CN103520064A - Blueberry lees nutritional mask and preparation method thereof - Google Patents
Blueberry lees nutritional mask and preparation method thereof Download PDFInfo
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- CN103520064A CN103520064A CN201310521959.5A CN201310521959A CN103520064A CN 103520064 A CN103520064 A CN 103520064A CN 201310521959 A CN201310521959 A CN 201310521959A CN 103520064 A CN103520064 A CN 103520064A
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Abstract
The invention discloses a blueberry lees nutritional mask and a preparation method thereof. The blueberry lees nutritional mask is mainly prepared through the steps that: blueberry lees are subjected to treatment steps such as juice removing and impurity removing, and is mixed with a film-forming substance, a moisturizing agent, a preservative, an antioxidant, pearl powder, aromatic substance, and vitamin, such that the mask is obtained. The mask is composed of the components of, by weight: 45 parts of a mask base liquid, 50-60 parts of pretreated blueberry lees, 2-3 parts of the moisturizing agent, 0.2-0.5 parts of the preservative, 0.1-0.2 parts of the antioxidant, 4-8 parts of the pearl powder, 0.02-0.04 parts of natural aromatic oil, and 3-6 parts of Vitamin E. According to the invention, lees produced during blueberry wine brewing are reasonably utilized, such that natural active components and nutritional health-care functional factors in the lees are utilized to a maximal extent. Therefore, application value and economic value of the lees are greatly improved. The product provided by the invention has nourishing, whitening, anti-oxidizing, anti-aging, antibacterial, anti-inflammatory, spot-removing, and other functions. With the mask, requirements of nourishing, health-care, and beautifying can be satisfied.
Description
Technical field
The present invention relates to nourishing pack preparation method, especially relate to a kind of nourishing pack preparation method that blueberry wine mud is primary raw material of take.
Background technology
Blue berry is a kind of evergreen shrubs, and fruit is blue berry.Blueberry juice is abundant, except containing conventional sugar, acid and Vc, is also rich in V
e, V
a, V
b, SOD, arbutin, protein, anthocyanidin, edible fiber and various mineral element.Especially vitamin and anthocyanidin content are several times even tens times of general fruit, and its nutrition and health care function is that any fruit can not be compared.Wherein the anthocyanidin of rich content has antioxidation, the health care effect of waiting for a long time, and is called as mankind's number one antioxidant.One of therefore, blue berry is listed in one of " the large health food of the mankind five " the large best nutritional food in the ，He“ world ten ".Blueberry wine has retained nutritional labeling and the health factor of natural blue berry to greatest extent, and long-term drink has looks improving and the skin nourishing, reduces the effects such as blood fat, slow down aging, enhancing immunity, anti-curing cancers.Blueberry wine is the superfine product in fruit wine, is described as " queen in wine ", " liquid golden " and " oral mankind's cosmetics ".
Exploitation blue berry fruit wine, can not only provide new fruit wine kind for drinks market, meets consumer demand, and can also bring good Social benefit and economic benefit.Main By product in brewing fruit wine is wine mud, contains a large amount of fruit residue and saccharomyces cerevisiae in wine mud, directly discharges not only serious environment pollution, and causes the wasting of resources.Saccharomyces cerevisiae starts self-dissolving after alcohol fermentation finishes, and yeast cells autolysate is mainly deposited in wine mud with the form of glycoprotein.Medical research shows that these zymosans have the effect of good immunocompetence and inhibition tumor growth, can increase the toxin in cell immunocompetent, adherent cell and be got rid of external.The wine mud producing in brewing fruit wine at present is mainly processed to organic fertilizer, animal feed etc.For blueberry wine mud, wherein except containing a large amount of saccharomyces cerevisiaes, in fruit residue, also contain active skull cap components and the health factors such as abundant polyphenol substance, anthocyanidin, vitamin, aminoacid, SOD, these materials have the effects such as good removing free radical, antioxidation, anti-aging, looks improving and the skin nourishing, if be used as fertilizer, feedstuff, can not reach its due value far away.Therefore, take blueberry wine mud as a series of new products of development of raw materials, improve its application and economic worth, is the problem that those skilled in the art pay close attention to.
The present invention be take blueberry wine mud and is prepared facial film as raw material, can utilize to greatest extent active skull cap components and health factor wherein, and can greatly improve its economic worth.Up to the present, about blueberry wine mud, for the preparation of facial film, also there is not report.
