CN103520064B - Blueberry lees nutritional mask and preparation method thereof - Google Patents
Blueberry lees nutritional mask and preparation method thereof Download PDFInfo
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- CN103520064B CN103520064B CN201310521959.5A CN201310521959A CN103520064B CN 103520064 B CN103520064 B CN 103520064B CN 201310521959 A CN201310521959 A CN 201310521959A CN 103520064 B CN103520064 B CN 103520064B
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Abstract
The invention discloses a blueberry lees nutritional mask and a preparation method thereof. The blueberry lees nutritional mask is mainly prepared through the steps that: blueberry lees are subjected to treatment steps such as juice removing and impurity removing, and is mixed with a film-forming substance, a moisturizing agent, a preservative, an antioxidant, pearl powder, aromatic substance, and vitamin, such that the mask is obtained. The mask is composed of the components of, by weight: 45 parts of a mask base liquid, 50-60 parts of pretreated blueberry lees, 2-3 parts of the moisturizing agent, 0.2-0.5 parts of the preservative, 0.1-0.2 parts of the antioxidant, 4-8 parts of the pearl powder, 0.02-0.04 parts of natural aromatic oil, and 3-6 parts of Vitamin E. According to the invention, lees produced during blueberry wine brewing are reasonably utilized, such that natural active components and nutritional health-care functional factors in the lees are utilized to a maximal extent. Therefore, application value and economic value of the lees are greatly improved. The product provided by the invention has nourishing, whitening, anti-oxidizing, anti-aging, antibacterial, anti-inflammatory, spot-removing, and other functions. With the mask, requirements of nourishing, health-care, and beautifying can be satisfied.
Description
Technical field
The present invention relates to nourishing pack preparation method, especially relate to a kind of nourishing pack preparation method being primary raw material with blueberry wine mud.
Background technology
Blue berry is a kind of evergreen shrubs, and fruit is blue berry.Blueberry juice enriches, and except containing except conventional sugar, acid and Vc, is also rich in V
e, V
a, V
b, SOD, arbutin, protein, anthocyanidin, edible fiber and various mineral element.Especially vitamin and anthocyanidin content are several times even tens times of general fruit, and its nutrition and health care function is that any one fruit can not be compared.Wherein the anthocyanidin of rich content has antioxidation, health care waits for a long time effect, is called as mankind's number one antioxidant.One of therefore, blue berry is listed in one of " the large health food of the mankind five ", and " the large best nutritional food in the world ten ".Blueberry wine remains nutritional labeling and the health factor of natural blueberry to greatest extent, and long-term drink has looks improving and the skin nourishing, reduces the effects such as blood fat, slow down aging, enhancing immunity, anti-curing cancers.Blueberry wine is the superfine product in fruit wine, is described as " in wine queen ", " liquid golden " and " oral humanization cosmetic ".
Exploitation blueberry fruit wine, can not only provide new fruit wine kind for Ko-ji insects, meet consumer demand, and can also bring good Social benefit and economic benefit.Main By product in brewing fruit wine is wine mud, containing a large amount of fruit residues and saccharomyces cerevisiae in wine mud, directly discharges not only serious environment pollution, and causes the wasting of resources.Saccharomyces cerevisiae starts self-dissolving after alcohol fermentation terminates, and yeast cells autolysate is mainly deposited in wine mud with the form of glycoprotein.Medical research shows that these zymosans have the effect of good immunocompetence and Tumor suppression growth, can increase the toxin in cell immunocompetent, adherent cell and be got rid of external.The wine mud produced in current brewing fruit wine is mainly processed to organic fertilizer, animal feed etc.For blueberry wine mud, wherein except containing except a large amount of saccharomyces cerevisiaes, also containing abundant active skull cap components and the health factor such as polyphenol substance, anthocyanidin, vitamin, aminoacid, SOD in fruit residue, these materials have the effects such as good scavenging free radicals, antioxidation, anti-aging, looks improving and the skin nourishing, if be used as fertilizer, feedstuff, its due value can not be reached far away.Therefore, with blueberry wine mud for a series of new product of development of raw materials, improving its application and economic worth, is the problem that those skilled in the art pay close attention to.
The present invention for facial film prepared by raw material, can utilize active skull cap components wherein and health factor with blueberry wine mud to greatest extent, and can greatly improve its economic worth.Up to the present, be used for the preparation of facial film about blueberry wine mud and also do not have report.
