CN105661666B - Mosquito repellent UV resistance socks and preparation method thereof - Google Patents
Mosquito repellent UV resistance socks and preparation method thereof Download PDFInfo
- Publication number
- CN105661666B CN105661666B CN201610119440.8A CN201610119440A CN105661666B CN 105661666 B CN105661666 B CN 105661666B CN 201610119440 A CN201610119440 A CN 201610119440A CN 105661666 B CN105661666 B CN 105661666B
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- Prior art keywords
- mosquito repellent
- resistance
- socks
- parts
- agent
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Classifications
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- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41B—SHIRTS; UNDERWEAR; BABY LINEN; HANDKERCHIEFS
- A41B11/00—Hosiery; Panti-hose
-
- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41B—SHIRTS; UNDERWEAR; BABY LINEN; HANDKERCHIEFS
- A41B17/00—Selection of special materials for underwear
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/144—Alcohols; Metal alcoholates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/165—Ethers
- D06M13/175—Unsaturated ethers, e.g. vinylethers
Abstract
The invention discloses a kind of mosquito repellent UV resistance socks and preparation method thereof.The mosquito repellent UV resistance socks are formed by the raw material weaving of following weight parts：60 80wt% cotton fibers and 20 40wt% spandexs.Mosquito repellent UV resistance socks of the invention, process stabilizing is good from raw material, and by checking on for each procedure, steady quality, in appearance, Density is uniform, abundant, pure color for performance, and forming of shaping, is the ideal chose of healthy life staying idle at home.
Description
Technical field
The present invention relates to a kind of socks, and in particular to a kind of mosquito repellent UV resistance socks and preparation method thereof.
Background technology
" socks " one word sees earliest《China notes at all times》, say：" three generations and week Zhu Jiao Wa, ankle is lain in band "." three generations "
It refer to China's summer on the books earliest, business, all periods, away from the present existing 3000 or four thousand years history." Jiao Wa " should be made of animal skin
Original socks, so writing " Wa ".Later, with the appearance of textile, socks are developed into cloth, fiber crops, silk by beast cloth again
Make , " Wa " " socks " are also correspondingly changed to, " socks " of the today described in us are finally reduced to step by step.The transmutation process of " socks " word,
The development process of Chinese civilization history is contained in fact.
The shape of ancient times socks can about divide three-chip type craft socks to have legging, frenulum socks, panty hose, point toe socks, light
Six kinds of socks and bottomless sock etc. of head.Wherein have the stocking leg of legging different in size, some length to belly, have only between ankle.Frenulum socks
In order that difficult for drop-off when wearing.Toe socks are divided to be that big toe is separated with other four toe, shape such as bifurcation shape.Bare headed socks and bottomless sock are multiplex
In the women of ancient times foot-binding, half socks are commonly called as.
Now, the species of socks is a lot, by the length point of the stocking leg, has stocking, Knee-sockses and short legging and ship socks (stealthy
Socks)；By stocking blank species point, there are registered permanent residence socks, rib cuff socks and elastic top hosiery；By using object point, there are men's socks, female's socks and Children's Socks.Circular knit hosiery
By stocking blank, the stocking leg and the portion of tissue of stocking foot 3.The specification of socks, is represented with socks size, and socks number are with the reality of the stocking sole
Border length dimension is standard, so knowing that the pin of oneself just can choose the socks for fitting after long.By the original that socks are used
Material is different, and it is also different in socks series.
With the continuous improvement that people are pursued healthy living, the performance of socks is not limited solely to it is warming, attractive in appearance etc.,
Also it is aided with the various health cares such as more massages, antibacterial, anti-mite, moisture absorbing and sweat releasing, antistatic, uvioresistant and safeguard function.
The invention provides a kind of mosquito repellent UV resistance socks, multi-functional demand of the people to socks is met.
The content of the invention
For deficiencies of the prior art, one of the technical problems to be solved by the invention are to provide a kind of mosquito repellent
UV resistance socks.
