CN105907459A - Preparation method of oil from peony seeds and Moringa oleifera seeds - Google Patents
Preparation method of oil from peony seeds and Moringa oleifera seeds Download PDFInfo
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- CN105907459A CN105907459A CN201610385112.2A CN201610385112A CN105907459A CN 105907459 A CN105907459 A CN 105907459A CN 201610385112 A CN201610385112 A CN 201610385112A CN 105907459 A CN105907459 A CN 105907459A
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- flos moutan
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- moringa seeds
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
- C11B1/04—Pretreatment of vegetable raw material
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/02—Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
- A23D9/04—Working-up
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/06—Production of fats or fatty oils from raw materials by pressing
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/10—Production of fats or fatty oils from raw materials by extracting
- C11B1/106—Production of fats or fatty oils from raw materials by extracting using ultra-sounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/001—Refining fats or fatty oils by a combination of two or more of the means hereafter
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/008—Refining fats or fatty oils by filtration, e.g. including ultra filtration, dialysis
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/12—Refining fats or fatty oils by distillation
Abstract
The invention discloses a preparation method of oil from peony seeds and Moringa oleifera seeds, and the oil has the advantages of simple processes and long-term storage without any preservatives, and the oil can embody health care values of peony seeds and Moringa oleifera seeds. The method comprises the following steps: peony seeds and Moringa oleifera seeds are cleaned and dried; shells are broken; a cold pressing machine is used for carrying out cold pressing separately; after cold pressing, crushed slags of peony seeds and Moringa oleifera seeds are dried and pulverized separately; circulated extraction is carried out with supersonic wave; finally, extracted oil from peony seeds and Moringa oleifera seeds are mixed according to a certain proportion in order to obtain the oil from peony seeds and Moringa oleifera seeds. The oil has the substantial effects for adjusting functions of human body, moistening lung, soothing intestine, beautifying and protecting skins, resisting microorganisms and inflammation, preventing aging, promoting comprehensive health of human body, and improving life quality of people.
Description
Technical field
The present invention relates to Paeonia suffruticosa edible oil processing technique field, particularly relate to the preparation method of a kind of Paeonia suffruticosa oil ben.
Background technology
Seed of Flos Moutan is the elite crystallization of peony plant, has passed on outside all characteristics that Paeonia suffruticosa itself has, and it more has medicine and the nutritional labeling of oneself uniqueness, and seed of Paeonia suffruticosa is by shell and the nut of kind shell double shielding, has natural " long-lived " gene.The vegetable oil extracted by seed of Flos Moutan is the distinctive woody macadamia nut oil of China; nutritious and unique; there is again medical care effect; peony seed oil unsaturated fatty acid content reaches more than 90%; especially estimable is that unsaturated fatty acid linolenic acid content therein is more than 40%; and it is difficult to oxide deposition at positions such as human vas wall, heart coronary arteries; especially have good protective effect to liver, these advantages make it play important function in medical science and nutrition and become preferable edible oil just.
Moringa seeds is the seed of Moringa tree, good using value is suffered from fields such as medicines and health protections, in terms of reducing blood fat and blood pressure, weight-reducing, regulation the intestines and stomach, hepatoprotective alleviating alcohol addiction and strengthening body immunity, all there is significant curative effect, it addition, it has significant effect in sterilization, weight reducing, blood fat reducing, blood pressure lowering, regulation gastrointestinal function, hepatoprotective, uvioresistant, skin moistening, nourishing hair, moisturizing etc.；Oil ben has unique characteristic, that is, the most excellent non-oxidizability, need not add any synergist or preservative in its storage, even if so, it can preserve at normal temperatures never degenerates for about 1 year, does not becomes sour, will not produce rancidity.
In order to expand the value in the edible oil field of seed of Flos Moutan, inventor have developed the preparation method of a kind of Paeonia suffruticosa oil ben, after the fluid utilizing seed of Flos Moutan and moringa seeds to be extracted merges, makes Paeonia suffruticosa Moringa edible oil；The Paeonia suffruticosa oil ben that the present invention is produced combines the health-care effect of seed of Flos Moutan and moringa seeds, such that it is able to reduce blood fat and blood pressure, regulation the intestines and stomach, the hepatoprotective of human body, reduce weight, regulate function of human body, strengthen the effect such as body immunity.