Summary of the invention
For the current limitation to the application of blueberry wine mud, the object of this invention is to provide a kind of blueberry wine mud nourishing pack and preparation method thereof.This nourishing pack has the effects such as nourishing and whitening, antioxidation, anti-aging, antibacterial, antiinflammatory, dispelling stain, farthest can utilize the nutrient substance in wine mud and health factor, can greatly improve its using value and economic worth.
To achieve these goals, the present invention takes following technical solution:
A kind of blueberry wine mud nourishing pack, is characterized in that this facial film is made up of the raw material of following weight portion:
Facial film base fluid 45 parts, 50 ~ 60 parts, pretreatment blueberry wine mud, wetting agent 2 ~ 3 parts, antiseptic 0.2 ~ 0.5 part, antioxidant 0.1 ~ 0.2 part, Margarita powder 4 ~ 8 parts, natural aromatic oil 0.02 ~ 0.04 part, vitamin E 3 ~ 6 parts.
Above-mentioned blueberry wine mud nourishing pack is preferably made up of the raw material of following weight portion:
Facial film base fluid 45 parts, 55 ~ 60 parts, pretreatment blueberry wine mud, wetting agent 2 ~ 3 parts, antiseptic 0.3 ~ 0.4 part, antioxidant 0.1 ~ 0.2 part, Margarita powder 5 ~ 7 parts, natural aromatic oil 0.02 ~ 0.03 part, vitamin E 4 ~ 5 parts.
Described wetting agent is preferably glycerol; Antiseptic is preferably methyl hydroxybenzoate; Antioxidant is preferably dibenzylatiooluene.
Above-mentioned facial film base fluid is the mixture that solution A and solution B form by weight 2:1; Wherein, solution A is the mixed aqueous solution of citric acid and chitosan composition; Solution B is the mixed aqueous solution of sodium carboxymethyl cellulose and gelatin composition.Solution A is preferably mass concentration to be 8% ~ 10% citric acid and mass concentration be 6% ~ 8% the mixed aqueous solution of chitosan composition; Solution B is preferably mass concentration to be 3% ~ 4% sodium carboxymethyl cellulose and mass concentration be 3% ~ 4% the mixed aqueous solution of gelatin composition.Most preferably solution A is mass concentration to be 10% citric acid and mass concentration be 8% the mixed aqueous solution of chitosan composition; Most preferably solution B is mass concentration to be 3% sodium carboxymethyl cellulose and mass concentration be 3% the mixed aqueous solution of gelatin composition.The preparation method that described facial film base fluid is concrete is: 1) add in deionized water by chitosan and citric acid, is heated to 60 ~ 70 DEG C and makes it dissolve completely, stir and make solution A; 2) sodium carboxymethyl cellulose and gelatin are added in deionized water, be heated to 50 ~ 60 DEG C and make it dissolve completely, stir and make solution B; 3) under temperature is 40 ~ 50 DEG C of conditions, solution B and solution A are mixed homogeneously by weight 2:1 and obtains facial film base fluid.
In above-mentioned blueberry wine mud nourishing pack, the pre-treatment step of pretreatment blueberry wine mud is: by flocculation, centrifugal, ultrasonic, filtration, carry out de-juice, remove impurity to blueberry wine mud.
Described flocculation treatment is, adds the composite flocculation agent that blueberry wine mud weighs 0.2% ~ 0.4%, stirs 20 ~ 30 minutes, and wherein, composite flocculation agent is bodied ferric sulfate and the chitosan mixture according to weight ratio 1:1; Described centrifugal treating is, by the wine mud after flocculation under 4000g/min centrifugal 15 ~ 20 minutes, sloughs rice wine juice; Described supersound process is diluted by 2:1 ratio with demineralised water by the wine mud sloughing rice wine juice, then ultrasound wave 500W process 25 ~ 30 minutes; Described filtration treatment is crossed with 200 mesh filter screens by the wine mud after ultrasonic to filter impurity.
The preparation method of above-mentioned blueberry wine mud nourishing pack comprises the following steps:
1) first by flocculation, centrifugal, ultrasonic, filtration treatment carries out de-juice to blueberry wine mud, remove impurity obtains pretreatment blueberry wine mud;
2) solution A is prepared: citric acid and chitosan are mixed and made into aqueous solution;
Preparation solution B: sodium carboxymethyl cellulose and gelatin are mixed and made into aqueous solution;
According to the ratio of 2:1 by solution A and solution B mix homogeneously, obtain facial film base fluid;
3) in 45 parts of facial film base fluids, add 50 ~ 60 parts, pretreatment liquor mud, wetting agent 2 ~ 3 parts, antiseptic 0.2 ~ 0.5 part, antioxidant 0.1 ~ 0.2 part, Margarita powder 4 ~ 8 parts, natural aromatic oil 0.02 ~ 0.04 part, vitamin E 3 ~ 6 parts, stir, colloid mill is milled and is processed at least twice.
