CN105708782A - Preparation method of anthocyanin cream pack - Google Patents
Preparation method of anthocyanin cream pack Download PDFInfo
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- CN105708782A CN105708782A CN201610159450.4A CN201610159450A CN105708782A CN 105708782 A CN105708782 A CN 105708782A CN 201610159450 A CN201610159450 A CN 201610159450A CN 105708782 A CN105708782 A CN 105708782A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
- A61K8/988—Honey; Royal jelly, Propolis
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/007—Preparations for dry skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/84—Products or compounds obtained by lyophilisation, freeze-drying
Abstract
The invention provides a preparation method of an anthocyanin cream pack. The anthocyanin cream pack is mainly prepared from blueberries, red heart dragon fruits, cucumbers, pearl powder, olive oil and the like. The cream pack is lavender in appearance, and has the effects of nourishing the skin, improving skin elasticity, relieving wrinkles, removing stains, whitening the skin and the like. Compared with existing similar methods, the method has the advantages that the core element of garden stuff digestion cream is prepared through the vacuum freeze drying and secondary ultrasonic cooperated ethyl alcohol digestion concentration method, the anthocyanin biological activities of blueberries and red heart dragon fruits are effectively reserved, and the function of nourishing the skin is enhanced; on the basis of the oleyl alcohol two-phase supplementing method, the skin water locking and moisturizing effects are greatly improved, the nutrient absorbing efficiency of the skin is improved due to the fact that the cream pack is used as a medium, and the anthocyanin cream pack becomes a novel health care mask particularly suitable for consumers with dry and neutral skin and has the good market popularization value.
Description
Technical field
The preparation method that the present invention relates to a kind of cream pack, the preparation method of especially a kind of anthocyanidin cream pack, belong to cosmetic technical field.
Background technology
Anthocyanidin is the supplementary of the defying age of pure natural, and research proves that anthocyanidin is that mankind nowadays finds maximally effective antioxidant, and its antioxygenic property exceeds 50 times than vitamin E, exceeds 20 times than vitamin C.The biological effectiveness of human body is 100% by it, within 20 minutes, just can detect in blood after taking.Anthocyanidin has the good reputation of " oral cosmetics for skin " in Europe, especially vaccinium oxycoccus pigment, skin nutrition, strengthen skin immunization power, various allergic conditions can be tackled, also can maintain the flowing stablizing, strengthening capillary vessel circulation, raising blood capillary and vein of normal cell linkages, blood vessel, and then reach healing rapidly of abnormal skin.Anthocyanidin is natural sunlight overcover, it is possible to prevent ultraviolet damage skin.
U.S.'s mankind's nutrient research center discovery blue berry is the fruit that anthocyanidin content is the abundantest, and blue berry ranks the first in more than 40 oxidation resistances planted in fruit and vegerable, and it can prevent generating ahead of time of wrinkle of skin, is the maximally effective antioxidant of current nature.Skin elasticity can be improved, reduce dermatosis and ripple, even eliminate cicatrix, dispelling stain, skin whitening.
Hylocereus undatus is a kind of low-energy fruit, rich in water soluble dietary fiber, has the effects such as defying age, whitening, fat-reducing, blood sugar lowering, it is possible to Constipation.Red heart Hylocereus undatus is the rare kind in Hylocereus undatus, rich in anthocyanidin in its fruit and peel, after incision, its pulp colour visible is aglow, nutritious, function is unique, it contains the rare vegetable albumin of general plant, abundant vitamin C and water solublity meals fiber.Red heart Hylocereus undatus rich in anthocyanidin have antioxidation, free radical resisting, defying age, enhancing blood vessel elasticity, improve blood circulation and promote skin smoothness, it is suppressed that the effect of inflammation and allergy.
The present invention adopts gentle extraction process to prepare Fruit powder and fruit and vegerable lixiviate cream with blue berry and red heart Hylocereus undatus etc. for raw material, anthocyanidin isoreactivity composition specific to blue berry and red heart Hylocereus undatus is made to maximize the retention, it is aided with glycerol again, cream pack prepared into by Fructus Canarii albi wet goods raw material, compensate at present on the market in similar products preparation process anthocyanidin go to pot the low problem of the content caused, obtained cream pack is suitable for each age group consumer group especially xerosis cutis, wrinkle is many, the women having mottle uses, it it is the functional facial film of a kind of great market popularization value.