Summary of the invention
The invention aims to solve the deficiency that above-mentioned technical problem exists, it is provided that a kind of technique is simple, be not added with any preservative, can preserve, embody simultaneously the preparation method of the Paeonia suffruticosa oil ben of seed of Flos Moutan and moringa seeds health value for a long time.
The present invention first by seed of Flos Moutan and moringa seeds through over cleaning, drying, broken shell, carry out cold pressing respectively with cold pressing expeller, the most respectively seed of Flos Moutan disintegrating slag and the moringa seeds disintegrating slag of cold pressing are passed through drying, pulverize, carry out ultrasound wave circulation again to extract, finally the peony seed oil extracted and oil ben are mixed and made into Paeonia suffruticosa oil ben according to certain ratio.
The used technical scheme of the present invention is as follows:
Step one, broken shell cleaning, drying: select seed of Flos Moutan and the moringa seeds of full grains respectively, seed of Flos Moutan and moringa seeds are carried out broken shell with rejuvenator respectively, then it is carried out, with dehydrator, the seed of Flos Moutan core after cleaning is dried, dry 30 ~ 45 minutes under temperature 30-50 degree, with dehydrator, moringa seeds core after cleaning is dried 10 ~ 20 minutes, make the moisture of seed of Flos Moutan Renhe moringa seeds core control between 0.2 ~ 3%；
Step 2, cold pressing expeller cold pressing: with cold pressing expeller, the seed of Flos Moutan Renhe moringa seeds core dried in step one is carried out cold pressing respectively, and oil cold pressing gone out with defecator separates with disintegrating slag, fluid contains and preserves；The seed of Flos Moutan pressed oil that cold pressing is gone out and the modulation of moringa seeds pressed oil are mixed into Paeonia suffruticosa Moringa pressed oil；
Step 3, the drying of seed of Flos Moutan disintegrating slag, pulverizing: the seed of Flos Moutan disintegrating slag in step 2 and moringa seeds disintegrating slag are respectively put in low frequency microwave stove and carry out microwave drying, it is dried to water content less than 0.5-1%, seed of Flos Moutan disintegrating slag is respectively put into pulverizer with moringa seeds disintegrating slag pulverize, the granularity of the seed of Flos Moutan disintegrating slag after pulverizing and moringa seeds disintegrating slag is in 0.1 μm 10 μm, 1 or the interval grain size intervals of more than 1 in 0.044mm 0.074mm, 0.074-1mm；
Step 4, seed of Flos Moutan is extracted with moringa seeds disintegrating slag: the seed of Flos Moutan disintegrating slag in step 3 and the moringa seeds disintegrating slag in step 3 are respectively put in ultrasound wave circulation extractor, add the ethanol of disintegrating slag weight 10 times and the mixed liquor of petroleum ether, carry out ultrasonic extraction 20min, wherein the volume ratio of ethanol and petroleum ether is 7:3, ultrasonic power is 400W, filter after extraction, solvent is distilled off, then it is dried to constant weight in extract is placed in hot air drier, respectively obtains seed of Flos Moutan and extract oil with moringa seeds；The seed of Flos Moutan extracted is extracted oil and moringa seeds extraction oil modulation is mixed into Paeonia suffruticosa Moringa and extracts oil；
Step 5, the preparation of Paeonia suffruticosa oil ben: extract oily and edible vegetable oil by obtaining Paeonia suffruticosa Moringa in the Paeonia suffruticosa Moringa pressed oil obtained in step 2, step 4, mix, after mix homogeneously, after packing, obtain the Paeonia suffruticosa oil ben of the present invention.
The main purpose that seed of Flos Moutan and moringa seeds rejuvenator wherein carry out in step one skin breaking is to peel the shell of seed of Flos Moutan and moringa seeds off, take its core and carry out producing of Paeonia suffruticosa oil ben, because the existence of the shell of seed of Flos Moutan and moringa seeds can affect colourity and the purity extracting fluid, a lot of residue can be left during extracting oil, cause the existence having abnormal flavour in the oil produced；The difference of the time of the drying of seed of Flos Moutan and moringa seeds, the water absorption being primarily due to seed of Flos Moutan is bigger than the water absorption of moringa seeds, if drying time deficiency can not make the moisture of seed of Flos Moutan and moringa seeds control between 0.2 ~ 3%；The moisture of seed of Flos Moutan and moringa seeds controls between 0.2 ~ 3%, because moisture 0.2 ~ 3% is seed of Flos Moutan and the poised state of moringa seeds structure moisture at normal temperatures, make seed of Flos Moutan and moringa seeds by the drying functions of dehydrator because cleaning the moisture absorbed and going out；The main purpose of do so is in order to avoid seed of Flos Moutan and moringa seeds are because unnecessary water content is mixed in the oil of institute's cold pressing, thus improves the purity of Paeonia suffruticosa or oil ben, improves the edibility of Paeonia suffruticosa oil ben.
