CN105659072B - 监测聚合反应控制参数的方法和实施所述方法的相关装置 - Google Patents

监测聚合反应控制参数的方法和实施所述方法的相关装置 Download PDF

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CN105659072B
CN105659072B CN201480055493.7A CN201480055493A CN105659072B CN 105659072 B CN105659072 B CN 105659072B CN 201480055493 A CN201480055493 A CN 201480055493A CN 105659072 B CN105659072 B CN 105659072B
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polymerization
polymerization reaction
mixture
control parameter
nir
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CN105659072A (zh
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F·博纳奇尼
E·曼托瓦尼
A·费兰多
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Versalis SpA
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    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
    • G01N21/27—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands using photo-electric detection ; circuits for computing concentration
    • G01N21/272—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands using photo-electric detection ; circuits for computing concentration for following a reaction, e.g. for determining photometrically a reaction rate (photometric cinetic analysis)
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F112/00—Homopolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring
    • C08F112/02—Monomers containing only one unsaturated aliphatic radical
    • C08F112/04—Monomers containing only one unsaturated aliphatic radical containing one ring
    • C08F112/06—Hydrocarbons
    • C08F112/08—Styrene
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
    • G01N21/31—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
    • G01N21/35—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light
    • G01N21/3577—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light for analysing liquids, e.g. polluted water
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
    • G01N21/31—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
    • G01N21/35—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light
    • G01N21/359—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light using near infrared light
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/84—Systems specially adapted for particular applications
    • G01N21/85—Investigating moving fluids or granular solids
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/84—Systems specially adapted for particular applications
    • G01N21/85—Investigating moving fluids or granular solids
    • G01N21/8507—Probe photometers, i.e. with optical measuring part dipped into fluid sample
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2201/00—Features of devices classified in G01N21/00
    • G01N2201/06—Illumination; Optics
    • G01N2201/061—Sources
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2201/00—Features of devices classified in G01N21/00
    • G01N2201/08—Optical fibres; light guides
    • G01N2201/0826—Fibre array at source, distributing
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2201/00—Features of devices classified in G01N21/00
    • G01N2201/12—Circuits of general importance; Signal processing
    • G01N2201/13—Standards, constitution

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  • Physics & Mathematics (AREA)
  • Chemical & Material Sciences (AREA)
  • Spectroscopy & Molecular Physics (AREA)
  • Health & Medical Sciences (AREA)
  • Pathology (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Mathematical Physics (AREA)
  • Engineering & Computer Science (AREA)
  • Theoretical Computer Science (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Investigating Or Analysing Materials By Optical Means (AREA)
  • Polymerisation Methods In General (AREA)
  • Investigating Or Analysing Materials By The Use Of Chemical Reactions (AREA)
CN201480055493.7A 2013-11-19 2014-11-18 监测聚合反应控制参数的方法和实施所述方法的相关装置 Active CN105659072B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
IT001916A ITMI20131916A1 (it) 2013-11-19 2013-11-19 Metodo per monitorare un parametro di controllo di una reazione di polimerizzazione e relativo apparato per attuare detto metodo
ITMI2013A001916 2013-11-19
PCT/IB2014/066129 WO2015075629A1 (en) 2013-11-19 2014-11-18 Method for monitoring a control parameter of a polymerization reaction and relative apparatus for implementing said method

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CN105659072A CN105659072A (zh) 2016-06-08
CN105659072B true CN105659072B (zh) 2020-02-14

