel oil；Using this production engine easily to start, power is big, and oil consumption is identical with oil product, life-time service not carbon deposit and colloid, and mechanical wear is little, and tail gas hazardous emission, less than national standard, is a kind of for any Diesel engine and the fuel oil of diesel burning systems.
Summary of the invention:
The technical problem to be solved is to overcome the defect of prior art, it is provided that a kind of paper low temperature EVA hot-melt adhesive and Semen Maydis oil blended fuel and preparation method thereof.
The technical problem to be solved realizes by the following technical solutions.
A kind of paper low temperature EVA hot-melt adhesive and Semen Maydis oil blended fuel, it is characterised in that: include that the raw material of following weight portion forms:
Potassium permanganate 4-6 part, methanol 9-11 part, ethylene glycol 9-11 part, tetramethylolmethane 4-6 part, sulfolane 9-11 part, zinc naphthenate 19-21 part, distilled water 200-220 part, skin material 100-120 part, spray 5-7 part, Semen Maydis oil 150-200 part, EVA resin 25-29 part, low molecular weight polyethylene 2-5 part, calcium carbonate 2-4 part, thermoplastic phenolic resin 20-25 part, dibutyl phthalate 10-13 part, essence 1-2 part, 40% caustic-soda aqueous solution 1-2 part；
Also include Semen sojae atricolor 150-200 part, water 20-30 part, essence 5-6 part, modified amine and polyamide mixture 10-15 part, Pulvis Talci 20-25 part, Fructus Forsythiae 0.5-1 part, Radix Isatidis 1-2 part, Folium Isatidis 1-2 part.
A kind of polyvinyl acetate-Semen sojae atricolor blended fuel, it is characterised in that: the preparation method of described fuel oil, comprise the following steps:
1) skin material is put in distilled water, soak with vinegar, soak 1-2 days；
2) take spray to pulverize, be immersed in Semen Maydis oil, distill 3-4 hour, add essence, continue distillation 3-4 hour, take out liquid；
3) take out step 2) in liquid mix with EVA resin, low molecular weight polyethylene, beat 3 hours；
4) take out step 1) in skin material, skin material is put in the liquid in step 3, heating, heating-up temperature is 100 DEG C, heats 10-12 hour；
5) by 40% aqueous solution of nitric acid mixing behind 2-3 hour of heating skin material, heat 10-12 hour, then take calcium carbonate, thermoplastic phenolic resin, dibutyl phthalate stirring mixing；
6) hereafter taking glue once every 6 hours, take glue in three times, taking glue amount proportion for three times is 3:2:1；
7) from Semen sojae atricolor, separate albumen 8%-20%, carbamide 15%-17%, sodium polyphosphate 1%-10% simultaneously, carbamide is dispersed in water, it is mixed and made into urea liquid, adding albumen, stirring 1-2 hour, adds sodium polyphosphate at normal temperatures, continue stirring 2-3 hour, finally being added by essence, high-temperature stirring 20 minutes, temperature controls at 90-95 DEG C；
8) Pulvis Talci is added, stirring, cold preservation 1 hour, then modified amine is added stirring with polyamide mixture, after having stirred, distill out liquid, take out impurity, obtain adjuvant；
9) take Fructus Forsythiae, Radix Isatidis, Folium Isatidis, wrap up with earth, dry, remove earth, clean, put into steam box and toast 1 minute, add in alembic, distill 10 minutes, take out Fructus Forsythiae, Radix Isatidis, Folium Isatidis；
10) take step 6) in colloid, as in reactor, heating, again by the potassium permanganate in raw material, methanol, ethylene glycol, tetramethylolmethane, sulfolane, zinc naphthenate, all add in reactor, react 1-2 hour, finally adjuvant is added, continue reaction 2-3 hour, go the removal of impurity, obtain fuel oil.
The invention has the beneficial effects as follows: the fuel oil of preparation in the present invention, it has preparation technology simple and convenient, and the quality of fuel oil is high, good energy saving property, free from admixture after combustion, combustion process does not has black smoke simultaneously, be not pungent, environment friendly and pollution-free, the most in the application, relative to common vegetable oil length burning time 20%, adhesive force is strong, and using effect is obvious.
Detailed description of the invention:
For the technological means making the present invention realize, creation characteristic, reach purpose and be easy to understand with effect, below in conjunction with specific embodiment, the present invention is expanded on further.
Specific embodiment 1: a kind of paper low temperature EVA hot-melt adhesive and Semen Maydis oil blended fuel, the raw material including following weight portion forms:
4 parts of potassium permanganate, methanol 9 parts, ethylene glycol 9 parts, tetramethylolmethane 4 parts, sulfolane 9 parts, zinc naphthenate 19 parts, distilled water 200 parts, skin material 100 parts, spray 5 parts, Semen Maydis oil 150 parts, EVA resin 25 parts, low molecular weight polyethylene 2 parts, calcium carbonate 2 parts, thermoplastic phenolic resin 20 parts, dibutyl phthalate 10 parts, 1 part of essence, 40% caustic-soda aqueous solution 1 part；
Also include Semen sojae atricolor 150 parts, 20 parts of water, 5 parts of essence, modified amine and polyamide mixture 10 parts, Pulvis Talci 20 parts, Fructus Forsythiae 0.5 part, Radix Isatidis 1 part, Folium Isatidis 1 part.