The two of the technical problems to be solved by the invention are to provide the preparation method of above-mentioned mosquito repellent UV resistance socks.
Technical problem of the invention, is achieved by following technical proposals：
A kind of mosquito repellent UV resistance socks, are formed by the raw material weaving of following weight parts：60-80wt% cotton fibers and 20-
40wt% spandexs.
The mosquito repellent UV resistance socks are obtained by mosquito repellent UV resistance process step again.
The mosquito repellent UV resistance process step is that the mosquito repellent UV resistance socks are impregnated in mosquito repellent UV resistance finishing agent, institute
The mosquito repellent UV resistance finishing agent stated is made up of the raw material of following weight parts：0.1-0.3 parts of aloe essential oil, 0.1-0.3 parts of lemongrass essence
Oil, 0.1-0.5 portions of UV-531,0.1-0.5 portions of bleeding agent, 5-15 portions of ethanol, 0.1-0.5 portions of chela
Mixture, 95-105 part water.
Described bleeding agent is mixed by 40-60wt% aerosol OTs and 40-60wt% tridecyl sodium sulfonates
Conjunction is formed.
Preferably, described chelating agent is by 40-60wt% ethylene diamine tetra methylene phosphonic acids five sodium-salt and 40-60wt% amino three
Methylenephosphonic acid five sodium-salt is mixed.
Present invention also offers the preparation method of above-mentioned mosquito repellent UV resistance socks, it is characterised in that comprise the following steps：
(1) cotton fiber and spandex weaved using conventional method, be processed into socks；
(2) above-mentioned socks are carried out into mosquito repellent UV resistance treatment.
Preferably, the step (2) is under the conditions of 65-85 DEG C, socks to be impregnated into 20- in mosquito repellent UV resistance finishing agent
30min, after dehydration, dries 5-10min under the conditions of 70-90 DEG C.
Described mosquito repellent UV resistance finishing agent is made up of the raw material of following weight parts：0.1-0.3 parts of aloe essential oil, 0.1-
0.3 part of oil of Cymbopogon winterianus, 0.1-0.5 parts of UV-531,0.1-0.5 parts of bleeding agent, 5-15 parts of ethanol,
0.1-0.5 parts of chelating agent, 95-105 parts of water.
Specifically, in the present invention：
Aloe essential oil, i.e. aloe, No. CAS：100084-89-7.
Oil of Cymbopogon winterianus, No. CAS：73049-78-2.
UV-531, No. CAS：1843-05-6.
Aerosol OT, No. CAS：577-11-7.
Tridecyl sodium sulfonate, No. CAS：5802-89-1.
Ethylene diamine tetra methylene phosphonic acid five sodium-salt, No. CAS：7651-99-2.
ATMP five sodium-salt, No. CAS：2235-43-0.
Ethanol, No. CAS：64-17-5.
Mosquito repellent UV resistance socks of the invention, process stabilizing is good from raw material, by checking on for each procedure, steady quality,
In appearance, Density is uniform, abundant, pure color for performance, and forming of shaping, is the ideal chose of healthy life staying idle at home.
Specific embodiment
With reference to embodiment, the present invention is described further, as described below, is only to preferable implementation of the invention
Example, not does the limitation of other forms to the present invention, and any those skilled in the art are possibly also with the disclosure above
Technology contents be changed to the Equivalent embodiments of equal change.It is every without departing from the present invention program content, according to the present invention
Technical spirit any simple modification that following examples are made or equivalent variations, all fall within protection scope of the present invention.
Embodiment 1
Mosquito repellent UV resistance socks raw material (percentage by weight)：(cotton fiber is long-staple cotton to 70wt% cotton fibers, and its length is
40mm, fineness is 7200nm) and 30wt% spandexs (using Du Pont's spandex thread, 70D).