Wherein in step 2, the seed of Flos Moutan Renhe moringa seeds core dried carries out cold pressing with cold pressing expeller respectively, and pressed oil is first expressed oil, and therefore color and luster is good, taste is pure, the beneficiating ingredient of spilling is many, nutritional labeling is complete；
But the fuel-displaced ratio using the method oil of cold pressing is relatively low, there is more oil and do not extract completely in the disintegrating slag of seed of Flos Moutan and moringa seeds.
Seed of Flos Moutan pressed oil and moringa seeds pressed oil modulation mixed proportion that wherein step 2 goes out cold pressing can mix with arbitrary proportion.
Wherein in step 3, it is dried with low frequency microwave and can significantly improve dry rate, and microwave has extremely strong penetrance, heat inside and outside can realizing simultaneously, moisture migration from inside to outside can be accelerated under conditions of low power density, the seed of Flos Moutan processed through low frequency microwave can be effectively improved oil yield, and low frequency cold drying can effectively reduce nutritional labeling and lose.
Wherein in step 3, seed of Flos Moutan disintegrating slag and moringa seeds disintegrating slag being pulverized respectively with pulverizer, Task-size Controlling is in 0.1 μm 10 μm, 1 or the interval grain size intervals of more than 1 in 0.044mm 0.074mm, 0.074-1mm；Because seed of Flos Moutan, moringa seeds quality are hard, cell wall is thicker, cold pressing cannot break the cell wall of seed of Flos Moutan, moringa seeds completely, the present invention reaches superfine powder by the way of pulverizing, can make seed of Flos Moutan, the cell wall of moringa seeds is completely severed, and makes intracellular effective ingredient the most fully discharge, and improves dissolution rate and the dissolution rate of effective ingredient in seed of Flos Moutan, moringa seeds, further, also synchronize to improve seed of Flos Moutan and moringa seeds oil yield.
Wherein step 4 uses ultrasonic and circulated extraction, after testing, ultrasonic and circulated extraction and traditional supercritical CO2Extraction is compared, and cost can reduce 50-60%, and extraction ratio can improve 30-65%, and technique is simple, easily operates.
The seed of Flos Moutan that wherein step 4 extracts extracts oil and moringa seeds extraction oil modulation mixed proportion is arbitrary proportion mixing.
Obtain Paeonia suffruticosa Moringa in the Paeonia suffruticosa Moringa pressed oil that wherein obtains in step 5 step 2, step 4 extracting oily and edible vegetable oil mixed proportion is that arbitrary proportion mixes.
Beneficial effects of the present invention: the present invention provides the preparation method of a kind of Paeonia suffruticosa oil ben, cold-press and ultrasonic extraction is used to combine, not only oil yield is high, and the Paeonia suffruticosa oil ben with more fully nutritive value can be obtained, the Paeonia suffruticosa oil ben produced has and is not added with any preservative, can preserve for a long time, embody seed of Flos Moutan and moringa seeds health value simultaneously, function of human body can be regulated, lung moistening width intestinal, U.S. face skin protection, anti-inflammation, defying age, and effect are notable, human body total health can be promoted, improve the quality of the life of people.
Detailed description of the invention
Being described further the present invention below in conjunction with specific embodiment, these embodiments are merely to illustrate the present invention rather than limit the scope of the present invention.