Inventor is by further illustrating the addition of chitosan in facial film again by following test after a large amount of preliminary experiments:
1) chitosan dosage is on the impact of filming performance:
Get 3% sodium carboxymethyl cellulose and 3% gelatin-compounded solution 15 parts, the concentration adding Different Weight part is the chitosan aqueous solution of 8% (containing mass concentration in aqueous solution is 10% citric acid) and stirs, add 55 parts, pretreatment blueberry wine mud respectively on this basis, all the other carry out according to step described in embodiment 1.Get a certain amount of facial film uniform spreading made on flat board, be cut into the rectangular of 1cm × 10cm, measure its hot strength and elongation at break, observe the impact of different chitosan dosage on film property, test result is as follows:
2) fungistatic effect of chitosan:
Get 3% sodium carboxymethyl cellulose and 3% gelatin-compounded solution 15 weight portion, the concentration adding Different Weight part is that the chitosan aqueous solution of 8% (containing mass concentration in aqueous solution is 10% citric acid) stirs, add pretreatment blueberry wine mud 55 weight portion on this basis respectively and obtain different mixtures, then getting different mixtures joins in bacterium solid culture medium by weight 1:5 ratio, flat board is coated with equivalent, isocyatic lactic acid bacteria culture solution, observe its fungistatic effect, result is as follows:
Consider the impact of chitosan dosage on filming performance and fungistatic effect, preferred concentration be 8% chitosan aqueous solution (in aqueous solution be 10% citric acid containing mass concentration) to add parts by weight be 30 weight portions.
The invention provides a kind of blueberry wine mud nourishing pack and preparation method thereof.Containing the abundant active skull cap components such as zymosan, polyphenol substance, anthocyanidin, vitamin, aminoacid, SOD in blueberry wine mud, there is effects such as increasing cellular immunity, toxin expelling, scavenging free radicals.The present invention uses sodium carboxymethyl cellulose and gelatin as film forming matter in facial film, and it is fast that these two kinds of materials have film forming under 1:1 content, and film forming is flexible, the not easily feature such as broken; In addition, also add a certain amount of natural alkaline polysaccharide chitosan, it not only has the auxiliary filming performances such as good toughness, extensibility, also has antibacterial, antiinflammatory, enhancing skin to effects such as the immunity of bacteriological infection simultaneously.In addition, by not only maintaining the effective ingredient in wine mud to the pretreatment of blueberry wine mud, to decrease in wine mud too much ethanol to the stimulation of skin simultaneously.
Compared with prior art, facial film of the present invention has the effects such as nourishing and whitening, antioxidation, anti-aging, antibacterial, antiinflammatory, dispelling stain, meets the needs that society people pursue looks improving and the skin nourishing; Utilize that wine is clay decreases the pollution of wine mud discharge to environment as facial film, turn waste into wealth, make rational use of resources, reduce the wasting of resources, compare with feedstuff with utilizing the clay fertilizer of doing of blueberry wine, utilize it to make nourishing pack, more fully, Appropriate application nutrient substance wherein and health factor, substantially increase its application and economic worth; Meanwhile, the inventive method is simple to operate, saves time, and cost is low.
Detailed description of the invention
The present invention is further illustrated below by way of specific embodiment.But the detail of embodiment only for explaining the present invention, should not be construed as limited overall technical solution.
Wine mud preparation method: select fully ripe Vaccinium ashei fruit, adds fermentation tank, SO after making beating fragmentation
2add compound pectinase 50mg/L, sucrose 100g/L, yeast 800mg/L after process, stir, make temperature control 25 DEG C ~ 28 DEG C lucifuge fermentations; When fermentation liquid proportion is less than 0.996, measure pol and alcoholic strength, when pol is less than 2g/L, be separated immediately and stop fermentation, gained fermentation tank lower sediment is blueberry wine mud.