Specific embodiment 2: a kind of paper low temperature EVA hot-melt adhesive and Semen Maydis oil fuel combination oil plant oil, the raw material including following weight portion forms:
6 parts of potassium permanganate, methanol 11 parts, ethylene glycol 11 parts, tetramethylolmethane 6 parts, sulfolane 11 parts, zinc naphthenate 21 parts, distilled water 220 parts, skin material 120 parts, spray 7 parts, Semen Maydis oil 200 parts, EVA resin 29 parts, low molecular weight polyethylene 5 parts, calcium carbonate 4 parts, thermoplastic phenolic resin 25 parts, dibutyl phthalate 13 parts, 2 parts of essence, 40% caustic-soda aqueous solution 2 parts；
Also include Semen sojae atricolor 200 parts, 30 parts of water, 6 parts of essence, modified amine and polyamide mixture 15 parts, Pulvis Talci 25 parts, Fructus Forsythiae 1 part, Radix Isatidis 2 parts, Folium Isatidis 2 parts.
A kind of polyvinyl acetate-Semen sojae atricolor blended fuel preparation method, comprises the following steps:
1) skin material is put in distilled water, soak with vinegar, soak 1-2 days；
2) take spray to pulverize, be immersed in Semen Maydis oil, distill 3-4 hour, add essence, continue distillation 3-4 hour, take out liquid；
3) take out step 2) in liquid mix with EVA resin, low molecular weight polyethylene, beat 3 hours；
4) take out step 1) in skin material, skin material is put in the liquid in step 3, heating, heating-up temperature is 100 DEG C, heats 10-12 hour；
5) by 40% aqueous solution of nitric acid mixing behind 2-3 hour of heating skin material, heat 10-12 hour, then take calcium carbonate, thermoplastic phenolic resin, dibutyl phthalate stirring mixing；
6) hereafter taking glue once every 6 hours, take glue in three times, taking glue amount proportion for three times is 3:2:1；
7) from Semen sojae atricolor, separate albumen 8%-20%, carbamide 15%-17%, sodium polyphosphate 1%-10% simultaneously, carbamide is dispersed in water, it is mixed and made into urea liquid, adding albumen, stirring 1-2 hour, adds sodium polyphosphate at normal temperatures, continue stirring 2-3 hour, finally being added by essence, high-temperature stirring 20 minutes, temperature controls at 90-95 DEG C；
8) Pulvis Talci is added, stirring, cold preservation 1 hour, then modified amine is added stirring with polyamide mixture, after having stirred, distill out liquid, take out impurity, obtain adjuvant；
9) take Fructus Forsythiae, Radix Isatidis, Folium Isatidis, wrap up with earth, dry, remove earth, clean, put into steam box and toast 1 minute, add in alembic, distill 10 minutes, take out Fructus Forsythiae, Radix Isatidis, Folium Isatidis；
10) take step 6) in colloid, as in reactor, heating, again by the potassium permanganate in raw material, methanol, ethylene glycol, tetramethylolmethane, sulfolane, zinc naphthenate, all add in reactor, react 1-2 hour, finally adjuvant is added, continue reaction 2-3 hour, go the removal of impurity, obtain fuel oil.
The ultimate principle of the present invention, principal character and advantages of the present invention have more than been shown and described.Skilled person will appreciate that of the industry; the present invention is not restricted to the described embodiments; the principle that the present invention is simply described described in above-described embodiment and description; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements both fall within scope of the claimed invention.Claimed scope is defined by appending claims and equivalent thereof.
Claims (2)
1. a paper low temperature EVA hot-melt adhesive and Semen Maydis oil blended fuel, it is characterised in that: include with
The raw material composition of lower weight portion:
Potassium permanganate 4-6 part, methanol 9-11 part, ethylene glycol 9-11 part, tetramethylolmethane 4-6 part, sulfolane
9-11 part, zinc naphthenate 19-21 part, distilled water 200-220 part, skin material 100-120 part, spray 5-7 part,
Semen Maydis oil 150-200 part, EVA resin 25-29 part, low molecular weight polyethylene 2-5 part, calcium carbonate
2-4 part, thermoplastic phenolic resin 20-25 part, dibutyl phthalate 10-13 part, essence 1-2 part,
40% caustic-soda aqueous solution 1-2 part；
Also include Semen sojae atricolor 150-200 part, water 20-30 part, essence 5-6 part, modified amine and polyamide mixture
10-15 part, Pulvis Talci 20-25 part, Fructus Forsythiae 0.5-1 part, Radix Isatidis 1-2 part, Folium Isatidis 1-2 part.