Embodiment 1
A kind of preparation method of Paeonia suffruticosa oil ben:
Step one, broken shell cleaning, drying: select seed of Flos Moutan and the moringa seeds of full grains respectively, seed of Flos Moutan and moringa seeds are carried out broken shell with rejuvenator respectively, then it is carried out, with dehydrator, the seed of Flos Moutan core after cleaning is dried, dry 45 minutes at temperature 30 degree, with dehydrator, moringa seeds core after cleaning is dried 10 minutes, make the moisture of seed of Flos Moutan Renhe moringa seeds core control between 0.2%；
Step 2, cold pressing expeller cold pressing: with cold pressing expeller, the seed of Flos Moutan Renhe moringa seeds core dried in step one is carried out cold pressing respectively, and oil cold pressing gone out with defecator separates with disintegrating slag, fluid contains and preserves；The seed of Flos Moutan pressed oil that cold pressing is gone out and the modulation of moringa seeds pressed oil are mixed into Paeonia suffruticosa Moringa pressed oil；
Step 3, the drying of seed of Flos Moutan disintegrating slag, pulverizing: the seed of Flos Moutan disintegrating slag in step 2 and moringa seeds disintegrating slag are respectively put in low frequency microwave stove and carry out microwave drying, it is dried to water content less than 0.5%, seed of Flos Moutan disintegrating slag is respectively put into pulverizer with moringa seeds disintegrating slag pulverize, the granularity of the seed of Flos Moutan disintegrating slag after pulverizing and moringa seeds disintegrating slag is in 0.1 μm 10 μm, 1 or the interval grain size intervals of more than 1 in 0.044mm 0.074mm, 0.074-1mm；
Step 4, seed of Flos Moutan is extracted with moringa seeds disintegrating slag: the seed of Flos Moutan disintegrating slag in step 3 and the moringa seeds disintegrating slag in step 3 are respectively put in ultrasound wave circulation extractor, add the ethanol of disintegrating slag weight 10 times and the mixed liquor of petroleum ether, carry out ultrasonic extraction 20min, wherein the volume ratio of ethanol and petroleum ether is 7:3, ultrasonic power is 400W, filter after extraction, solvent is distilled off, then it is dried to constant weight in extract is placed in hot air drier, respectively obtains seed of Flos Moutan and extract oil with moringa seeds；The seed of Flos Moutan extracted is extracted oil and moringa seeds extraction oil modulation is mixed into Paeonia suffruticosa Moringa and extracts oil；
Step 5, the preparation of Paeonia suffruticosa oil ben: extract oily and edible vegetable oil by obtaining Paeonia suffruticosa Moringa in the Paeonia suffruticosa Moringa pressed oil obtained in step 2, step 4, mix, after mix homogeneously, after packing, obtain the Paeonia suffruticosa oil ben of the present invention.
Embodiment 2
A kind of preparation method of Paeonia suffruticosa oil ben:
Step one, broken shell cleaning, drying: select seed of Flos Moutan and the moringa seeds of full grains respectively, seed of Flos Moutan and moringa seeds are carried out broken shell with rejuvenator respectively, then it is carried out, with dehydrator, the seed of Flos Moutan core after cleaning is dried, dry 30 minutes at temperature 50 degree, with dehydrator, moringa seeds core after cleaning is dried 20 minutes, make the moisture of seed of Flos Moutan Renhe moringa seeds core control between 3%；
Step 2, cold pressing expeller cold pressing: with cold pressing expeller, the seed of Flos Moutan Renhe moringa seeds core dried in step one is carried out cold pressing respectively, and oil cold pressing gone out with defecator separates with disintegrating slag, fluid contains and preserves；The seed of Flos Moutan pressed oil that cold pressing is gone out and the modulation of moringa seeds pressed oil are mixed into Paeonia suffruticosa Moringa pressed oil；
Step 3, the drying of seed of Flos Moutan disintegrating slag, pulverizing: the seed of Flos Moutan disintegrating slag in step 2 and moringa seeds disintegrating slag are respectively put in low frequency microwave stove and carry out microwave drying, it is dried to water content less than 1%, seed of Flos Moutan disintegrating slag is respectively put into pulverizer with moringa seeds disintegrating slag pulverize, the granularity of the seed of Flos Moutan disintegrating slag after pulverizing and moringa seeds disintegrating slag is in 0.1 μm 10 μm, 1 or the interval grain size intervals of more than 1 in 0.044mm 0.074mm, 0.074-1mm；
Step 4, seed of Flos Moutan is extracted with moringa seeds disintegrating slag: the seed of Flos Moutan disintegrating slag in step 3 and the moringa seeds disintegrating slag in step 3 are respectively put in ultrasound wave circulation extractor, add the ethanol of disintegrating slag weight 10 times and the mixed liquor of petroleum ether, carry out ultrasonic extraction 20min, wherein the volume ratio of ethanol and petroleum ether is 7:3, ultrasonic power is 400W, filter after extraction, solvent is distilled off, then it is dried to constant weight in extract is placed in hot air drier, respectively obtains seed of Flos Moutan and extract oil with moringa seeds；The seed of Flos Moutan extracted is extracted oil and moringa seeds extraction oil modulation is mixed into Paeonia suffruticosa Moringa and extracts oil；
Step 5, the preparation of Paeonia suffruticosa oil ben: extract oily and edible vegetable oil by obtaining Paeonia suffruticosa Moringa in the Paeonia suffruticosa Moringa pressed oil obtained in step 2, step 4, mix, after mix homogeneously, after packing, obtain the Paeonia suffruticosa oil ben of the present invention.