Summary of the invention
The invention reside in offer a kind of with blue berry, red heart Hylocereus undatus for primary raw material, with Fruit powder, fruit and vegerable lixiviate cream be core adding ingredient, the preparation method that is applicable to the anthocyanidin cream pack of neutral, dry skin.
For achieving the above object, the technical solution used in the present invention is as follows:
The preparation method that the present invention provides a kind of anthocyanidin cream pack, it is characterised in that prepare the core adding ingredient Fruit powder used by anthocyanidin cream pack and realized by cryogenic vacuum freeze drying process, prepare particular by following steps:
Choose the blue berry of new harvesting, foreign material are cleaned with tap water, choose fresh full red heart Hylocereus undatus, peeling, sarcocarp is cut into bulk (each 2cm of length, width and height is advisable), take 15～18 parts of blue berries by weight, 9～12 parts of red heart Hylocereus undatus mixing are placed in quick freeze 2～3h in-20 DEG C～-15 DEG C cryogenic refrigerators, blue berry red heart Hylocereus undatus mixture after freezing is transferred in freeze dryer dryness storehouse, vacuum drying 4～6h under-20 DEG C～-10 DEG C conditions, to heater plate in dryness storehouse until dryness storehouse temperature is 30 DEG C～45 DEG C, and regulate heat preservation and dryness 4～6h when dryness storehouse vacuum pressure is 80Pa～100Pa, keep lowering the temperature when dryness storehouse vacuum pressure 80Pa～100Pa, 2～3h is maintained after temperature is down to 20 DEG C～30 DEG C, obtain the blue berry red heart Hylocereus undatus mixture after vacuum lyophilization, the blue berry red heart Hylocereus undatus mixture removing major part free water through cryogenic vacuum lyophilization was pulverized 40 mesh sieves, obtain Fruit powder.
The preparation method that the present invention provides a kind of anthocyanidin cream pack, it is characterized in that the core adding ingredient fruit and vegerable lixiviate cream prepared used by anthocyanidin cream pack is realized by " vacuum lyophilization+twice ultrasonic ripple coordinates alcohol steep concentration method " technique, prepared particular by following steps:
(1) blue berry of new harvesting is chosen, foreign material are cleaned with tap water, choose fresh full red heart Hylocereus undatus, peeling, sarcocarp is cut into bulk (each 2cm of length, width and height is advisable), choose fresh cucumber, peeling, clean and be cut into bulk (each 2cm of length, width and height is advisable), take 15～18 parts of blue berries by weight, 9～12 parts of red heart Hylocereus undatuss, 6～12 parts of Fructus Cucumidis sativi mixing are placed in quick freeze 2～3h in-20 DEG C～-15 DEG C cryogenic refrigerators, fruit and vegerable mixture after freezing is transferred in freeze dryer dryness storehouse, vacuum drying 3～5h under-20 DEG C～-10 DEG C conditions, to heater plate in dryness storehouse until dryness storehouse temperature is 30 DEG C～45 DEG C, and regulate heat preservation and dryness 4～6h when dryness storehouse vacuum pressure is 80Pa～100Pa, keep lowering the temperature when dryness storehouse vacuum pressure 80Pa～100Pa, 2～3h is maintained after temperature is down to 20 DEG C～30 DEG C, obtain the fruit and vegerable mixture after vacuum lyophilization, the fruit and vegerable mixture removing major part free water through cryogenic vacuum lyophilization was pulverized 40 mesh sieves, obtain fruit vegetable powder；
(2) fruit vegetable powder is transferred in reaction vessel, add the pure water of 2～3 times of weight portions, temperature 30 DEG C～40 DEG C, under the ul-trasonic irradiation that power is 36～40W, extract 2～3h obtain fruit and vegerable extracting solution, extract complete rotary evaporation devices and fruit and vegerable extracting solution is concentrated into the 1/3～1/2 of original volume, stand 2～4h, preliminary filtration, obtains fruit and vegerable filtrate；
(3) in fruit and vegerable filtrate, add 70% ethanol of 6～8 times of weight portions, 50 DEG C～60 DEG C waters bath with thermostatic control, power 36～40W ul-trasonic irradiation under lixiviate 20～30min, by centrifuging, filtrate centrifugal 15～20min under the rotating speed of 3000～4000r/min is removed residue, then Slag recovering is transferred in reaction vessel, and extracted again once by above step, merging filtrate, keeps 40 DEG C～50 DEG C waters bath with thermostatic control to make filtrate moisture be down to about 30%～40%, obtains fruit and vegerable lixiviate cream.
