CN105685137A - Preparation method of Chinese herbal medicine pesticide - Google Patents

Preparation method of Chinese herbal medicine pesticide Download PDF

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Publication number
CN105685137A
CN105685137A CN201610227113.4A CN201610227113A CN105685137A CN 105685137 A CN105685137 A CN 105685137A CN 201610227113 A CN201610227113 A CN 201610227113A CN 105685137 A CN105685137 A CN 105685137A
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China
Prior art keywords
filtrate
preparation
radix
herbal medicine
marmite
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CN201610227113.4A
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Chinese (zh)
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储志强
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Individual
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Priority to CN201610227113.4A priority Critical patent/CN105685137A/en
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/34Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
    • A01N43/40Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom six-membered rings
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40Liliopsida [monocotyledons]
    • A01N65/46Stemonaceae [Stemona family], e.g. croomia

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Zoology (AREA)
  • Agronomy & Crop Science (AREA)
  • Plant Pathology (AREA)
  • Dentistry (AREA)
  • Wood Science & Technology (AREA)
  • Environmental Sciences (AREA)
  • Biotechnology (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Pest Control & Pesticides (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention discloses a preparation method of Chinese herbal medicine pesticide. The preparation method includes the steps of firstly, weighing radix stemonae, nicotine, tripterygium glycosides, radix sophorae flavescentis, semen strychni, cyrtomium fortunei, rhizoma chuanxiong, pericarpium citri reticulatae, flos magnolia and herba portulacae, well mixing, adding into a marmite, adding water into the marmite for decocting for 30-40 minutes, and filtering to obtain filtrate for standby, wherein the weight of the water is 12-15 times of the total weight of the materials; secondly, transferring the filtrate into a sterilizing room, and sterilizing at high temperature of 100-110 DEG C; thirdly, bottling qualified filtrate obtained after inspection, wherein each bottle contains 25g of the qualified filtrate. Compared with the prior art, the Chinese herbal medicine pesticide has the advantages that the Chinese herbal medicine pesticide does not damage human health, does not destroy ecological environments, and the like.