Summary of the invention
Limitation at present blueberry wine mud being applied, the object of this invention is to provide a kind of blueberry wine mud nourishing pack and preparation method thereof.This nourishing pack has the effects such as nourishing and whitening, antioxidation, anti-aging, antibiotic, antiinflammatory, dispelling stain, can farthest utilize nutrient substance and health factor in wine mud, can greatly improve its using value and economic worth.
To achieve these goals, the present invention takes following technical solution:
A mud nourishing pack, is characterized in that this facial film made by the raw material of following weight portion:
45 parts of facial film base fluids, 50～60 parts, pretreatment blueberry wine mud, 2～3 parts of wetting agents, 0.2～0.5 part of antiseptic, 0.1～0.2 part of antioxidant, 4～8 parts of Margarita powder, 0.02～0.04 part of natural aromatic oil, 3～6 parts of vitamin Es.
Above-mentioned blueberry wine mud nourishing pack is preferably made by the raw material of following weight portion:
45 parts of facial film base fluids, 55～60 parts, pretreatment blueberry wine mud, 2～3 parts of wetting agents, 0.3～0.4 part of antiseptic, 0.1～0.2 part of antioxidant, 5～7 parts of Margarita powder, 0.02～0.03 part of natural aromatic oil, 4～5 parts of vitamin Es.
Described wetting agent is preferably glycerol; Antiseptic is preferably methyl hydroxybenzoate; Antioxidant is preferably dibenzylatiooluene.
Above-mentioned facial film base fluid is the mixture that solution A and solution B form by weight 2:1; Wherein, solution A is the mixed aqueous solution that citric acid and chitosan form; Solution B is the mixed aqueous solution that sodium carboxymethyl cellulose and gelatin form.It is the mixed aqueous solution that 8%～10% citric acid and the mass concentration chitosan that is 6%～8% forms that solution A is preferably mass concentration; It is the mixed aqueous solution that 3%～4% sodium carboxymethyl cellulose and the mass concentration gelatin that is 3%～4% forms that solution B is preferably mass concentration.Most preferably solution A is that mass concentration is the mixed aqueous solution that 10% citric acid and the mass concentration chitosan that is 8% forms; Most preferably solution B is that mass concentration is the mixed aqueous solution that 3% sodium carboxymethyl cellulose and the mass concentration gelatin that is 3% forms.The concrete preparation method of described facial film base fluid is: 1) chitosan and citric acid are added in deionized water, be heated to 60～70 ℃ it is dissolved completely, stir and make solution A; 2) sodium carboxymethyl cellulose and gelatin are added in deionized water, be heated to 50～60 ℃ it is dissolved completely, stir and make solution B; 3) in temperature, be under 40～50 ℃ of conditions, solution B is mixed homogeneously and obtained facial film base fluid by weight 2:1 with solution A.
In above-mentioned blueberry wine mud nourishing pack, the pre-treatment step of pretreatment blueberry wine mud is: by flocculation, centrifugal, ultrasonic, filtration, blueberry wine mud is taken off to juice, remove impurity.
Described flocculation treatment is, adds blueberry wine mud to weigh 0.2%～0.4% composite flocculation agent, stirs 20～30 minutes, and wherein, composite flocculation agent is that bodied ferric sulfate and chitosan are according to the mixture of weight ratio 1:1; Described centrifugal treating is, by the wine mud after flocculation under 4000g/min centrifugal 15～20 minutes, sloughs rice wine juice; Described supersound process is for to dilute in 2:1 ratio the wine mud of sloughing rice wine juice with deionized water, then ultrasound wave 500W processes 25～30 minutes; Described filtration treatment is for to remove by filter impurity by the wine mud after ultrasonic with 200 mesh filter screens.
The preparation method of above-mentioned blueberry wine mud nourishing pack comprises the following steps:
1) first by flocculation, centrifugal, ultrasonic, filtration treatment to blueberry wine mud take off juice, remove impurity obtains pretreatment blueberry wine mud;
2) prepare solution A: citric acid and chitosan are mixed and made into aqueous solution;
Preparation solution B: sodium carboxymethyl cellulose and gelatin are mixed and made into aqueous solution;
According to the ratio of 2:1, by solution A and solution B mix homogeneously, obtain facial film base fluid;
3) in 45 parts of facial film base fluids, add 50～60 parts, pretreatment liquor mud, 2～3 parts of wetting agents, 0.2～0.5 part of antiseptic, 0.1～0.2 part of antioxidant, 4～8 parts of Margarita powder, 0.02～0.04 part of natural aromatic oil, 3～6 parts of vitamin Es, stir, colloid mill is milled and is processed at least twice.