Mosquito repellent UV resistance finishing agent raw material (weight portion)：0.2 part of aloe essential oil, 0.2 part of oil of Cymbopogon winterianus, 0.3 part of 2- hydroxyl-
4- oxy-octyl benzophenones, 0.3 part of bleeding agent, 10 parts of ethanol, 0.3 part of chelating agent, 100 parts of deionized waters.
Described bleeding agent is by 50wt% aerosol OTs and the stirring mixing of 50wt% tridecyls sodium sulfonate
Uniformly obtain.
Described chelating agent is by 50wt% ethylene diamine tetra methylene phosphonic acids five sodium-salt and the sodium of 50wt% ATMPs five
Salt is uniformly mixed and obtains.
Present invention also offers the preparation method of above-mentioned mosquito repellent UV resistance socks, comprise the following steps：
(1) use braider, according to a conventional method by cotton fiber and spandex weave into socks blank cloth (grammes per square metre is 160 grams/it is flat
Square rice), according to the technique and requirement that make socks, after socks blank cloth is cut, it is processed into socks；
(2) aloe essential oil, oil of Cymbopogon winterianus, UV-531, bleeding agent, ethanol, chelating agent are added
To enter be uniformly mixed in deionized water, obtain mosquito repellent UV resistance finishing agent；Socks are placed on the anti-purple of mosquito repellent that temperature is 75 DEG C
25min is impregnated in outer finishing agent, wherein socks and the mass ratio of mosquito repellent UV resistance finishing agent are 1:10 (i.e. 1kg socks 10kg
Mosquito repellent UV resistance finishing agent impregnates), after dehydration, 8min is dried under the conditions of 80 DEG C；Obtain mosquito repellent UV resistance socks.
Embodiment 2
It is substantially the same manner as Example 1, differ only in：Described bleeding agent is only aerosol OT.
To the mosquito repellent UV resistance socks of embodiment 2.
Embodiment 3
It is substantially the same manner as Example 1, differ only in：Described bleeding agent is only tridecyl sodium sulfonate.Obtain reality
Apply the mosquito repellent UV resistance socks of example 3.
Embodiment 4
It is substantially the same manner as Example 1, differ only in：Described chelating agent is only the sodium of ethylene diamine tetra methylene phosphonic acid five
Salt.Obtain the mosquito repellent UV resistance socks of embodiment 4.
Embodiment 5
It is substantially the same manner as Example 1, differ only in：Described chelating agent is only ATMP five sodium-salt.
Obtain the mosquito repellent UV resistance socks of embodiment 5.
Test case 1
Mosquito repellent UV resistance socks to embodiment 1-5 carry out anti-ultraviolet property test test, using GB/T18830-2009
The evaluation of ultraviolet resistance of fabric, is tested.UPF is (referred to as：UPF) the transmission measurement of value, UVA
Data are shown in Table 1.
Table 1：Anti-ultraviolet property tests table
Comparing embodiment 1-3, embodiment 1 (aerosol OT, tridecyl sodium sulfonate compounding) uvioresistant
Effect, hence it is evident that better than embodiment 2-3 (single raw material in aerosol OT, tridecyl sodium sulfonate)；Compare implementation
Example 1 and embodiment 4-5, embodiment 1 (ethylene diamine tetra methylene phosphonic acid five sodium-salt, ATMP five sodium-salt compounding) uvioresistant
Line effect, hence it is evident that better than embodiment 4-5 (single originals in ethylene diamine tetra methylene phosphonic acid five sodium-salt, ATMP five sodium-salt
Material).
Test case 2
Mosquito repellent UV resistance socks to embodiment 1-5 carry out mosquito repellent test,
Experiment is at dusk 18:00-20:00 is carried out, and small white mouse is fixed on one block of three-ply board of 10cm × 15cm, mouse body
Surface covers a silk stocking, and is fixed in surrounding with elastic, and then putting it into feeding has in 1000 mosquito cages of mosquito, timing 3
Minute, observe and record mosquito during this period and stop the number of times that falls on sample cloth cover, in triplicate, embodiment is used with comparative example
Color is identical.Test data is shown in Table 2.