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EP (1) EP3071954B1 (enExample)
JP (1) JP6619736B2 (enExample)
KR (1) KR102209231B1 (enExample)
CN (1) CN105659072B (enExample)
BR (1) BR112016007745B1 (enExample)
ES (1) ES2804087T3 (enExample)
HU (1) HUE051229T2 (enExample)
IT (1) ITMI20131916A1 (enExample)
MX (1) MX368418B (enExample)
MY (1) MY185715A (enExample)
PL (1) PL3071954T3 (enExample)
PT (1) PT3071954T (enExample)
RU (1) RU2662039C1 (enExample)
SA (1) SA516371040B1 (enExample)
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GB201704447D0 (en) * 2017-03-21 2017-05-03 Asterope Ltd Wire coating determination
WO2019235542A1 (ja) * 2018-06-07 2019-12-12 横河電機株式会社 光学分析システム及び光学分析方法
CN108872144B (zh) * 2018-09-13 2021-02-12 中国农业大学 一种用于厌氧消化过程的在线监测装置
EP3711852A1 (de) * 2019-03-21 2020-09-23 Covestro Deutschland AG Verfahren und vorrichtung zur quantitativen überwachung der zusammensetzung einer oligomer-/monomermischung
EP4231000A4 (en) * 2020-10-13 2024-11-20 Nippon Shokubai Co., Ltd. PREDICTION METHOD AND PREDICTION DEVICE
JP7603629B2 (ja) 2022-03-14 2024-12-20 Dic株式会社 樹脂物性値予測装置及び樹脂物性値の予測方法
CN117309793B (zh) * 2023-10-25 2024-05-07 连云港石化有限公司 一种苯乙烯装置聚合物测定方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0764843A2 (fr) * 1995-09-25 1997-03-26 SOLVAY (Société Anonyme) Procédé et dispositif de contrôle de la qualité de latex de polyméres vinyliques halogénés
EP1223186A1 (en) * 2000-12-22 2002-07-17 Mitsubishi Gas Chemical Company, Inc. Process for production of polyamide
CN1914254A (zh) * 2003-12-09 2007-02-14 菲纳科技股份有限公司 生产聚合物的方法

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US5604132A (en) * 1995-01-23 1997-02-18 Olin Corporation Process flow injection analyzer and method
DE19805612A1 (de) * 1998-02-12 1999-08-19 Bayer Ag Verfahren zur kontrollierten Herstellung oder Modifizierung von polymeren Produkten mittels IR-ATR-Spektroskopie
JP2000159897A (ja) * 1998-11-27 2000-06-13 Mitsui Chemicals Inc 高分子化合物の不良品分離方法
US8263722B2 (en) * 2004-03-24 2012-09-11 Exxonmobil Chemical Patents Inc. Process for making ethylene interpolymers and interpolymers made thereby; compositions and electrical devices containing such interpolymers
CA2470887C (en) * 2004-06-14 2014-10-21 Nova Chemicals Corporation Detection of gels in a solution polymerization
KR100863412B1 (ko) * 2006-03-13 2008-10-14 주식회사 엘지화학 1-알켄-아크릴레이트계 공중합체의 제조방법
US8843324B2 (en) * 2011-02-03 2014-09-23 Nova Chemicals (International) S.A. Double derivative NIR process control
CN102288575B (zh) * 2011-07-25 2013-03-06 哈尔滨工业大学 在线监测甲氨基阿维菌素反应的装置

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0764843A2 (fr) * 1995-09-25 1997-03-26 SOLVAY (Société Anonyme) Procédé et dispositif de contrôle de la qualité de latex de polyméres vinyliques halogénés
US5898056A (en) * 1995-09-25 1999-04-27 Solvay (Societe Anonyme) Process and device for monitoring the quality of latices of halogen-containing vinyl polymers
EP1223186A1 (en) * 2000-12-22 2002-07-17 Mitsubishi Gas Chemical Company, Inc. Process for production of polyamide
CN1914254A (zh) * 2003-12-09 2007-02-14 菲纳科技股份有限公司 生产聚合物的方法

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KR20160088304A (ko) 2016-07-25
US20160231230A1 (en) 2016-08-11
WO2015075629A1 (en) 2015-05-28
MX368418B (es) 2019-10-02
MY185715A (en) 2021-05-31
PL3071954T3 (pl) 2020-10-05
EP3071954A1 (en) 2016-09-28
US9714899B2 (en) 2017-07-25
BR112016007745B1 (pt) 2020-11-24
MX2016005767A (es) 2016-07-18
ES2804087T3 (es) 2021-02-03
EP3071954B1 (en) 2020-04-08
PT3071954T (pt) 2020-07-09
SA516371040B1 (ar) 2017-12-03
ITMI20131916A1 (it) 2015-05-20
JP6619736B2 (ja) 2019-12-11
KR102209231B1 (ko) 2021-01-29
RU2662039C1 (ru) 2018-07-23
JP2016538536A (ja) 2016-12-08
CN105659072A (zh) 2016-06-08
HUE051229T2 (hu) 2021-03-01
RU2016116157A (ru) 2017-12-25
SI3071954T1 (sl) 2020-08-31

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