The preparation method that the present invention provides a kind of anthocyanidin cream pack, it is characterized in that the oil-phase medium prepared used by anthocyanidin cream pack is prepared by the following method: take 12～18 parts of Margarita powder, 6～9 parts of Mel, 16～22 parts of olive oil, 2～3 parts of isopropyl palmitate (IPP) mix and blends by weight, it is positioned over-10 DEG C～-4 DEG C refrigerator freezing 3～5h, take out and add 3～5 fruits powder, 3～5 parts of Semen Tritici aestivi germ oils, stir and obtain oil-phase medium.
The preparation method that the present invention provides a kind of anthocyanidin cream pack, it is characterized in that the alcohol phase medium prepared used by anthocyanidin cream pack is prepared by the following method: take 12～18 parts of deionized waters, 6～8 parts of glycerol, 3～5 parts of palmityl alcohol mix and blends by weight, it is positioned over-10 DEG C～-4 DEG C refrigerator freezing 3～5h, take out and add 6～12 parts of fruit and vegerable lixiviate cream, 3～5 parts of propylene glycol, 2～4 parts of butanediols, stir and obtain alcohol phase medium.
The preparation method that the present invention provides a kind of anthocyanidin cream pack, it is characterized in that being realized by following steps: take 3～6 fruits powder, 2～4 parts of alcohol phase mediums, 6～8 parts of oil-phase mediums, 6～12 parts of fruit and vegerable lixiviate cream mix homogeneously, obtain anthocyanidin cream pack.
The preparation method that the present invention provides a kind of anthocyanidin cream pack, it is characterized in that the using method of this facial film is first to coordinate Cleansing Foam to clean face with clear water; take uniform application of the present invention in face; and pat gently; clean with clear water after 15～20 minutes, smear emulsion and carry out face lock water and protect.
The preparation method that the present invention provides a kind of anthocyanidin cream pack, mainly it is made up of blue berry, red heart Hylocereus undatus, Fructus Cucumidis sativi, Margarita powder, Fructus Canarii albi wet goods raw material, this cream pack outward appearance is lavender, has skin nutrition, improves skin elasticity, alleviates the effects such as wrinkle, dispelling stain, skin whitening；Compared with existing similar invention, the invention have the advantages that: one is nucleus fruit and vegerable lixiviate cream of the present invention is prepared by " vacuum lyophilization+twice ultrasonic ripple coordinates alcohol steep concentration method " technique, it is effectively retained the anthocyanidin biological activity of blue berry and red heart Hylocereus undatus, enhances the function of the skin nutrition of the present invention；Two is by " oleyl alcohol two-phase complementary method ", substantially increase the present invention lock water moisture-keeping efficacy to skin, the efficiency of skin absorption nutritional labeling is improve as medium, make the present invention become a kind of new type of health facial film being particularly well-suited to dryness, neutral skin consumer, there is good market popularization value.
Detailed description of the invention
Below in conjunction with embodiment, the present invention will be further described.
Embodiment 1:
The preparation method of a kind of anthocyanidin cream pack, specifically includes following steps:
(1) blue berry of new harvesting is chosen, foreign material are cleaned with tap water, choose fresh full red heart Hylocereus undatus, peeling, sarcocarp is cut into bulk (each 2cm of length, width and height is advisable), take 15 parts of blue berries by weight, the mixing of 9 parts of red heart Hylocereus undatuss is placed in-20 DEG C of cryogenic refrigerators quick freeze 2h, blue berry red heart Hylocereus undatus mixture after freezing is transferred in freeze dryer dryness storehouse, vacuum drying 4h under-20 DEG C of conditions, to heater plate in dryness storehouse until dryness storehouse temperature is 35 DEG C, and regulate heat preservation and dryness 4h when dryness storehouse vacuum pressure is 80Pa, keep lowering the temperature when dryness storehouse vacuum pressure 80Pa, 2h is maintained after temperature is down to 20 DEG C, obtain the blue berry red heart Hylocereus undatus mixture after vacuum lyophilization, the blue berry red heart Hylocereus undatus mixture removing major part free water through cryogenic vacuum lyophilization was pulverized 40 mesh sieves, obtain Fruit powder；