Table 2：Synthesis test table
Comparing embodiment 1-3, embodiment 1 (aerosol OT, tridecyl sodium sulfonate compounding) repelling effect,
It is substantially better than embodiment 2-3 (single raw material in aerosol OT, tridecyl sodium sulfonate)；Comparing embodiment 1 with
Embodiment 4-5, embodiment 1 (ethylene diamine tetra methylene phosphonic acid five sodium-salt, ATMP five sodium-salt compounding) repelling effect is bright
It is aobvious to be better than embodiment 4-5 (single raw material in ethylene diamine tetra methylene phosphonic acid five sodium-salt, ATMP five sodium-salt).
Test case 3
Mosquito repellent UV resistance finishing agent (mosquito repellent UV resistance finishing agent raw material (weight portion) of embodiment 1：0.2 part of aloe essential oil,
0.2 part of oil of Cymbopogon winterianus, 0.3 part of UV-531,0.3 part of bleeding agent, 10 parts of ethanol, 0.3 part of chelating
Agent, 100 parts of deionized waters) toxicity test：
(1) the oral acute toxicity of mosquito repellent UV resistance finishing agent；Mosquito repellent UV resistance finishing agent is taken to 40 Kunming of empty stomach 16h
The disposable oral gavage of the standard of kind small white mouse, mosquito repellent UV resistance arranges agent dose and is up to 1000mg/kg.Observation animal is with daily
Poison performance, seven days terminate experiment, and in whole experiment process, without any poisoning manifestations, diet and motion are equal for each group experimental animal
Normally, none animal dead.
(2) to skin irritation：10 big ear tag quasi-experiments of Japan are cut respectively with the backbone diamond wool of rabbit, will be impregnated
The gauze of mosquito repellent UV resistance finishing agent is crossed, is applied on the exposed skin in right side.Application site skin is observed after 24 hours, not
There are the irritations such as erythema and oedema, according to skin irritatin strength grading standard, the mosquito repellent UV resistance finishing agent belongs to skin
Non-stimulated material.
(3) to eye irritation：By mosquito repellent UV resistance finishing agent, the right side of the big ear tag quasi-experiment of Japan with rabbit is directly instilled
Eye, left eye is compared, passive closure 5 seconds, then clean with normal saline flushing, is observed after 24 hours, and eyes are without exception, root
According to eye irritation strength grading standard, the mosquito repellent UV resistance finishing agent belongs to non-stimulated material to eyes.
Claims (5)
1. a kind of mosquito repellent UV resistance socks, it is characterised in that formed by the raw material weaving of following weight parts：60-80wt% cotton fibers
With 20-40wt% spandexs；
The mosquito repellent UV resistance socks are obtained by mosquito repellent UV resistance process step again；
The mosquito repellent UV resistance process step is that the mosquito repellent UV resistance socks are impregnated in mosquito repellent UV resistance finishing agent, described
Mosquito repellent UV resistance finishing agent is made up of the raw material of following weight parts：0.1-0.3 parts of aloe essential oil, 0.1-0.3 parts of oil of Cymbopogon winterianus,
0.1-0.5 parts of UV-531,0.1-0.5 parts of bleeding agent, 5-15 parts of ethanol, 0.1-0.5 parts of chelating
Agent, 95-105 parts of water；
Described bleeding agent is by 40-60wt% aerosol OTs and the mixing of 40-60wt% tridecyls sodium sulfonate
Into.
2. mosquito repellent UV resistance socks as claimed in claim 1, it is characterised in that described chelating agent is by 40-60wt% ethylenediamines
Four methylenephosphonic acid five sodium-salts and 40-60wt% ATMP five sodium-salts are mixed.
3. the preparation method of the mosquito repellent UV resistance socks according to any one of claim 1-2, it is characterised in that including following
Step：
(1) cotton fiber and spandex weaved using conventional method, be processed into socks；
(2) above-mentioned socks are carried out into mosquito repellent UV resistance treatment.