Described a kind of paper low temperature EVA hot-melt adhesive the most according to claim 1 and Semen Maydis oil mixing
Fuel oil, it is characterised in that: the preparation method of described fuel oil, comprise the following steps:
1) skin material is put in distilled water, soak with vinegar, soak 1-2 days；
2) take spray to pulverize, be immersed in Semen Maydis oil, distill 3-4 hour, add essence, continue
Distill 3-4 hour, take out liquid；
3) take out step 2) in liquid mix with EVA resin, low molecular weight polyethylene, beat 3 hours；
4) take out step 1) in skin material, skin material is put in the liquid in step 3, heating, heating temperature
Degree is 100 DEG C, heats 10-12 hour；
5) by 40% aqueous solution of nitric acid mixing behind 2-3 hour of heating skin material, heat 10-12 hour, then
Take calcium carbonate, thermoplastic phenolic resin, dibutyl phthalate stirring mixing；
6) hereafter taking glue once every 6 hours, take glue in three times, taking glue amount proportion for three times is 3:2:1；
7) from Semen sojae atricolor, separate albumen 8%-20%, carbamide 15%-17%, sodium polyphosphate 1%-10% simultaneously,
Carbamide is dispersed in water, is mixed and made into urea liquid, add albumen, at normal temperatures stirring 1-2 hour,
Add sodium polyphosphate, continue stirring 2-3 hour, finally essence is added, high-temperature stirring 20 minutes,
Temperature controls at 90-95 DEG C；
8) Pulvis Talci is added, stirring, cold preservation 1 hour, then modified amine is stirred with the addition of polyamide mixture
Mix, after having stirred, distill out liquid, take out impurity, obtain adjuvant；
9) take Fructus Forsythiae, Radix Isatidis, Folium Isatidis, wrap up with earth, dry, remove earth, clean, put
Enter baking 1 minute in steam box, add in alembic, distill 10 minutes, take out Fructus Forsythiae, Radix Isatidis, greatly
Folium Isatidis；
10) take step 6) in colloid, as in reactor, heating, then by the permanganic acid in raw material
Potassium, methanol, ethylene glycol, tetramethylolmethane, sulfolane, zinc naphthenate, all add in reactor, instead
Answer 1-2 hour, finally adjuvant is added, continue reaction 2-3 hour, go the removal of impurity, obtain fuel oil.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610111566.0A CN105713681A (en) | 2016-02-27 | 2016-02-27 | Low-temperature EVA hot melt adhesive-corn oil mixed fuel oil for paper and preparation method of mixed fuel oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610111566.0A CN105713681A (en) | 2016-02-27 | 2016-02-27 | Low-temperature EVA hot melt adhesive-corn oil mixed fuel oil for paper and preparation method of mixed fuel oil |
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| CN105713681A true CN105713681A (en) | 2016-06-29 |
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| CN201610111566.0A Pending CN105713681A (en) | 2016-02-27 | 2016-02-27 | Low-temperature EVA hot melt adhesive-corn oil mixed fuel oil for paper and preparation method of mixed fuel oil |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1319647A (en) * | 2001-03-20 | 2001-10-31 | 中油燃料油有限公司 | High sulfur heavy fuel desulfurating agent and use thereof |
| CN101302450A (en) * | 2008-07-15 | 2008-11-12 | 周凯亮 | Biosynthetic diesel and preparation thereof |
| CN103396857A (en) * | 2013-06-25 | 2013-11-20 | 雷学军 | Device and method for planting and comprehensive utilization of fast-growing plants to replace fossil energy |
| CN104694178A (en) * | 2015-01-30 | 2015-06-10 | 安徽海德石油化工有限公司 | Method for preparing fuel oil |
| CN104711043A (en) * | 2015-01-30 | 2015-06-17 | 安徽海德石油化工有限公司 | Novel burner plant oil and preparation method thereof |
-
2016
- 2016-02-27 CN CN201610111566.0A patent/CN105713681A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1319647A (en) * | 2001-03-20 | 2001-10-31 | 中油燃料油有限公司 | High sulfur heavy fuel desulfurating agent and use thereof |
| CN101302450A (en) * | 2008-07-15 | 2008-11-12 | 周凯亮 | Biosynthetic diesel and preparation thereof |
| CN103396857A (en) * | 2013-06-25 | 2013-11-20 | 雷学军 | Device and method for planting and comprehensive utilization of fast-growing plants to replace fossil energy |
| CN104694178A (en) * | 2015-01-30 | 2015-06-10 | 安徽海德石油化工有限公司 | Method for preparing fuel oil |
| CN104711043A (en) * | 2015-01-30 | 2015-06-17 | 安徽海德石油化工有限公司 | Novel burner plant oil and preparation method thereof |
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Application publication date: 20160629 |