(2) blue berry of new harvesting is chosen, foreign material are cleaned with tap water, choose fresh full red heart Hylocereus undatus, peeling, sarcocarp is cut into bulk (each 2cm of length, width and height is advisable), choose fresh cucumber, peeling, clean and be cut into bulk (each 2cm of length, width and height is advisable), take 15 parts of blue berries by weight, 9 parts of red heart Hylocereus undatuss, the mixing of 6 portions of Fructus Cucumidiss sativi is placed in-20 DEG C of cryogenic refrigerators quick freeze 2h, fruit and vegerable mixture after freezing is transferred in freeze dryer dryness storehouse, vacuum drying 3h under-20 DEG C of conditions, to heater plate in dryness storehouse until dryness storehouse temperature is 30 DEG C, and regulate heat preservation and dryness 4h when dryness storehouse vacuum pressure is 80Pa, keep lowering the temperature when dryness storehouse vacuum pressure 80Pa, 2h is maintained after temperature is down to 20 DEG C, obtain the fruit and vegerable mixture after vacuum lyophilization, the fruit and vegerable mixture removing major part free water through cryogenic vacuum lyophilization was pulverized 40 mesh sieves, obtain fruit vegetable powder；
(3) fruit vegetable powder is transferred in reaction vessel, add the pure water of 2 times of weight portions, temperature 30 DEG C, under the ul-trasonic irradiation that power is 36W, extract 2h obtain fruit and vegerable extracting solution, extract complete rotary evaporation devices and fruit and vegerable extracting solution is concentrated into the 1/2 of original volume, stand 2h, preliminary filtration, obtains fruit and vegerable filtrate；
(4) in fruit and vegerable filtrate, add 70% ethanol of 6 times of weight portions, 50 DEG C of waters bath with thermostatic control, power 36W ul-trasonic irradiation under lixiviate 20min, by centrifuging, filtrate centrifugal 15min under the rotating speed of 3600r/min is removed residue, then Slag recovering is transferred in reaction vessel, and extracted again once by above step, merging filtrate, keeps 40 DEG C of waters bath with thermostatic control to make filtrate moisture be down to about 30%, obtains fruit and vegerable lixiviate cream；
(5) take 12 parts of Margarita powder, 6 parts of Mel, 16 parts of olive oil, 2 parts of isopropyl palmitate (IPP) mix and blends by weight, be positioned over-10 DEG C of refrigerator freezing 3h, take out and add 3 fruits powder, 3 parts of Semen Tritici aestivi germ oils, stir and obtain oil-phase medium；
(6) take 12 parts of deionized waters, 6 parts of glycerol, 3 parts of palmityl alcohol mix and blends by weight, be positioned over-10 DEG C of refrigerator freezing 3h, take out and add 6 parts of fruit and vegerable lixiviate cream, 3 parts of propylene glycol, 2 parts of butanediols, stir and obtain alcohol phase medium；
(7) take 5 fruits powder, 3 parts of alcohol phase mediums, 6 parts of oil-phase mediums, 8 parts of fruit and vegerable lixiviate cream mix homogeneously, obtain anthocyanidin cream pack.
Embodiment 2:
The preparation method of a kind of anthocyanidin cream pack, specifically includes following steps:
(1) blue berry of new harvesting is chosen, foreign material are cleaned with tap water, choose fresh full red heart Hylocereus undatus, peeling, sarcocarp is cut into bulk (each 2cm of length, width and height is advisable), take 18 parts of blue berries by weight, the mixing of 12 parts of red heart Hylocereus undatuss is placed in-15 DEG C of cryogenic refrigerators quick freeze 3h, blue berry red heart Hylocereus undatus mixture after freezing is transferred in freeze dryer dryness storehouse, vacuum drying 6h under-10 DEG C of conditions, to heater plate in dryness storehouse until dryness storehouse temperature is 45 DEG C, and regulate heat preservation and dryness 5h when dryness storehouse vacuum pressure is 100Pa, keep lowering the temperature when dryness storehouse vacuum pressure 100Pa, 3h is maintained after temperature is down to 30 DEG C, obtain the blue berry red heart Hylocereus undatus mixture after vacuum lyophilization, the blue berry red heart Hylocereus undatus mixture removing major part free water through cryogenic vacuum lyophilization was pulverized 40 mesh sieves, obtain Fruit powder；