4. the preparation method of mosquito repellent UV resistance socks according to claim 3, it is characterised in that the step (2) is in 65-
Under the conditions of 85 DEG C, socks are impregnated into 20-30min in mosquito repellent UV resistance finishing agent, after dehydration, dried under the conditions of 70-90 DEG C
5-10min。
5. the preparation method of mosquito repellent UV resistance socks according to claim 4, it is characterised in that described mosquito repellent UV resistance is whole
Reason agent is made up of the raw material of following weight parts：0.1-0.3 parts of aloe essential oil, 0.1-0.3 parts of oil of Cymbopogon winterianus, 0.1-0.5 parts of 2- hydroxyl
Base -4- oxy-octyl benzophenones, 0.1-0.5 parts of bleeding agent, 5-15 parts of ethanol, 0.1-0.5 parts of chelating agent, 95-105 parts of water.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610119440.8A CN105661666B (en) | 2016-03-03 | 2016-03-03 | Mosquito repellent UV resistance socks and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610119440.8A CN105661666B (en) | 2016-03-03 | 2016-03-03 | Mosquito repellent UV resistance socks and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105661666A CN105661666A (en) | 2016-06-15 |
| CN105661666B true CN105661666B (en) | 2017-06-06 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201610119440.8A Active CN105661666B (en) | 2016-03-03 | 2016-03-03 | Mosquito repellent UV resistance socks and preparation method thereof |
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Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112281498A (en) * | 2019-07-22 | 2021-01-29 | 新乡市护神特种织物有限公司 | Ultraviolet-proof and mosquito-proof fabric and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102190591A (en) * | 2010-03-12 | 2011-09-21 | 陈郁 | Metal complex, preparation method and application thereof |
| CN104382242A (en) * | 2014-12-10 | 2015-03-04 | 江南大学 | Anti-flea knitted stocking |
| CN104499273A (en) * | 2014-11-17 | 2015-04-08 | 浙江梦娜袜业股份有限公司 | Mosquito-repelling and mite-resisting finishing agent for silk stockings and silk stocking production technology |
| CN105131174A (en) * | 2015-08-20 | 2015-12-09 | 广东德美精细化工股份有限公司 | Durable uvioresistant finishing agent applicable to both cotton and terylene and preparation method thereof |
| CN105200645A (en) * | 2015-08-21 | 2015-12-30 | 沈汇明 | Production process of woolen loose socks |
-
2016
- 2016-03-03 CN CN201610119440.8A patent/CN105661666B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102190591A (en) * | 2010-03-12 | 2011-09-21 | 陈郁 | Metal complex, preparation method and application thereof |
| CN104499273A (en) * | 2014-11-17 | 2015-04-08 | 浙江梦娜袜业股份有限公司 | Mosquito-repelling and mite-resisting finishing agent for silk stockings and silk stocking production technology |
| CN104382242A (en) * | 2014-12-10 | 2015-03-04 | 江南大学 | Anti-flea knitted stocking |
| CN105131174A (en) * | 2015-08-20 | 2015-12-09 | 广东德美精细化工股份有限公司 | Durable uvioresistant finishing agent applicable to both cotton and terylene and preparation method thereof |
| CN105200645A (en) * | 2015-08-21 | 2015-12-30 | 沈汇明 | Production process of woolen loose socks |
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| CN105661666A (en) | 2016-06-15 |
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Effective date of registration: 20190710 Address after: 223600 Intelligent Knitting Industrial Park, Shuyang Economic and Technological Development Zone, Suqian City, Jiangsu Province (east of 205 National Road north of Youfu Road) Patentee after: Jiangsu Southwest Intelligent Textile Co., Ltd. Address before: 311825 Yuanxiang Government of Kengxi Village, Paitou Town, Zhuji City, Shaoxing City, Zhejiang Province Patentee before: Xu Mengkui |