Embodiment 1:
Get the blueberry wine mud 1kg that fermentation has just terminated to obtain, add composite flocculation agent bodied ferric sulfate and chitosan according to the mixture 2g of weight ratio 1:1, stir 20 minutes, under 4000g/min centrifugal 15 minutes, supernatant discarded, obtains wine mud 0.72kg.Diluted by the wine mud deionized water sloughing wine juice after centrifugal, the part by weight of wine mud and deionized water is 2:1, ultrasound wave 500W process 25 minutes, then crosses with 200 mesh filter screens and filters impurity, obtain pretreatment blueberry wine mud.4g chitosan, 5g citric acid are added in 50ml deionized water, is heated to 60 DEG C and makes it dissolve completely, stir and make solution A; Sodium carboxymethyl cellulose and each 1.5g of gelatin are added in 50ml deionized water, is heated to 50 DEG C and makes it dissolve completely, stir and make solution B.At 45 DEG C, 15g solution B is joined in 30g solution A, be constantly uniformly mixed to obtain 45g facial film base fluid.Add in facial film base fluid pretreatment blueberry wine mud 55g, glycerol 2g, methyl hydroxybenzoate 0.3g, dibenzylatiooluene 0.1g, Margarita powder 5g, natural aromatic oil 0.02g(Guangzhou this daily use chemicals development in science and technology company limited of the Chinese one hundred produce), vitamin E 4g, stir, namely milling treatment of colloid obtains blueberry wine mud nourishing pack for twice.
Embodiment 2:
Get the blueberry wine mud 2kg that fermentation has just terminated to obtain, add composite flocculation agent bodied ferric sulfate and chitosan stirs 30 minutes according to the mixture 6g of weight ratio 1:1, under 4000g/min centrifugal 20 minutes, supernatant discarded, obtains wine mud 1.45kg.By centrifugal slough rice wine juice after wine mud add deionized water 0.725kg and dilute, ultrasound wave 500W process 30 minutes, then crosses with 200 mesh filter screens and filters impurity, obtain pretreatment blueberry wine mud.8g chitosan, 10g citric acid are added in 100ml deionized water, is heated to 70 DEG C and makes it dissolve completely, stir and make solution A; Sodium carboxymethyl cellulose and each 3g of gelatin are added in 100ml deionized water, is heated to 60 DEG C and makes it dissolve completely, stir and make solution B.At 50 DEG C, 30g solution B is joined in 60g solution A, be constantly uniformly mixed to obtain facial film base fluid.Add in facial film base fluid processed blueberry wine mud 120g, glycerol 6g, methyl hydroxybenzoate 0.8g, dibenzylatiooluene 0.4g, Margarita powder 14g, natural aromatic oil 0.06g(Guangzhou this daily use chemicals development in science and technology company limited of the Chinese one hundred produce), vitamin e1 0g, stir, namely milling treatment of colloid obtains blueberry wine mud nourishing pack for twice.
Below by way of concrete clinical trial example, effect of the present invention is described:
(1) with embodiment blueberry wine mud facial film for test sample, choosing have xerosis cutis, have young volunteer 25 people of acne try out, the age is 20 ~ 35 years old.Before experimenter sleeps every day after cleaning skin, using clear water cleaning skin again, 2 times weekly after blueberry wine mud facial film is spread on facial 15-20 minute, 4 weeks is 1 cycle.After 4 weeks, statistical result shows: effective (show as skin obviously to bleach, more smooth exquisiteness, acne is obviously desalinated.) 23 people, account for 92%; Effectively (show as whiteness of skin, smooth, acne is desalinated.) be 1 people, account for 4.0%; Unfruitful is 1 people, accounts for 4%.Therefore, blueberry wine mud facial film has obvious moisturizing whitening function and antimicrobial and anti-inflammation efficacy, and above-mentioned person on probation does not all produce any side effect and untoward reaction.
(2) with embodiment blueberry wine mud facial film for test sample, select have skin splash more person in middle and old age's volunteer 25 people try out, the age is 40 ~ 60 years old.Before experimenter sleeps every day after cleaning skin, using clear water cleaning skin again, 2 times weekly after blueberry wine mud facial film is spread on facial 15-20 minute, 4 weeks is 1 cycle.After 4 weeks, statistical result shows: effective (show as skin obviously to bleach, smooth exquisiteness, mottle obviously reduces, and wrinkle is desalinated.) be 22 people, account for 88%; Effectively (show as whiteness of skin, smooth, mottle, wrinkle are desalinated.) be 2 people, account for 8.0%; Unfruitful is 1 people, accounts for 4%.Therefore, blueberry wine mud facial film has obvious antioxidation, anti-aging, dispelling stain effect, and above-mentioned person on probation does not all produce any side effect and untoward reaction.