Inventor further illustrates the addition of chitosan in facial film after by a large amount of preliminary experiments again by following test:
1) impact of chitosan dosage on filming performance:
Get 15 parts of 3% sodium carboxymethyl cellulose and 3% gelatin-compounded solution, the chitosan aqueous solution that the concentration that adds Different Weight part is 8% (containing mass concentration in aqueous solution is 10% citric acid) also stirs, add respectively on this basis 55 parts, pretreatment blueberry wine mud, all the other carry out according to step described in embodiment 1.Get a certain amount of facial film uniform spreading of making on flat board, be cut into the rectangular of 1cm * 10cm, measure its hot strength and elongation at break, observe the impact of different chitosan dosage on film property, test result is as follows:
2) fungistatic effect of chitosan:
Get 3% sodium carboxymethyl cellulose and 3% gelatin-compounded solution 15 weight portions, the chitosan aqueous solution that the concentration that adds Different Weight part is 8% (containing mass concentration in aqueous solution is 10% citric acid) stirs, add respectively on this basis pretreatment blueberry wine mud 55 weight portions and obtain different mixtures, then getting different mixtures joins in bacterium solid culture medium by weight 1:5 ratio, on flat board, be coated with equivalent, isocyatic lactic acid bacteria culture solution, observe its fungistatic effect, result is as follows:
Consider the impact of chitosan dosage on filming performance and fungistatic effect, it is 30 weight portions that the chitosan aqueous solution that preferred concentration is 8% (containing mass concentration in aqueous solution is 10% citric acid) is added parts by weight.
The invention provides a kind of blueberry wine mud nourishing pack and preparation method thereof.In blueberry wine mud, contain the active skull cap components such as abundant zymosan, polyphenol substance, anthocyanidin, vitamin, aminoacid, SOD, there is the effects such as the cellular immunity of increasing, toxin expelling, removing free radical.The present invention uses sodium carboxymethyl cellulose and gelatin as film forming matter in facial film, and it is fast that these two kinds of materials have film forming under 1:1 content, the features such as film forming is flexible, difficult fragmentation; In addition, also added a certain amount of natural alkaline polysaccharide chitosan, it not only has the auxiliary filming performances such as good toughness, extensibility, also has the effects such as immunity that antibacterial, antiinflammatory, enhancing skin are infected antibacterial simultaneously.In addition, by the pretreatment of blueberry wine mud not only having been kept to the effective ingredient in wine mud, also reduced the too much stimulation of ethanol to skin in wine mud simultaneously.
Compared with prior art, facial film of the present invention has the effects such as nourishing and whitening, antioxidation, anti-aging, antibiotic, antiinflammatory, dispelling stain, meets the needs that society people pursue looks improving and the skin nourishing; Utilize that wine is clay has reduced the pollution of wine mud discharge to environment as facial film, turn waste into wealth, make rational use of resources, reduce the wasting of resources, with utilize the clay fertilizer of doing of blueberry wine and compare with feedstuff, utilize it to make nourishing pack, more fully, rationally utilized nutrient substance and health factor wherein, greatly improved its application and economic worth; Meanwhile, the inventive method is simple to operate, saves time, and cost is low.
The specific embodiment
By specific embodiment, further illustrate the present invention below.But the detail of embodiment only, for explaining the present invention, should not be construed as limited overall technical solution.
Wine mud preparation method: select the Vaccinium ashei fruit of abundant maturation, add fermentation tank, SO after making beating fragmentation
2after processing, add compound pectinase 50mg/L, sucrose 100g/L, yeast 800mg/L, stir, make temperature be controlled at 25 ℃～28 ℃ lucifuge fermentations; When fermentation liquid proportion is less than 0.996, measure pol and alcoholic strength, when pol is less than 2g/L, separated termination fermented immediately, and gained fermentation tank lower sediment is blueberry wine mud.
Embodiment 1:
Get fermentation and just finished the blueberry wine mud 1kg obtaining, add composite flocculation agent bodied ferric sulfate and chitosan according to the mixture 2g of weight ratio 1:1, stir 20 minutes, under 4000g/min centrifugal 15 minutes, supernatant discarded, obtained wine mud 0.72kg.The wine mud of sloughing wine juice after centrifugal is diluted with deionized water, and the part by weight of wine mud and deionized water is 2:1, and ultrasound wave 500W processes 25 minutes, then with 200 mesh filter screens, removes by filter impurity, obtains pretreatment blueberry wine mud.4g chitosan, 5g citric acid are added in 50ml deionized water, be heated to 60 ℃ it is dissolved completely, stir and make solution A; Sodium carboxymethyl cellulose and each 1.5g of gelatin are added in 50ml deionized water, be heated to 50 ℃ it is dissolved completely, stir and make solution B.At 45 ℃, 15g solution B is joined in 30g solution A, be constantly uniformly mixed to obtain 45g facial film base fluid.In facial film base fluid, add pretreatment blueberry wine mud 55g, glycerol 2g, methyl hydroxybenzoate 0.3g, dibenzylatiooluene 0.1g, Margarita powder 5g, the natural aromatic oil 0.02g(Guangzhou Chinese one hundred this daily use chemicals development in science and technology company limited to produce), vitamin E 4g, stir, milling treatment of colloid obtains blueberry wine mud nourishing pack for twice.