Description

A kind of preparation method of pesticide made of Chinese medicinal herbs
Technical field
The present invention relates to agricultural insecticide field, in particular the preparation method of a kind of pesticide made of Chinese medicinal herbs。
Background technology
Insecticide is primarily used for the medicine of preventing and treating agricultural pests and urban health insect, development along with the science and technology of China and economy, the kind of insecticide increases, drug effect also significantly improves, therefore a large amount of use of insecticide has also effectively promoted increasing of melon fruits and vegetables Isoquant, and agricultural also develops rapidly therewith。
China is traditional large agricultural country and populous nation, and existing insecticide is mainly chemical pesticide, the such as DDT of organochlorine class, Gamma Hexaochlorocyclohexane, 5a,6,9,9a-hexahydro-6,9-methano-2,4, toxaphene etc., wherein, insecticide in the market is used to spray at melon and fruit long-time, after vegetables etc. are upper, melon and fruit, vegetable etc. can produce very big drug residue, this results in drug residue and has been concentrated in food chain, people eat the melon and fruit containing drug residue, during vegetable, not only can reduce the immunity of human body, and other chronic diseases can be produced, thus damaging the healthy of people, especially when drug residue is excessive, easily promote human body that poisoning situation occurs, the death of people even can be caused time serious, additionally, spray chemical pesticide for a long time, surrounding can be produced very big pollution, even the ecosystem of surrounding can be produced very big destruction, therefore, it is badly in need of existing chemical classes insecticide is improved。
Summary of the invention
It is an object of the invention to overcome the deficiencies in the prior art, it is provided that the preparation method of a kind of pesticide made of Chinese medicinal herbs, to overcome existing chemosynthesis insecticide infringement health and to destroy the defect of ecological environment。
The present invention is achieved by the following technical solutions: the preparation method of a kind of pesticide made of Chinese medicinal herbs, comprises the following steps:
(1) weighing the Radix Stemonae, nicotine, Radix Tripterygii Wilfordii, Radix Sophorae Flavescentis, Semen Strychni, Rhizoma Osmundae, Rhizoma Chuanxiong, Pericarpium Citri Reticulatae, Flos Magnoliae, Herba Portulacae, then join in marmite after each component mix homogeneously, then adding water in marmite decocts, and then filters, and filtrate is standby;
(2) filtrate is transferred in sterilization chamber, carries out sterilizing;
(3) after the assay was approved, by bottled for filtrate, 25 grams every bottle。
Preferably: each raw material is according to mass percent: Radix Stemonae 22%-28%, nicotine 12%-18%, Radix Tripterygii Wilfordii 12%-18%, Radix Sophorae Flavescentis 8%-12%, Semen Strychni 2%-8%, Rhizoma Osmundae 6%-10%, Rhizoma Chuanxiong 2%-8%, Pericarpium Citri Reticulatae 6%-10%, Flos Magnoliae 2%-8%, Herba Portulacae 2%-6%。
The using method of pesticide made of Chinese medicinal herbs of the present invention is: when the melon fruits and vegetables insect pest phase, by pesticide made of Chinese medicinal herbs dilute with water 200-400 times obtained by the present invention, then melon fruits and vegetables is sprayed。
Component effect of the present invention is as follows:
The Radix Stemonae: sweet, bitter, tepor, return lung meridian, be usually used in parasite killing。
Radix Tripterygii Wilfordii: bitter, pungent, cool, it is usually used in removing toxic substances, parasite killing, kills maggot, wriggler, water-snail eradication, poison Mus。
Radix Sophorae Flavescentis: bitter in the mouth, cold in nature, heat clearing and damp drying, wind dispelling insecticide。
Semen Strychni: bitter in the mouth, cold, poison, returns liver, spleen two warp greatly。
Rhizoma Osmundae: pungent, bitter, cold, enter lung meridian, heat-clearing and toxic substances removing, be usually used in parasite killing。
Rhizoma Chuanxiong: pungent, temperature。Return liver, gallbladder, pericardium channel, blood-activating and qi-promoting, wind-expelling pain-stopping。
Pericarpium Citri Reticulatae: warm in nature, acrid in the mouth, bitter in the mouth, enter spleen channel, stomach warp, lung meridian, be usually used in sterilization。
Flos Magnoliae: pungent, warm, nontoxic, raw beard and hair, removes tapeworm。
Herba Portulacae: cold in nature, sweet in the mouth acid;Enter the heart, liver, spleen, large intestine channel, heat-clearing and toxic substances removing, dust-collection sterilization。
The present invention has the advantage that compared to existing technology
Each component that the preparation method of a kind of pesticide made of Chinese medicinal herbs of the present invention adopts is Chinese crude drug, environmental protection, surrounding will not be produced environmental pollution, effectively avoid the defect destroying periphery ecological environment because adopting the insecticide of chemosynthesis, it addition, the present invention is good by the pesticide made of Chinese medicinal herbs therapeutic effect prepared by Chinese crude drug, and do not have drug residue, health will not be produced any infringement, and the preparation method of the present invention is fairly simple, is suitable for wide popularization and application。