Claims (3)
1. a blueberry wine mud nourishing pack, is characterized in that this facial film is made up of the raw material of following weight portion:
Facial film base fluid 45 parts, 50 ~ 60 parts, pretreatment blueberry wine mud, wetting agent 2 ~ 3 parts, antiseptic 0.2 ~ 0.5 part, antioxidant 0.1 ~ 0.2 part, Margarita powder 4 ~ 8 parts, natural aromatic oil 0.02 ~ 0.04 part, vitamin E 3 ~ 6 parts; Described facial film base fluid is the mixture that solution A and solution B are mixed by weight 2:1; Wherein, solution A is mass concentration to be 8% ~ 10% citric acid and mass concentration be 6% ~ 8% the mixed aqueous solution of chitosan composition; Solution B is mass concentration to be 3% ~ 4% sodium carboxymethyl cellulose and mass concentration be 3% ~ 4% the mixed aqueous solution of gelatin composition; Described wetting agent is glycerol; Antiseptic is methyl hydroxybenzoate; Antioxidant is dibenzylatiooluene, and the concrete pre-treatment step of described pretreatment blueberry wine mud is: by the flocculation of blueberry wine mud, centrifugal, ultrasonic, filtering and impurity removing.
2. blueberry wine mud nourishing pack according to claim 1, is characterized in that this facial film is made up of the raw material of following weight portion:
Facial film base fluid 45 parts, 55 ~ 60 parts, pretreatment blueberry wine mud, wetting agent 2 ~ 3 parts, antiseptic 0.3 ~ 0.4 part, antioxidant 0.1 ~ 0.2 part, Margarita powder 5 ~ 7 parts, natural aromatic oil 0.02 ~ 0.03 part, vitamin E 4 ~ 5 parts.
3. a preparation method for blueberry wine mud nourishing pack according to claim 1, is characterized in that the method follows these steps to be prepared:
1) first by flocculation, centrifugal, ultrasonic, filter de-juice is carried out to blueberry wine mud, remove impurity process obtains pretreatment blueberry wine mud;
2) solution A is prepared: citric acid and chitosan are mixed and made into aqueous solution;
Preparation solution B: sodium carboxymethyl cellulose and gelatin are mixed and made into aqueous solution;
According to the ratio of 2:1 by solution A and solution B mix homogeneously, obtain facial film base fluid;
3) in 45 weight portion facial film base fluids, pretreatment blueberry wine mud 50 ~ 60 weight portion, wetting agent 2 ~ 3 weight portion, antiseptic 0.2 ~ 0.5 weight portion, antioxidant 0.1 ~ 0.2 weight portion, Margarita powder 4 ~ 8 weight portion, natural aromatic oil 0.02 ~ 0.04 weight portion, vitamin E 3 ~ 6 weight portion is added, stir, colloid mill is milled and is processed at least twice.
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CN105708782A (en) * | 2016-03-21 | 2016-06-29 | 赵洪军 | Preparation method of anthocyanin cream pack |
CN106580803A (en) * | 2017-01-18 | 2017-04-26 | 贵州省生物研究所 | Natural mask |
CN108354848B (en) * | 2018-03-01 | 2021-09-14 | 北方民族大学 | Wine lees mask and preparation method thereof |
Citations (2)
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CN102641233A (en) * | 2012-05-18 | 2012-08-22 | 通德集团有限公司 | Rhodiola crenulata facial mask with whitening and moisturizing effects |
CN103315926A (en) * | 2012-03-20 | 2013-09-25 | 董根荣 | Chinese medicinal facial mask possessing efficacies on removing spots and smoothing crease, and preparation method thereof |
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CN103315926A (en) * | 2012-03-20 | 2013-09-25 | 董根荣 | Chinese medicinal facial mask possessing efficacies on removing spots and smoothing crease, and preparation method thereof |
CN102641233A (en) * | 2012-05-18 | 2012-08-22 | 通德集团有限公司 | Rhodiola crenulata facial mask with whitening and moisturizing effects |
Non-Patent Citations (1)
Title |
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佚名."OBDAN wine mud facemask".《COSDNA:http://www.cosdna.com/eng/cosmetic_ac9692074.html》.2012,第1页中表格. * |
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