Embodiment 2:
Get fermentation and just finished the blueberry wine mud 2kg obtaining, add composite flocculation agent bodied ferric sulfate and chitosan to stir 30 minutes according to the mixture 6g of weight ratio 1:1, under 4000g/min centrifugal 20 minutes, supernatant discarded, obtained wine mud 1.45kg.By centrifugal slough after rice wine juice wine mud add deionized water 0.725kg and dilute, ultrasound wave 500W processes 30 minutes, then with 200 mesh filter screens, removes by filter impurity, obtains pretreatment blueberry wine mud.8g chitosan, 10g citric acid are added in 100ml deionized water, be heated to 70 ℃ it is dissolved completely, stir and make solution A; Sodium carboxymethyl cellulose and each 3g of gelatin are added in 100ml deionized water, be heated to 60 ℃ it is dissolved completely, stir and make solution B.At 50 ℃, 30g solution B is joined in 60g solution A, be constantly uniformly mixed to obtain facial film base fluid.In facial film base fluid, add the blueberry wine mud 120g, the glycerol 6g that processed, methyl hydroxybenzoate 0.8g, dibenzylatiooluene 0.4g, Margarita powder 14g, the natural aromatic oil 0.06g(Guangzhou Chinese one hundred this daily use chemicals development in science and technology company limited to produce), vitamin e1 0g, stir, milling treatment of colloid obtains blueberry wine mud nourishing pack for twice.
Below by concrete clinical trial example explanation effect of the present invention:
(1) take embodiment blueberry wine mud facial film is test sample, and choosing has xerosis cutis, has young volunteer 25 people of acne on probation, and the age is 20～35 years old.Before experimenter sleeps every day after cleaning skin, use clear water cleaning skin after blueberry wine mud facial film is spread on to facial 15-20 minute, 2 times weekly 4 weeks is 1 cycle again.After 4 weeks, statistical result shows: effective (show as skin and obviously bleach, exquisiteness Paint Gloss, acne is obviously desalinated.) 23 people, account for 92%; Effectively (show as whiteness of skin, smooth, acne desalination.) be 1 people, account for 4.0%; Unfruitful is 1 people, accounts for 4%.Therefore, blueberry wine mud facial film has obvious moisturizing whitening function and antimicrobial and anti-inflammation efficacy, and above-mentioned person on probation does not all produce any side effect and untoward reaction.
(2) take embodiment blueberry wine mud facial film is test sample, and choosing has more person in middle and old age's volunteer 25 people of skin splash on probation, and the age is 40～60 years old.Before experimenter sleeps every day after cleaning skin, use clear water cleaning skin after blueberry wine mud facial film is spread on to facial 15-20 minute, 2 times weekly 4 weeks is 1 cycle again.After 4 weeks, statistical result shows: effective (show as skin and obviously bleach, smooth exquisiteness, mottle obviously reduces, wrinkle desalination.) be 22 people, account for 88%; Effectively (show as whiteness of skin, smooth, mottle, wrinkle desalination.) be 2 people, account for 8.0%; Unfruitful is 1 people, accounts for 4%.Therefore, blueberry wine mud facial film has obvious antioxidation, anti-aging, dispelling stain effect, and above-mentioned person on probation does not all produce any side effect and untoward reaction.
Claims (10)
1. a blueberry wine mud nourishing pack, is characterized in that this facial film made by the raw material of following weight portion:
45 parts of facial film base fluids, 50～60 parts, pretreatment blueberry wine mud, 2～3 parts of wetting agents, 0.2～0.5 part of antiseptic, 0.1～0.2 part of antioxidant, 4～8 parts of Margarita powder, 0.02～0.04 part of natural aromatic oil, 3～6 parts of vitamin Es.