Detailed description of the invention
Below embodiments of the invention being elaborated, the present embodiment is carried out under premised on technical solution of the present invention, gives detailed embodiment and concrete operating process, but protection scope of the present invention is not limited to following embodiment。
Embodiment 1
A kind of pesticide made of Chinese medicinal herbs, according to mass percent, composed of the following components: the Radix Stemonae 25%, nicotine 15%, Radix Tripterygii Wilfordii 15%, Radix Sophorae Flavescentis 10%, Semen Strychni 5%, Rhizoma Osmundae 8%, Rhizoma Chuanxiong 5%, Pericarpium Citri Reticulatae 8%, Flos Magnoliae 5%, Herba Portulacae 4%。
The preparation method of said herbal medicine pesticide, comprises the following steps:
(1), according to above-mentioned mass percent, weigh the Radix Stemonae, nicotine, Radix Tripterygii Wilfordii, Radix Sophorae Flavescentis, Semen Strychni, Rhizoma Osmundae, Rhizoma Chuanxiong, Pericarpium Citri Reticulatae, Flos Magnoliae, Herba Portulacae, then join in marmite after each component mix homogeneously, then add water in marmite and decoct, the quality of water is 13 times of each constituent mass summation, decocting time is 35 minutes, then filters, and filtrate is standby;
(2), filtrate is transferred in sterilization chamber, carries out high temperature sterilize when 105 DEG C;
(3), after the assay was approved, by bottled for filtrate, 25 grams every bottle。
Embodiment 2
A kind of pesticide made of Chinese medicinal herbs, according to mass percent, composed of the following components: the Radix Stemonae 28%, nicotine 12%, Radix Tripterygii Wilfordii 12%, Radix Sophorae Flavescentis 12%, Semen Strychni 2%, Rhizoma Osmundae 10%, Rhizoma Chuanxiong 8%, Pericarpium Citri Reticulatae 10%, Flos Magnoliae 3%, Herba Portulacae 3%。
The preparation method of said herbal medicine pesticide, comprises the following steps:
(1), according to above-mentioned mass percent, weigh the Radix Stemonae, nicotine, Radix Tripterygii Wilfordii, Radix Sophorae Flavescentis, Semen Strychni, Rhizoma Osmundae, Rhizoma Chuanxiong, Pericarpium Citri Reticulatae, Flos Magnoliae, Herba Portulacae, then join in marmite after each component mix homogeneously, then add water in marmite and decoct, the quality of water is 15 times of each constituent mass summation, decocting time is 40 minutes, then filters, and filtrate is standby;
(2), filtrate is transferred in sterilization chamber, carries out high temperature sterilize when 110 DEG C;
(3), after the assay was approved, by bottled for filtrate, 25 grams every bottle。
Embodiment 3
A kind of pesticide made of Chinese medicinal herbs, according to mass percent, composed of the following components: the Radix Stemonae 22%, nicotine 18%, Radix Tripterygii Wilfordii 18%, Radix Sophorae Flavescentis 8%, Semen Strychni 8%, Rhizoma Osmundae 6%, Rhizoma Chuanxiong 6%, Pericarpium Citri Reticulatae 6%, Flos Magnoliae 4%, Herba Portulacae 4%。
The preparation method of said herbal medicine pesticide, comprises the following steps:
(1), according to above-mentioned mass percent, weigh the Radix Stemonae, nicotine, Radix Tripterygii Wilfordii, Radix Sophorae Flavescentis, Semen Strychni, Rhizoma Osmundae, Rhizoma Chuanxiong, Pericarpium Citri Reticulatae, Flos Magnoliae, Herba Portulacae, then join in marmite after each component mix homogeneously, then add water in marmite and decoct, the quality of water is 12 times of each constituent mass summation, decocting time is 30 minutes, then filters, and filtrate is standby;
(2), filtrate is transferred in sterilization chamber, carries out high temperature sterilize when 100 DEG C;
(3), after the assay was approved, by bottled for filtrate, 25 grams every bottle。
Experimental example
By the embodiment 1-3 pesticide made of Chinese medicinal herbs prepared respectively dilute with water 200 times, 300 times, 400 times, and test the suppression ratio of the pesticide made of Chinese medicinal herbs Pieris rapae to greengrocery of variable concentrations, aphid and leaf folder, in Table 1。
Table 1 is suppression ratio (%) to Pieris rapae, aphid and leaf folder after the embodiment 1-3 pesticide made of Chinese medicinal herbs prepared dilution
As can be seen from Table 1, the pesticide made of Chinese medicinal herbs of the present invention has good insecticidal effect, and wherein embodiment 1 is the highest to the suppression ratio of insect, is highly preferred selection, and same pesticide made of Chinese medicinal herbs extension rate is more low, and the suppression ratio of insect is more high。
The foregoing is only presently preferred embodiments of the present invention, not in order to limit the present invention, all any amendment, equivalent replacement and improvement etc. made within the spirit and principles in the present invention, should be included within protection scope of the present invention。