(2) blue berry of new harvesting is chosen, foreign material are cleaned with tap water, choose fresh full red heart Hylocereus undatus, peeling, sarcocarp is cut into bulk (each 2cm of length, width and height is advisable), choose fresh cucumber, peeling, clean and be cut into bulk (each 2cm of length, width and height is advisable), take 18 parts of blue berries by weight, 12 parts of red heart Hylocereus undatuss, the mixing of 12 portions of Fructus Cucumidiss sativi is placed in-15 DEG C of cryogenic refrigerators quick freeze 2.5h, fruit and vegerable mixture after freezing is transferred in freeze dryer dryness storehouse, vacuum drying 5h under-10 DEG C of conditions, to heater plate in dryness storehouse until dryness storehouse temperature is 45 DEG C, and regulate heat preservation and dryness 5h when dryness storehouse vacuum pressure is 100Pa, keep lowering the temperature when dryness storehouse vacuum pressure 100Pa, 3h is maintained after temperature is down to 30 DEG C, obtain the fruit and vegerable mixture after vacuum lyophilization, the fruit and vegerable mixture removing major part free water through cryogenic vacuum lyophilization was pulverized 40 mesh sieves, obtain fruit vegetable powder；
(3) fruit vegetable powder is transferred in reaction vessel, add the pure water of 3 times of weight portions, temperature 40 DEG C, under the ul-trasonic irradiation that power is 40W, extract 3h obtain fruit and vegerable extracting solution, extract complete rotary evaporation devices and fruit and vegerable extracting solution is concentrated into the 1/2 of original volume, stand 4h, preliminary filtration, obtains fruit and vegerable filtrate；
(4) in fruit and vegerable filtrate, add 70% ethanol of 8 times of weight portions, 560 DEG C of waters bath with thermostatic control, power 40W ul-trasonic irradiation under lixiviate 30min, by centrifuging, filtrate centrifugal 20min under the rotating speed of 4000r/min is removed residue, then Slag recovering is transferred in reaction vessel, and extracted again once by above step, merging filtrate, keeps 50 DEG C of waters bath with thermostatic control to make filtrate moisture be down to about 340%, obtains fruit and vegerable lixiviate cream；
(5) take 18 parts of Margarita powder, 9 parts of Mel, 22 parts of olive oil, 3 parts of isopropyl palmitate (IPP) mix and blends by weight, be positioned over-4 DEG C of refrigerator freezing 5h, take out and add 5 fruits powder, 5 parts of Semen Tritici aestivi germ oils, stir and obtain oil-phase medium；
(6) take 18 parts of deionized waters, 8 parts of glycerol, 5 parts of palmityl alcohol mix and blends by weight, be positioned over-4 DEG C of refrigerator freezing 5h, take out and add 12 parts of fruit and vegerable lixiviate cream, 5 parts of propylene glycol, 4 parts of butanediols, stir and obtain alcohol phase medium；
(7) take 6 fruits powder, 4 parts of alcohol phase mediums, 8 parts of oil-phase mediums, 12 parts of fruit and vegerable lixiviate cream mix homogeneously, obtain anthocyanidin cream pack.
Above example is merely to illustrate technical scheme, but not is limited；Although being described in detail by invention with reference to previous embodiment, but for the person of ordinary skill of the art, still the technical scheme described in previous embodiment can be modified, or wherein portion of techniques feature is carried out equivalent replacement；And to these amendments or replacement, do not make the essence of appropriate technical solution depart from the spirit and scope of present invention technical scheme required for protection.
Claims (1)
1. a preparation method for anthocyanidin cream pack, specifically includes following steps:
(1) blue berry of new harvesting is chosen, foreign material are cleaned with tap water, choose fresh full red heart Hylocereus undatus, peeling, sarcocarp is cut into bulk (each 2cm of length, width and height is advisable), take 15～18 parts of blue berries by weight, 9～12 parts of red heart Hylocereus undatus mixing are placed in quick freeze 2～3h in-20 DEG C～-15 DEG C cryogenic refrigerators, blue berry red heart Hylocereus undatus mixture after freezing is transferred in freeze dryer dryness storehouse, vacuum drying 4～6h under-20 DEG C～-10 DEG C conditions, to heater plate in dryness storehouse until dryness storehouse temperature is 30 DEG C～45 DEG C, and regulate heat preservation and dryness 4～6h when dryness storehouse vacuum pressure is 80Pa～100Pa, keep lowering the temperature when dryness storehouse vacuum pressure 80Pa～100Pa, 2～3h is maintained after temperature is down to 20 DEG C～30 DEG C, obtain the blue berry red heart Hylocereus undatus mixture after vacuum lyophilization, the blue berry red heart Hylocereus undatus mixture removing major part free water through cryogenic vacuum lyophilization was pulverized 40 mesh sieves, obtain Fruit powder；