2. blueberry wine mud nourishing pack according to claim 1, is characterized in that this facial film made by the raw material of following weight portion:
45 parts of facial film base fluids, 55～60 parts, pretreatment blueberry wine mud, 2～3 parts of wetting agents, 0.3～0.4 part of antiseptic, 0.1～0.2 part of antioxidant, 5～7 parts of Margarita powder, 0.02～0.03 part of natural aromatic oil, 4～5 parts of vitamin Es.
3. blueberry wine mud nourishing pack according to claim 1, is characterized in that described wetting agent is glycerol; Antiseptic is methyl hydroxybenzoate; Antioxidant is dibenzylatiooluene.
4. blueberry wine mud nourishing pack according to claim 1 and 2, is characterized in that, described facial film base fluid is the mixture that solution A and solution B are mixed by weight 2:1; Wherein, solution A is the mixed aqueous solution that citric acid and chitosan form; Solution B is the mixed aqueous solution that sodium carboxymethyl cellulose and gelatin form.
5. blueberry wine mud nourishing pack according to claim 4, is characterized in that, solution A is that mass concentration is the mixed aqueous solution that 8%～10% citric acid and the mass concentration chitosan that is 6%～8% forms; Solution B is that mass concentration is the mixed aqueous solution that 3%～4% sodium carboxymethyl cellulose and the mass concentration gelatin that is 3%～4% forms.
6. blueberry wine mud nourishing pack according to claim 1 and 2, is characterized in that the concrete pre-treatment step of described pretreatment blueberry wine mud is: by the flocculation of blueberry wine mud, centrifugal, ultrasonic, filtering and impurity removing.
7. blueberry wine mud nourishing pack according to claim 6, it is characterized in that described flocculation, centrifugal treating are: in blueberry wine mud, add composite flocculation agent, stir 20～30 minutes, wherein, composite flocculation agent is that bodied ferric sulfate and chitosan are according to the mixture of weight ratio 1:1; Then under 4000g/min centrifugal 15～20 minutes, slough rice wine juice.
8. blueberry wine mud nourishing pack according to claim 7, the addition that it is characterized in that described composite flocculation agent is that blueberry wine mud weighs 0.2%～0.4%.
9. blueberry wine mud nourishing pack according to claim 6, it is characterized in that described ultrasonic and filtration treatment is for to dilute in 2:1 ratio the wine mud of sloughing rice wine juice with deionized water, then ultrasound wave 500W processes 25～30 minutes, finally with 200 mesh filter screens, removes by filter impurity.
10. a preparation method for the blueberry wine mud nourishing pack described in claim 1 or 2, is characterized in that the method follows these steps to be prepared:
1) first by flocculation, centrifugal, ultrasonic, filter to blueberry wine mud take off juice, remove impurity processing obtains pretreatment blueberry wine mud;
2) prepare solution A: citric acid and chitosan are mixed and made into aqueous solution;
Preparation solution B: sodium carboxymethyl cellulose and gelatin are mixed and made into aqueous solution;
According to the ratio of 2:1, by solution A and solution B mix homogeneously, obtain facial film base fluid;
3) in 45 weight portion facial film base fluids, add pretreatment blueberry wine mud 50～60 weight portions, wetting agent 2～3 weight portions, antiseptic 0.2～0.5 weight portion, antioxidant 0.1～0.2 weight portion, Margarita powder 4～8 weight portions, natural aromatic oil 0.02～0.04 weight portion, vitamin E 3～6 weight portions, stir, colloid mill is milled and is processed at least twice.
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Cited By (3)
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| CN105708782A (en) * | 2016-03-21 | 2016-06-29 | 赵洪军 | Preparation method of anthocyanin cream pack |
| CN106580803A (en) * | 2017-01-18 | 2017-04-26 | 贵州省生物研究所 | Natural mask |
| CN108354848A (en) * | 2018-03-01 | 2018-08-03 | 马海军 | A kind of dregs of grape wine clay mask and preparation method thereof |
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| CN103315926A (en) * | 2012-03-20 | 2013-09-25 | 董根荣 | Chinese medicinal facial mask possessing efficacies on removing spots and smoothing crease, and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105708782A (en) * | 2016-03-21 | 2016-06-29 | 赵洪军 | Preparation method of anthocyanin cream pack |
| CN106580803A (en) * | 2017-01-18 | 2017-04-26 | 贵州省生物研究所 | Natural mask |
| CN108354848A (en) * | 2018-03-01 | 2018-08-03 | 马海军 | A kind of dregs of grape wine clay mask and preparation method thereof |
| CN108354848B (en) * | 2018-03-01 | 2021-09-14 | 北方民族大学 | Wine lees mask and preparation method thereof |
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| CN103520064B (en) | 2015-04-08 |
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