Claims (3)
1. the preparation method of a Paeonia suffruticosa oil ben, it is characterized in that: step one, broken shell cleaning, drying: select seed of Flos Moutan and the moringa seeds of full grains respectively, seed of Flos Moutan and moringa seeds are carried out broken shell with rejuvenator respectively, then it is carried out, with dehydrator, the seed of Flos Moutan core after cleaning is dried, dry 30 ~ 45 minutes under temperature 30-50 degree, with dehydrator, moringa seeds core after cleaning is dried 10 ~ 20 minutes, make the moisture of seed of Flos Moutan Renhe moringa seeds core control between 0.2 ~ 3%；Step 2, cold pressing expeller cold pressing: with cold pressing expeller, the seed of Flos Moutan Renhe moringa seeds core dried in step one is carried out cold pressing respectively, and oil cold pressing gone out with defecator separates with disintegrating slag, fluid contains and preserves；The seed of Flos Moutan pressed oil that cold pressing is gone out and the modulation of moringa seeds pressed oil are mixed into Paeonia suffruticosa Moringa pressed oil；Step 3, the drying of seed of Flos Moutan disintegrating slag, pulverizing: the seed of Flos Moutan disintegrating slag in step 2 and moringa seeds disintegrating slag are respectively put in low frequency microwave stove and carry out microwave drying, it is dried to water content less than 0.5-1%, seed of Flos Moutan disintegrating slag is respectively put into pulverizer with moringa seeds disintegrating slag and pulverizes；Step 4, seed of Flos Moutan is extracted with moringa seeds disintegrating slag: the seed of Flos Moutan disintegrating slag in step 3 and the moringa seeds disintegrating slag in step 3 are respectively put in ultrasound wave circulation extractor, add the ethanol of disintegrating slag weight 10 times and the mixed liquor of petroleum ether, carry out ultrasonic extraction 20min, ultrasonic power is 400W, filter after extraction, solvent is distilled off, is dried to constant weight in then extract is placed in hot air drier, respectively obtain seed of Flos Moutan and extract oil with moringa seeds；The seed of Flos Moutan extracted is extracted oil and moringa seeds extraction oil modulation is mixed into Paeonia suffruticosa Moringa and extracts oil；Step 5, the preparation of Paeonia suffruticosa oil ben: extract oily and edible vegetable oil by obtaining Paeonia suffruticosa Moringa in the Paeonia suffruticosa Moringa pressed oil obtained in step 2, step 4, mix, after mix homogeneously, after packing, obtain the Paeonia suffruticosa oil ben of the present invention.
The preparation method of a kind of Paeonia suffruticosa oil ben the most according to claim 1, it is characterized in that: the granularity of seed of Flos Moutan disintegrating slag and moringa seeds disintegrating slag after pulverizing in step 3 is in 0.1 μm 10 μm, 1 or the interval grain size intervals of more than 1 in 0.044mm 0.074mm, 0.074-1mm.
The preparation method of a kind of Paeonia suffruticosa oil ben the most according to claim 1, it is characterised in that: in step 4, the volume ratio of ethanol and petroleum ether is 7:3.
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| CN106561843A (en) * | 2016-11-17 | 2017-04-19 | 河南洛阳红牡丹产业研发有限公司 | Method for preparing peony and sunflower seed oil |
| CN107699336A (en) * | 2017-10-27 | 2018-02-16 | 山东三星玉米产业科技有限公司 | The preparation method of anti-oxidant corn ready-mixed oil |
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| CN107699336A (en) * | 2017-10-27 | 2018-02-16 | 山东三星玉米产业科技有限公司 | The preparation method of anti-oxidant corn ready-mixed oil |
| CN108271865A (en) * | 2017-12-29 | 2018-07-13 | 河南洛阳红牡丹产业研发有限公司 | A kind of production method of tree peony fresh milk |
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Application publication date: 20160831 |