(2) blue berry of new harvesting is chosen, foreign material are cleaned with tap water, choose fresh full red heart Hylocereus undatus, peeling, sarcocarp is cut into bulk (each 2cm of length, width and height is advisable), choose fresh cucumber, peeling, clean and be cut into bulk (each 2cm of length, width and height is advisable), take 15～18 parts of blue berries by weight, 9～12 parts of red heart Hylocereus undatuss, 6～12 parts of Fructus Cucumidis sativi mixing are placed in quick freeze 2～3h in-20 DEG C～-15 DEG C cryogenic refrigerators, fruit and vegerable mixture after freezing is transferred in freeze dryer dryness storehouse, vacuum drying 3～5h under-20 DEG C～-10 DEG C conditions, to heater plate in dryness storehouse until dryness storehouse temperature is 30 DEG C～45 DEG C, and regulate heat preservation and dryness 4～6h when dryness storehouse vacuum pressure is 80Pa～100Pa, keep lowering the temperature when dryness storehouse vacuum pressure 80Pa～100Pa, 2～3h is maintained after temperature is down to 20 DEG C～30 DEG C, obtain the fruit and vegerable mixture after vacuum lyophilization, the fruit and vegerable mixture removing major part free water through cryogenic vacuum lyophilization was pulverized 40 mesh sieves, obtain fruit vegetable powder；
(3) fruit vegetable powder is transferred in reaction vessel, add the pure water of 2～3 times of weight portions, temperature 30 DEG C～40 DEG C, under the ul-trasonic irradiation that power is 36～40W, extract 2～3h obtain fruit and vegerable extracting solution, extract complete rotary evaporation devices and fruit and vegerable extracting solution is concentrated into the 1/3～1/2 of original volume, stand 2～4h, preliminary filtration, obtains fruit and vegerable filtrate；
(4) in fruit and vegerable filtrate, add 70% ethanol of 6～8 times of weight portions, 50 DEG C～60 DEG C waters bath with thermostatic control, power 36～40W ul-trasonic irradiation under lixiviate 20～30min, by centrifuging, filtrate centrifugal 15～20min under the rotating speed of 3000～4000r/min is removed residue, then Slag recovering is transferred in reaction vessel, and extracted again once by above step, merging filtrate, keeps 40 DEG C～50 DEG C waters bath with thermostatic control to make filtrate moisture be down to about 30%～40%, obtains fruit and vegerable lixiviate cream；
(5) 12～18 parts of Margarita powder, 6～9 parts of Mel, 16～22 parts of olive oil, 2～3 parts of isopropyl palmitate (IPP) mix and blends are taken by weight, it is positioned over-10 DEG C～-4 DEG C refrigerator freezing 3～5h, take out and add 3～5 fruits powder, 3～5 parts of Semen Tritici aestivi germ oils, stir and obtain oil-phase medium；
(6) 12～18 parts of deionized waters, 6～8 parts of glycerol, 3～5 parts of palmityl alcohol mix and blends are taken by weight, it is positioned over-10 DEG C～-4 DEG C refrigerator freezing 3～5h, take out and add 6～12 parts of fruit and vegerable lixiviate cream, 3～5 parts of propylene glycol, 2～4 parts of butanediols, stir and obtain alcohol phase medium；
(7) take 3～6 fruits powder, 2～4 parts of alcohol phase mediums, 6～8 parts of oil-phase mediums, 6～12 parts of fruit and vegerable lixiviate cream mix homogeneously, obtain anthocyanidin cream pack.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610159450.4A CN105708782A (en) | 2016-03-21 | 2016-03-21 | Preparation method of anthocyanin cream pack |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610159450.4A CN105708782A (en) | 2016-03-21 | 2016-03-21 | Preparation method of anthocyanin cream pack |
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| Publication Number | Publication Date |
|---|---|
| CN105708782A true CN105708782A (en) | 2016-06-29 |
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| CN201610159450.4A Pending CN105708782A (en) | 2016-03-21 | 2016-03-21 | Preparation method of anthocyanin cream pack |
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| CN106137875A (en) * | 2016-08-24 | 2016-11-23 | 广州睿森生物科技有限公司 | A kind of compositions and facial film |
| CN106821934A (en) * | 2017-03-09 | 2017-06-13 | 马健 | A kind of after-sun cleawhite pack |
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| CN106137875A (en) * | 2016-08-24 | 2016-11-23 | 广州睿森生物科技有限公司 | A kind of compositions and facial film |
| CN106137875B (en) * | 2016-08-24 | 2018-09-28 | 广州睿森生物科技有限公司 | A kind of composition and facial mask |
| CN106821934A (en) * | 2017-03-09 | 2017-06-13 | 马健 | A kind of after-sun cleawhite pack |
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