Claims (2)

1. the preparation method of a pesticide made of Chinese medicinal herbs, it is characterised in that: comprise the following steps:
(1) weighing the Radix Stemonae, nicotine, Radix Tripterygii Wilfordii, Radix Sophorae Flavescentis, Semen Strychni, Rhizoma Osmundae, Rhizoma Chuanxiong, Pericarpium Citri Reticulatae, Flos Magnoliae, Herba Portulacae, then join in marmite after each component mix homogeneously, then adding water in marmite decocts, and then filters, and filtrate is standby;
(2) filtrate is transferred in sterilization chamber, carries out sterilizing;
(3) after the assay was approved, by bottled for filtrate, 25 grams every bottle。
2. the preparation method of a kind of pesticide made of Chinese medicinal herbs according to claim 1, it is characterised in that: each raw material is according to mass percent: Radix Stemonae 22%-28%, nicotine 12%-18%, Radix Tripterygii Wilfordii 12%-18%, Radix Sophorae Flavescentis 8%-12%, Semen Strychni 2%-8%, Rhizoma Osmundae 6%-10%, Rhizoma Chuanxiong 2%-8%, Pericarpium Citri Reticulatae 6%-10%, Flos Magnoliae 2%-8%, Herba Portulacae 2%-6%。
CN201610227113.4A 2016-04-13 2016-04-13 Preparation method of Chinese herbal medicine pesticide Pending CN105685137A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106135327A (en) * 2016-07-19 2016-11-23 陈素云 A kind of Chinese herbal and crude drugs preparations preventing and treating Fructus Momordicae pest and disease damage and preparation method thereof
CN107232248A (en) * 2017-05-19 2017-10-10 山西省肿瘤研究所 Anti- Pesticide with Chinese medicinal material eliminated aphis and preparation method thereof
CN107593818A (en) * 2017-10-13 2018-01-19 河南省三禾药业有限公司 A kind of biological control medicament of Radix Isatidis pest and disease damage and preparation method and application

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CN101223892A (en) * 2008-01-25 2008-07-23 辛贵有 Toosendanin-containing compound pesticide and preparing method thereof
CN101611729A (en) * 2008-06-29 2009-12-30 王兴鹏 The compound method of a kind of plant medical agent control rice fulgorid worm
CN102283260A (en) * 2011-09-07 2011-12-21 杜肇南 Biologic bactericide prepared from plant sources
CN103190451A (en) * 2013-04-07 2013-07-10 海南正业中农高科股份有限公司 Oligochitosan and plant source substance-containing agricultural composition and applications
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Publication number Priority date Publication date Assignee Title
CN101223892A (en) * 2008-01-25 2008-07-23 辛贵有 Toosendanin-containing compound pesticide and preparing method thereof
CN101611729A (en) * 2008-06-29 2009-12-30 王兴鹏 The compound method of a kind of plant medical agent control rice fulgorid worm
CN102283260A (en) * 2011-09-07 2011-12-21 杜肇南 Biologic bactericide prepared from plant sources
CN103371193A (en) * 2012-04-12 2013-10-30 谢红英 Plant source biopesticide
CN103190451A (en) * 2013-04-07 2013-07-10 海南正业中农高科股份有限公司 Oligochitosan and plant source substance-containing agricultural composition and applications

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106135327A (en) * 2016-07-19 2016-11-23 陈素云 A kind of Chinese herbal and crude drugs preparations preventing and treating Fructus Momordicae pest and disease damage and preparation method thereof
CN107232248A (en) * 2017-05-19 2017-10-10 山西省肿瘤研究所 Anti- Pesticide with Chinese medicinal material eliminated aphis and preparation method thereof
CN107593818A (en) * 2017-10-13 2018-01-19 河南省三禾药业有限公司 A kind of biological control medicament of Radix Isatidis pest and disease damage and preparation method and application

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Application publication date: 20160622

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